CN105647285A - Environment-friendly ink and preparation method thereof - Google Patents
Environment-friendly ink and preparation method thereof Download PDFInfo
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- CN105647285A CN105647285A CN201610201445.5A CN201610201445A CN105647285A CN 105647285 A CN105647285 A CN 105647285A CN 201610201445 A CN201610201445 A CN 201610201445A CN 105647285 A CN105647285 A CN 105647285A
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- ink
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
- C09D11/17—Writing inks characterised by colouring agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses environment-friendly ink and a preparation method thereof. The environment-friendly ink is composed of, by weight, 18-23 parts of tobacco material, 2-5 parts of camellia oil, 3-8 parts of octopus ink, 0.5-2 parts of Radix phytolaccae and 25-33 parts of locust bean gum. The preparation method includes: hulling seeds of camellia tree, drying and boiling at high temperature for 20 min, baking at high temperature for 20 min, smashing, squeezing, and filtering to obtain the camellia oil; drying and smashing Radix phytolaccae, adding an alcohol water solution for backflow extraction and ethyl acetate extraction, depressurizing and concentrating extract containing ethyl acetate to be dry to obtain the Radix phytolaccae extract; mixing the tobacco material, the camellia oil, the octopus ink, the Radix phytolaccae extract and the locust beam gum, adding water for stirring, sealing for standing, pestling, turning for forming, shaping, and airing to obtain the environment-friendly ink. The environment-friendly ink has the advantages of high hardness, less proneness to breakage, bright color, high blackness, high stability, high lightproof performance and quickness in drying after writing and is convenient to grind, smooth in writing, uniform in writing track and long in storage life.
Description
Technical field
The present invention relates to the technical field of ink, specifically a kind of environmental protection ink and preparation method thereof.
Background technology
Ink is that ancient Chinese is write and paint the china ink stick used. The primary raw material of ink is white carbon black, pine soot, glue etc., is the carbon existence with noncrystalline kenel. Ground by inkstone water and can produce the prepared Chinese ink for brush writing, exist with the solution of colloid in water. Wherein Huizhou inkstick is the treasure in China Han ink skill, is also one of " writing brush, ink stick, ink slab and paper " well-known at home and abroad. Gain the name because originating in ancient Huizhou mansion. Huizhou inkstick is a kind of special pigment being mainly for traditional calligraphy, drawing use being made for primary raw material with pine soot, Oleum Verniciae fordii cigarette, paint cigarette, glue. Through light a cigarette and expect, press mill, dry, frustrate limit, paint in gold, operation is refining forms for mounted box etc., finished product have the black profit of color and luster, heavily fortified point and have light, to enter paper not dizzy, lick pen not glue, prolonged do not take off, fragrance is strong, the feature such as mothproof. Successive dynasties Huizhou inkstick is various in style, mainly has paint cigarette, oil smoke, pine soot, full cigarette, clean cigarette, subtracts glue, perfuming etc. Senior paint cigarette ink, plants what famous and precious material was made with Oleum Verniciae fordii cigarette, Moschus, Borneolum Syntheticum, native gold, Margarita powder etc. more than 10. Huizhou inkstick integrates the art such as drawing, calligraphy, engraving, moulding, makes Miboin body become an a kind of comprehensive gem of art. Huizhou inkstick manufacture skill is complicated, and different schools are respectively arranged with the manufacture skill of oneself uniqueness, close not unofficial biography.
Although traditional ink is good, but the preservation of ink is highly difficult, now retains a small amount of Gu Mo, but mostly broken or damaged, and only few little Chinese stick is intact. Additionally, there is also some defects when using, it is dense that rub-down ink is difficult to mill, easily wraps up in pen when writing, wield the pen not smooth, not easily do, poor-performing.
Summary of the invention
It is an object of the invention to provide that a kind of hardness is high, non-friable, bright in color, dense black, environmental protection ink that light resistance is good and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of environmental protection ink, is made up of according to the raw material of weight portion following: cigarette material 18-23 part, Camellia oil 2-5 part, Octopus prepared Chinese ink 3-8 part, Radix phytolaccae extract 0.5-2 part, locust bean gum 25-33 part.
As the further scheme of the present invention: described environmental protection ink, it is made up of according to the raw material of weight portion following: cigarette material 19-22 part, Camellia oil 3-4 part, Octopus ink 4-6 part, Radix phytolaccae extract 1-1.5 part, locust bean gum 27-31 part.
As the further scheme of the present invention: described environmental protection ink, it is made up of according to the raw material of weight portion following: 20 parts of cigarette material, Camellia oil 3.5 parts, 5 parts of Octopus ink, Radix phytolaccae extract 1.2 parts, locust bean gum 29 parts.
The preparation method of described environmental protection ink, is made up of following steps:
1) preparation of Octopus ink: extract Octopus prepared Chinese ink black particle from Octopus ink sac, adds preservative and a small amount of water stirring, prepares Octopus ink;
2) preparation of Radix phytolaccae extract: being dried by Radix Phytolaccae and pulverize raw material to 60-80 order, adding volumetric concentration is the ethanol water of 95%, heating is to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate; In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and do not contain the aqueous solution of ethyl acetate; Extract containing ethyl acetate is evaporated to and dry obtains Radix phytolaccae extract;
3) preparation of Camellia oil: the seed of tea oil tree is shelled, high temperature dry boil 20 minutes, high-temperature baking 20 minutes, pulverizings, oil expression, filtration; Prepare Camellia oil;
4) by cigarette material, Camellia oil, Octopus ink, Radix phytolaccae extract, locust bean gum mixing, add the water of quality 0.2-0.4 times of cigarette material, be stirred, after stirring, then stand 2-3h at 45-48 DEG C of lower seal, then carry out pestle and smash and turn over the type of breaking into, carry out shaping, dry in the air ink again, prepares environmental protection ink.
Compared with prior art, the invention has the beneficial effects as follows:
The ink that the present invention prepares in the interaction of each raw material and when adopting above-mentioned preparation technology, have that hardness is high, non-friable, bright in color, dense black, stability is high, light resistance good, write after dry rapidly feature, can also conveniently grind, reduce milling time, fineness meets application demand, haftplatte test performance also increases, and the prepared Chinese ink of the present invention is wield the pen when writing, smoothness, person's handwriting are uniform, preserve the life-span long, overall performance and quality have advantage, are suitable to calligraphy, the creation of paintings and collection.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments. Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art obtain under not making creative work premise, broadly fall into the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of environmental protection ink, it is made up of according to the raw material of weight portion following: 18 parts of cigarette material, Camellia oil 2 parts, 3 parts of Octopus ink, Radix phytolaccae extract 0.5 part, locust bean gum 25 parts.
The preparation of Octopus ink: extract Octopus prepared Chinese ink black particle from Octopus ink sac, adds preservative and a small amount of water stirring, prepares Octopus ink;
The preparation of Camellia oil: the seed of tea oil tree is shelled, high temperature dry boil 20 minutes, high-temperature baking 20 minutes, pulverizings, oil expression, filtration; Prepare Camellia oil.
Embodiment 2
In the embodiment of the present invention, a kind of environmental protection ink, it is made up of according to the raw material of weight portion following: 23 parts of cigarette material, Camellia oil 5 parts, 8 parts of Octopus ink, Radix phytolaccae extract 2 parts, locust bean gum 33 parts.
The preparation of Octopus ink: extract Octopus prepared Chinese ink black particle from Octopus ink sac, adds preservative and a small amount of water stirring, prepares Octopus ink.
The preparation of Camellia oil: the seed of tea oil tree is shelled, high temperature dry boil 20 minutes, high-temperature baking 20 minutes, pulverizings, oil expression, filtration; Prepare Camellia oil.
Embodiment 3
In the embodiment of the present invention, a kind of environmental protection ink, it is made up of according to the raw material of weight portion following: 19 parts of cigarette material, Camellia oil 3 parts, 4 parts of Octopus ink, Radix phytolaccae extract 1 part, locust bean gum 27 parts.
The preparation of Octopus ink: extract Octopus prepared Chinese ink black particle from Octopus ink sac, adds preservative and a small amount of water stirring, prepares Octopus ink.
The preparation of Camellia oil: the seed of tea oil tree is shelled, high temperature dry boil 20 minutes, high-temperature baking 20 minutes, pulverizings, oil expression, filtration; Prepare Camellia oil.
Embodiment 4
In the embodiment of the present invention, a kind of environmental protection ink, it is made up of according to the raw material of weight portion following: 22 parts of cigarette material, Camellia oil 4 parts, 6 parts of Octopus ink, Radix phytolaccae extract 1.5 parts, locust bean gum 31 parts.
Preparation process is consistent with embodiment 3.
Embodiment 5
In the embodiment of the present invention, a kind of environmental protection ink, it is made up of according to the raw material of weight portion following: 20 parts of cigarette material, Camellia oil 3.5 parts, 5 parts of Octopus ink, Radix phytolaccae extract 1.2 parts, locust bean gum 29 parts.
Preparation process is consistent with embodiment 3.
Comparative example 1
Except not containing Octopus ink, its formula, preparation process are consistent with embodiment 5.
Comparative example 2
Except not containing Radix phytolaccae extract, its formula, preparation process are consistent with embodiment 5.
Comparative example 3
Except not containing Octopus ink, Radix phytolaccae extract and Camellia oil, its formula, preparation process are consistent with embodiment 5.
Table 1 is by the black test result table of embodiment 1-5 Yu comparative example 1-3
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Fineness (micron) | 26 | 26 | 26 | 26 | 26 | 26 | 26 | 26 |
| Haftplatte is tested | 9.5 | 9.5 | 9.6 | 9.6 | 9.7 | 9.1 | 9.2 | 9 |
| Adhesive force (10=is best, and 0=is worst) | 10 | 10 | 10 | 10 | 10 | 9 | 9 | 8 |
| (8=is colour-fast, and 0=is tight for resistance to optical tests Heavily fade) | 8 | 8 | 8 | 8 | 8 | 8 | 8 | 8 |
| Color and luster | Well | Well | Well | Well | Well | Well | Well | Generally |
| Blackness | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black |
| Hardness | In hardness, not broken do not split | In hardness, not broken do not split | Hardness is big, not broken does not split | Hardness is big, not broken does not split | Hardness is big, not broken does not split | Hardness is big, has crackle | In hardness, there is crackle | Hardness is little, frangible |
| Rub-down ink | Very easily grind dense | Very easily grind dense | Easily mill is dense | Easily mill is dense | Easily mill is dense | Not easily grind dense | Not easily grind dense | Not easily grind dense |
| Wield the pen fluency | Well | Well | Well | Well | Well | Generally | Generally | Wrap up in pen |
| Uniformity | Well | Well | Well | Well | Well | Generally | Generally | Poor |
| Drying time (s) | 28 | 25 | 20 | 19 | 17 | 94 | 68 | 102 |
| Stability | Well | Well | Well | Well | Well | Well | Well | Well |
From upper table, embodiment of the present invention 1-5 is compared with the ink of comparative example 1-3, it main advantage is that and can conveniently grind, reduce milling time, meeting application demand (26 microns or following) in fineness, haftplatte test performance also increases, and the hardness of ink is relatively large, non-friable, its bright in color, dense black; And the present invention is in use, ink color thick black, smoothness of wieling the pen when writing, person's handwriting are uniform, and prepared Chinese ink uniformity is good, stability is high, light resistance is good, just can dry rapidly less than half a minute, and overall performance and quality also have advantage. Illustrate that the present invention is when the combined effect of each component and above-mentioned preparation technology, has above-mentioned advantage.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when without departing substantially from the spirit of the present invention or basic feature, it is possible to realize the present invention in other specific forms. Therefore, no matter from which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the invention rather than described above limits, it is intended that all changes in the implication of the equivalency dropping on claim and scope included in the present invention.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but not each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should be made as a whole by those skilled in the art, and the technical scheme in each embodiment through appropriately combined, can also form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. an environmental protection ink, it is characterised in that be made up of according to the raw material of weight portion following: cigarette material 18-23 part, Camellia oil 2-5 part, Octopus ink 3-8 part, Radix phytolaccae extract 0.5-2 part, locust bean gum 25-33 part.
2. environmental protection according to claim 1 ink, it is characterised in that be made up of according to the raw material of weight portion following: cigarette material 19-22 part, Camellia oil 3-4 part, Octopus ink 4-6 part, Radix phytolaccae extract 1-1.5 part, locust bean gum 27-31 part.
3. environmental protection according to claim 2 ink, it is characterised in that be made up of according to the raw material of weight portion following: 20 parts of cigarette material, Camellia oil 3.5 parts, 5 parts of Octopus ink, Radix phytolaccae extract 1.2 parts, locust bean gum 29 parts.
4. one kind as arbitrary in claim 1-3 as described in environmental protection ink preparation method, it is characterised in that be made up of following steps:
1) preparation of Octopus ink: extract Octopus prepared Chinese ink black particle from Octopus ink sac, adds preservative and a small amount of water stirring, prepares Octopus ink;
2) preparation of Radix phytolaccae extract: being dried by Radix Phytolaccae and pulverize raw material to 60-80 order, adding volumetric concentration is the ethanol water of 95%, heating is to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate; In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and do not contain the aqueous solution of ethyl acetate; Extract containing ethyl acetate is evaporated to and dry obtains Radix phytolaccae extract;
3) preparation of Camellia oil: the seed of tea oil tree is shelled, high temperature dry boil 20 minutes, high-temperature baking 20 minutes, pulverizings, oil expression, filtration; Prepare Camellia oil;
4) by cigarette material, Camellia oil, Octopus ink, Radix phytolaccae extract, locust bean gum mixing, add the water of quality 0.2-0.4 times of cigarette material, be stirred, after stirring, then stand 2-3h at 45-48 DEG C of lower seal, then carry out pestle and smash and turn over the type of breaking into, carry out shaping, dry in the air ink again, prepares environmental protection ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610201445.5A CN105647285A (en) | 2016-03-31 | 2016-03-31 | Environment-friendly ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610201445.5A CN105647285A (en) | 2016-03-31 | 2016-03-31 | Environment-friendly ink and preparation method thereof |
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| CN105647285A true CN105647285A (en) | 2016-06-08 |
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| CN201610201445.5A Pending CN105647285A (en) | 2016-03-31 | 2016-03-31 | Environment-friendly ink and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107446411A (en) * | 2017-09-20 | 2017-12-08 | 安徽良才墨业有限公司 | A kind of natural liquid ink formulations and preparation method thereof |
| CN107488377A (en) * | 2017-09-20 | 2017-12-19 | 安徽良才墨业有限公司 | A kind of type moth-proof china ink stick and preparation method thereof |
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| CN104886163A (en) * | 2015-06-19 | 2015-09-09 | 湖北中医药大学 | Botanical pesticide compound phytolacca acinosa and magnolia officinalis microemulsion and preparation method thereof |
| CN105153804A (en) * | 2015-08-24 | 2015-12-16 | 蚌埠市神龙笔业有限公司 | Natural waterborne paint ink and preparation method thereof |
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2016
- 2016-03-31 CN CN201610201445.5A patent/CN105647285A/en active Pending
Patent Citations (4)
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| EP2522700A1 (en) * | 2011-05-11 | 2012-11-14 | Saint-Gobain Glass France | Water soluble printing paste |
| CN102533003A (en) * | 2012-03-01 | 2012-07-04 | 黄山市歙县聚墨堂墨业有限公司 | Non-cracking ink |
| CN104886163A (en) * | 2015-06-19 | 2015-09-09 | 湖北中医药大学 | Botanical pesticide compound phytolacca acinosa and magnolia officinalis microemulsion and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446411A (en) * | 2017-09-20 | 2017-12-08 | 安徽良才墨业有限公司 | A kind of natural liquid ink formulations and preparation method thereof |
| CN107488377A (en) * | 2017-09-20 | 2017-12-19 | 安徽良才墨业有限公司 | A kind of type moth-proof china ink stick and preparation method thereof |
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Application publication date: 20160608 |