CN105648752A - Environment-friendly fabric softener and preparation method thereof - Google Patents
Environment-friendly fabric softener and preparation method thereof Download PDFInfo
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- CN105648752A CN105648752A CN201610112248.6A CN201610112248A CN105648752A CN 105648752 A CN105648752 A CN 105648752A CN 201610112248 A CN201610112248 A CN 201610112248A CN 105648752 A CN105648752 A CN 105648752A
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- acid ammonium
- softening agent
- polyoxyethylene ether
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The invention discloses an environment-friendly fabric softener. The environment-friendly fabric softener comprises raw materials in percentage by mass as follows: 4%-8% of di(tallow acyl ethyl) hydroxyethyl methylammonium methosulfate, 2%-5% of di(fatty acyl amide ethyl) polyoxyethylene ether methylammonium methosulfate, 5%-10% of an alcohol solvent, 1%-4% of an emulsifier, 1%-2% of a tackifier and the balance of deionized water. The invention discloses a preparation method of the environment-friendly fabric softener. The environment-friendly fabric softener which has excellent softening performance is obtained through reasonable matching of raw material with the preparation process.
Description
Technical field
The present invention relates to textile processing used additives technical field, be specifically related to a kind of environment-friendlytype type fabric softening agent and preparation method thereof.
Background technology
Softening agent is a kind of material that a class can change the kinematics and static friction coefficient of fiber, and when changing fiber confficient of static friction, feel touches smooth sense, it is easy to move on fiber or fabric; When changing the coefficient of kinetic friction, the fine structure between fiber and fiber is prone to be mutually shifted, and namely fiber or fabric are easily deformable; The comprehensive sensation of the two is exactly soft.
In recent years, along with the expansion of scientific and technological development and weaving free trade, environmental protection consciousness is also progressively deep into the aspects such as social and economic activities, and world commerce particularly country textile trade attaches great importance to environmental protection and ecological index, and industry releases green product one after another. This also determines people's selection principle to softening agent: under the premise that human body and environment are produced the least possible side effect; just consider how to play its optimal efficacy; this trend makes the production of softening agent and research and development all suffer from a kind of challenge; how to provide the consumer with the safest the most maximally effective goods; simultaneously; consider the protection to environment; the goods produced have excellent biological degradability again, are current Chemical Manufacture enterprise and one of target that textile fabrics enterprise to realize.
Summary of the invention
For problems of the prior art, the invention provides a kind of fabric softener having the feature of environmental protection and flexibility concurrently and preparation method thereof.
This invention address that the technical scheme that above-mentioned technical problem adopts is: a kind of environment-friendlytype type fabric softening agent, it is made up of following raw material: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl, alcoholic solvent, emulsifying agent, viscosifier and deionized water;
The mass percent of described raw material is: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 4��8%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 2��5%, alcoholic solvent 5��10%, emulsifying agent 1��4%, viscosifier 1��2%, surplus are deionized water.
Further, described alcoholic solvent is ethanol, propanol or 3-propanol.
Further, described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:1��4; Softening agent system can be played good emulsification by described emulsifying agent, and it is little, the impact of environment is little on the zest of skin, belongs to environmentally friendly material in emulsifier/surfactant.
Further, described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 40��80% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, comprise the following steps: Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyl and double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl are added to alcoholic solvent, heating is to 65��75 DEG C, add after being uniformly mixed to the deionized water solution of 70��85 DEG C of emulsifying agents, viscosifier are added after stirring, after insulated and stirred 20��30min, natural cooling, filtration, fill.
In the raw material of the present invention, long alkyl chain in double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyls and double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyl molecular structure ensure that its flexibility, the introducing of multiamide base improves its biological degradability, the insertion of polyoxyethylene groups improves its hydrophilic, and acid amide type quaternary ammonium salt itself is strong to fibers adsorption ability, the not easily feature of eluting, has good flexibility, antistatic behaviour, yellowing resistance and biological degradability; Double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyls and double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls are the thickening to profit software architecture through the emulsifying of emulsifying agent and viscosifier in the solution, and a softness obtaining the present invention is excellent and the softening agent of environmental protection.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further.
Embodiment 1: a kind of environment-friendlytype type fabric softening agent, it is made up of following raw material: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl, alcoholic solvent, emulsifying agent, viscosifier and deionized water;
The mass percent of described raw material is: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 6%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 3%, alcoholic solvent 8%, emulsifying agent 2%, viscosifier 1%, surplus are deionized water.
Further, described alcoholic solvent is ethanol; Described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, its mass ratio is 1:2, softening agent system can be played good emulsification by described emulsifying agent, and it is little, the impact of environment is little on the zest of skin, belongs to environmentally friendly material in emulsifier/surfactant; Described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 60% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, comprise the following steps: Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyl and double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl are added to alcoholic solvent, heating is to 70 DEG C, add after being uniformly mixed to the deionized water solution of 70 DEG C of emulsifying agents, viscosifier are added after stirring, after insulated and stirred 25min, natural cooling, filtration, fill.
Embodiment 2: a kind of environment-friendlytype type fabric softening agent, it is made up of following raw material: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl, alcoholic solvent, emulsifying agent, viscosifier and deionized water;
The mass percent of described raw material is: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 8%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 2%, alcoholic solvent 10%, emulsifying agent 1%, viscosifier 2%, surplus are deionized water.
Further, described alcoholic solvent is propanol; Described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:1; Described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 80% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, comprise the following steps: Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyl and double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl are added to alcoholic solvent, heating is to 75 DEG C, add after being uniformly mixed to the deionized water solution of 85 DEG C of emulsifying agents, viscosifier are added after stirring, after insulated and stirred 25min, natural cooling, filtration, fill.
Embodiment 3: a kind of environment-friendlytype type fabric softening agent, it is by the raw material of following mass percent: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 4%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 5%, alcoholic solvent 5%, emulsifying agent 4%, viscosifier 1%, surplus are deionized water.
Further, described alcoholic solvent is 3-propanol; Described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:4; Described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 40% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, concrete steps are with embodiment 1.
Embodiment 4: a kind of environment-friendlytype type fabric softening agent, it is by the raw material of following mass percent: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 4%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 2%, alcoholic solvent 5%, emulsifying agent 1%, viscosifier 1%, surplus are deionized water.
Further, described alcoholic solvent is ethanol; Described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:2; Described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 50% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, concrete steps are with embodiment 2.
Embodiment 3: a kind of environment-friendlytype type fabric softening agent, it is by the raw material of following mass percent: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 8%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 5%, alcoholic solvent 10%, emulsifying agent 4%, viscosifier 2%, surplus are deionized water.
Further, described alcoholic solvent is ethanol; Described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:3; Described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 70% of thickening dosage.
Further, the preparation method of described a kind of environment-friendlytype type fabric softening agent, concrete steps are with embodiment 1.
The softening agent of above-described embodiment 1-5 gained is carried out performance test, test base thing is polyester cotton blending fabric lining, to fabric, the softening agent of embodiment gained is carried out padding finishing and drying and shaping etc. according to common production standard process, then flexibility, washability and yellowing-resistant performance test are carried out, wherein, flexibility contacts for professional person and marks (full marks 5 points), and washability is with reference to GB/T3921-2008 standard, and yellowing resistance is with reference to IS0105-X18:2007 standard;Concrete outcome is as shown in the table.
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example * | Blank * |
| Flexibility | 5 | 5 | 5 | 5 | 5 | 5 | 0 |
| Washability | 20 | 18 | 19 | 17 | 17 | 10 | 20 |
| Yellowing resistance | 4 | 3 | 3 | 3 | 3 | 2 | 2 |
* comparative example is common amino-silicone oil softening agent, and the soft treatment technique of fabric is that fabric is carried out the process such as padding finishing and drying and shaping by common production standard by it; The blank fabric for not carrying out softening agent process.
The flexibility of the fabric after softening agent of the present invention processes is suitable with commercially available common amino-silicone oil softening agent, but washability and yellowing resistance are substantially better than common amido silicon oil, and the feature of environmental protection of the softening agent of the present invention is substantially better than common amino-silicone oil softening agent and other commercially available softening agents.
Claims (5)
1. an environment-friendlytype type fabric softening agent, it is characterised in that be made up of following raw material: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl, alcoholic solvent, emulsifying agent, viscosifier and deionized water;
The mass percent of described raw material is: double; two Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyls 4��8%, double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl 2��5%, alcoholic solvent 5��10%, emulsifying agent 1��4%, viscosifier 1��2%, surplus are deionized water.
2. a kind of environment-friendlytype type fabric softening agent according to claim 1, it is characterised in that: described alcoholic solvent is ethanol, propanol or 3-propanol.
3. a kind of environment-friendlytype type fabric softening agent according to claim 1, it is characterised in that: described emulsifying agent is the complex of the sweet benzene diether of first and fatty alcohol-polyoxyethylene ether, and its mass ratio is 1:1��4.
4. a kind of environment-friendlytype type fabric softening agent according to claim 1, it is characterised in that: described viscosifier are alkyl alcoholamine phosphate ester and polyethylene glycol stearate diester, and described alkyl alcoholamine phosphate ester accounts for the 40��80% of thickening dosage.
5. the preparation method of a kind of environment-friendlytype type fabric softening agent according to claim 1, it is characterized in that, comprise the following steps: Adeps Bovis seu Bubali acyl ethyl-hydroxyethyl methylsulfuric acid ammonium methyl and double; two fatty acid amide ethyl polyoxyethylene ether methylsulfuric acid ammonium methyl are added to alcoholic solvent, heating is to 65��75 DEG C, add after being uniformly mixed to the deionized water solution of 70��85 DEG C of emulsifying agents, viscosifier are added after stirring, after insulated and stirred 20��30min, natural cooling, filtration, fill.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610112248.6A CN105648752A (en) | 2016-02-29 | 2016-02-29 | Environment-friendly fabric softener and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610112248.6A CN105648752A (en) | 2016-02-29 | 2016-02-29 | Environment-friendly fabric softener and preparation method thereof |
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| CN105648752A true CN105648752A (en) | 2016-06-08 |
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| CN201610112248.6A Pending CN105648752A (en) | 2016-02-29 | 2016-02-29 | Environment-friendly fabric softener and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106283640A (en) * | 2016-08-31 | 2017-01-04 | 威莱(广州)日用品有限公司 | A kind of softener and preparation method thereof |
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| CN101641432A (en) * | 2007-03-22 | 2010-02-03 | 株式会社Lg生活健康 | Composition for textile softener having low temperature activity and textile softener sheet comprising the same |
| CN103061147A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Composite antibacterial softening agent |
| CN103061146A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Preparation method of composite antibacterial softening agent |
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2016
- 2016-02-29 CN CN201610112248.6A patent/CN105648752A/en active Pending
Patent Citations (4)
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|---|---|---|---|---|
| CN1227593A (en) * | 1996-06-03 | 1999-09-01 | 普罗格特-甘布尔公司 | Fabric softening compositions |
| CN101641432A (en) * | 2007-03-22 | 2010-02-03 | 株式会社Lg生活健康 | Composition for textile softener having low temperature activity and textile softener sheet comprising the same |
| CN103061147A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Composite antibacterial softening agent |
| CN103061146A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Preparation method of composite antibacterial softening agent |
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| 魏代军 等: ""双牛脂酰乙基羟乙基甲基硫酸甲酯铵柔软剂单体的合成"", 《中国洗涤用品工业》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106283640A (en) * | 2016-08-31 | 2017-01-04 | 威莱(广州)日用品有限公司 | A kind of softener and preparation method thereof |
| CN106283640B (en) * | 2016-08-31 | 2017-07-28 | 威莱(广州)日用品有限公司 | A kind of softener and preparation method thereof |
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Application publication date: 20160608 |