CN105616325A - 珍珠质紧致补水面膜及其制备方法 - Google Patents

珍珠质紧致补水面膜及其制备方法 Download PDF

Info

Publication number
CN105616325A
CN105616325A CN201610063498.5A CN201610063498A CN105616325A CN 105616325 A CN105616325 A CN 105616325A CN 201610063498 A CN201610063498 A CN 201610063498A CN 105616325 A CN105616325 A CN 105616325A
Authority
CN
China
Prior art keywords
nacre
stock solution
phase
moisturizing
skin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610063498.5A
Other languages
English (en)
Other versions
CN105616325B (zh
Inventor
周树立
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hainan Jingrun Zhenzhu Biological Technology Co Ltd
Original Assignee
Hainan Jingrun Zhenzhu Biological Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hainan Jingrun Zhenzhu Biological Technology Co Ltd filed Critical Hainan Jingrun Zhenzhu Biological Technology Co Ltd
Priority to CN201610063498.5A priority Critical patent/CN105616325B/zh
Publication of CN105616325A publication Critical patent/CN105616325A/zh
Application granted granted Critical
Publication of CN105616325B publication Critical patent/CN105616325B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42—Amides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/676—Ascorbic acid, i.e. vitamin C
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

本发明属日用化妆品技术领域，涉及一种珍珠质紧致补水面膜及其制备方法，组分包括添加珍珠提取物的水解珍珠粉、多种氨基酸、甜菜碱、透明质酸钠、糖类同分异构体、植物提取物、醇类、酯类等。本发明利用添加珍珠提取物的水解珍珠粉，协同多种氨基酸，同时辅以甜菜碱，透明质酸钠，糖类同分异构体等保湿补水因子，赋予肌肤丰润营养，增加肌肤弹性，让肌肤紧致润滑，具有工艺简单、营养全面、效果明显等特点，是一种可使肌肤紧致润滑的美容护肤佳品。

Description

珍珠质紧致补水面膜及其制备方法
技术领域
本发明属日用化妆品技术领域，涉及一种面膜及其制备方法，具体是一种珍珠质紧致补水面膜及其制备方法。
背景技术
皮肤位于人体表面，是人体的第一道防线，尤其是皮肤角质层具有十分重要的功能。角质层中的水是重要的塑形物，其相对含量约为10％～15％。随着年龄增加，皮肤角质层中的自然保湿因子含量逐渐减少，使皮肤水合能力下降，仅能达到正常皮肤的75％。同时，皮肤受内源性因素的影响，会表现出松弛、出现细小皱纹、干燥、脱屑、脆性增加、修复功能减退等现象。随着社会的发展，生活质量的提高，人们尤其是女性对于面部的美容护肤越来越讲究。
面膜作为美容保养品的一种载体，之所以比一般化妆品速效，在于它的密闭性，当面膜贴附在皮肤上，其营养成分与皮肤紧密贴合，并与外界空气阻隔，一方面让水分和营养物质缓缓渗透入表皮角质层，另一方面也防止膜内水分和营养成分流失，角质层细胞会在这种湿润的环境中吸收到足够的营养。在揭下面膜后皮肤呈现出柔软、细腻和光泽。
珍珠一直被公认为美容佳品，其美容机理是珍珠中含有各种人体所需的氨基酸和微量元素，珍珠中含有的营养成分与人类肌肤所需养分接近，很容易被人体吸收。
发明内容
本发明的目的是提供一种珍珠质紧致补水面膜及其制备方法，利用添加珍珠提取物的水解珍珠，协同多种氨基酸，同时辅以甜菜碱，透明质酸钠，糖类同分异构体等保湿补水因子，赋予肌肤丰润营养，增加肌肤弹性，让肌肤紧致润滑。
本发明所采用的技术方案：
一种珍珠质紧致补水面膜，含有以下重量百分比组分：
A相：珍珠质原液水解珍珠2～10％
羟乙基脲1.0～6％
聚甘油-60.2～2％
猴面包树(ADANSONIADIGITATA)果肉提取物0.0001～1.0％
黄原胶0.0001～0.1％
小核菌(SCLEROTIUMROLFSSII)胶0.001～1.0％
赖氨酸0.0001～2.0％
组氨酸0.0001～2.0％
精氨酸0.0001～2.0％
天冬氨酸0.0001～2.0％
苏氨酸0.0001～2.0％
丝氨酸0.0001～2.0％
谷氨酸0.0001～2.0％
脯氨酸0.0001～2.0％
甘氨酸0.0001～2.0％
丙氨酸0.0001～2.0％
缬氨酸0.0001～2.0％
异亮氨酸0.0001～2.0％
亮氨酸0.0001～2.0％
酪氨酸0.0001～2.0％
苯丙氨酸0.0001～2.0％
野大豆(GLYCINESOJA)籽提取物0.0001～2.0％
透明质酸钠0.0001～2.0％
糖类同分异构体0.0001～2.0％
PEG/PPG-17/6共聚物0.1～2.0％
1,2-戊二醇0.00001～1.0％
羟苯基丙酰胺苯甲酸0.00001～1.0％
抗坏血酸棕榈酸酯0.00001～1.0％
甘油0.001～1.0％
羟苯甲酯0.00001～0.1％
羟苯乙酯0.00001～0.1％
羟苯丙酯0.00001～0.1％
羟苯丁酯0.00001～0.1％
羟苯异丁酯0.00001～0.1％
柠檬酸三乙酯0.01～1.0％
苯氧乙醇0.0001～0.1％
B相：丁二醇2～10％
甜菜碱2～8％
尿囊素0.01～0.5％
丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物0.05～0.5％
羟乙基纤维素0.01～1.0％
EDTA二钠0.01～0.1％
对羟基苯乙酮0.1～1.0％
纯水to100％
C相：三乙醇胺0.01～0.5％
D相：香精0.001～0.3％
PEG-50氢化蓖麻油0.0001～0.1％
壬基酚聚醚-140.0001～0.1％
丙二醇0.0001～0.1％
苯甲醇0.01～0.5％。
所述珍珠质原液水解珍珠是取海水珍珠粒经破碎去核后得到珍珠质；珍珠质经过超微粉碎得到细粉，细粉加水后按珍珠质粉重量的0.1～0.5％的比例加植物蛋白酶于45～50℃条件下搅拌5～8h，滤布过滤掉残渣，得到澄清液体；澄清液体用分子截留量100道尔顿膜过滤，浓缩到10％，得到珍珠质原液；常温下按体积比：珍珠质原液：水解珍珠＝1:18～25的比例将珍珠质原液和水解珍珠混合，搅拌均匀，备用。
本发明所提供的珍珠质紧致补水面膜的制备方法，其步骤如下：
1)将B相加入到乳化锅中高速均质3～6分钟，加热至80～85℃，均质2～5分钟，保温25～40分钟。
2)冷却至55～60℃加入C相搅拌均匀。
3)冷却至25～30℃加入A相和D相，搅拌均匀，理化指标检验合格后，出料得到面膜精华液；用25ml～30ml面膜精华液浸泡天丝无纺布得到珍珠质紧致补水面膜。
面膜使用方法：清洁面部后，将面膜轻敷于面部，15～20分钟即可。
本发明利用添加珍珠提取物的水解珍珠，协同多种氨基酸，同时辅以甜菜碱，透明质酸钠，糖类同分异构体等保湿补水因子，赋予肌肤丰润营养，增加肌肤弹性，让肌肤紧致润滑，具有工艺简单、营养全面、效果明显等特点，是一种可使肌肤紧致润滑的美容护肤佳品。
具体实施方式
下面通过实例对本发明作进一步说明，但不作为对本发明的限定。
各实施例的组成配方见表1，以重量百分比表示。
表1各实施例的组成配方
上述实施例中，实施例1、2的珍珠质原液水解珍珠的制备工艺：
取海水珍珠粒经破碎去核后得到珍珠质；珍珠质经过超微粉碎得到细粉，细粉加10倍水，按珍珠质粉重量的0.2％的比例加木瓜蛋白酶于45～50℃条件下搅拌6h，滤布过滤掉残渣，得到澄清液体；澄清液体用分子截留量100道尔顿膜过滤，浓缩到10％，得到珍珠质原液；常温下按体积比：珍珠质原液：水解珍珠＝1:20的比例将珍珠质原液和水解珍珠混合，搅拌均匀，备用。
上述实施例中，实施例3、4的珍珠质原液水解珍珠的制备工艺：
取海水珍珠粒经破碎去核后得到珍珠质；珍珠质经过超微粉碎得到细粉，细粉加8倍水，按珍珠质粉重量的0.5％的比例加菠萝蛋白酶于45～50℃条件下搅拌8h，滤布过滤掉残渣，得到澄清液体；澄清液体用分子截留量100道尔顿膜过滤，浓缩到10％，得到珍珠质原液；常温下按体积比：珍珠质原液：水解珍珠＝1:23的比例将珍珠质原液和水解珍珠混合，搅拌均匀，备用。
上述实施例中，实施例5、6的珍珠质原液水解珍珠的制备工艺：
取海水珍珠粒经破碎去核后得到珍珠质；珍珠质经过超微粉碎得到细粉，细粉加12倍水，按珍珠质粉重量的0.3％的比例加木瓜蛋白酶于45～50℃条件下搅拌7h，滤布过滤掉残渣，得到澄清液体；澄清液体用分子截留量100道尔顿膜过滤，浓缩到10％，得到珍珠质原液；常温下按体积比：珍珠质原液：水解珍珠＝1:25的比例将珍珠质原液和水解珍珠混合，搅拌均匀，备用。
上述实施例的制备工艺如下：
1)将B相加入到乳化锅中高速均质4分钟，加热至80～85℃，均质2分钟，保温30分钟。
2)冷却至55～60℃加入C相搅拌均匀。
3)冷却至25～30℃加入A相和D相，搅拌均匀，理化指标检验合格后，出料得到面膜精华液；用25ml～30ml面膜精华液浸泡天丝无纺布得到珍珠质紧致补水面膜。
功效验证：
随机挑选180名志愿者，每个实施例试用者30人，每周2-3次，连续使用一个月，结果见表2，效果分三个等级：
紧致补水效果明显：皮肤明显紧致，用后皮肤水润，紧致水润效果保持一整天。
紧致补水效果一般：皮肤有变紧致，用后皮肤水润，紧致水润效果保持半天。
紧致补水效果无变化：皮肤紧致水润不明显。
表2各实施例使用效果
实施案例 明显 一般 无结果
实施例1 15 12 3
实施例2 13 14 46 -->
实施例3 14 13 4
实施例4 14 14 2
实施例5 12 16 2
实施例6 15 13 2
由上述使用效果可以看出，使用本发明紧致补水效果有效率达到90％以上。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。

Claims (3)

1.一种珍珠质紧致补水面膜，其特征在于，含有以下重量百分比组分：
A相：珍珠质原液水解珍珠2～10％
羟乙基脲1.0～6％
聚甘油-60.2～2％
猴面包树果肉提取物0.0001～1.0％
黄原胶0.0001～0.1％
小核菌胶0.001～1.0％
赖氨酸0.0001～2.0％
组氨酸0.0001～2.0％
精氨酸0.0001～2.0％
天冬氨酸0.0001～2.0％
苏氨酸0.0001～2.0％
丝氨酸0.0001～2.0％
谷氨酸0.0001～2.0％
脯氨酸0.0001～2.0％
甘氨酸0.0001～2.0％
丙氨酸0.0001～2.0％
缬氨酸0.0001～2.0％
异亮氨酸0.0001～2.0％
亮氨酸0.0001～2.0％
酪氨酸0.0001～2.0％
苯丙氨酸0.0001～2.0％
野大豆籽提取物0.0001～2.0％
透明质酸钠0.0001～2.0％
糖类同分异构体0.0001～2.0％
PEG/PPG-17/6共聚物0.1～2.0％
1,2-戊二醇0.00001～1.0％
羟苯基丙酰胺苯甲酸0.00001～1.0％
抗坏血酸棕榈酸酯0.00001～1.0％
甘油0.001～1.0％
羟苯甲酯0.00001～0.1％
羟苯乙酯0.00001～0.1％
羟苯丙酯0.00001～0.1％
羟苯丁酯0.00001～0.1％
羟苯异丁酯0.00001～0.1％
柠檬酸三乙酯0.01～1.0％
苯氧乙醇0.0001～0.1％
B相：丁二醇2～10％
甜菜碱2～8％
尿囊素0.01～0.5％
丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物0.05～0.5％
羟乙基纤维素0.01～1.0％
EDTA二钠0.01～0.1％
对羟基苯乙酮0.1～1.0％
纯水to100％
C相：三乙醇胺0.01～0.5％
D相：香精0.001～0.3％
PEG-50氢化蓖麻油0.0001～0.1％
壬基酚聚醚-140.0001～0.1％
丙二醇0.0001～0.1％
苯甲醇0.01～0.5％；
所述珍珠质原液水解珍珠是取海水珍珠粒经破碎去核后得到珍珠质；珍珠质经过超微粉碎得到细粉，细粉加水后按珍珠质粉重量的0.1～0.5％的比例加植物蛋白酶于45～50℃条件下搅拌5～8h，滤布过滤掉残渣，得到澄清液体；澄清液体用分子截留量100道尔顿膜过滤，浓缩到10％，得到珍珠质原液；常温下按体积比：珍珠质原液：水解珍珠＝1:18～25的比例将珍珠质原液和水解珍珠混合，搅拌均匀，备用。
2.一种权利要求1所述的珍珠质紧致补水面膜的制备方法，其特征在于，其步骤如下：
1)将B相加入到乳化锅中高速均质3～6分钟，加热至80～85℃，均质2～5分钟，保温25～40分钟；
2)冷却至55～60℃加入C相搅拌均匀；
3)冷却至25～30℃加入A相和D相，搅拌均匀，理化指标检验合格后，出料得到面膜精华液；用25ml～30ml面膜精华液浸泡天丝无纺布得到珍珠质紧致补水面膜。
3.根据权利要求1所述的珍珠质紧致补水面膜，其特征在于：所述植物蛋白酶是木瓜蛋白酶或菠萝蛋白酶。
CN201610063498.5A 2016-01-30 2016-01-30 珍珠质紧致补水面膜及其制备方法 Active CN105616325B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610063498.5A CN105616325B (zh) 2016-01-30 2016-01-30 珍珠质紧致补水面膜及其制备方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610063498.5A CN105616325B (zh) 2016-01-30 2016-01-30 珍珠质紧致补水面膜及其制备方法

Publications (2)

Publication Number Publication Date
CN105616325A true CN105616325A (zh) 2016-06-01
CN105616325B CN105616325B (zh) 2019-01-08

Family

ID=56031956

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610063498.5A Active CN105616325B (zh) 2016-01-30 2016-01-30 珍珠质紧致补水面膜及其制备方法

Country Status (1)

Country Link
CN (1) CN105616325B (zh)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265748A (zh) * 2016-08-08 2017-01-04 广东荣辉珍珠养殖有限公司 一种富含活性肽的纳米珍珠粉的制备方法
CN107233230A (zh) * 2017-07-24 2017-10-10 卢旺 一种舒缓中和化妆品组合物及其制备方法
CN107496336A (zh) * 2017-10-02 2017-12-22 海南京润珍珠生物技术股份有限公司 水衡净透拍拍珍珠化妆水及其制备方法
CN107582505A (zh) * 2017-10-02 2018-01-16 海南京润珍珠生物技术股份有限公司 珍珠氨基酸熬夜焕亮面膜及其制备方法
CN107625721A (zh) * 2017-10-02 2018-01-26 海南京润珍珠生物技术股份有限公司 焕肤熬夜精华及其制备方法
CN109316377A (zh) * 2018-10-11 2019-02-12 西安医学院 一种含有融合蛋白的复方精华液及制备方法
CN112089678A (zh) * 2020-10-28 2020-12-18 北海市海真珠化妆品有限公司 一种不含防腐剂的保湿珍珠面膜及其制备方法
CN112716877A (zh) * 2019-10-28 2021-04-30 广东名辰堂健康产业股份有限公司 一种含天然成分的水润紧致蚕丝面膜
CN114381861A (zh) * 2020-10-22 2022-04-22 立肯诺(上海)新材料科技有限公司 一种珍珠氨基酸水刺无纺布及其制备方法

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
LESLIEFR: "京润珍珠珍珠蚕丝凝萃紧致面膜", 《COSDNA》 *
木子生活馆: "面膜到底有没有用", 《微口网》 *
海南京润珍珠生物技术股份有限公司: "京润珍珠珍珠原液密集补水面膜", 《国产非特殊用途化妆品备案服务平台》 *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106265748A (zh) * 2016-08-08 2017-01-04 广东荣辉珍珠养殖有限公司 一种富含活性肽的纳米珍珠粉的制备方法
CN107233230A (zh) * 2017-07-24 2017-10-10 卢旺 一种舒缓中和化妆品组合物及其制备方法
CN107496336A (zh) * 2017-10-02 2017-12-22 海南京润珍珠生物技术股份有限公司 水衡净透拍拍珍珠化妆水及其制备方法
CN107582505A (zh) * 2017-10-02 2018-01-16 海南京润珍珠生物技术股份有限公司 珍珠氨基酸熬夜焕亮面膜及其制备方法
CN107625721A (zh) * 2017-10-02 2018-01-26 海南京润珍珠生物技术股份有限公司 焕肤熬夜精华及其制备方法
CN109316377A (zh) * 2018-10-11 2019-02-12 西安医学院 一种含有融合蛋白的复方精华液及制备方法
CN112716877A (zh) * 2019-10-28 2021-04-30 广东名辰堂健康产业股份有限公司 一种含天然成分的水润紧致蚕丝面膜
CN114381861A (zh) * 2020-10-22 2022-04-22 立肯诺(上海)新材料科技有限公司 一种珍珠氨基酸水刺无纺布及其制备方法
CN114381861B (zh) * 2020-10-22 2023-02-28 立肯诺(上海)新材料科技有限公司 一种珍珠氨基酸水刺无纺布及其制备方法
CN112089678A (zh) * 2020-10-28 2020-12-18 北海市海真珠化妆品有限公司 一种不含防腐剂的保湿珍珠面膜及其制备方法

Also Published As

Publication number Publication date
CN105616325B (zh) 2019-01-08

Similar Documents

Publication Publication Date Title
CN105616325A (zh) 珍珠质紧致补水面膜及其制备方法
CN105640868B (zh) 珍珠氨基酸熬夜莹润面膜及其制备方法
CN104367537A (zh) 一种滋润美颜面膜及其制备方法
CN105640867A (zh) 珍珠原液密集补水面膜及其制备方法
CN103565699B (zh) 一种黑果枸杞祛斑美白抗衰老精华液及其制备方法
CN110547976A (zh) 一种含裂裥菌素化妆品用添加剂
CN105687080A (zh) 珍珠贝泌素亮采补水面膜及其制备方法
CN1803124A (zh) γ－聚谷氨酸及γ－聚谷氨酸盐及其水凝胶的用途
CN101744757A (zh) 含天然有机成分的无防腐保湿紧肤化妆品
CN103800253B (zh) 一种保湿清爽洁面膏
CN105395412A (zh) 一种补水面膜
CN105078873A (zh) 一种具有紧致美白功效的生物护肤组合物
CN108125892A (zh) 一种海洋生物保湿抗衰老化妆品组合物
CN111419755B (zh) 一种沉香富勒烯精华液及其制备方法
CN101172095A (zh) 含有蜂王浆的蛋白水解物的化妆材料
CN106109268A (zh) 一种美白精华晚霜及其制备方法
CN107510617A (zh) 藻蓝蛋白保护剂及其制备方法和藻蓝蛋白组合物与保湿化妆水
CN109998937A (zh) 含有甘油葡糖苷（αGG）的系列化妆品及其制备方法
CN104736135A (zh) 化妆品组合物
CN102802603A (zh) 胶原产生减少抑制剂、包含该胶原产生减少抑制剂的皮肤外用组合物和化妆品
CN110478288A (zh) 一种皮肤抗衰老组合成分
CN112675060B (zh) 一种抵抗皮肤衰老的组合物、护肤品及其制备方法
CN108309919A (zh) 羊胎盘肽-骨胶原蛋白多肽组合物、含有该组合物的面膜液
CN102631301A (zh) 一种丝瓜水溶液
CN108635276A (zh) 一种祛皱的护肤组合物及其应用

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant