CN105640409B - It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory - Google Patents

It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory Download PDF

Info

Publication number
CN105640409B
CN105640409B CN201610081959.1A CN201610081959A CN105640409B CN 105640409 B CN105640409 B CN 105640409B CN 201610081959 A CN201610081959 A CN 201610081959A CN 105640409 B CN105640409 B CN 105640409B
Authority
CN
China
Prior art keywords
towel
extract
lavatory
going
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201610081959.1A
Other languages
Chinese (zh)
Other versions
CN105640409A (en
Inventor
李伏君
蒋加拉
孟君
縢晖
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhuzhou Qianjin Pharmaceutical Co Ltd
Original Assignee
Zhuzhou Qianjin Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhuzhou Qianjin Pharmaceutical Co Ltd filed Critical Zhuzhou Qianjin Pharmaceutical Co Ltd
Priority to CN201610081959.1A priority Critical patent/CN105640409B/en
Publication of CN105640409A publication Critical patent/CN105640409A/en
Application granted granted Critical
Publication of CN105640409B publication Critical patent/CN105640409B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47KSANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
    • A47K10/00Body-drying implements; Toilet paper; Holders therefor
    • A47K10/16Paper towels; Toilet paper; Holders therefor
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/74Rubiaceae (Madder family)
    • A61K36/744Gardenia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/75Rutaceae (Rue family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0012Galenical forms characterised by the site of application
    • A61K9/0034Urogenital system, e.g. vagina, uterus, cervix, penis, scrotum, urethra, bladder; Personal lubricants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/70Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
    • A61K9/7007Drug-containing films, membranes or sheets
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/333Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/39Complex extraction schemes, e.g. fractionation or repeated extraction steps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/53Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Medical Informatics (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Gynecology & Obstetrics (AREA)
  • Reproductive Health (AREA)
  • Urology & Nephrology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a kind of with antibacterial, disinfection towel of going to the lavatory, and the towel of going to the lavatory is formed by the base fabric for having adsorbed antibacterial disinfection medical fluid;The medical fluid includes the active constituent of following parts by weight:8-12 parts of Cortex Dictamni extract, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, 6-10 parts of capejasmine extract.The towel of going to the lavatory has the effect of the remaining urine of the absorption small private parts after an action of the bowels of women, to keep pudendum cleaning dry and comfortable;Meanwhile the medical fluid of absorption has antibacterial, sterilization and antiinflammation, provides good articles for the small cleaning after an action of the bowels of women, has broad application prospects.

Description

It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
Technical field
The present invention relates to a kind of with antibacterial, disinfection towel of going to the lavatory, while being related to the preparation of above-mentioned towel of going to the lavatory.
Background technique
As attention degree of the masses for personal hygiene aggravates, with antibacterial, disinfection hygienic articles at present As much-sought-after item.Such as:
Chinese patent CN1062467C discloses a kind of clean-preserving agent, is 1-3% by weight ratio0Borneol, crude drug in whole contains Amount be every milliliter 0.3-0.5 grams, alcohol that remaining is 10-15% concentration forms, crude drug in whole include climbing groundsel, cortex dictamni, radix saposhnikoviae, Folium artemisiae argyi, frutus cnidii, Chinese gall, borneol, which is added, when preparation, after primary medicinal alcohol is soaked, leaked can be prepared by.By above-mentioned guarantor The first woven fabric of clean dose of infiltration can be made into moist-retaining tissues, can be used in preventing and treating skin disease and gynaecological disease.
Although above-mentioned clean-preserving agent has preferable antibacterial, disinfection and antiinflammation, found in practical application, exist with Lower Railway Project:
1) women is small after an action of the bowels, and private parts itself is due to there are urine left, needing to inhale using the excellent paper handkerchief of the water imbibition of dry state Urine, clean is received, and the small requirement for absorbing urine cleaning private parts after an action of the bowels is not achieved in wet tissue.
2) borneol has refrigerant experience sense, and human body is also easy to produce dependence, and the reproductive system for being harmful to women is used for a long time Health.
Chinese patent CN101869537B discloses a kind of wet tissue of clean yin of Ms that can be sterilized, sterilize.The Ms is clean The solution of dark and damp towel is made of lactic acid, benzethonium chloride, propylene glycol, sorbierite, medicinal menthol, water.When preparation, cut, The cotton spun laced fabric sterilize, sterilized is immersed in leaching in prepared solution (being equivalent to antibacterial, disinfection medical fluid) 3-5 hour is steeped, sealed, sterile packs to obtain wet tissue.Wet tissue sealed package, is easy to carry about with one made from above-mentioned medical fluid, user Just.Place need not be avoided, be not necessarily to cleaning ware, only needing wet tissue one to open can reach clean purpose into lavatory wiping.
Although above-mentioned wet tissue has preferable sterilizing cleaning effect, found in practical application, there are wet tissues inherently It is hygrometric state, the remaining urine of the small private parts after an action of the bowels of women can not be absorbed, be not able to maintain the shortcomings that private parts dry and comfortable effect.
In addition to the above-mentioned known product enumerated, on the market much with wet tissue that is antibacterial, sterilizing, drug ingedient is in addition to containing There are certain medicinal herb components, while being also added to some chemical drug ingredient such as benzethonium chlorides, long-time service has skin and mucous membrane Irritation, and the normal pH value of vagina is easily influenced, it is easy to the breeding of germ, mould instead.
Therefore, need to be proposed that one kind is antibacterial, disinfection is significant and urine convenient for female cleans the dry state women paper used Towel.
Summary of the invention
To overcome the above disadvantages, the present invention provides a kind of with antibacterial, disinfection towel of going to the lavatory, the towel of going to the lavatory Base fabric by having adsorbed antibacterial disinfection medical fluid is formed;The medical fluid includes the active constituent of following parts by weight:Cortex Dictamni extract 8-12 parts, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, 6-10 parts of capejasmine extract.
The concrete mode of above-mentioned " absorption " includes infiltration or spraying etc..
Above-mentioned parts by weight are μ g, mg, g, one of kg well known in the art, or are its multiple, such as 1/100,1/10,10 Times, 100 times etc..
Preferably, the medical fluid includes the active constituent of following parts by weight:10 parts of Cortex Dictamni extract, capillary extract 15 Part, 12 parts of Herba Senecionis Scandentis extract, 8 parts of capejasmine extract.
Medical fluid of the present invention provides active constituent with cortex dictamni, oriental wormwood, climbing groundsel, cape jasmine combination, wherein cortex dictamni The main active of extract is dictamine, and the main active of capillary extract is capillarin, Herba Senecionis Scandentis extract master Wanting active constituent is senecionine, and the main active of capejasmine extract is Gardenoside, above-mentioned active constituent compatible use, Ensure quality of liquid medicine.
Ordinary commercial products can be used in above-mentioned active constituent, in order to ensure towel of going to the lavatory is antibacterial, the effect of disinfection, the present invention The Cortex Dictamni extract, capillary extract, Herba Senecionis Scandentis extract, capejasmine extract are preferably extracted by method as described below It obtains.
Cortex Dictamni extract, capillary extract, Herba Senecionis Scandentis extract are after being extracted after crushing raw material with ethanol solution It is concentrated to obtain.
Specifically, the extracting method of the Cortex Dictamni extract is as follows:By cortex dictamni grinding and sieving (preferably 30 mesh), press According to 1:15-1:20 solid-liquid ratio (g:Ml), 80-90min, concentration extraction are extracted with the EtOH Sonicate of volume fraction 85%-95% Liquid at medicinal extract (preferably relative density be 1.1-1.3 medicinal extract) to get;Wherein, preferably the frequency of ultrasonic extraction is 20-60kHz, Power is 400-1200W.
It is preferred that cortex dictamni is smashed it through 30 meshes, according to 1:16-1:19 solid-liquid ratio (g:Ml), volume fraction is used The EtOH Sonicate of 88%-92% extracts 83-87min, concentrated extracting solution at the medicinal extract of relative density 1.1-1.3 to get.Wherein, The frequency of ultrasonic extraction is 40kHz, power 500W.
Using said extracted method, the recovery rate of effective component dictamine can be made to greatly improve, make the suppression in prescription Bacterium bactericidal effect is also improved simultaneously.
The extracting method of the capillary extract is as follows:By oriental wormwood grinding and sieving (preferably 30 mesh), according to 1:10-1:20 Solid-liquid ratio (g:Ml), with the ethyl alcohol of volume fraction 60%-80% at 60-80 DEG C ultrasonic extraction 20-40min, concentration extraction Liquid at medicinal extract (preferably relative density be 1.1-1.3 medicinal extract) to get;Wherein, preferably the frequency of ultrasonic extraction is 20-60kHz, Power is 400-1200W.
It is preferred that oriental wormwood is smashed it through 30 meshes, according to 1:13-1:18 solid-liquid ratio (g:Ml), with volume fraction 65%- 75% ethyl alcohol ultrasonic extraction 25-35min at 65-75 DEG C, the medicinal extract that concentrated extracting solution is 1.1-1.3 at relative density, i.e., ?.Wherein, the frequency of ultrasonic extraction is 40kHz, power 500W.
Using said extracted method, it can make that the recovery rate of effective component capillarin greatly improves, other have bacteriostasis efficacy Flavone compound yield up to 4-6% so that in prescription restraining and sterilizing bacteria effect simultaneously be also improved.
The extracting method of the Herba Senecionis Scandentis extract is as follows:Climbing groundsel is put in 55-65 DEG C of insulating box dry 0.5-2h, Grinding and sieving (preferably 30 meshes);2-4 is extracted at 55-65 DEG C with the 50-70% ethyl alcohol for being equivalent to 10-14 times of its quality Secondary, extraction time is 1-3h every time, respectively combined extract and be condensed into medicinal extract (preferably relative density be 1.1-1.3 leaching Cream);
It is preferred that climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, 30 meshes are smashed it through;With being equivalent to 12 times of its quality 60% ethyl alcohol extracts 3 times at 60 DEG C, and extraction time is respectively 2h, 1.5h, 1h, combined extract and is condensed into relatively close respectively Degree be 1.1-1.3 medicinal extract to get.
Using said extracted method, the recovery rate of effective component senecionine can be made to greatly improve, other have antibacterial function The phenolic acid compound recovery rate of effect can also be promoted, so that the restraining and sterilizing bacteria effect in prescription is also improved simultaneously.
Capejasmine extract be after cape jasmine is crushed after ester extracts through being concentrated to get.
Specifically, the extracting method of the capejasmine extract is as follows:By cape jasmine grinding and sieving (preferably 30 meshes), according to 1:Solid-liquid ratio (the g of (45-55):Ml), to be extracted 1-3 times at 65-80 DEG C with ethyl acetate, extraction time is 1-4h every time, point Other combined extract and be condensed into medicinal extract (preferably relative density be 1.1-1.3 medicinal extract);
Using such extracting method, it can be ensured that the extraction yield of Gardenoside can effectively ensure the restraining and sterilizing bacteria effect of prescription.
It is preferred that cape jasmine is smashed it through 30 meshes, according to 1:Solid-liquid ratio (the g of (48-52):Ml), with ethyl acetate in 70- Extracted 1-2 times at 76 DEG C, extraction time is respectively 2-3.5h, respectively combined extract and be condensed into relative density be 1.1-1.3 Medicinal extract;
Using preferred extracting method, the extraction yield of Gardenoside can be further provided for, increase rate is up to 0.2%- 0.5%, improve the restraining and sterilizing bacteria effect of prescription.
Medical fluid of the present invention still further comprises solvent in addition to above-mentioned active constituent, i.e., the described medical fluid by activity at Dispersion is formed in a solvent.It is preferred that the dosage of the solvent is 200-900 parts by weight.
Specifically, medical fluid of the present invention is used as solvent with ethanol water, water, propylene glycol, glycerine etc., with more advantageous In dispersion of active ingredients, it is ensured that medical fluid/towel of going to the lavatory quality.
When the solvent is ethanol water, volumetric concentration is advisable in 50-75%, preferably 60-70%.
It further include spice additive in medical fluid of the present invention, the odor additive includes pure natural spice or artificial fragrant Material.
Wherein, the pure natural spice is selected from one or more of elscholtiza, borneol, oriental wormwood, peppermint hydrosol and yellow wormwood artemisia;Institute It states plants essential oil and is selected from Chinese torreya essential oil, mother chrysanthemum flower essential oil, daphne odera essential oil, pinecone essential oil, mugwort oil, thyme essential oil, You Jia One or more of sharp essential oil, tea tree ethereal oil and camphor tree essential oil.
Preferably, various plants essential oils and chemical synthesis essence, especially Elsholtzia cilita essential oil, argy wormwood may be selected in the artificial flavors Oil, daphne odera essential oil and camphor tree essential oil, such essential oil is preferably to be added medical fluid of the present invention, further to adjust gas Taste increases effect.
The dosage of above-mentioned spice additive, which is subject to, can make the medical fluid form pleasant fragrance, when selection plants essential oil When, ideal dosage is 0.1%-0.3%, can specifically be adjusted according to actual conditions.
Towel of the present invention of going to the lavatory is wet tissue or dry towel, and the base fabric is selected from non-woven fabrics or domestic paper, the domestic paper It is preferred that wettable domestic paper.Wherein, domestic paper refers to paper for daily use, refer to for look after it is personal at home, it is outgoing it is equal used in all kinds of defend Raw wiping paper, including roll toilet paper, extraction-type toilet paper, Boxed facial tissue, pocket face-tissue, paper handkerchief, napkin paper, wiping hand Paper, kitchen towels.Wettable domestic paper refers to that wet strength is preferable in domestic paper, can wipe at home and not allow in the case where getting wet Easily rupturable paper.
When the towel of going to the lavatory is wet tissue, non-woven fabrics or domestic paper is may be selected in the base fabric, i.e., the medical fluid is infiltrated institute Stating base fabric can be obtained towel wet tissue of going to the lavatory.This field conventional technology can be used in the preparation method for towel wet tissue of going to the lavatory, in order to Obtain the optimal towel wet tissue of going to the lavatory of effect, the present invention is preferably during towel wet tissue is gone to the lavatory in infiltration, use of the medical fluid with respect to base fabric Amount is 4-6ml/g, after infiltration, drains the moisture for towel of going to the lavatory, reaches the wet tissue water content of this field routine.For Medical fluid is set preferably to play antibacterial, disinfection, the infiltration amount that the present invention preferably controls final products herb liquid is 4.5- 5.5g/g being advisable.
When the towel of going to the lavatory is dry towel, domestic paper is may be selected in the base fabric, the needle slurry of the preferably described domestic paper Usage amount is 85% or more, and moisture is less than 9.0%.
Alternatively, the index of the ideal domestic paper at least meets 3 of following index or more (preferably meeting):Thickness For 0.05-0.07mm, longitudinal dry tensile strength is 2000-3200mN, and lateral dry tensile strength is 290-370mN, elongation 9%-11%, 2mm~5mm hole eye number≤6/㎡, single layer transverse direction suction range are not less than 20mm/100s, and the double-deck transverse direction suction range is not less than 40mm/100s。
Preferably, the wettable domestic paper with a thickness of 0.05-0.06mm, longitudinal dry tensile strength is 2480-3000mN, Lateral dry tensile strength is 290-320mN, elongation 10%-11%, 2mm~5mm hole eye number≤6 Ge/㎡, single layer transverse direction suction range Not less than 20mm/100s, the double-deck transverse direction suction range is not less than 40mm/100s.
The life stationery base fabric that the present invention can select further includes such as permanent wettable water paper handkerchief of peace product promise.
The present invention goes to the lavatory the medicine liquid spray the dry towel of towel to obtain the final product on base fabric (and can be described as body paper), the specific spray of medical fluid The amount of spilling can be by those skilled in the art depending on the conventional selection of this field, foundation actual conditions, and medical fluid of the present invention exists Fountain height in base fabric is preferably 0.006-0.008ml/g, and what this fountain height was prepared go to the lavatory, and towel medicine liquid spray is uniform, humidity It is suitable for being easy to use.
In addition, above-mentioned base fabric has preferably covered one layer of smears, such base fabric softness moisturizing, while water imbibition on its surface It is good, more skin-friendly strong with the towel water lock ability of going to the lavatory that this base fabric is prepared.The smears can be selected from commonly used in the art Substance plays optimal effect in order to enable smears can preferably cooperate with medical fluid described herein, and the present invention is preferred Above-mentioned smears is selected from one of moisturizer, softening agent, creams or a variety of, and (smears is opposite for its further preferred coating weight In the mass percent dosage of base fabric) it is 18-25%.Wherein, the moisturizer be selected from glycerol, polyglycereol, transparent Bronsted acid sodium, One or more of aloe extract.
Invention also provides the preparation methods of above-mentioned towel of going to the lavatory, as one of technical solution of the present invention, when described When towel of going to the lavatory is wet tissue, preparation method specifically comprises the following steps:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, cape jasmine is taken to mention Take 6-10 parts of object, it is spare;
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly;
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, it is fixed Hold to 700-900 parts;Or it is further added in the supernatant and adds solvent constant volume again after spice additive and disappear to get antibacterial Poison liquid;
(4) by the antibacterial disinfection medical fluid infiltration base fabric to get.
Preferably, step (4) herb liquid is 4-6ml/g with respect to the dosage of base fabric.
Preferably, the solvent is 50-75% ethanol solution or water.
Wherein, step (2) is predissolve step, and the 8-12% of the partial solvent preferred solvent total volume, predissolve has The abundant dissolution for helping active constituent, improves the quality of medical fluid.
As another technical solution of the invention, when the towel of going to the lavatory is dry towel, preparation method specifically include as Lower step:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, cape jasmine is taken to mention Take 6-10 parts of object, it is spare;
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly;
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, it is fixed Hold to 200-400 parts;Or it is further added in the supernatant and adds solvent constant volume again after spice additive and disappear to get antibacterial Poison liquid;
(4) by the antibacterial disinfection medical fluid be sprayed at scrim surfaces to get.
Fountain height of the medical fluid of the present invention in base fabric is preferably 0.006-0.008ml/g,
Preferably, the solvent is 50-75% ethanol solution or glycerine.
Step (2) is predissolve step, and the 8-12% of the partial solvent preferred solvent total volume, predissolve helps to live The abundant dissolution of property ingredient, improves the quality of medical fluid.
Currently, life paper conversion mainly includes two processes:Preceding processing and post-processing.Preceding processing refers to that body paper produces, rear to add Work refer to the body paper after cutting is embossed, the processing such as Amscomatic.The present invention is in order to enable final products are more soft wet Profit, pro-skin sense is stronger, and each layer of paper handkerchief is tightly combined, and is easy to use, and in this application, has been especially added with completely new middle processing skill Art, which is to carry out roller coating or spray treatment to body paper using smears before post-processing, in addition, changing existing " being first embossed, rear to fold " mode, using completely new " first folding, rear to be embossed " mode.
Concrete operations are:In step (4), first base fabric is coated using smears, is then cut into base fabric specified Breadth, then folded, be embossed, fold and embossing process in by the antibacterial disinfection medical fluid or antibacterial disinfection medical fluid It is sprayed on the surface of base fabric with fragrance, finally product is packed, is sterilized.
The specification of towel of the present invention of going to the lavatory can be adjusted according to actual conditions, and optimal size is:10cm × 14cm, thickness 16 layers, white embossing, with the fragrance tasteless, the fragrant and a variety of different type of Chinese medicine is light.
Towel of the present invention of going to the lavatory has the following advantages that:
(1) Cortex Dictamni extract in the present invention in the present invention, capillary extract, Herba Senecionis Scandentis extract, cape jasmine are extracted Four kinds of ingredient combinations of object use, and have heat-clearing and damp-drying drug, eliminate dampness with aromatics, restraining and sterilizing bacteria, can prevent microorganism infection, and when use has Cleaning, comfortable, health-care effect.
(2) medical fluid tool of the invention is antibacterial, sterilization and antiinflammation, to skin and vaginal mucosa without any irritation and Side effect, it is fragrant odour, easy to carry.
(3) go to the lavatory towel soft comfortable, good water absorption, the fungistatic effect prepared using medical fluid of the present invention is significant and has The features such as easily disperse.
(4) the advantages that medical fluid of the present invention and towel of going to the lavatory are provided with low in cost, long shelf-life, high stability.
Detailed description of the invention
Fig. 1 is the preparation technology flow chart of towel dry towel of the invention of going to the lavatory.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
All raw materials of the present invention are known commercially available product, and the detection method being related to or operation are such as without special Explanation is the common detection methods or operation of this field.Cortex Dictamni extract involved in following embodiment, a thousand li light extraction Object, capillary extract, capejasmine extract extract by the following method.
Cortex Dictamni extract:Cortex dictamni is smashed it through into 30 meshes, according to 1:18 solid-liquid ratio (g:Ml), volume fraction is used 90% EtOH Sonicate extracts 85min, and concentrated extracting solution is at the medicinal extract of relative density 1.1~1.3 to get, wherein ultrasonic extraction Frequency be 40kHz, power 500W.
Herba Senecionis Scandentis extract:Climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, smashes it through 30 meshes;With being equivalent to it 12 times of 60% ethyl alcohol of quality extracts 3 times at 60 DEG C, and extraction time is respectively 2h, 1.5h, 1h, combined extract and is concentrated respectively At relative density be 1.1-1.3 medicinal extract to get.
Capillary extract:Oriental wormwood is smashed it through into 30 meshes, according to 1:15 solid-liquid ratio (g:Ml), with volume fraction 70% Ethyl alcohol at 70 DEG C ultrasonic extraction 30min, concentrated extracting solution at the medicinal extract that relative density is 1.1~1.3 to get, wherein it is super The frequency that sound extracts is 40kHz, power 500W.
Capejasmine extract:Cape jasmine is smashed it through into 30 meshes, according to 1:50 solid-liquid ratio (g:Ml), with ethyl acetate 74 It is extracted 2 times at DEG C, extraction time is respectively 3h, 2h, combined extract and is condensed into the leaching that relative density is 1.1-1.3 respectively Cream.
Although a kind of above-mentioned specific embodiment for being only exemplified by each extract, it will be appreciated by those skilled in the art that Be be not limited to other extracting methods (method especially in the limited range of the present invention) of ad hoc fashion similarly can be with It realizes essentially identical extraction effect, can be used for realizing the present invention, this is no longer particularly limited.
Only as explaining, such as Cortex Dictamni extract obtained may be equally applied to the present invention in accordance with the following methods:
Cortex Dictamni extract:Cortex dictamni is smashed it through into 30 meshes, according to 1:16 or 1:19 solid-liquid ratio (g:Ml), body is used Fraction 88 or 92% EtOH Sonicate extract 83-87min, concentrated extracting solution at the medicinal extract of relative density 1.1~1.3 to get, Wherein, the frequency of ultrasonic extraction is 60kHz, power 400W.
The parameter of wettable domestic paper used in following embodiment is as follows:With a thickness of 0.05-0.06mm, longitudinal dry tensile strength For 2480-3000mN, lateral dry tensile strength is 290-320mN, and elongation 10%-11%, 2mm~5mm hole eye number≤6 Ge/㎡ is single The lateral suction range of layer is not less than 20mm/100s, and the double-deck transverse direction suction range is not less than 40mm/100s.
It will be appreciated by persons skilled in the art that other suitable paper products can in addition to above-mentioned preferred wettable domestic paper It is equally used for realizing the present invention.
Embodiment 1
Present embodiments provide a kind of with antibacterial, disinfection towel of going to the lavatory, which is wet tissue, towel Chinese medicine of going to the lavatory The infiltration amount of liquid is 4-6g/g;Wherein the base fabric is non-woven fabrics;The specific prescription of the medical fluid is as follows:Cortex Dictamni extract 8 Part, 12 parts of capillary extract, 10 parts of Herba Senecionis Scandentis extract, 6 parts of capejasmine extract, 1 part of daphne odera essential oil, 800 parts of water.
Embodiment 2
Present embodiments provide a kind of with antibacterial, disinfection towel of going to the lavatory, which is dry towel, the towel of going to the lavatory Base fabric by having adsorbed antibacterial disinfection medical fluid is formed, and the base fabric is wettable domestic paper;The specific prescription of the medical fluid is as follows:It is white 10 parts of fresh hide extract, 15 parts of capillary extract, 12 parts of Herba Senecionis Scandentis extract, 8 parts of capejasmine extract, 1 part of daphne odera essential oil, 60% 300 parts of ethyl alcohol, medical fluid are 0.006-0.008ml/g to the fountain height of wettable domestic paper.
Embodiment 3
Present embodiments provide a kind of with antibacterial, disinfection towel of going to the lavatory, which is dry towel, the towel of going to the lavatory Base fabric by having adsorbed antibacterial disinfection medical fluid is formed;The base fabric is wettable domestic paper;The specific prescription of the medical fluid is as follows:It is white 12 parts of fresh hide extract, 18 parts of capillary extract, 15 parts of Herba Senecionis Scandentis extract, 10 parts of capejasmine extract, 300 parts of glycerine, medicine Liquid is 0.006-0.008ml/g to the fountain height of wettable domestic paper.
Embodiment 4
Present embodiments provide a kind of with antibacterial, disinfection towel of going to the lavatory, which is dry towel, the towel of going to the lavatory Base fabric by having adsorbed antibacterial disinfection medical fluid is formed;The base fabric is wettable domestic paper;The specific prescription of the medical fluid is as follows:It is white 10 parts of fresh hide extract, 16 parts of capillary extract, 15 parts of Herba Senecionis Scandentis extract, 9 parts of capejasmine extract, 70% 300 parts of ethyl alcohol, suppression It is 0.006-0.008ml/g to the fountain height of wettable domestic paper that bacterium, which sterilizes medical fluid,.
Embodiment 5
A kind of method prepared described in embodiment 1 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, capillary extract, capejasmine extract are dissolved in 80 parts of water, are stirred Uniformly;
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, daphne odera essential oil is added thereto, so After add remaining water, be uniformly mixed up to antibacterial disinfection medical fluid;
(3) non-woven fabrics that the antibacterial disinfection medical fluid infiltration is cut into suitable dimension, is packed to obtain the final product.
Embodiment 6
A kind of method prepared described in embodiment 2 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically Include the following steps (as shown in Figure 1):
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, capillary extract, capejasmine extract are dissolved in 30 part of 60% ethyl alcohol In, it stirs evenly;
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, daphne odera essential oil is added thereto, is mended Add remaining ethyl alcohol, is uniformly mixed up to antibacterial disinfection medical fluid;
(3) first wettable domestic paper (and can claim body paper) is coated with using rolling method using glycerol (coating weight 20%), then Paper product is cut into 10cm × 14cm breadth, then folded, be embossed, by the antibacterial disinfection in folding and embossing process Medical fluid (fountain height 0.006-0.008ml/g) is sprayed on the surface of paper product, is finally packed to product, ethylene oxide sterilizing To obtain the final product.
Embodiment 7
A kind of method prepared described in embodiment 3 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, capillary extract, capejasmine extract are dissolved in 36 parts of glycerine, It stirs evenly;
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, add remaining glycerine, is uniformly mixed Up to antibacterial disinfection medical fluid;
(3) first wettable domestic paper is coated with using polyglycereol (coating weight 18%) using rolling method, then cuts paper product It at 10cm × 14cm breadth, then folded, be embossed, be sprayed on the antibacterial disinfection medical fluid in embossing process folding The surface (fountain height 0.006-0.008ml/g) of paper product, finally product is packed, ethylene oxide sterilizing to obtain the final product.
Embodiment 8
A kind of method prepared described in embodiment 4 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, capillary extract, capejasmine extract are dissolved in 24 part of 70% ethyl alcohol In, it stirs evenly;
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, add remaining ethyl alcohol, is uniformly mixed i.e. Obtain antibacterial disinfection medical fluid;
(3) first wettable domestic paper is used using softening agent SME-4 (polyoxyethylene stearic acid ester, coating weight 25%) and is sprayed Method coating, then cuts into 10cm × 14cm breadth for paper product, is then folded, is embossed, will in folding and embossing process The antibacterial disinfection medical fluid is sprayed on the surface (fountain height 0.006-0.008ml/g) of paper product, is finally packed, is gone out to product Bacterium to obtain the final product.
Below by way of fungistatic effect, the stability etc. for testing medical fluid of the present invention and towel of going to the lavatory, the present invention is protected Technical solution be further described.
The experiment of one fungistatic effect of experimental example
1, medical fluid fungistatic effect is tested
1.1 experiment reagents (see Table 1 for details):
Table 1:
Licorice, camomile extract and aloe extract etc. can be right by commercially available in above-mentioned control group Preparation according to Fructus Gleditsiae Abnormalis extract in group 6 can refer to China application CN103340816.
1.2 experimental method
Experimental strain:Staphylococcus aureus, Candida albicans, Escherichia coli, Pseudomonas aeruginosa, hemolytic streptococcus;Tool The reference of body experimental procedure《15979-2002 disposable sanitary articles sanitary standard》Regulation.
1.3 experimental result
Experimental result is shown in Table 2:
Table 2:Bacteriostasis rate (%)
Above-mentioned experiment is repeated with the medical fluid of other embodiments of the present invention, obtains essentially identical experiment conclusion.
2, wet tissue fungistatic effect is tested
2.1 experiment reagents (see Table 3 for details):
Table 3:
Experimental group 1 The preparation-obtained wet tissue of embodiment 5 (the infiltration amount of medical fluid is 5g/g, and liquid formula is with embodiment 1)
Compare blank group With experimental group 1, difference is only that wet tissue preparation method:Non-woven fabrics is infiltrated using physiological saline
Control group 1 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 1
Control group 2 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 2
Control group 3 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 3
Control group 4 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 4
Control group 5 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 5
Control group 6 With experimental group 1, difference is only that wet tissue preparation method:Using the active constituent of control group 6
2.2 experimental method:
With 2.1.
2.3 experimental result
See Table 4 for details for experimental result.
Table 4:Bacteriostasis rate (%)
3, dry towel fungistatic effect experiment
3.1 experiment reagents (see Table 5 for details):
Table 5:
Experimental group 1 The preparation-obtained dry towel of embodiment 6 (liquid formula is with embodiment 2)
Compare blank group With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of blank control group
Control group 1 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 1
Control group 2 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 2
Control group 3 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 3
Control group 4 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 4
Control group 5 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 5
Control group 6 With experimental group 1, difference is only that dry towel preparation method:Using the active constituent of control group 6
3.2 experimental method:With 2.2;
3.3 experimental result
See Table 6 for details for experimental result.
Table 6:Bacteriostasis rate (%)
4, wet tissue and the experiment of the long-time stability of dry towel
Experimental subjects:Table 3 after placing 3,6,12 and 24 months after preparation respectively and wet tissue and dry towel in table 5;
Experimental method:With 2.2 and 3.2;
Experimental result is shown in Table 7.
Table 7:Bacteriostasis rate (%)
Two wet tissue of experimental example, dry towel skin irritation test
Laboratory sample:Dry towel in wet tissue and table 2 in table 1
Experimental method:Experiment before rabbit back spinal diamond wool is cut for 24 hours, unhairing range or so give 5cm × 5cm, one For testing, skin is cleaned for compareing, using warm water in side for side, then wipes laboratory sample on a side test skin, Wiping 1 time daily, 1h observes skin wound repair after wiping, and continuous wiping 30 days records experimental result.
Experimental result:As shown in table 8.
8 skin irritation test result of table:
Three wet tissue of experimental example, the experiment of dry towel vaginal irritation
Laboratory sample:Dry towel in wet tissue and table 2 in table 1
Experimental method:SD rat is taken, female, regular grade, weight 220-240g is randomly divided into 16 groups, every group 4.Reference 3.8 in disinfection technology standard (third edition) 1999.11, dry towel, wet tissue are placed in animal intravaginal, contacted with vagina mucosa 2h, puts to death animal after 12h, takes out vagina local organization, and observation is whether there is or not congested, oedema phenomenon, referring to disinfection technology standard (the Three editions) the standards of grading scoring of skin wound repair intensity and skin irritatin strength grading in 1999.11, it carries out to vagina mucosa The evaluation of stimulus intensity.
Experimental result:It is shown in Table 9.
9 vaginal irritation experimental result of table:
Wet tissue of the present invention, dry towel are 0 to rat vagina mucosal irritation reaction top mean value, belong to nonirritant, Shelf-life is 36 months or more.
Experimental example four is gone to the lavatory towel comprehensive quality test experiments
1, by carrying out test discovery to towel of going to the lavatory described in embodiment 6~8, the towel of going to the lavatory being related in above-described embodiment Dry towel can reach index as shown in table 10, and properties are superior to GB/T 20808-2011 to the regulation of super soft paper.
It goes to the lavatory described in 10 embodiment 6-8 of table the product index of the dry towel of towel
2, to embodiment 6 go to the lavatory towel and common commercially available towel products compare, three control groups, control group are set The 1 nose noble's face tissue produced for Japanese king's paper industry, control group 2 is a tissue of Ni Piao company production, and control group 3 is Heng An group heart chief minister's seal tea family of languages column paper handkerchief, as a result as shown in table 11.
Table 11 is gone to the lavatory towel product actual measurement physical index and correlation data
As can be seen from Table 11, the present invention goes to the lavatory, and towel moisture content is suitable, and pliability is good, and has good dry drawing Power and wet tensile strength, entire product sense of touch is soft and moist, and pro-skin sense is strong.
Experimental example five is gone to the lavatory towel material test experiments
The present invention further compared going to the lavatory the material of towel and conventional paper handkerchief, and specific targets are as follows:
1, body-sensing
Body-sensing refers to comfort when consumer's physical examination product, and the comfort of product is better, and body-sensing is better.Material Body-sensing comfort be realized by improving 3 indexs of moisture feeling of the flexibility of paper, surface sophistication and paper, and then reach with Nowadays the domestic paper that women generally uses is compared, and has apparent sense of touch otherness.
(1) flexibility
The pliability of domestic paper includes bulk softness and Surface softness.Bulk softness refers to when people with the hands squeeze The softness of paper can be experienced when platen towel;Surface softness refers to finger tip slight amount, and touches paper back and forth and felt Softness by paper.According to GB/T 20808-2011 to the regulation of super soft paper, single-part stationery pliability is necessary≤40mN.
(2) surface sophistication
Currently without specific detection means, mainly by user's finger tip slight amount, and paper is touched back and forth and is felt Judged by the softness of paper, belongs to an importance in body-sensing.
(3) moisture feeling
Moisture feeling belongs to the new concept in domestic paper, is put forward for the first time for the application.According to GB/T 20808-2011 to super soft paper Regulation, delivery moisture be≤9%.
2, water imbibition
Mainly measured by lateral suction range, according to GB/T 20808-2011 to the regulation of super soft paper, single-part stationery Lateral suction range is greater than 20mm/100s.
3, breaking up property
For tissue Related product, breaking up property is mainly influenced by the additive amount of wet strength agent.Good paper product can reach It abandons after to use in closestool, does not block closestool and sewer, it is degradable, it is free from environmental pollution.
4, toughness
Lateral tensile index and longitudinal wet tensile index are better than GB/T 20808-2011 to the regulation of super soft paper, to reach To that will not be broken easily when body paper normal use use, deform.
It is found by comparison, its pliability of currently marketed paper handkerchief is of the present invention small generally between 38-40mN Solution its pliability of towel is 30 ± 2mN, belongs to the high-class product in super soft paper;The moisture of paper handkerchief is commonly 7% or so on Vehicles Collected from Market, The present invention goes to the lavatory, and towel water conservation moisture pick-up properties is good, and paper handkerchief moisture content remains between 15-18%, and exquisiteness is good, and sense of touch is soft Profit, pro-skin sense are strong;In addition, the present invention goes to the lavatory, the water imbibition of towel also meets national standard, and has good easily disperse, uses After abandon in closestool, do not block closestool and sewer, it is degradable, it is free from environmental pollution.
In addition to this, table 12 has also listed other differences of go to the lavatory towel and conventional paper handkerchief of the invention.
Table 12 is gone to the lavatory the difference of towel and conventional paper handkerchief
Experimental example six is gone to the lavatory towel market questionnaire investigation
The present invention has carried out questionnaire investigation to towel of going to the lavatory simultaneously, as a result as shown in table 13:There is 70.29% women to think very Like going to the lavatory the texture of towel, 26.43% women waits and see.Generally speaking, the public to the degree of recognition of product close to 80%, There are extraordinary market prospects.
Degree of recognition of 13 public of table to towel product of going to the lavatory at this stage
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, this is to this It is for the technical staff of field it will be apparent that these changes and improvements all fall within the protetion scope of the claimed invention.This hair Bright claimed range is defined by the appending claims and its equivalent thereof.

Claims (21)

1. a kind of with antibacterial, disinfection towel of going to the lavatory, it is characterised in that:The towel of going to the lavatory is by having adsorbed antibacterial disinfection medical fluid Base fabric formed;By weight, the active constituent of the medical fluid is as follows:8-12 parts of Cortex Dictamni extract, capillary extract 12- 18 parts, 10-15 parts of Herba Senecionis Scandentis extract, 6-10 parts of capejasmine extract;
The extracting method of the Cortex Dictamni extract is as follows:By cortex dictamni grinding and sieving, according to 1:15-1:20 solid-liquid ratio, Extract 80-90min with the EtOH Sonicate of volume fraction 85%-95%, concentrated extracting solution at medicinal extract to get;
The extracting method of the capillary extract is as follows:By oriental wormwood grinding and sieving, according to 1:10-1:20 solid-liquid ratio, uses body The ethyl alcohol of fraction 60%-80% ultrasonic extraction 20-40min at 60-80 DEG C, concentrated extracting solution at medicinal extract to get;
The extracting method of the Herba Senecionis Scandentis extract is as follows:Climbing groundsel is put in 55-65 DEG C of insulating box dry 0.5-2h, is crushed After be sieved;It is extracted 2-4 times at 55-65 DEG C with the 50-70% ethyl alcohol for being equivalent to 10-14 times of its quality, extraction time is every time 1-3h combined extract and is condensed into medicinal extract respectively;
The extracting method of the capejasmine extract is as follows:By cape jasmine grinding and sieving, according to 1:The solid-liquid ratio of (45-55), uses vinegar Acetoacetic ester extracts 1-3 times at 65-80 DEG C, and extraction time is 1-4h every time, combined extract and is condensed into medicinal extract respectively.
2. towel of going to the lavatory as described in claim 1, it is characterised in that:By weight, the active constituent of the medical fluid is as follows:It is white 10 parts of fresh hide extract, 15 parts of capillary extract, 12 parts of Herba Senecionis Scandentis extract, 8 parts of capejasmine extract.
3. towel of going to the lavatory as claimed in claim 1 or 2, it is characterised in that:The extracting method of the Cortex Dictamni extract is as follows:It will Cortex dictamni smashes it through 30 meshes, according to 1:16-1:19 solid-liquid ratio is extracted with the EtOH Sonicate of volume fraction 88%-92% 83-87min, concentrated extracting solution at the medicinal extract of relative density 1.1-1.3 to get;
And/or:
The extracting method of the capillary extract is as follows:Oriental wormwood is smashed it through into 30 meshes, according to 1:13-1:18 solid-liquid ratio, With the ethyl alcohol of volume fraction 65%-75%, ultrasonic extraction 25-35min, concentrated extracting solution are at relative density at 65-75 DEG C 1.1-1.3 medicinal extract to get;
And/or:
The extracting method of the Herba Senecionis Scandentis extract is as follows:Climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, smashes it through 30 Mesh;It is extracted 3 times at 60 DEG C with 12 times of 60% ethyl alcohol of its quality is equivalent to, extraction time is respectively 2h, 1.5h, 1h, difference Combined extract and be condensed into relative density be 1.1-1.3 medicinal extract to get;
And/or:
The extracting method of the capejasmine extract is as follows:Cape jasmine is smashed it through into 30 meshes, according to 1:The solid-liquid ratio of (48-52), It is extracted 1-2 times at 70-76 DEG C with ethyl acetate, extraction time is respectively 2-3.5h, combined extract and is condensed into phase respectively To density be 1.1-1.3 medicinal extract to get.
4. towel of going to the lavatory as claimed in claim 1 or 2, it is characterised in that:The medical fluid with ethanol water, water, propylene glycol or Glycerine is as solvent.
5. towel of going to the lavatory as claimed in claim 4, it is characterised in that:The dosage of the solvent is 200-900 parts by weight.
6. towel of going to the lavatory as claimed in claim 3, it is characterised in that:The medical fluid is with ethanol water, water, propylene glycol or the third three Alcohol is as solvent.
7. towel of going to the lavatory as claimed in claim 6, it is characterised in that:It is preferred that the dosage of the solvent is 200-900 parts by weight.
8. the towel of going to the lavatory as described in any one of claim 1,2,6, it is characterised in that:It further include fragrance addition in the medical fluid Agent, the spice additive include pure natural spice or artificial flavors.
9. towel of going to the lavatory as claimed in claim 3, it is characterised in that:It further include spice additive in the medical fluid, the fragrance Additive includes pure natural spice or artificial flavors.
10. towel of going to the lavatory as claimed in claim 4, it is characterised in that:It further include spice additive in the medical fluid, the fragrance Additive includes pure natural spice or artificial flavors.
11. towel of going to the lavatory as claimed in claim 8, it is characterised in that:The pure natural spice is selected from elscholtiza, borneol, oriental wormwood, thin One or more of lotus hydrosol and yellow wormwood artemisia;The artificial flavors include plants essential oil and chemical synthesis essence;The plant essence Oil is selected from Chinese torreya essential oil, mother chrysanthemum flower essential oil, daphne odera essential oil, pinecone essential oil, mugwort oil, thyme essential oil, eucalyptus quintessence oil, tea Set one or more of essential oil and camphor tree essential oil.
12. the towel of going to the lavatory as described in any one of claim 1,2,6,9,10,11, it is characterised in that:The towel of going to the lavatory is wet Towel or dry towel.
13. towel of going to the lavatory as claimed in claim 3, it is characterised in that:The towel of going to the lavatory is wet tissue or dry towel.
14. towel of going to the lavatory as claimed in claim 4, it is characterised in that:The towel of going to the lavatory is wet tissue or dry towel.
15. towel of going to the lavatory as claimed in claim 8, it is characterised in that:The towel of going to the lavatory is wet tissue or dry towel.
16. towel of going to the lavatory as described in claim 1, it is characterised in that:The base fabric is selected from non-woven fabrics or domestic paper.
17. towel of going to the lavatory as claimed in claim 16, it is characterised in that:When the towel of going to the lavatory is wet tissue, base fabric is selected from non-woven fabrics Or domestic paper, when the towel of going to the lavatory is dry towel, base fabric is selected from domestic paper.
18. towel of going to the lavatory as claimed in claim 12, it is characterised in that:The base fabric is selected from non-woven fabrics or domestic paper.
19. towel of going to the lavatory as claimed in claim 18, it is characterised in that:When the towel of going to the lavatory is wet tissue, base fabric is selected from non-woven fabrics Or domestic paper, when the towel of going to the lavatory is dry towel, base fabric is selected from domestic paper.
20. a kind of preparation method for towel of going to the lavatory, it is characterised in that:It is described go to the lavatory towel be wet tissue, preparation method specifically include as Lower step:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, capejasmine extract are taken It is 6-10 parts, spare;
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly;
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, be settled to 700-900 parts;Or it is further added in the supernatant after spice additive and adds solvent constant volume again to get antibacterial disinfectant Liquid;
(4) by the antibacterial disinfection medical fluid infiltration base fabric to get;
Or, the towel of going to the lavatory is dry towel, preparation method specifically comprises the following steps:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of capillary extract, 10-15 parts of Herba Senecionis Scandentis extract, capejasmine extract are taken It is 6-10 parts, spare;
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly;
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, be settled to 200-400 parts;Or it is further added in the supernatant after spice additive and adds solvent constant volume again to get antibacterial disinfectant Liquid;
(4) by the antibacterial disinfection medical fluid be sprayed at scrim surfaces to get.
21. the preparation method for towel of going to the lavatory as claimed in claim 20, it is characterised in that:When preparing dry towel, step (4) it is specific Operation is:First base fabric is coated using smears, then base fabric is cut into specified breadth, then folded, pressed The antibacterial disinfection medical fluid or antibacterial disinfection medical fluid and fragrance are sprayed on the surface of base fabric by flower in folding and embossing process, Finally product is packed, is sterilized to obtain the final product.
CN201610081959.1A 2016-02-05 2016-02-05 It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory Active CN105640409B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610081959.1A CN105640409B (en) 2016-02-05 2016-02-05 It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610081959.1A CN105640409B (en) 2016-02-05 2016-02-05 It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory

Publications (2)

Publication Number Publication Date
CN105640409A CN105640409A (en) 2016-06-08
CN105640409B true CN105640409B (en) 2018-11-16

Family

ID=56488331

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610081959.1A Active CN105640409B (en) 2016-02-05 2016-02-05 It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory

Country Status (1)

Country Link
CN (1) CN105640409B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109722942A (en) * 2017-10-30 2019-05-07 于凤 A kind of dustless paper handkerchief of functionality and preparation method thereof
CN109722931A (en) * 2017-10-31 2019-05-07 株洲千金药业股份有限公司 A kind of go to the lavatory towel and its method of the preparation of prescriptions worth thousand gold dregs of a decoction resource regeneration
CN107753998A (en) * 2017-12-04 2018-03-06 株洲千金药业股份有限公司 A kind of feminine hygiene articles of bacteriostatic and disease prevention and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1300623A (en) * 1999-12-20 2001-06-27 张发平 Chinese patent medicine
CN101879301A (en) * 2010-06-23 2010-11-10 党彬 Chinese medicinal herb preparation for treating chronic cervicitis
CN103070963A (en) * 2013-02-25 2013-05-01 梁贵文 Traditional Chinese medicine preparation for treating candida albicans infection diseases
CN104523477A (en) * 2014-12-08 2015-04-22 成都顺发消洗科技有限公司 Preparation method for disinfecting wet wipe

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1300623A (en) * 1999-12-20 2001-06-27 张发平 Chinese patent medicine
CN101879301A (en) * 2010-06-23 2010-11-10 党彬 Chinese medicinal herb preparation for treating chronic cervicitis
CN103070963A (en) * 2013-02-25 2013-05-01 梁贵文 Traditional Chinese medicine preparation for treating candida albicans infection diseases
CN104523477A (en) * 2014-12-08 2015-04-22 成都顺发消洗科技有限公司 Preparation method for disinfecting wet wipe

Also Published As

Publication number Publication date
CN105640409A (en) 2016-06-08

Similar Documents

Publication Publication Date Title
CN105534372B (en) It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
CN103340816B (en) Special private care wet tissue for women
CN105727353A (en) Liquid medicine having bacteriostatic and sterilizing effects and application thereof
CN101129322A (en) Multiple-effect bathing powder for nursing skin, method of manufacturing and method of using the same
US20130202668A1 (en) Personal Towelette with Cooling Composition for Relief of Heat Symptoms
CN105640409B (en) It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
CN107137293A (en) A kind of oil-control biological cleanser and preparation method thereof
CN105560498B (en) It is a kind of with antibacterial, disinfection medical fluid and its application
CN106038422A (en) Washing composition and preparation method and application thereof
CN103583515A (en) Novel disinfection liquid for wet tissue and preparation method for disinfection cotton wet tissue
CN105616294B (en) It is a kind of that there is antibacterial, disinfection liquid and its application
CN109568235A (en) A kind of wet tissue and its manufacturing method with caring function
CN105534373B (en) It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
CN109481724A (en) A kind of antibacterial warms up palace and dispels peculiar smell super-absorbent sanitary napkin and preparation method thereof
CN104490679B (en) A kind of composite bactericidal hand cleanser and preparation method thereof
CN105708756B (en) It is a kind of with antibacterial, disinfection towel and preparation method thereof of going to the lavatory
CN112641699A (en) Antibacterial wet tissue and preparation method thereof
CN105749084B (en) It is a kind of with antibacterial, disinfection medical fluid and its application
CN107754000A (en) A kind of feminine care non-woven fabrics of bacteriostatic and disease prevention and its application
CN103520034B (en) Herba Lysimachiae foenum-graeci quintessence oil antibacterial wet tissue and preparation method thereof
CN109602868A (en) Plant essence liquid and preparation method thereof and sanitary napkin application
CN107929801A (en) A kind of feminine care non-woven fabrics for preventing menstruation infection and its application
WO2020057285A1 (en) Atractylodes oil and/or cassia twig oil, production method therefor and use thereof
CN106880698A (en) A kind of plants essential oil and preparation method for treating child's property vaginitis
CN107088235A (en) The application of soapberry and its extract in amenities is prepared

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CB03 Change of inventor or designer information

Inventor after: Li Fujun

Inventor after: Jiang Jiala

Inventor after: Meng Jun

Inventor after: Teng Hui

Inventor before: Li Fujun

Inventor before: Jiang Jiala

Inventor before: Meng Jun

Inventor before: Jun Hui

CB03 Change of inventor or designer information