CN105820658A - Stable ink and preparation method thereof - Google Patents
Stable ink and preparation method thereof Download PDFInfo
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- CN105820658A CN105820658A CN201610201487.9A CN201610201487A CN105820658A CN 105820658 A CN105820658 A CN 105820658A CN 201610201487 A CN201610201487 A CN 201610201487A CN 105820658 A CN105820658 A CN 105820658A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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Abstract
The invention discloses stable ink. The stable ink is characterized being prepared from the following raw materials in parts by weight: 15 to 25 parts of tobacco materials, 2 to 6 parts of walnut oil, 3 to 9 parts of spice extracts, 0.5 to 2.5 parts of pokeweed extracts, 25 to 35 parts of thickeners, 4 to 8 parts of anti-settling agents, 1 to 5 parts of stabilizers, 2 to 6 parts of wetting agents and 2 to 6 parts of preservatives. The preparation method of the stable ink comprises the following steps: carrying out constant-temperature decompression and drying on spices, grinding, enzymatic hydrolysis, ultrasonic treatment, centrifugation and concentration to obtain the spice extracts; drying and grinding pokeweed, adding an ethanol aqueous solution to carry out reflux extraction, adding ethyl acetate to perform extraction, carrying out vacuum concentration on extract liquid containing ethyl acetate to be dried to obtain the pokeweed extracts; mixing the tobacco materials, the walnut oil, the spice extracts, the pokeweed extracts and the thickeners, then adding water and stirring, sealing and allowing standing still, pestling, turning, beating and forming, shaping, and drying ink to obtain the stable and easily dried ink. The stable ink disclosed by the invention has high hardness, difficult breakage, bright color, concentrated blackness, high stability, good light fastness, convenient grinding, smooth writing and pen movement, uniform handwriting and long preservation life.
Description
Technical field
The present invention relates to the technical field of ink, particularly relate to a kind of stable ink and preparation method thereof.
Background technology
Ink is that ancient Chinese is write and paint the china ink stick used.The primary raw material of ink is white carbon black, pine soot, glue etc., is the carbon existence with noncrystalline kenel.Being ground by inkstone water and can produce the prepared Chinese ink for brush writing, in water, the solution with colloid exists.Treasure during wherein Huizhou inkstick is China Han ink skill, is also one of " writing brush, ink stick, ink slab and paper " well-known at home and abroad.Gain the name because originating in ancient Huizhou mansion.Huizhou inkstick is a kind of special pigment used mainly for traditional calligraphy, drawing being made for primary raw material with pine soot, Oleum Verniciae fordii cigarette, paint cigarette, glue.Through light a cigarette and expect, press mill, dry, frustrate limit, paint in gold, the operation such as mounted box is refined forms, finished product have the black profit of color and luster, heavily fortified point and have light, enter that paper is not dizzy, lick pen not glue, prolonged do not take off, fragrance is strong, the feature such as mothproof.Successive dynasties Huizhou inkstick is various in style, mainly has paint cigarette, oil smoke, pine soot, full cigarette, clean cigarette, subtracts glue, perfuming etc..Senior paint cigarette ink, plants what famous and precious material was made with Oleum Verniciae fordii cigarette, Moschus, Borneolum Syntheticum, native gold, Margarita powder etc. more than 10.Huizhou inkstick integrates the art such as drawing, calligraphy, engraving, moulding, makes Miboin body become an a kind of comprehensive gem of art.Huizhou inkstick manufacture skill is complicated, and different schools are respectively arranged with the manufacture skill of oneself uniqueness, close not unofficial biography.
Although traditional ink is good, but the preservation of ink is highly difficult, now retains a small amount of Gu Mo, but the most broken or damaged, and the most few little Chinese stick is intact.Additionally, there is also some defects when using, it is dense that rub-down ink is difficult to mill, easily wraps up in pen when writing, wield the pen the most smooth, be difficult to do, poor-performing.
Summary of the invention
In order to overcome the defect of above-mentioned prior art, it is an object of the invention to provide a kind of stable ink and preparation method thereof.
The present invention takes techniques below scheme to realize: a kind of stable ink, is made up of according to the raw material of weight portion following: cigarette material 15-25 part, walnut oil 2-6 part, spice extract 3-9 part, Radix phytolaccae extract 0.5-2.5 part, thickening agent 25-35 part, sagging inhibitor 4-8 part, stabilizer 1-5 part, wetting agent 2-6 part, preservative 2-6 part.
Above-mentioned stable ink, is made up of according to the raw material of weight portion following: cigarette material 19-22 part, walnut oil 3-5 part, spice extract 4-8 part, Radix phytolaccae extract 1-2 part, thickening agent 27-33 part, sagging inhibitor 5-7 part, stabilizer 2-4 part, wetting agent 3-5 part, preservative 3-5 part.
Above-mentioned stable ink, is made up of according to the raw material of weight portion following: 20 parts of cigarette material, walnut oil 3.5 parts, spice extract 5 parts, Radix phytolaccae extract 1.2 parts, thickening agent 29 parts, sagging inhibitor 6 parts, stabilizer 3 parts, wetting agent 4 parts, preservative 4 parts.
The preparation method of above-mentioned stable ink, comprises the steps of:
1) preparation of spice extract: spice extract is carried out constant temperature drying under reduced pressure, after pulverizing, 60-80 mesh sieves, and obtains spice extract dry powder standby；Add the water of spice extract dry powder quality 3-4 times, add the pectase of spice extract dry powder quality 8-15%, at 40-42 DEG C, stir 1.8-2h, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, ultrasonic time be 50-60min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 5-10min every time, take supernatant and merge, be concentrated into the 10%-15% of original volume, preparing spice extract；
2) preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 60-80 mesh, adding volumetric concentration is the ethanol water of 95%, is heated to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate；In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and the aqueous solution not containing ethyl acetate；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract；
3) by cigarette material, walnut oil, spice extract, Radix phytolaccae extract, thickening agent, sagging inhibitor, stabilizer, wetting agent, preservative mixing, add the water of cigarette material quality 0.2-0.4 times, it is stirred, after stirring, 2-3h is stood again at 45-48 DEG C of lower seal, then carry out pestle and smash and turn over the type of breaking into, then carry out shaping, dry in the air ink, prepares the most dry stable ink.
The method have the advantages that the present invention is at the interaction of each raw material and the ink for preparing under conditions of using above-mentioned preparation technology in sum, there is hardness high, non-friable, bright in color, dense black, stability is high, light resistance is good, the feature being dried rapidly after writing, can also conveniently grind, reduce milling time, fineness meets application demand, haftplatte test performance also increases, the smoothness and the prepared Chinese ink of the present invention is wield the pen when writing, person's handwriting is uniform, preserve the life-span long, overall performance and quality have advantage, be suitable to calligraphy, the creation of paintings and collection.
Detailed description of the invention
Embodiment 1
In the embodiment of the present invention, a kind of the most dry stable ink, is made up of according to the raw material of weight portion following: 18 parts of cigarette material, walnut oil 2 parts, spice extract 3 parts, Radix phytolaccae extract 0.5 part, thickening agent 25 parts, sagging inhibitor 6 parts, stabilizer 3 parts, wetting agent 4 parts, preservative 4 parts.
The preparation of spice extract: spice extract is carried out constant temperature drying under reduced pressure, after pulverizing, 60 mesh sieve, and obtain spice extract dry powder standby；Add the water of spice extract dry powder quality 3 times, add the pectase of spice extract dry powder quality 8%, at 40 DEG C, stir 1.8h, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, ultrasonic time be 50min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 5min every time, take supernatant and merge, be concentrated into the 10% of original volume, preparing spice extract.The preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 60 mesh, adding volumetric concentration is the ethanol water of 95%, is heated to 58 DEG C of reflux, extract, 6h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate；In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and the aqueous solution not containing ethyl acetate；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, walnut oil, spice extract, Radix phytolaccae extract, thickening agent mixing, add the water of cigarette material quality 0.2 times, be stirred, after stirring, then stand 2h at 45 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, carry out shaping, dry in the air ink again, prepares the most dry stable ink.
Embodiment 2
In the embodiment of the present invention, a kind of the most dry stable ink, is made up of according to the raw material of weight portion following: 23 parts of cigarette material, walnut oil 5 parts, spice extract 8 parts, Radix phytolaccae extract 2 parts, thickening agent 33 parts, sagging inhibitor 5 parts, stabilizer 2 parts, wetting agent 3 parts, preservative 3 parts.
The preparation of spice extract: spice extract is carried out constant temperature drying under reduced pressure, after pulverizing, 80 mesh sieve, and obtain spice extract dry powder standby；Add the water of spice extract dry powder quality 4 times, add the pectase of spice extract dry powder quality 15%, at 42 DEG C, stir 2h, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, ultrasonic time be 60min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 10min every time, take supernatant and merge, be concentrated into the 15% of original volume, preparing spice extract.The preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 80 mesh, adding volumetric concentration is the ethanol water of 95%, is heated to 60 DEG C of reflux, extract, 6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate；In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and the aqueous solution not containing ethyl acetate；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, walnut oil, spice extract, Radix phytolaccae extract, thickening agent mixing, add the water of cigarette material quality 0.4 times, be stirred, after stirring, then stand 3h at 48 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, carry out shaping, dry in the air ink again, prepares the most dry stable ink.
Embodiment 3
In the embodiment of the present invention, a kind of the most dry stable ink, is made up of according to the raw material of weight portion following: 19 parts of cigarette material, walnut oil 3 parts, spice extract 4 parts, Radix phytolaccae extract 1 part, thickening agent 27 parts, sagging inhibitor 7 parts, stabilizer 3 parts, wetting agent 5 parts, preservative 4 parts.
The preparation of spice extract: spice extract is carried out constant temperature drying under reduced pressure, after pulverizing, 70 mesh sieve, and obtain spice extract dry powder standby；Add the water of spice extract dry powder quality 3.5 times, add the pectase of spice extract dry powder quality 12%, at 41 DEG C, stir 1.9h, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, ultrasonic time be 55min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 8min every time, take supernatant and merge, be concentrated into the 12% of original volume, preparing spice extract.The preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 70 mesh, adding volumetric concentration is the ethanol water of 95%, is heated to 59 DEG C of reflux, extract, 6.2h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate；In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and the aqueous solution not containing ethyl acetate；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract.By cigarette material, walnut oil, spice extract, Radix phytolaccae extract, thickening agent mixing, add the water of cigarette material quality 0.3 times, be stirred, after stirring, then stand 2.5h at 47 DEG C of lower seals, then carry out pestle and smash and turn over the type of breaking into, carry out shaping, dry in the air ink again, prepares the most dry stable ink.
Embodiment 4
In the embodiment of the present invention, a kind of the most dry stable ink, is made up of according to the raw material of weight portion following: 22 parts of cigarette material, walnut oil 4 parts, spice extract 6 parts, Radix phytolaccae extract 1.5 parts, thickening agent 31 parts, sagging inhibitor 5 parts, stabilizer 2 parts, wetting agent 3 parts, preservative 3 parts.
Preparation process is consistent with embodiment 3.
Embodiment 5
In the embodiment of the present invention, a kind of the most dry stable ink, is made up of according to the raw material of weight portion following: 20 parts of cigarette material, walnut oil 3.5 parts, spice extract 5 parts, Radix phytolaccae extract 1.2 parts, thickening agent 29 parts, sagging inhibitor 8 parts, stabilizer 5 parts, wetting agent 6 parts, preservative 6 parts.
Preparation process is consistent with embodiment 3.
Comparative example 1
In addition to not containing spice extract, its formula, preparation process are consistent with embodiment 5.
Comparative example 2
In addition to not containing Radix phytolaccae extract, its formula, preparation process are consistent with embodiment 5.
Comparative example 3
In addition to not containing spice extract, Radix phytolaccae extract, its formula, preparation process are consistent with embodiment 5.
Understand from above-described embodiment, embodiment of the present invention 1-5 is compared with the ink of comparative example 1-3, it main advantage is that and can conveniently grind, reduce milling time, meeting application demand (26 microns or less) in fineness, haftplatte test performance also increases, and the hardness of ink is relatively large, non-friable, its bright in color, dense black；And the present invention is in use, ink color thick black, smoothness of wieling the pen when writing, person's handwriting are uniform, and prepared Chinese ink uniformity is good, stability is high, light resistance is good, just can be dried rapidly less than half a minute, and overall performance and quality also have advantage.Illustrate that the present invention, under conditions of the common effect and above-mentioned preparation technology of each component, has above-mentioned advantage.
The above is embodiments of the invention, therefore all equivalence changes done according to structure, feature and the principle described in the present patent application scope or modification, in the range of being all included in present patent application.
Claims (4)
1. a stable ink, it is characterized in that, be made up of according to the raw material of weight portion following: cigarette material 15-25 part, walnut oil 2-6 part, spice extract 3-9 part, Radix phytolaccae extract 0.5-2.5 part, thickening agent 25-35 part, sagging inhibitor 4-8 part, stabilizer 1-5 part, wetting agent 2-6 part, preservative 2-6 part.
Stable ink the most according to claim 1, it is characterized in that, be made up of according to the raw material of weight portion following: cigarette material 19-22 part, walnut oil 3-5 part, spice extract 4-8 part, Radix phytolaccae extract 1-2 part, thickening agent 27-33 part, sagging inhibitor 5-7 part, stabilizer 2-4 part, wetting agent 3-5 part, preservative 3-5 part.
Stable ink the most according to claim 2, it is characterized in that, be made up of according to the raw material of weight portion following: 20 parts of cigarette material, walnut oil 3.5 parts, spice extract 5 parts, Radix phytolaccae extract 1.2 parts, thickening agent 29 parts, sagging inhibitor 6 parts, stabilizer 3 parts, wetting agent 4 parts, preservative 4 parts.
4. the preparation method of the stable ink as described in claim 1-3 is arbitrary, it is characterised in that comprise the steps of:
1) preparation of spice extract: spice extract is carried out constant temperature drying under reduced pressure, after pulverizing, 60-80 mesh sieves, and obtains spice extract dry powder standby；Add the water of spice extract dry powder quality 3-4 times, add the pectase of spice extract dry powder quality 8-15%, at 40-42 DEG C, stir 1.8-2h, prepare enzymolysis solution, then enzymolysis solution is carried out supersound process, sonification power is 1000W, ultrasonic time be 50-60min, 3000r/min rotating speed under centrifugal treating 3 times, be centrifuged 5-10min every time, take supernatant and merge, be concentrated into the 10%-15% of original volume, preparing spice extract；
2) preparation of Radix phytolaccae extract: by Radix Phytolaccae drying pulverizing raw material to 60-80 mesh, adding volumetric concentration is the ethanol water of 95%, is heated to 58-60 DEG C of reflux, extract, 6-6.5h, and ceramic membrane filter once obtains filtrate, and filtering residue repeats reflux, extract, once, merging filtrate；In filtrate, add ethyl acetate extract, the extract that ethyl acetate must be contained and the aqueous solution not containing ethyl acetate；It is evaporated to the extract containing ethyl acetate dry obtain Radix phytolaccae extract；
3) by cigarette material, walnut oil, spice extract, Radix phytolaccae extract, thickening agent, sagging inhibitor, stabilizer, wetting agent, preservative mixing, add the water of cigarette material quality 0.2-0.4 times, it is stirred, after stirring, 2-3h is stood again at 45-48 DEG C of lower seal, then carry out pestle and smash and turn over the type of breaking into, then carry out shaping, dry in the air ink, prepares the most dry stable ink.
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| CN201610201487.9A CN105820658A (en) | 2016-03-31 | 2016-03-31 | Stable ink and preparation method thereof |
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| CN201610201487.9A CN105820658A (en) | 2016-03-31 | 2016-03-31 | Stable ink and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446411A (en) * | 2017-09-20 | 2017-12-08 | 安徽良才墨业有限公司 | A kind of natural liquid ink formulations and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446411A (en) * | 2017-09-20 | 2017-12-08 | 安徽良才墨业有限公司 | A kind of natural liquid ink formulations and preparation method thereof |
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Application publication date: 20160803 |
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