CN105778623A - Stable and easy-dry ink and preparation method thereof - Google Patents
Stable and easy-dry ink and preparation method thereof Download PDFInfo
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- CN105778623A CN105778623A CN201610201469.0A CN201610201469A CN105778623A CN 105778623 A CN105778623 A CN 105778623A CN 201610201469 A CN201610201469 A CN 201610201469A CN 105778623 A CN105778623 A CN 105778623A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses stable and easy-dry ink and a preparation method thereof. The ink is prepared from the following raw materials in parts by weight: 18-23 parts of a smoking material, 2-5 parts of pine seed oil, 3-8 parts of hazelnut shell extract, 0.5-2 parts of pokeberry root extract and 25-33 parts of Arabic gum. The preparation method comprises the following steps: carrying out constant temperature reduced pressure drying on hazelnut shells, smashing, and carrying out enzymolysis, ultrasonic treatment, centrifugation and concentration to obtain hazelnut extract; drying and smashing pokeberry root, adding ethanol water, carrying out reflux extraction, extracting with ethyl acetate, and carrying out reduced pressure concentration on extract liquor containing acetate until the extract liquor is dried, so that the pokeberry root extract is obtained; mixing the smoking material, pine seed oil, hazelnut shell extract, pokeberry root extract and Arabic gum, then adding water and stirring, sealing and standing, pestling, turning over, ramming, moulding, setting, and airing ink, so that the stable and easy-dry ink is obtained. The stable and easy-dry ink has the characteristics of high hardness, unbreakable property, bright colour, thick black colour, high stability, good light resistance and quick drying after writing, grinding is convenient, brushstroke is smooth during writing, handwriting is uniform, and preservation life is long.
Description
Technical field
The present invention relates to the technical field of ink, a kind of the most dry stable ink and preparation method thereof.
Background technology
Ink is that ancient Chinese is write and paint the china ink stick used.The primary raw material of ink is white carbon black, pine soot, glue etc., is carbon unit
Element is with the existence of noncrystalline kenel.Ground by inkstone water and can produce the prepared Chinese ink for brush writing, with colloid in water
Solution exists.Treasure during wherein Huizhou inkstick is China Han ink skill, is also one of " writing brush, ink stick, ink slab and paper " well-known at home and abroad.Because producing
Gain the name in ancient Huizhou mansion.Huizhou inkstick is that the one being made for primary raw material with pine soot, Oleum Verniciae fordii cigarette, paint cigarette, glue is mainly for biography
The special pigment that system calligraphy, drawing use.Through light a cigarette and expect, press mill, dry, frustrate limit, paint in gold, the operation such as mounted box is refined forms,
Finished product have the black profit of color and luster, heavily fortified point and have light, enter that paper is not dizzy, lick pen not glue, prolonged do not take off, fragrance is strong, the feature such as mothproof.Successive dynasties
Huizhou inkstick is various in style, mainly has paint cigarette, oil smoke, pine soot, full cigarette, clean cigarette, subtracts glue, perfuming etc..Senior paint cigarette ink, is to use Oleum Verniciae fordii
Cigarette, Moschus, Borneolum Syntheticum, native gold, Margarita powder etc. more than 10 plant what famous and precious material was made.The skills such as Huizhou inkstick collection drawing, calligraphy, engraving, moulding
Art, in one, makes Miboin body become an a kind of comprehensive gem of art.Huizhou inkstick manufacture skill is complicated, and it is only that different schools are respectively arranged with oneself
Special manufacture skill, close not unofficial biography.
Although traditional ink is good, but the preservation of ink is highly difficult, now retains a small amount of Gu Mo, but the most broken or broken
Damaging, the most few little Chinese stick is intact.Additionally, there is also some defects when using, it is dense that rub-down ink is difficult to mill, easily wraps up in when writing
Pen, wield the pen the most smooth, be difficult to do, poor-performing.
Summary of the invention
It is an object of the invention to provide that a kind of hardness is high, non-friable, bright in color, dense black, light resistance are good stable easily
Dry ink and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of the most dry stable ink, is made up of according to the raw material of weight portion following: cigarette material 18-23 part, pine-seed oil 2-5 part, Semen coryli heterophyllae
Shell extract 3-8 part, Radix phytolaccae extract 0.5-2 part, arabic gum 25-33 part.
As the further scheme of the present invention: described the most dry stable ink, it is made up of according to the raw material of weight portion following: cigarette
Material 19-22 part, pine-seed oil 3-4 part, hazelnut shell extract 4-6 part, Radix phytolaccae extract 1-1.5 part, arabic gum 27-31 part.
As the further scheme of the present invention: described the most dry stable ink, it is made up of according to the raw material of weight portion following: cigarette
Expect 20 parts, pine-seed oil 3.5 parts, hazelnut shell extract 5 parts, Radix phytolaccae extract 1.2 parts, arabic gum 29 parts.
The preparation method of described the most dry stable ink, comprises the steps of:
1) preparation of hazelnut shell extract: hazelnut shell is carried out constant temperature drying under reduced pressure, after pulverizing, 60-80 mesh sieves, and obtains Semen coryli heterophyllae
Shell dry powder is standby；Add the water of hazelnut shell dry powder quality 3-4 times, add the pectase of hazelnut shell dry powder quality 8-15%,
Stirring 1.8-2h at 40-42 DEG C, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, super
The sound time be 50-60min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 5-10min every time, take supernatant and merge,
It is concentrated into the 10%-15% of original volume, prepares hazelnut shell extract；
2) preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 60-80 mesh, add the ethanol water that volumetric concentration is 95%
Solution, is heated to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, closes
And filtrate；In filtrate, add ethyl acetate extract, must be containing the extract of ethyl acetate with do not contain ethyl acetate
Aqueous solution；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract；
3) by cigarette material, pine-seed oil, hazelnut shell extract, Radix phytolaccae extract, arabic gum mixing, cigarette material quality 0.2-is added
The water of 0.4 times, is stirred, and after stirring, then stands 2-3h at 45-48 DEG C of lower seal, then carries out pestle and smashes and break into turning over
Type, then carry out shaping, dry in the air ink, prepares the most dry stable ink.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention at the interaction of each raw material and the ink for preparing under conditions of using above-mentioned preparation technology, have hardness high,
Non-friable, bright in color, dense black, stability is high, light resistance good, write after the feature that is dried rapidly, additionally it is possible to convenient grind, subtract
Few milling time, fineness meets application demand, and haftplatte test performance also increases, and luck write by the prepared Chinese ink of the present invention
Pen is smooth, person's handwriting is uniform, preserves the life-span long, and overall performance and quality have advantage, are suitable to calligraphy, the creation of paintings and collection.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of the most dry stable ink, it is made up of according to the raw material of weight portion following: 18 parts of cigarette material, Semen Pini
Oil 2 parts, hazelnut shell extract 3 parts, Radix phytolaccae extract 0.5 part, arabic gum 25 parts.
The preparation of hazelnut shell extract: hazelnut shell is carried out constant temperature drying under reduced pressure, after pulverizing, 60 mesh sieve, and obtain Semen coryli heterophyllae
Shell dry powder is standby；Add the water of hazelnut shell dry powder quality 3 times, add the pectase of hazelnut shell dry powder quality 8%, at 40 DEG C
Stirring 1.8h, prepares enzymolysis solution, then enzymolysis solution is carried out supersound process, and sonification power is 1000W, and ultrasonic time is
Centrifugal treating 3 times under the rotating speed of 50min, 3000r/min, are centrifuged 5min every time, take supernatant and merge, are concentrated into original volume
10%, prepare hazelnut shell extract.The preparation of Radix phytolaccae extract: Radix Phytolaccae is dried pulverizing raw material to 60 mesh, addition volumetric concentration is
The ethanol water of 95%, is heated to 58 DEG C of reflux, extract, 6h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, one
Secondary, merging filtrate；In filtrate, add ethyl acetate extract, must be containing the extract of ethyl acetate with do not contain acetic acid second
The aqueous solution of ester；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, pine-seed oil, hazel
Sub-shell extract, Radix phytolaccae extract, arabic gum mix, and add the water of cigarette material quality 0.2 times, are stirred, stir
After, then stand 2h at 45 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, then carry out shaping, dry in the air ink, prepares stable the most dry
Ink.
Embodiment 2
In the embodiment of the present invention, a kind of the most dry stable ink, it is made up of according to the raw material of weight portion following: 23 parts of cigarette material, Semen Pini
Oil 5 parts, hazelnut shell extract 8 parts, Radix phytolaccae extract 2 parts, arabic gum 33 parts.
The preparation of hazelnut shell extract: hazelnut shell is carried out constant temperature drying under reduced pressure, after pulverizing, 80 mesh sieve, and obtain Semen coryli heterophyllae
Shell dry powder is standby；Add the water of hazelnut shell dry powder quality 4 times, add the pectase of hazelnut shell dry powder quality 15%, at 42 DEG C
Stirring 2h, prepares enzymolysis solution, then enzymolysis solution is carried out supersound process, and sonification power is 1000W, and ultrasonic time is 60min,
Centrifugal treating 3 times under the rotating speed of 3000r/min, are centrifuged 10min every time, take supernatant and merge, are concentrated into the 15% of original volume,
Prepare hazelnut shell extract.The preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 80 mesh, adding volumetric concentration is 95%
Ethanol water, be heated to 60 DEG C of reflux, extract, 6.5h, ceramic membrane filter once filtrate, filtering residue repeat reflux, extract, one
Secondary, merging filtrate；In filtrate, add ethyl acetate extract, must be containing the extract of ethyl acetate with do not contain acetic acid second
The aqueous solution of ester；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, pine-seed oil, hazel
Sub-shell extract, Radix phytolaccae extract, arabic gum mix, and add the water of cigarette material quality 0.4 times, are stirred, stir
After, then stand 3h at 48 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, then carry out shaping, dry in the air ink, prepares stable the most dry
Ink.
Embodiment 3
In the embodiment of the present invention, a kind of the most dry stable ink, it is made up of according to the raw material of weight portion following: 19 parts of cigarette material, Semen Pini
Oil 3 parts, hazelnut shell extract 4 parts, Radix phytolaccae extract 1 part, arabic gum 27 parts.
The preparation of hazelnut shell extract: hazelnut shell is carried out constant temperature drying under reduced pressure, after pulverizing, 70 mesh sieve, and obtain Semen coryli heterophyllae
Shell dry powder is standby；Add the water of hazelnut shell dry powder quality 3.5 times, add the pectase of hazelnut shell dry powder quality 12%, at 41 DEG C
Lower stirring 1.9h, prepares enzymolysis solution, then enzymolysis solution is carried out supersound process, and sonification power is 1000W, and ultrasonic time is
Centrifugal treating 3 times under the rotating speed of 55min, 3000r/min, are centrifuged 8min every time, take supernatant and merge, are concentrated into original volume
12%, prepare hazelnut shell extract.The preparation of Radix phytolaccae extract: Radix Phytolaccae is dried pulverizing raw material to 70 mesh, addition volumetric concentration is
The ethanol water of 95%, is heated to 59 DEG C of reflux, extract, 6.2h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract,
Once, merging filtrate；In filtrate, add ethyl acetate extract, must be containing the extract of ethyl acetate with do not contain acetic acid
The aqueous solution of ethyl ester；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, pine-seed oil,
Hazelnut shell extract, Radix phytolaccae extract, arabic gum mix, and add the water of cigarette material quality 0.3 times, are stirred, and stirring is all
After even, then stand 2.5h at 47 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, then carry out shaping, dry in the air ink, prepare stable easily
Dry ink.
Embodiment 4
In the embodiment of the present invention, a kind of the most dry stable ink, it is made up of according to the raw material of weight portion following: 22 parts of cigarette material, Semen Pini
Oil 4 parts, hazelnut shell extract 6 parts, Radix phytolaccae extract 1.5 parts, arabic gum 31 parts.
Preparation process is consistent with embodiment 3.
Embodiment 5
In the embodiment of the present invention, a kind of the most dry stable ink, it is made up of according to the raw material of weight portion following: 20 parts of cigarette material, Semen Pini
Oil 3.5 parts, hazelnut shell extract 5 parts, Radix phytolaccae extract 1.2 parts, arabic gum 29 parts.
Preparation process is consistent with embodiment 3.
Comparative example 1
In addition to not containing hazelnut shell extract, its formula, preparation process are consistent with embodiment 5.
Comparative example 2
In addition to not containing Radix phytolaccae extract, its formula, preparation process are consistent with embodiment 5.
Comparative example 3
In addition to not containing hazelnut shell extract, Radix phytolaccae extract, its formula, preparation process are consistent with embodiment 5.
Table 1 is by the black test result table of embodiment 1-5 Yu comparative example 1-3
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Fineness (micron) | 26 | 26 | 26 | 26 | 26 | 26 | 26 | 26 |
| Haftplatte is tested | 9.5 | 9.5 | 9.6 | 9.6 | 9.7 | 9.1 | 9.2 | 9 |
| Adhesive force (10=is best, and 0=is worst) | 10 | 10 | 10 | 10 | 10 | 9 | 9 | 8 |
| (8=is colour-fast, and 0=is tight for resistance to optical tests Heavily fade) | 8 | 8 | 8 | 8 | 8 | 8 | 8 | 8 |
| Color and luster | Well | Well | Well | Well | Well | Well | Well | Typically |
| Blackness | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black | Dense black |
| Hardness | In hardness, the most broken Do not split | In hardness, the most broken Do not split | Hardness is big, the most broken Do not split | Hardness is big, the most broken Do not split | Hardness is big, the most broken Do not split | Hardness is big, has Crackle | In hardness, have Crackle | Hardness is little, Frangible |
| Rub-down ink | Easily grind dense | Easily grind dense | Easily mill is dense | Easily mill is dense | Easily mill is dense | It is difficult to grind dense | It is difficult to grind dense | It is difficult to grind dense |
| Wield the pen fluency | Well | Well | Well | Well | Well | Typically | Typically | Wrap up in pen |
| Uniformity | Well | Well | Well | Well | Well | Typically | Typically | Poor |
| Drying time (s) | 28 | 25 | 20 | 19 | 17 | 94 | 68 | 102 |
| Stability | Well | Well | Well | Well | Well | Well | Well | Well |
Knowable to from upper table, embodiment of the present invention 1-5 is compared with the ink of comparative example 1-3, and it main advantage is that and can facilitate
Grinding, reduce milling time, meet application demand (26 microns or less) in fineness, haftplatte test performance also increases, ink
Hardness relatively large, non-friable, its bright in color, dense black；And the present invention is in use, ink color thick black, when writing
Wield the pen smoothness, person's handwriting is uniform, and prepared Chinese ink uniformity is good, stability is high, light resistance is good, just can be dried rapidly less than half a minute, whole
Body performance and quality also have advantage.Illustrate that the present invention acts on and under conditions of above-mentioned preparation technology the common of each component,
There is above-mentioned advantage.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (4)
1. a most dry stable ink, it is characterised in that be made up of according to the raw material of weight portion following: cigarette material 18-23 part, Semen Pini
Oil 2-5 part, hazelnut shell extract 3-8 part, Radix phytolaccae extract 0.5-2 part, arabic gum 25-33 part.
The most dry stable ink the most according to claim 1, it is characterised in that be made up of according to the raw material of weight portion following:
Cigarette material 19-22 part, pine-seed oil 3-4 part, hazelnut shell extract 4-6 part, Radix phytolaccae extract 1-1.5 part, arabic gum 27-31 part.
The most dry stable ink the most according to claim 2, it is characterised in that be made up of according to the raw material of weight portion following:
20 parts of cigarette material, pine-seed oil 3.5 parts, hazelnut shell extract 5 parts, Radix phytolaccae extract 1.2 parts, arabic gum 29 parts.
4. the preparation method of the stable the most dry ink as described in claim 1-3 is arbitrary, it is characterised in that by following steps
Composition:
1) preparation of hazelnut shell extract: hazelnut shell is carried out constant temperature drying under reduced pressure, after pulverizing, 60-80 mesh sieves, and obtains Semen coryli heterophyllae
Shell dry powder is standby；Add the water of hazelnut shell dry powder quality 3-4 times, add the pectase of hazelnut shell dry powder quality 8-15%,
Stirring 1.8-2h at 40-42 DEG C, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, super
The sound time be 50-60min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 5-10min every time, take supernatant and merge,
It is concentrated into the 10%-15% of original volume, prepares hazelnut shell extract；
2) preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 60-80 mesh, add the ethanol water that volumetric concentration is 95%
Solution, is heated to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, closes
And filtrate；In filtrate, add ethyl acetate extract, must be containing the extract of ethyl acetate with do not contain ethyl acetate
Aqueous solution；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract；
3) by cigarette material, pine-seed oil, hazelnut shell extract, Radix phytolaccae extract, arabic gum mixing, cigarette material quality 0.2-is added
The water of 0.4 times, is stirred, and after stirring, then stands 2-3h at 45-48 DEG C of lower seal, then carries out pestle and smashes and break into turning over
Type, then carry out shaping, dry in the air ink, prepares the most dry stable ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610201469.0A CN105778623A (en) | 2016-03-31 | 2016-03-31 | Stable and easy-dry ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610201469.0A CN105778623A (en) | 2016-03-31 | 2016-03-31 | Stable and easy-dry ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105778623A true CN105778623A (en) | 2016-07-20 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610201469.0A Pending CN105778623A (en) | 2016-03-31 | 2016-03-31 | Stable and easy-dry ink and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107011735A (en) * | 2017-05-11 | 2017-08-04 | 黄山市古城歙砚有限公司 | A kind of ink of high fineness and preparation method thereof |
| CN115353769A (en) * | 2022-08-24 | 2022-11-18 | 安徽省绩溪旭龙山庄四宝文化有限公司 | Preparation method of Huizhou ink with uniform blackness |
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| JP2008106080A (en) * | 2006-10-23 | 2008-05-08 | Pilot Ink Co Ltd | Water-based ink composition for writing utensil and writing utensil comprising the same housed therein |
| CN102533003A (en) * | 2012-03-01 | 2012-07-04 | 黄山市歙县聚墨堂墨业有限公司 | Non-cracking ink |
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- 2016-03-31 CN CN201610201469.0A patent/CN105778623A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008106080A (en) * | 2006-10-23 | 2008-05-08 | Pilot Ink Co Ltd | Water-based ink composition for writing utensil and writing utensil comprising the same housed therein |
| CN102533003A (en) * | 2012-03-01 | 2012-07-04 | 黄山市歙县聚墨堂墨业有限公司 | Non-cracking ink |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107011735A (en) * | 2017-05-11 | 2017-08-04 | 黄山市古城歙砚有限公司 | A kind of ink of high fineness and preparation method thereof |
| CN115353769A (en) * | 2022-08-24 | 2022-11-18 | 安徽省绩溪旭龙山庄四宝文化有限公司 | Preparation method of Huizhou ink with uniform blackness |
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