CN105595009A - Feed additive for laying gooses in egg producing period and preparation method thereof - Google Patents
Feed additive for laying gooses in egg producing period and preparation method thereof Download PDFInfo
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention discloses a feed additive for laying gooses in an egg producing period and a preparation method thereof. The feed additive is prepared from pericarpium citri reticulatae, Sculellaria barbata, turmeric, semen cassia, curcuma zedoary, lucid ganoderma, Shuishangyao (a Chinese medicine), hawthorns, sparganium stoloniferum, rhaponticum uniforum, folium sennae, chamomile, fructus piperis longi, radix puerariae, dicranostigma leptopodum, polygonum multiflorum and specious alpinia seed. The feed additive has the beneficial effects that the nutrition demands of the laying gooses in the egg producing period are met; meanwhile, the cholesterol content of goose eggs of the laying gooses is reduced, and the quality of the goose eggs is improved; and furthermore, development of immune organs of the laying gooses can be promoted, the immunity of the organ is enhanced, glands are stimulated to release FSH and LH, follicle maturity and ovulation are accelerated, and the egg yield of the laying gooses is increased.
Description
Technical field
The present invention relates to egg goose feed addictive, particularly a kind of feed addictive for egg geese in laying period and preparation method thereof.
Background technology
Along with people's growth in the living standard, people require also more and more higher to food, wish edible pollution-free food. And goose egg provides the nutriment of various abundances, meet people's demand. The protein content of goose egg is lower than egg, and fat content, higher than other eggs, also contains multivitamin and mineral matter in goose egg. People choose eggs, more like the goose egg that yolk color is darker. On market, once there is being added with the additive of coloring agent, a lot of additives mostly are chemical synthetic drug, hormone etc., the egg geese in laying period ubiquity medicine that these additives raise out can remain in goose body, finally brings harm in various degree by food chain to human body. Along with the fast development of aquaculture and improving constantly of living standard, how people from amount to qualitative change, therefore, provide best in quality to the demand of goose egg, local flavor is delicious, the goose egg of safety, nutrition is the direction of animal husbandry future development.
Along with the popularization of the good supporting strain of egg goose and the development of feed industry, the egg laying performance of commodity egg goose is greatly improved, but meanwhile the quality of goose egg is on the contrary in continuous decline, the natural flavour mountaineous of goose egg do not existed, the antibiotic that particularly serious is in feed and the residual health that is just threatening the mankind of chemicals. Along with the raising of people's living standard, people change to mass type from scalar type the requirement of livestock products, and safety, green, healthy food more and more become people's first-selection. In various livestock products, all contain abundant cholesterol, take in appropriate cholesterol and be conducive to health, but the too high angiocardiopathy of can bringing out of cholesterol intake. Along with the raising of animal husbandry level, China especially town dweller's diet structure has a very large change, and meat, egg, milk consumption figure significantly raise per capita, and energy absorption level obviously improves, and the cholesterol intake in various sources increases. Goose egg is as the popular animal food of cheapness, and the past enjoys people's favor always, but because goose egg is a main source (also containing a large amount of cholesterol in the liver of animal and heart) of cholesterol, people have had new misgivings to edible goose egg. MaNamara has analyzed deliver for 1994 ~ 1996 years 10 independently clinical testing papers, point out under low meals condition, healthy edible 1 ~ 2 piece of goose egg consumer's every day is very little to lipid, but edible more goose egg, great majority research still shows the trend that blood fat raises. The high cholesterol count of goose egg may cause or increase the weight of the angiocardiopathies such as mankind's high fat of blood, coronary heart disease, atherosclerotic. Goose egg is nutritious, proportional balancing method, is the good protein foods of the mankind, if give up it because of cholesterol problem, is tantamount to be put off easily by a slight risk.
How to address the above problem, be the problem that the present invention faces.
Summary of the invention
In order to meet the nutritional need of egg goose, improve the quality of goose egg, promote the growth of egg goose immune organ, the invention provides a kind of feed addictive for egg geese in laying period and preparation method thereof.
In order to realize foregoing invention object, the invention provides a kind of feed addictive for egg geese in laying period, wherein, described feed addictive comprises following raw material: dried orange peel, Sculellaria barbata, turmeric, cassia seed, curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi, Radix Rhapontici seu Radix Echinopsis, folium sennae, chamomile, the Bi roots of grass, the root of kudzu vine, slenderstalk dicranostigma herb, the fleece-flower root and beautiful galangal seed.
Described feed addictive is made up of the raw material of following parts by weight: dried orange peel 10-20 weight portion, Sculellaria barbata 12-32 weight portion, turmeric 11-21 weight portion, cassia seed 13-27 weight portion, curcuma zedoary 14-21 weight portion, glossy ganoderma 10-30 weight portion, narrowsepal loosestrife herb 15-35 weight portion, hawthorn 11-22 weight portion, rhizoma scirpi 12-34 weight portion, Radix Rhapontici seu Radix Echinopsis 10-35 weight portion, folium sennae 10-22 weight portion, chamomile 14-30 weight portion and Bi roots of grass 15-18 weight portion.
Described feed addictive is made up of the raw material of following parts by weight: dried orange peel 12-20 weight portion, Sculellaria barbata 14-30 weight portion, turmeric 13-20 weight portion, cassia seed 15-26 weight portion, curcuma zedoary 15-20 weight portion, glossy ganoderma 12-30 weight portion, narrowsepal loosestrife herb 15-33 weight portion, hawthorn 13-22 weight portion, rhizoma scirpi 14-32 weight portion, Radix Rhapontici seu Radix Echinopsis 10-34 weight portion, folium sennae 10-18 weight portion, chamomile 14-30 weight portion and Bi roots of grass 16-18 weight portion.
Described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions and the Bi roots of grass 17 weight portions.
Described feed addictive is made up of the raw material of following parts by weight: dried orange peel 10-20 weight portion, Sculellaria barbata 12-32 weight portion, turmeric 11-21 weight portion, cassia seed 13-27 weight portion, curcuma zedoary 14-21 weight portion, glossy ganoderma 10-30 weight portion, narrowsepal loosestrife herb 15-35 weight portion, hawthorn 11-22 weight portion, rhizoma scirpi 12-34 weight portion, Radix Rhapontici seu Radix Echinopsis 10-35 weight portion, folium sennae 10-22 weight portion, chamomile 14-30 weight portion, Bi roots of grass 15-18 weight portion, root of kudzu vine 11-19 weight portion, slenderstalk dicranostigma herb 0.1-0.5 weight portion, fleece-flower root 12-20 weight portion and beautiful galangal seed 15-35 weight portion.
Described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions, the Bi roots of grass 17 weight portions, the root of kudzu vine 12 weight portions, slenderstalk dicranostigma herb 0.3 weight portion, the fleece-flower root 16 weight portions and beautiful galangal seed 21 weight portions.
The formulation of described feed addictive is pulvis, and its preparation method is:
The first step, by described raw material, mark is than mixing by weight, and input pulverizer is pulverized or directly chopping, pack into and decoct in container, add suitable quantity of water to make its submergence medicinal material, soak after 30-50 minute, be heated to seethe with excitement after 30-50 minute, separate fried liquid, the dregs of a decoction again add water and decoct 2-3 time, isolate respectively fried liquid at every turn, merge all fried liquid, after filtering, get filtrate and abandon filter residue again;
Second step, after filtrate is cooling, adding with respect to liquid weight 1-2 determining alcohol doubly after concentrated is 80-90% ethanol, fully mix, placement is spent the night, and makes its precipitation, after getting its supernatant liquid filtering next day, obtain filtrate, the ethanol that sediment is 50-60% with determining alcohol is cleaned, and collects washing lotion and merges with filtrate, decompression is regained after ethanol, leave standstill 0.5-1 hour, make precipitation completely, filter, filtrate low-temperature evaporation, obtains paste;
The 3rd step: paste is put into spray dryer dry, ensure that EAT is at 180 DEG C-200 DEG C, 70 DEG C-90 DEG C of leaving air temps, are ground into 200 order-300 orders subsequently, obtain pulvis.
The formulation of described feed addictive is powder, and its preparation method is:
The first step, mixes curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi in described ratio, the ethanol that to use with respect to the determining alcohol of 3～5 times of mixture quality obtaining be 80%～90% dissolves, and adds hot reflux and extracts after 1～3 hour, and filtration, obtains the first filtered fluid; Filter residue is used to the ethanol dissolving with respect to the determining alcohol 80%～90% of 1～2 times of the mixture quality obtaining again, add hot reflux and extract after 1～2 hour, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, decompression recycling ethanol to be concentrated into liquor strength be 0.7～0.9g crude drug/mL, the large pore resin absorption column wash-out that is 5L through volume, first use deionized water or the distilled water wash-out of 5 times of resin column volumes, be 80%～90% ethanol elution with the determining alcohol of 3 times of resin column volumes again, collect ethanol eluate, reduced pressure concentration is removed ethanol, is dried and is ground into powder;
Second step, folium sennae, chamomile and the Bi roots of grass are mixed in described ratio, add the ethanol with respect to the determining alcohol 80%～90% of 2～4 times of the mixture quality obtaining, heating and refluxing extraction 1～2 time, extract merges, with the centrifugal removal of impurities of tube centrifuge, the lotion that when extract after removal of impurities is evaporated to 60 DEG C under the condition of 60 DEG C～70 DEG C, relative density is 1.20～1.23, is dried to powder by the lotion after concentrated with spray dryer;
The 3rd step, mixes surplus stock medicinal material in described ratio, add the water-soluble solution of 2～4 times with respect to the mixture quality obtaining, and heating decocts 2～4 hours, filters; Filter residue is used to the water-soluble solution of 1～2 times with respect to the mixture quality obtaining again, and heating decocts 1～2 hour again, filters; Merge the filtered fluid of twice, reduced pressure concentration is removed moisture, is dried and is ground into powder;
The 4th step, the powder that the first step, second step and the 3rd step are obtained mixes, and is screened into subsequently 80～120 object fine powders, and the fine powder of acquisition is dropped in mixing and blending machine and stirred, and obtains powder.
The addition of described feed addictive in feed is to add 5-10kg in feed per ton, is preferably in feed per ton and adds 7-9kg.
The invention has the beneficial effects as follows: not only meet the nutritional need of egg geese in laying period, and reduced the cholesterol level of egg goose goose egg, improved the quality of goose egg; In addition, can also promote the growth of egg goose immune organ, improve the immunity of body, stimulate body of gland to discharge FSH and LH, accelerate follicle maturity and ovulation, and then improved the laying rate of egg goose.
Detailed description of the invention
The invention provides a kind of feed addictive for egg geese in laying period, comprise following raw material: dried orange peel, Sculellaria barbata, turmeric, cassia seed, curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi, Radix Rhapontici seu Radix Echinopsis, folium sennae, chamomile, the Bi roots of grass, the root of kudzu vine, slenderstalk dicranostigma herb, the fleece-flower root and beautiful galangal seed.
The characteristic of above-mentioned raw materials is as follows:
The Bi roots of grass: nature and flavor: pungent, heat. Gui Jing: return stomach, large intestine channel. Cure mainly: warming spleen and stomach for dispelling cold, lower gas pain relieving. For coldness and pain in the epigastrium, vomiting, has loose bowels, antimigraine; Control toothache outward.
Beautiful galangal seed: nature and flavor: warm in nature, taste is pungent, puckery. Cure mainly: dry temperature dispelling cold, eliminating phlegm preventing malaria, stomach is warmed up in invigorating the spleen. Be interrupted stagnant, indigestion, vomiting and diarrhoea for trusted subordinate's crymodynia, fullness and oppression of chest and abdomen, phlegm.
Folium sennae: nature and flavor: sweet, bitter, cold. Gui Jing: return large intestine channel. Cure mainly: the row that purges heat is stagnant, defaecation, Li Shui. Stagnant for thermojunction, constipation stomachache, oedema turgor.
Rhizoma scirpi: nature and flavor: taste is pungent; Bitter; Property is put down. Gui Jing: liver; The spleen channel. Cure mainly: the stasis of blood of dispelling is stimulated the menstrual flow; Broken blood eliminating mass; Promoting the circulation of qi disappears long-pending. Main amenorrhea due to stagnation of blood; Dysmenorrhoea; Postpartum, stasis blocking was suffered from abdominal pain; Fall dozen stasis of blood swollen; Enclosed mass in abdomen; Dyspeptic abdominalgia
Narrowsepal loosestrife herb: source: " Guizhou folk medicine ". Nature and flavor: property is flat, and bitter is sour and astringent. Cure mainly: blood is broken in promoting the circulation of qi detumescence, removing toxic substances. Control through closing internal lesion caused by overexertion, furunculosis.
Curcuma zedoary: nature and flavor: pungent, bitter, temperature. Gui Jing: return liver, the spleen channel. Cure mainly: blood is broken in promoting the circulation of qi, long-pending pain relieving disappears. For Dan lump in the abdomen lump in the abdomen, hemostasis is through closing, dyspepsia distending pain; Early cervical carcinoma.
Slenderstalk dicranostigma herb: source: Papaveraceae slenderstalk dicranostigma herb platymiscium slenderstalk dicranostigma herb Dicranostigmaleptopodum(Maxim.) Fedde, with all herbal medicine. Spring and summer gathers, and dries. Nature and flavor: bitter, puckery, cool. Poisonous. Cure mainly: clearing heat and detoxicating, swelling and pain relieving, desinsection. For tonsillitis, toothache, scrofula; Favus of the scalp is controlled in external application, ringworm of the body.
Sculellaria barbata: nature and flavor: pungent, bitter, cold. Gui Jing: return lung, liver, kidney channel. Cure mainly: clearing heat and detoxicating, stagnation resolvation diuresis. For furuncle swelling toxin, abscess of throat, venomous snake bite, falls and flutters the pain of injury, oedema, jaundice.
Dried orange peel: warm in nature, taste is pungent, bitter; Return spleen, lung channel, for diseases such as fullness and oppression of chest and abdomen. The pungent loose logical temperature of orange peel, fragrant odour, is longer than and regulates the flow of vital energy, can enter spleen lung, thus can go loose sluggishness of lung-QI, again can promoting the circulation of qi wide in, gather around the diseases such as the full and taste stagnation of the circulation of vital energy of stagnant, chest diaphragm ruffian, abdominal fullness and distention for lung qi, for damp retention in middle-jiao, gastral cavity abdomen ruffian is swollen, have loose bowels in loose stool, and the phlegm disease such as cough more.
Turmeric: warm in nature, taste is pungent, bitter; Return spleen, Liver Channel, there is broken blood gas, inducing meastruation to relieve menalgia effect. Twinge amenorrhoea, abdominal mass, rheumatism shoulder arm pain, tumbling and swelling for the chest side of body.
Cassia seed: cassia seed bitter, sweet, salty, cold nature, enters liver, kidney, large intestine channel; Relax bowel, lipopenicillinase improving eyesight, treatment constipation and high fat of blood, hypertension. Clear liver and improve vision, sharp water defaecation, has laxative action, reducing blood pressure and blood fat.
Glossy ganoderma: property is sweet, flat; The thoughts of returning home, liver, spleen, lung, the kidney Five Classics. Cure mainly consumptive disease, cough, asthma, insomnia, indigestion, malignant tumour etc. Animal pharmacology shows experiment: glossy ganoderma has inhibitory action to nervous system, and the circulatory system has step-down and strengthens the effect of cardiac contractile force, and respiratory system is had to phlegm-dispelling functions, in addition, protects in addition liver, improves immunologic function, antibacterially waits effect.
Hawthorn: taste acid, sweet, slightly warm in nature, enters spleen, stomach, Liver Channel, and for food digesting stomach fortifying, the promoting the circulation of qi stasis of blood of faling apart, is mainly used to treat accumulation of food in the stomach and intes tine due to indigestion, have loose bowels, dysentery, hawthorn is the staple for the treatment of indigestion, hawthorn can increase the secretion of peptic digest enzyme, promotes digestion; Shigella dysenteriae, Pseudomonas aeruginosa, staphylococcus aureus etc. are had to obvious inhibitory action.
Radix Rhapontici seu Radix Echinopsis: bitter is salty, trembles with fear into stomach, large intestine channel. Have clearing heat and detoxicating, the carbuncle that disappears, lactogenesis, effect that relaxing muscles and tendons is promoted blood circulation. Cure mainly for acute mastitis and swell and ache, ulcer carbuncle on the back, scrofula sore, alactation, arthritis with fixed pain caused by dampness contraction, arthralgia, toxic-heat and blood stasis, hemorrhoid hemorrhage. " detailed outline " recorded: " Gu Dongyuan thinks hand for Radix Rhapontici seu Radix Echinopsis, lower milk, the heat that disappears poison, apocenosis, hemostasis, myogenic, desinsection, the positive bright medicine of foot, and ancient prescription is controlled ulcer carbuncle on the back, to claim also headed by Radix Rhapontici seu Radix Echinopsis soup. When Pang Anchang treatise on Febrile Diseases is controlled ulcer and separates in advance, row acne rash heat, uses Radix Rhapontici seu Radix Echinopsis leaf, cloud without with fructus gardeniae for it, also get its cold can be antipyretic, therefore lid do not know its can enter sun bright also. ".
Chamomile: mildly bitter flavor, Gan Xiang, improving eyesight, move back irascibility, Cure for insomnia, reduces blood pressure, and can invigorate, refresh oneself. Strengthen memory, reduce cholesterol. Expelling phlegm and arresting coughing, can effectively alleviate bronchitis and asthma, the courbature that can releive headache, antimigraine or flu cause, in and hydrochloric acid in gastric juice, releive neural helpful.
The root of kudzu vine: nature and flavor are sweet pungent is flat; Be included into spleen, stomach warp. There is a liter positive expelling pathogenic factors from muscles and skin, promoting eruption antidiarrheal, relieving restlessness stops warm effect. Cold, the warm headache Xiang Qiang that cures the wound, dysphoria with smothery sensation is quenched one's thirst, has loose bowels, dysentery, ecchymosis is not saturating, hypertension, angina pectoris, deafness.
The fleece-flower root: slightly warm in nature, bitter, sweet, puckery; Return liver, kidney channel. There is nourishing the blood and yin; Relax bowel; Preventing malaria; Dispel the wind; Effect of removing toxic substances. Cure mainly deficiency of blood Light-headedness; Palpitaition; Insomnia; The soreness and weakness of waist and knees of the deficiency of liver-yin and kidney-yin; Poliosis; Tinnitus; Seminal emission; The dry constipation of intestines; Chronic malaria body void; Rubella itch; Sore carbuncle; Scrofula; Hemorrhoid.
Below adopt embodiment to describe embodiments of the present invention in detail, to the present invention, how application technology means solve technical problem whereby, and the implementation procedure of reaching technique effect can fully understand and implement according to this.
Embodiment 1 feed addictive 1
The embodiment of the present invention provides a kind of feed addictive for egg geese in laying period, and described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions and the Bi roots of grass 17 weight portions;
The first step, by described raw material, mark is than mixing by weight, and input pulverizer is pulverized or directly chopping, pack into and decoct in container, add suitable quantity of water to make its submergence medicinal material, soak after 40 minutes, be heated to seethe with excitement after 35 minutes, separate fried liquid, the dregs of a decoction again add water and decoct 3 times, isolate respectively fried liquid at every turn, merge all fried liquid, after filtering, get filtrate and abandon filter residue again;
Second step, after filtrate is cooling, adding with respect to the determining alcohol of 2 times of liquid weights after concentrated is 85% ethanol, fully mix, placement is spent the night, and makes its precipitation, after getting its supernatant liquid filtering next day, obtain filtrate, the ethanol that sediment is 55% with determining alcohol is cleaned, and collects washing lotion and merges with filtrate, decompression is regained after ethanol, leave standstill 0.5 hour, make precipitation completely, filter, filtrate low-temperature evaporation, obtains paste;
The 3rd step: paste is put into spray dryer dry, ensure that EAT is at 200 DEG C, 80 DEG C of leaving air temps, are ground into 250 orders subsequently, obtain pulvis.
The addition of above-mentioned feed addictive in feed is to add 10kg in feed per ton.
Embodiment 2 feed addictives 2
The invention provides a kind of feed addictive for egg geese in laying period, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions, the Bi roots of grass 17 weight portions, the root of kudzu vine 12 weight portions, slenderstalk dicranostigma herb 0.3 weight portion, the fleece-flower root 16 weight portions and beautiful galangal seed 21 weight portions;
The first step, mixes curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi in described ratio, the ethanol that to use with respect to the determining alcohol of 4 times of mixture quality obtaining be 85% dissolves, and adds hot reflux and extracts after 2 hours, and filtration, obtains the first filtered fluid; Filter residue is used to the ethanol dissolving with respect to the determining alcohol 85% of 1.5 times of the mixture quality obtaining again, add hot reflux and extract after 2 hours, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, decompression recycling ethanol to be concentrated into liquor strength be 0.8g crude drug/mL, the large pore resin absorption column wash-out that is 5L through volume, first use deionized water or the distilled water wash-out of 5 times of resin column volumes, be 85% ethanol elution with the determining alcohol of 3 times of resin column volumes again, collect ethanol eluate, reduced pressure concentration is removed ethanol, is dried and is ground into powder;
Second step, folium sennae, chamomile and the Bi roots of grass are mixed in described ratio, add the ethanol with respect to the determining alcohol 90% of 3 times of the mixture quality obtaining, heating and refluxing extraction 2 times, extract merges, with the centrifugal removal of impurities of tube centrifuge, the lotion that when extract after removal of impurities is evaporated to 60 DEG C under the condition of 65 DEG C, relative density is 1.22, the lotion after concentrated is dried to powder with spray dryer;
The 3rd step, mixes surplus stock medicinal material in described ratio, add the water-soluble solution of 3 times with respect to the mixture quality obtaining, and heating decocts 4 hours, filters; Filter residue is used to the water-soluble solution of 1.5 times with respect to the mixture quality obtaining again, and heating decocts 2 hours again, filters; Merge the filtered fluid of twice, reduced pressure concentration is removed moisture, is dried and is ground into powder;
The 4th step, the powder that the first step, second step and the 3rd step are obtained mixes, and is screened into subsequently 80～120 object fine powders, and the fine powder of acquisition is dropped in mixing and blending machine and stirred, and obtains powder.
The addition of above-mentioned feed addictive in feed is to add 8kg in per ton gram of feed.
Toxicity test
(1) 40 of application NIH mouse, SPF level, male and female half and half, body weight 18～22g, carries out acute toxicity test. Mouse is divided into two groups at random, and 20 every group, i.e. control group and administration group, fasting 12 hours before experiment; Feed addictive 1 prepared by embodiments of the invention 1 is dissolved in water, (concentration is 6.58g crude drug/ml, maximum concentration) gavage, gavage volume is that 5ml/kg(is that single-dose dosage is 32.9 crude drugs/kg), control group gives equivalent physiological saline, administration in a day 2 times, delivery time 6 hours, Continuous Observation 14 days after administration, and record mouse toxic reaction and death toll. Experimental result shows: with control group comparison, after administration, mouse has no notable difference, experiment Continuous Observation 14 days, and mouse overall health of patients, diet, drinking-water, body weight gain are all normal.
(2) feed addictive that uses the embodiment of the present invention 2 to mouse by 10.78,20.35 and 16 weeks (1.0ml/100g body weight of 33.48g crude drug/kg continuous use, every day 2 times) and drug withdrawal after 4 weeks, result shows: the index such as the hair of Chinese medicine of the present invention to mouse, behavior, stool and urine, body weight, organ weights, blood picture, hepatic and renal function, blood sugar, blood fat all has no significant effect, internal organs naked eyes do not find that difference changes and histological examination result shows, medication 16 weeks and drug withdrawal are after 4 weeks, and Organs of Mice is all without obviously changing. Illustrate that toxicity is little after feed addictive of the present invention is to mouse long-term prescription, after drug withdrawal, also there is no difference reaction, application safety.
Contrast test
Sample plot is selected six and the egg goose goose field of choosing Haiyang City, Yantai, and company technique portion carries out the feeding experiment of 60 days by a definite date in the 5-6 month in 2012 in egg goose field. test choose 1800 55 week age normal egg goose, being divided into is immediately embodiment group 1, embodiment group 2 and control group, wherein, it is to add 10kg in conventional feed per ton that embodiment group 1 is utilized the addition of feed addictive 1 in conventional feed, it is to add 8kg in conventional feed per ton that embodiment group 2 is utilized the addition of feed addictive 2 in conventional feed, control group adopts traditional egg goose forage feed, duration of test, add up egg goose egg production and the egg size of each experimental group, and calculate egg goose laying rate and average egg weight, and quality and the cholesterol level of the goose egg of making a random inspection immediately, result is as table 1, shown in table 2 and table 3.
The table of comparisons of table 1 egg goose laying rate and average egg weight
| Project | Embodiment group 1 | Embodiment group 2 | Control group |
| Laying rate (%) | 91.96 | 92.15 | 82.53 |
| Average egg weight (g) | 75.327 | 75.286 | 73.848 |
Data from table 1: compared with the egg goose of feeding with conventional feed, the egg goose that uses the egg goose feed addictive of embodiment of the present invention group 1 and embodiment group 2 to feed, its laying rate exceeds 10% left and right, and its average egg weight exceeds 1.4g left and right.
The table 2 goose Egg Quality table of comparisons
| Project | Embodiment group 1 | Embodiment group 2 | Control group |
| Egg shape index | 1.332 | 1.327 | 1.316 |
| Eggshell strength (MPa) | 4.26 | 4.21 | 3.35 |
| Shell thickness (mm) | 0.363 | 0.357 | 0.349 |
| Yolk color (level) | 7.9 | 7.9 | 6.6 |
| Albumen height (mm) | 5.689 | 5.691 | 5.257 |
Data from table 2: the egg goose that uses the egg goose feed addictive of embodiment of the present invention group 1 and embodiment group 2 to feed, the egg goose goose egg that every index of quality of its goose egg is all fed higher than conventional feed.
The table 3 goose egg cholesterol level table of comparisons
| Project | Embodiment group 1 | Embodiment group 2 | Control group |
| Cholesterol (mg/) | 118.87 | 118.82 | 219.23 |
Data from table 3: the egg goose that uses the egg goose feed addictive of embodiment of the present invention group 1 and embodiment group 2 to feed, the cholesterol level of its goose egg is starkly lower than the egg goose goose egg that conventional feed is fed.
Known by above-mentioned experiment, the egg goose of the egg goose forage feed of proportioning of the present invention has not only been improved the quality of laying rate and goose egg, and obviously having reduced the content of cholesterol in goose egg, mixed feed of the present invention can be good at meeting the nutritional need of egg geese in laying period.
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (9)
1. the feed addictive for egg geese in laying period, it is characterized in that, described feed addictive comprises following raw material: dried orange peel, Sculellaria barbata, turmeric, cassia seed, curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi, Radix Rhapontici seu Radix Echinopsis, folium sennae, chamomile and the Bi roots of grass.
2. feed addictive according to claim 1, it is characterized in that, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 10-20 weight portion, Sculellaria barbata 12-32 weight portion, turmeric 11-21 weight portion, cassia seed 13-27 weight portion, curcuma zedoary 14-21 weight portion, glossy ganoderma 10-30 weight portion, narrowsepal loosestrife herb 15-35 weight portion, hawthorn 11-22 weight portion, rhizoma scirpi 12-34 weight portion, Radix Rhapontici seu Radix Echinopsis 10-35 weight portion, folium sennae 10-22 weight portion, chamomile 14-30 weight portion and Bi roots of grass 15-18 weight portion.
3. feed addictive according to claim 1 and 2, it is characterized in that, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 12-20 weight portion, Sculellaria barbata 14-30 weight portion, turmeric 13-20 weight portion, cassia seed 15-26 weight portion, curcuma zedoary 15-20 weight portion, glossy ganoderma 12-30 weight portion, narrowsepal loosestrife herb 15-33 weight portion, hawthorn 13-22 weight portion, rhizoma scirpi 14-32 weight portion, Radix Rhapontici seu Radix Echinopsis 10-34 weight portion, folium sennae 10-18 weight portion, chamomile 14-30 weight portion and Bi roots of grass 16-18 weight portion.
4. according to the feed addictive described in claim 1-3 any one, it is characterized in that, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions and the Bi roots of grass 17 weight portions.
5. according to the feed addictive described in claim 1-4 any one, it is characterized in that, described feed addictive also comprises that raw material is: the root of kudzu vine, slenderstalk dicranostigma herb, the fleece-flower root and beautiful galangal seed.
6. according to the feed addictive described in claim 1-5 any one, it is characterized in that, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 10-20 weight portion, Sculellaria barbata 12-32 weight portion, turmeric 11-21 weight portion, cassia seed 13-27 weight portion, curcuma zedoary 14-21 weight portion, glossy ganoderma 10-30 weight portion, narrowsepal loosestrife herb 15-35 weight portion, hawthorn 11-22 weight portion, rhizoma scirpi 12-34 weight portion, Radix Rhapontici seu Radix Echinopsis 10-35 weight portion, folium sennae 10-22 weight portion, chamomile 14-30 weight portion, Bi roots of grass 15-18 weight portion, root of kudzu vine 11-19 weight portion, slenderstalk dicranostigma herb 0.1-0.5 weight portion, fleece-flower root 12-20 weight portion and beautiful galangal seed 15-35 weight portion.
7. according to the feed addictive described in claim 1-6 any one, it is characterized in that, described feed addictive is made up of the raw material of following parts by weight: dried orange peel 16 weight portions, Sculellaria barbata 25 weight portions, turmeric 17 weight portions, cassia seed 24 weight portions, curcuma zedoary 16 weight portions, glossy ganoderma 28 weight portions, narrowsepal loosestrife herb 32 weight portions, hawthorn 20 weight portions, rhizoma scirpi 31 weight portions, Radix Rhapontici seu Radix Echinopsis 26 weight portions, folium sennae 15 weight portions, chamomile 23 weight portions, the Bi roots of grass 17 weight portions, the root of kudzu vine 12 weight portions, slenderstalk dicranostigma herb 0.3 weight portion, the fleece-flower root 16 weight portions and beautiful galangal seed 21 weight portions.
8. according to the feed addictive described in claim 1-7 any one, it is characterized in that, the formulation of feed addictive is pulvis, and its preparation method is:
The first step, by described raw material, mark is than mixing by weight, and input pulverizer is pulverized or directly chopping, pack into and decoct in container, add suitable quantity of water to make its submergence medicinal material, soak after 30-50 minute, be heated to seethe with excitement after 30-50 minute, separate fried liquid, the dregs of a decoction again add water and decoct 2-3 time, isolate respectively fried liquid at every turn, merge all fried liquid, after filtering, get filtrate and abandon filter residue again;
Second step, after filtrate is cooling, adding with respect to liquid weight 1-2 determining alcohol doubly after concentrated is 80-90% ethanol, fully mix, placement is spent the night, and makes its precipitation, after getting its supernatant liquid filtering next day, obtain filtrate, the ethanol that sediment is 50-60% with determining alcohol is cleaned, and collects washing lotion and merges with filtrate, decompression is regained after ethanol, leave standstill 0.5-1 hour, make precipitation completely, filter, filtrate low-temperature evaporation, obtains paste;
The 3rd step: paste is put into spray dryer dry, ensure that EAT is at 180 DEG C-200 DEG C, 70 DEG C-90 DEG C of leaving air temps, are ground into 200 order-300 orders subsequently, obtain pulvis.
9. a preparation method for the feed addictive as described in claim 1-7 any one, is characterized in that, the formulation of feed addictive is powder, and its preparation method is:
The first step, mixes curcuma zedoary, glossy ganoderma, narrowsepal loosestrife herb, hawthorn, rhizoma scirpi in described ratio, the ethanol that to use with respect to the determining alcohol of 3～5 times of mixture quality obtaining be 80%～90% dissolves, and adds hot reflux and extracts after 1～3 hour, and filtration, obtains the first filtered fluid; Filter residue is used to the ethanol dissolving with respect to the determining alcohol 80%～90% of 1～2 times of the mixture quality obtaining again, add hot reflux and extract after 1～2 hour, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, decompression recycling ethanol to be concentrated into liquor strength be 0.7～0.9g crude drug/mL, the large pore resin absorption column wash-out that is 5L through volume, first use deionized water or the distilled water wash-out of 5 times of resin column volumes, be 80%～90% ethanol elution with the determining alcohol of 3 times of resin column volumes again, collect ethanol eluate, reduced pressure concentration is removed ethanol, is dried and is ground into powder;
Second step, folium sennae, chamomile and the Bi roots of grass are mixed in described ratio, add the ethanol with respect to the determining alcohol 80%～90% of 2～4 times of the mixture quality obtaining, heating and refluxing extraction 1～2 time, extract merges, with the centrifugal removal of impurities of tube centrifuge, the lotion that when extract after removal of impurities is evaporated to 60 DEG C under the condition of 60 DEG C～70 DEG C, relative density is 1.20～1.23, is dried to powder by the lotion after concentrated with spray dryer;
The 3rd step, mixes surplus stock in described ratio, add the water-soluble solution of 2～4 times with respect to the mixture quality obtaining, and heating decocts 2～4 hours, filters; Filter residue is used to the water-soluble solution of 1～2 times with respect to the mixture quality obtaining again, and heating decocts 1～2 hour again, filters; Merge the filtered fluid of twice, reduced pressure concentration is removed moisture, is dried and is ground into powder;
The 4th step, the powder that the first step, second step and the 3rd step are obtained mixes, and is screened into subsequently 80～120 object fine powders, and the fine powder of acquisition is dropped in mixing and blending machine and stirred, and obtains powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610167198.1A CN105595009A (en) | 2016-03-23 | 2016-03-23 | Feed additive for laying gooses in egg producing period and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610167198.1A CN105595009A (en) | 2016-03-23 | 2016-03-23 | Feed additive for laying gooses in egg producing period and preparation method thereof |
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| CN105595009A true CN105595009A (en) | 2016-05-25 |
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| CN201610167198.1A Withdrawn CN105595009A (en) | 2016-03-23 | 2016-03-23 | Feed additive for laying gooses in egg producing period and preparation method thereof |
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| CN104323022A (en) * | 2014-11-05 | 2015-02-04 | 青岛悦邦达机械有限公司 | Egg goose feed and preparation method thereof |
| CN104886381A (en) * | 2015-05-16 | 2015-09-09 | 郭立俊 | Calcium fortifying feed for laying geese, and preparation method of calcium fortifying feed for laying geese |
| CN105053616A (en) * | 2015-07-28 | 2015-11-18 | 童国芳 | Hormone-free feed for egg-laying goose and preparation method thereof |
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- 2016-03-23 CN CN201610167198.1A patent/CN105595009A/en not_active Withdrawn
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|---|---|---|---|---|
| CN102860422A (en) * | 2011-07-06 | 2013-01-09 | 朱大威 | Process for preparing egg-laying goose feed |
| CN102885214A (en) * | 2011-07-19 | 2013-01-23 | 孙登建 | Chinese medicinal herb additive for preparing laying goose feed |
| CN103211108A (en) * | 2013-03-18 | 2013-07-24 | 方遒 | Spirulina laying goose feed |
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