CN105638716A - Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent - Google Patents

Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent Download PDF

Info

Publication number
CN105638716A
CN105638716A CN201610097015.3A CN201610097015A CN105638716A CN 105638716 A CN105638716 A CN 105638716A CN 201610097015 A CN201610097015 A CN 201610097015A CN 105638716 A CN105638716 A CN 105638716A
Authority
CN
China
Prior art keywords
pheromone
pericarpium zanthoxyli
trapper
parts
lure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610097015.3A
Other languages
Chinese (zh)
Inventor
谢寿安
吕淑杰
袁丽芳
刘绥鹏
郭新荣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Northwest A&F University
Original Assignee
Northwest A&F University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Northwest A&F University filed Critical Northwest A&F University
Priority to CN201610097015.3A priority Critical patent/CN105638716A/en
Publication of CN105638716A publication Critical patent/CN105638716A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N49/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01MCATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M1/00Stationary means for catching or killing insects
    • A01M1/02Stationary means for catching or killing insects with devices or substances, e.g. food, pheronones attracting the insects
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01MCATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M1/00Stationary means for catching or killing insects
    • A01M1/10Catching insects by using Traps
    • A01M1/106Catching insects by using Traps for flying insects
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/08Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
    • A01N25/10Macromolecular compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N27/00Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01MCATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M2200/00Kind of animal
    • A01M2200/01Insects
    • A01M2200/012Flying insects

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Insects & Arthropods (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catching Or Destruction (AREA)

Abstract

The invention discloses a lure agent of pheromones for controlling pepper flatheaded borer and a preparation method of the lure agent. Raw materials including, in parts by weight, 12 parts of aliphatic polyester, 80 parts of a solvent, 2.8 parts of pepper flatheaded borer pheromones, 1.5 parts of an antioxidant, 0.06 parts of a surfactant and 0.08 parts of an adhesive are prepared, wherein the pepper flatheaded borer pheromones comprise 0.4 parts of alpha-pinene, 0.4 parts of beta-pinene, 0.4 parts of beta-caryophyllene, 0.4 parts of alpha-phellandrene, 0.4 parts of myrcene, 0.4 parts of d-limonene and 0.4 parts of linalyl acetate; aliphatic polyester is preheated, the pheromones for controlling pepper flatheaded borer and the solvent are added, the mixture is uniformly stirred and cooled, the antioxidant is added, the mixture is heated, the surfactant and the adhesive are added, and the mixture is cooled to the room temperature; the mixture is stirred; the prepared mixture is metered, subpackaged and injected into dark brown glass bottles to be sealed, and a finished product of the pheromones for trapping the pepper flatheaded borer is prepared. The method is simple, the cost is lower, and the method has good slow-release effect and environment friendliness.

Description

A kind of lure of pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle and preparation method thereof
Technical field
The invention belongs to and prevent insect technical field, particularly relate to a kind of lure of pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle and preparation method thereof.
Background technology
Insect pheromone (pheromone) also known as insect pheromone, it be insecticide self produce to discharge a kind of in planting or between kind transmission information carry out the trace substance of chemical molecular communication and behavior manipulation. Modern science shows after deliberation: information that insect pheromone transmits (as: look for food, lure, gather function informations such as evacuating alarm and mate and oviposit) there is the specificity of height, every kind of pheromone that various insecticides discharge has specific stereochemical structure, by the mixture that is still made up of by a certain percentage several compounds of pheromone. In recent years; research and development and production technology activity about insect pheromone become increasingly active; it has become as the world today and has a strategic hot research field; research work in particular with insect pheromone pest control is more affected by people's strong interest and attention, and it is to controlling the quantity of insects' population, maintain biological chain benign structure, protecting human ecological environment all to have very important realistic meaning. Although the research work that China is in insect pheromone is started late, but, under the joint efforts of numerous biological engineering and life sciences worker, progressively start application message element and the generating capacity of injurious forest-insect, emergence period and population dynamic have been monitored early warning work. Pericarpium Zanthoxyli buprestid beetle, belongs to coleoptera, buprestid; Have another name called Stem Girdler, string skinworm etc. There is distribution Pericarpium Zanthoxyli main producing region, the whole nation. The harm of the area such as Longnan of Gansu Province, Sichuan Chuan Bei, Hancheng Region, Shaanxi is the heaviest; Specially evil Pericarpium Zanthoxyli, with larva moth food branch cortex, eats into into irregular burrow at cambium layer, causes that white or brown size juice flows out; The middle and lower part of general moth food trunk, the heaviest to be injured within the scope of trunk base portion 30 millimeters; Below 4-5 Chinese pricklyash is injured strain rate more than 70%. The harm of green pepper woods is caused showing great attention to of lot of domestic and foreign experts and scholars by Pericarpium Zanthoxyli buprestid beetle already, according to incomplete statistics: cause that green pepper woods loses every year up to 1,200,000,000 yuan due to Pericarpium Zanthoxyli buprestid beetle insect pest.Understand according to investigations: at vast Pericarpium Zanthoxyli planting area, the traditional method continuing to use spray spraying pesticide is remained for the preventing and controlling of Pericarpium Zanthoxyli buprestid beetle, people and animals and periphery ecological environment not only can be worked the mischief by this, also an innocent person can indiscriminately slaughter other beneficial insect, heavy damage population quantity and insecticide biological chain. Up to now, although also have some reports about research Pericarpium Zanthoxyli buprestid beetle life habit and chemistry, biology and artificial control's Pericarpium Zanthoxyli buprestid beetle insect pest.
But, there is not yet in-depth analysis Pericarpium Zanthoxyli buprestid beetle pheromone and utilize pheromone to carry out insect protected to control the pertinent literature of worm comprehensive control. This is that numerous bioscience worker is constantly exploring and wishing the key subjects solved always.
Summary of the invention
It is an object of the invention to provide a kind of lure of pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle and preparation method thereof, it is intended to solve to adopt Pericarpium Zanthoxyli buprestid beetle pheromone to carry out the problem that worm comprehensive control is controlled in insect protected.
The preparation method that it is an object of the invention to provide the lure of a kind of pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle, the preparation method of the lure of the pheromone of described preventing and treating Pericarpium Zanthoxyli buprestid beetle comprises the following steps:
According to parts by weight of fatty adoption ester 8-12 part, solvent 60-80 part, Pericarpium Zanthoxyli buprestid beetle pheromone 1.4-2.8 part, antioxidant 0.5-1.5 part, surfactant 0.02-0.06 part, adhesive agent 0.02-0.08 part prepares raw material; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.2-0.4 part of 7 kinds of chemical substances of linalyl acetate;
Aliphatic polyester is preheated, adds pheromone and the solvent of Pericarpium Zanthoxyli buprestid beetle, mixing, cooling, then add antioxidant, heating, add surfactant and adhesive agent, be cooled to room temperature, obtain mixture; Stir the mixture for;
Sub-bottle encapsulates, and is sealed in dark-brown vial through metering, distributing, packaging fill by the mixture prepared, and can be prepared by the pheromone finished product of trapping Pericarpium Zanthoxyli buprestid beetle insecticide.
Further, described by aliphatic polyester in 90 DEG C��105 DEG C preheatings, add pheromone and the solvent of Pericarpium Zanthoxyli buprestid beetle, mixing, be cooled to 55 DEG C��60 DEG C.
Further, the described antioxidant that adds again, heating is to 80 DEG C��85 DEG C.
Further, described mixture stirs under the speed of 250rpm��1500rpm.
Another object of the present invention is to the lure of the pheromone of the preventing and treating Pericarpium Zanthoxyli buprestid beetle providing the preparation method of the lure of the pheromone of a kind of described preventing and treating Pericarpium Zanthoxyli buprestid beetle to prepare, the lure of the pheromone of described preventing and treating Pericarpium Zanthoxyli buprestid beetle includes according to weight portion: aliphatic polyester 12 parts, solvent 80 parts, Pericarpium Zanthoxyli buprestid beetle pheromone 2.8 parts, antioxidant 1.5 parts, 0.06 part of surfactant, adhesive agent 0.08 part; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.4 part of 7 kinds of chemical substances of linalyl acetate.
Another object of the present invention is to the trapper providing the preparation method of the lure of the pheromone of a kind of described preventing and treating Pericarpium Zanthoxyli buprestid beetle to use, described trapper includes: fixed mount, trapper mainboard hook, trapper mainboard, trapper drawer, lure bottle five part form.
Trapper mainboard is fixed on fixed mount by hook, and lure bottle is suspended on trapper mainboard by rope yarn, and trapper drawer is arranged on the lower section of trapper mainboard.
Further, the using method of described trapper is as follows:
The first step, mounting and fixing support;
Second step, with hook trapper mainboard is suspended on fixed mount;
3rd step, the brown vial that will be equipped with pheromone are suspended in trapper;
Little drawer bottom 4th step, installation trapper mainboard, for holding the Pericarpium Zanthoxyli buprestid beetle lured.
Lure of pheromone of preventing and treating Pericarpium Zanthoxyli buprestid beetle provided by the invention and preparation method thereof, insect pheromone (pheromone) also known as insect pheromone, it be insecticide self produce to discharge a kind of in planting or between kind transmission information carry out the trace substance of chemical molecular communication and behavior manipulation. modern science shows after deliberation: information that insect pheromone transmits (as: look for food, lure, gather function informations such as evacuating alarm and mate and oviposit) there is the specificity of height, every kind of pheromone that various insecticides discharge has specific stereochemical structure, by the mixture that is still made up of by a certain percentage several compounds of pheromone. in recent years, research and development and production technology activity about insect pheromone become increasingly active, it has become as the world today and has a strategic hot research field, research work in particular with insect pheromone pest control is more affected by people's strong interest and attention, and it is to controlling the quantity of insects' population, maintain biological chain benign structure, protecting human ecological environment all to have very important realistic meaning. due to the active height of insect pheromone, high specificity, easy to use, do not injure the advantage such as natural enemy and nonpollution environment, the development of Pericarpium Zanthoxyli buprestid beetle pheromone and application, cause harm for effectively monitoring and sustainable control China Pericarpium Zanthoxyli buprestid beetle and have positive effect. the present invention, in conjunction with the taxis of insecticide, reaches the purpose of trapping pests, moreover it is possible to make male imago orientation cannot find female worm mating, within the scope of the economic threshold control the population density of insect. preparation method of the present invention is simple, less costly, low-carbon (LC), long-acting, stable, there is effect and the environment friendly of slow release, to person poultry safety, there are wide economy and ecological benefits, Pericarpium Zanthoxyli buprestid beetle can be retrieved every year and endanger the loss 1,200,000,000 yuan caused. this achievement is prone to industrialization, in addition pheromone baiting techniques is easy to operate, can save labour force 12,000,000 yuan every year, meet the developing direction of insect Harmless control in forest ecosystem, be adapted at China's Pericarpium Zanthoxyli growing area spread, there is wide popularizing application prospect. the present invention endangers the Biological Mechanism of Pericarpium Zanthoxyli in further investigation clear understanding Pericarpium Zanthoxyli buprestid beetle and utilizes Pericarpium Zanthoxyli buprestid beetle adult identification Pericarpium Zanthoxyli volatile compounds to lure on the basis of signal, with aliphatic polyester, solvent, Pericarpium Zanthoxyli Ji fourth first insect pheromone main component (australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, 7 kinds of chemical substances such as linalyl acetate), antioxidant, surfactant and adhesive agent be chemical raw material make a kind of Pericarpium Zanthoxyli buprestid beetle is had look for food the pheromone luring function and utilize pheromone trapping Pericarpium Zanthoxyli buprestid beetle, it has production easily, low cost of manufacture, lure function strong Pericarpium Zanthoxyli buprestid beetle, insect protected anthelminthic effect is good, non-environmental-pollution, to outstanding advantages such as people and animals and Natural Enemies of Insects nonhazardouss.
Accompanying drawing explanation
Fig. 1 is the preparation method flow chart of the lure of the pheromone of the preventing and treating Pericarpium Zanthoxyli buprestid beetle that the embodiment of the present invention provides.
Fig. 2 is the trapper structural representation that the embodiment of the present invention provides;
In figure: 1, fixed mount; 2, hook; 3, trapper mainboard; 4, lure bottle; 5, trapper drawer.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated. Should be appreciated that specific embodiment described herein is only in order to explain the present invention, is not intended to limit the present invention.
The pheromone of Pericarpium Zanthoxyli Ji fourth first insect is coordinated by the present invention with other auxiliary agents, is then immersed in lure by pheromone water dispersant, lure is loaded in trapper, then trapper is arranged on field, is used for luring Pericarpium Zanthoxyli Ji fourth first insect.
Below in conjunction with accompanying drawing, the application principle of the present invention is explained in detail.
The lure of the pheromone of the preventing and treating Pericarpium Zanthoxyli buprestid beetle of the embodiment of the present invention includes according to weight portion: aliphatic polyester 12 parts, solvent 80 parts, Pericarpium Zanthoxyli buprestid beetle pheromone 2.8 parts, antioxidant 1.5 parts, 0.06 part of surfactant, adhesive agent 0.08 part; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.4 part of 7 kinds of chemical substances of linalyl acetate.
As it is shown in figure 1, the preparation method of the lure of the pheromone of the preventing and treating Pericarpium Zanthoxyli buprestid beetle of the embodiment of the present invention comprises the following steps:
S101: according to parts by weight of fatty adoption ester 12 parts, solvent 80 parts, Pericarpium Zanthoxyli buprestid beetle pheromone 2.8 parts, antioxidant 1.5 parts, 0.06 part of surfactant, adhesive agent 0.08 part prepares raw material; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.4 part of 7 kinds of chemical substances of linalyl acetate;
S102: by aliphatic polyester in 90 DEG C��105 DEG C preheatings, add pheromone and the solvent of Pericarpium Zanthoxyli buprestid beetle, mixing, being cooled to 55 DEG C��60 DEG C, then add antioxidant, heating is to 80 DEG C��85 DEG C, add surfactant and adhesive agent, be cooled to room temperature, obtain mixture; Mixture is stirred under the speed of 250rpm��1500rpm;
S103: sub-bottle encapsulates, and is sealed in dark-brown vial through metering, distributing, packaging fill by the mixture prepared, can be prepared by the pheromone finished product of trapping Pericarpium Zanthoxyli buprestid beetle insecticide.
As in figure 2 it is shown, the trapper of the embodiment of the present invention specifically includes that fixed mount 1, hook 2, trapper mainboard 3, lure bottle 4, trapper drawer 5.
Trapper mainboard 3 is fixed on fixed mount 1 by linking up with 2, and lure bottle 4 is suspended on trapper mainboard 3 by rope yarn, and trapper drawer 5 is arranged on the lower section of trapper mainboard 3.
The trapper using method of the embodiment of the present invention:
The first step, mounting and fixing support;
Second step, with hook trapper mainboard is suspended on fixed mount;
3rd step, the brown vial that will be equipped with pheromone are suspended on trapper mainboard;
Little drawer (for holding the Pericarpium Zanthoxyli buprestid beetle lured) bottom 4th step, installation trapper mainboard.
Below in conjunction with test, the application effect of the present invention is explained in detail.
In order to verify the effect to Stem Girdler of host's volatile matter, utilize solid-phase microextraction and GC-MS to analyze the main volatile compound of Pericarpium Zanthoxyli, and adopt tentaculum electric potential (EAG) and Y-shaped olfactometer mensuration Stem Girdler to the electro physiology of host plant volatile and behavior reaction. Result shows that Pericarpium Zanthoxyli mainly can cause the Electroantennogram response of Stem Girdler containing 7 kinds of volatile components such as australene, nopinene, ��-caryophyllene, ��-phellandrene, rare, rare, the linalyl acetates of dextrorotation Fructus Citri Limoniae of Laurel.The lure trap effect of 7 kinds of various combinations such as australene, nopinene, ��-caryophyllene, ��-phellandrene, rare, rare, the linalyl acetate of dextrorotation Fructus Citri Limoniae of Laurel is compared research, having filtered out economical effective lure of applicable China Pericarpium Zanthoxyli planting area preventing and treating Pericarpium Zanthoxyli Ji Dingjia, the lure being namely made up of 7 kinds of chemical substances such as australene, nopinene, ��-caryophyllene, ��-phellandrene, rare, rare, the linalyl acetates of dextrorotation Fructus Citri Limoniae of Laurel is best information element lure.
The pheromone of the trapping Pericarpium Zanthoxyli buprestid beetle insecticide present invention proposed carries out following Efficacy Study Experimental in Adult's behavior sight chamber: described Adult's behavior sight chamber design-build becomes radius to be 60cm, high batten framework half V-arrangement four cell structure for 60cm. It is with centrage be round dot, the region of radius 30cm be set to adult release room, three parts will be divided into outer portion and separate three independent selection rooms of formation with plank again, the nylon cloth adopting 80 orders between adult release room and each selection room separates, on the nylon cloth of corresponding each selection room same position place be respectively provided with two diameters be 10cm circular holes confession adult select free in and out. Selecting indoor to place lure respectively at three, described lure absorbent cotton (0.5g) adsorbs the pheromone lure (1.0g) being made up of aliphatic polyester, solvent, Pericarpium Zanthoxyli Ji fourth first insect pheromone main component 7 kinds of chemical substances such as () australene, nopinene, ��-caryophyllene, ��-phellandrene, rare, rare, the linalyl acetates of dextrorotation Fructus Citri Limoniae of Laurel, antioxidant, surfactant and adhesive agent to be made. Adopt one-time regression orthogonal design, in triplicate. Choose the adult 50 that vitality is prosperous and powerful, 22:00 puts into adult release room at night, all light is turned off after putting worm, in next day 8:00 under red light, observe that numeration is each selects indoor adult quantity to be adult trapping number, calculating average trappability again, result of the test is carried out statistical analysis and significance test by application SSPS17.0 data analysis software. The survey showed that to the Harm of Pericarpium Zanthoxyli buprestid beetle for field, field: after trapper of layouting, the population quantity of Pericarpium Zanthoxyli buprestid beetle is remarkably decreased, the equal insect density of Pericarpium Zanthoxyli strain of being injured is dropped to 3.6 heads/plant by 18.5 heads/plant before preventing and treating, prevention effect is obvious, achieves good economy, society and ecological benefits.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all any amendment, equivalent replacement and improvement etc. made within the spirit and principles in the present invention, should be included within protection scope of the present invention.

Claims (7)

1. the preparation method of the lure of the pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle, it is characterised in that the preparation method of the lure of the pheromone of described preventing and treating Pericarpium Zanthoxyli buprestid beetle comprises the following steps:
According to parts by weight of fatty adoption ester 8-12 part, solvent 60-80 part, Pericarpium Zanthoxyli buprestid beetle pheromone 1.4-2.8 part, antioxidant 0.5-1.5 part, surfactant 0.02-0.06 part, adhesive agent 0.02-0.08 part prepares raw material; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.2-0.4 part of 7 kinds of chemical substances of linalyl acetate;
Aliphatic polyester is preheated, adds pheromone and the solvent of Pericarpium Zanthoxyli buprestid beetle, mixing, cooling, then add antioxidant, heating, add surfactant and adhesive agent, be cooled to room temperature, obtain mixture;Stir the mixture for;
Sub-bottle encapsulates, and is sealed in dark-brown vial through metering, distributing, packaging fill by the mixture prepared, and can be prepared by the pheromone finished product of trapping Pericarpium Zanthoxyli buprestid beetle insecticide.
2. the preparation method of the lure of the as claimed in claim 1 pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle, it is characterised in that described by aliphatic polyester in 90 DEG C��105 DEG C preheatings, add pheromone and the solvent of Pericarpium Zanthoxyli buprestid beetle, mix, be cooled to 55 DEG C��60 DEG C.
3. the preparation method of the lure of the pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle as claimed in claim 1, it is characterised in that the described antioxidant that adds again, heating is to 80 DEG C��85 DEG C.
4. the preparation method of the lure of the pheromone preventing and treating Pericarpium Zanthoxyli buprestid beetle as claimed in claim 1, it is characterised in that described mixture stirs under the speed of 250rpm��1500rpm.
5. the lure of the pheromone of the preventing and treating Pericarpium Zanthoxyli buprestid beetle that prepared by the preparation method of the lure of the pheromone of a preventing and treating Pericarpium Zanthoxyli buprestid beetle as claimed in claim 1, it is characterized in that, the lure of the pheromone of described preventing and treating Pericarpium Zanthoxyli buprestid beetle includes according to weight portion: aliphatic polyester 12 parts, solvent 80 parts, Pericarpium Zanthoxyli buprestid beetle pheromone 2.8 parts, antioxidant 1.5 parts, 0.06 part of surfactant, adhesive agent 0.08 part; Pericarpium Zanthoxyli buprestid beetle pheromone includes australene, nopinene, ��-caryophyllene, ��-phellandrene, Laurel is rare, dextrorotation Fructus Citri Limoniae is rare, each 0.4 part of 7 kinds of chemical substances of linalyl acetate.
6. the trapper that the preparation method of the lure of the pheromone of a preventing and treating Pericarpium Zanthoxyli buprestid beetle as claimed in claim 1 uses, it is characterized in that, described trapper includes: fixed mount, trapper mainboard hook, trapper mainboard, trapper drawer, lure bottle five part form;
Trapper mainboard is fixed on fixed mount by hook, and lure bottle is suspended on trapper mainboard by rope yarn, and trapper drawer is arranged on the lower section of trapper mainboard.
7. trapper as claimed in claim 6, it is characterised in that the using method of described trapper is as follows:
The first step, mounting and fixing support;
Second step, with hook trapper mainboard is suspended on fixed mount;
3rd step, the brown vial that will be equipped with pheromone are suspended in trapper;
Little drawer bottom 4th step, installation trapper mainboard, for holding the Pericarpium Zanthoxyli buprestid beetle lured.
CN201610097015.3A 2016-02-22 2016-02-22 Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent Pending CN105638716A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610097015.3A CN105638716A (en) 2016-02-22 2016-02-22 Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610097015.3A CN105638716A (en) 2016-02-22 2016-02-22 Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent

Publications (1)

Publication Number Publication Date
CN105638716A true CN105638716A (en) 2016-06-08

Family

ID=56488600

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610097015.3A Pending CN105638716A (en) 2016-02-22 2016-02-22 Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent

Country Status (1)

Country Link
CN (1) CN105638716A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108419807A (en) * 2018-01-31 2018-08-21 中国农业科学院烟草研究所 Yellow meal worm attractant and its application
CN111357779A (en) * 2018-12-26 2020-07-03 西北农林科技大学 Lure for preventing and controlling Chinese prickly ash and Giardia and preparation method thereof
CN111513065A (en) * 2020-05-15 2020-08-11 中国农业科学院植物保护研究所 Coffee bean weevil attractant composition and application thereof
CN111781313A (en) * 2020-07-28 2020-10-16 山西省林业科学研究院 Method for obtaining walnut small Jiding plant source attractant raw material and formula thereof
CN113940324A (en) * 2020-07-17 2022-01-18 北京依科曼生物技术股份有限公司 Preparation method of spodoptera frugiperda sex attractant core

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1305723A (en) * 2001-01-21 2001-08-01 西北农林科技大学无公害农药研究服务中心 Attractant for coleoptera pests of needle-leave forest and its preparing process
CN101061808A (en) * 2006-04-30 2007-10-31 中国林业科学研究院森林生态环境与保护研究所 Semanotus bifasciatus attractant, attractant core and the method of producing the same
CN101243835A (en) * 2008-02-04 2008-08-20 北京林业大学 Semanotus sinoauster attractant
CN101554178A (en) * 2009-04-14 2009-10-14 云南农业大学 Monochamus alternatus imago attractant and trap thereof
CN101987081A (en) * 2010-07-16 2011-03-23 钟术光 Controlled release preparation
CN104472483A (en) * 2014-12-31 2015-04-01 广州甘蔗糖业研究所 Proceras venosatus sex pheromone microsphere and preparing method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1305723A (en) * 2001-01-21 2001-08-01 西北农林科技大学无公害农药研究服务中心 Attractant for coleoptera pests of needle-leave forest and its preparing process
CN101061808A (en) * 2006-04-30 2007-10-31 中国林业科学研究院森林生态环境与保护研究所 Semanotus bifasciatus attractant, attractant core and the method of producing the same
CN101243835A (en) * 2008-02-04 2008-08-20 北京林业大学 Semanotus sinoauster attractant
CN101554178A (en) * 2009-04-14 2009-10-14 云南农业大学 Monochamus alternatus imago attractant and trap thereof
CN101987081A (en) * 2010-07-16 2011-03-23 钟术光 Controlled release preparation
CN104472483A (en) * 2014-12-31 2015-04-01 广州甘蔗糖业研究所 Proceras venosatus sex pheromone microsphere and preparing method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DAMON J. CROOK,ET.: ""Development of a host-based semiochemical lure for trapping emerald ash borer agrilus planipennis(coleopteran:buprestidae)"", 《ENVIRONMENTAL ENTOMOLOGY》 *
崔晓宁等: ""苹果小吉丁虫综合防控研究进展"", 《植物保护》 *
高焕婷等: ""花椒窄吉丁虫的生物学特性及其综合防治措施"", 《陕西农业科学》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108419807A (en) * 2018-01-31 2018-08-21 中国农业科学院烟草研究所 Yellow meal worm attractant and its application
CN111357779A (en) * 2018-12-26 2020-07-03 西北农林科技大学 Lure for preventing and controlling Chinese prickly ash and Giardia and preparation method thereof
CN111513065A (en) * 2020-05-15 2020-08-11 中国农业科学院植物保护研究所 Coffee bean weevil attractant composition and application thereof
CN113940324A (en) * 2020-07-17 2022-01-18 北京依科曼生物技术股份有限公司 Preparation method of spodoptera frugiperda sex attractant core
CN111781313A (en) * 2020-07-28 2020-10-16 山西省林业科学研究院 Method for obtaining walnut small Jiding plant source attractant raw material and formula thereof

Similar Documents

Publication Publication Date Title
CN105638716A (en) Lure agent of pheromones for controlling pepper flatheaded borer and preparation method of lure agent
CN101627757B (en) Dark melolonthidae sex pheromone and sex attractant
CN106900704B (en) Sex attractant core for fruit tree pest oriental fruit moth
CN103583517B (en) Attractant for luring and gathering dichocrocis punctiferalis and bait
CN102630641B (en) Method for continuously releasing parasitic natural enemy insects
CN105994213A (en) Insect trapping device and insect trapping method
CN205390075U (en) Pheromones of prevention and cure prickly ash buprestid beetle lure trapper of core use
CN203661852U (en) Sexual attracting type simple imago trapping and killing device
WO2018185243A1 (en) Compounds and compositions having knock-down or blood feed inhibition activity against insect pests
Kusch et al. Determinants of social structure in a northern population of black-tailed prairie dogs, Cynomys ludovicianus
CN102812954A (en) Composition of plutella xylostella pheromone disorientation silk
CN202211095U (en) Device for trapping red imported fire ants to be infected with entomogenous fungi
CN101069518A (en) Bait for killing solenopsis invicta Buren
CN201585361U (en) Suspended pest trap
CN102907285A (en) Comprehensive treatment method for preventing pine wood nematode disease from spreading
CN101502252A (en) Method for preventing and treating vegetable noctuid using attractant for spreading virus
CN101554158A (en) Emamectin-benzoate and methomyl microemulsion and preparation method thereof
CN104970016A (en) Attractant of tomicus yunnanensis
CN102369926A (en) Rhynchophorus ferrugineus aggregation pheromone attractant
CN103875662B (en) A kind of fragrant pear excellent phycitid sex attractant
CN203952210U (en) The killing device of a kind of red fire ant nuptial flight ant
CN104351238B (en) Pesticide composition containing picoxystrobin and pyrethroids, preparation and application thereof
Marsden Selective primary health care: strategies for control of disease in the developing world. XVI. Chagas' disease
CN111296382A (en) Intelligent ecological epidemic prevention cover for preventing and treating pine wood nematode disease
CN212437030U (en) Intelligent ecological epidemic prevention cover for preventing and treating pine wood nematode disease

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160608

WD01 Invention patent application deemed withdrawn after publication