CN105594753A - Method for preparing spraying agent used in orchards for dispelling birds - Google Patents
Method for preparing spraying agent used in orchards for dispelling birds Download PDFInfo
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- CN105594753A CN105594753A CN201510791743.XA CN201510791743A CN105594753A CN 105594753 A CN105594753 A CN 105594753A CN 201510791743 A CN201510791743 A CN 201510791743A CN 105594753 A CN105594753 A CN 105594753A
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Abstract
The invention discloses a method for preparing a spraying agent used in orchards for dispelling birds, and belongs to the technical field of agriculture. Aiming at the problems that a traditional bird preventing way has poor effect, consumes a lot of manpower and material resources and wastes a lot of money, the invention provides the method for preparing the spraying agent used in the orchards for dispelling the birds. The method comprises the steps: firstly, mixing eagle meat, cinereous vulture dung and accipitridae dung, then adding ethanol and aminophylline into the mixture, and carrying out reflux extraction on the mixture; next carrying out mixed enzymolysis on reflux residues and an enzyme, extracting an enzymatic hydrolysate, mixing the enzymatic hydrolysate with the reflux liquid, and then mixing with 1-methylcyclopropene, calcium propionate and sodium benzoate; and finally, soaking marigold petals and ageratum conyzoides petals in the obtained liquid, to obtain the spraying agent used in the orchards for dispelling the birds.
Description
Technical field
The invention discloses a kind of preparation method who disperses birds spray for orchard, belong to agricultural technology field.
Background technology
Birds are useful to the mankind on the one hand, also make troubles to the mankind on the other hand. After the fruit maturation in orchard, birds are largeAmount is flown into agricultural orchard, and to rob carpophagous Disasters also more and more serious. In order to protect birds, promote the ecological balance, reduce birdThe harm of class to orchard, also ensures simultaneously and must not injure the normal harvest in orchard under the prerequisite of birds, at airport periphery andBirds are driven at orchard place. For this reason, the mankind extensively adopt the methods such as dummy drives, sound is driven, employment is driven at present, but drive bird effectFruit is poor, and people carrys out bird and flies often, and people also walks bird, can not effectively drive.
At present, the anti-bird mode in orchard is to place scarecrow, erect block and manually drive etc. as main, and effect on driving birds is limited,The shortcoming existing has: (one) scarecrow and block that only short-term is effective, through certain hour, when aquatic bird progressively adapts to it, can weighNewly be gathered in orchard and search for food; (2) manually drive and need make an inspection tour and can not be interrupted, expend a large amount of human and material resources.
Summary of the invention
The technical problem that the present invention mainly solves: for traditional anti-bird mode weak effect, expend a large amount of human and material resources,And the problem of waste pile, the invention provides the preparation method who disperses birds spray for orchard, and the present invention firstBy using hawk meat, cinereous vulture ight soil and vulture hawk ight soil to mix, then add wherein ethanol and aminophylline, it is refluxed and is carriedGet, retell backflow residue and enzyme, carry out mixed enzymolysis, extract enzymolysis liquid and mix with phegma, then by its 1-methyl ring, propionic acidCalcium and Sodium Benzoate mix, finally by the soaked with liquid marigold petal obtaining and Ageratum conyzoides petal, obtain a kind of forBirds spray is dispersed in orchard.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
(1) get 2 ~ 3kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture excrementJust mix with vulture hawk ight soil, get 1 ~ 2kg mixing ight soil and put into container, mix with minced meat, then add wherein qualityMark is 80 ~ 90% the complete immersion mixture of ethanolic solution, then adds wherein 500 ~ 700g aminophylline, is warming up to 70 ~ 80DEG C, refluxing 2 ~ 4 times, return time is 30 ~ 40min, collects phegma, for subsequent use;
(2) by solid matter remaining after above-mentioned backflow and composite flavor protease in mass ratio 10:1 mix, thenPut it in container, adding wherein temperature is the distilled water of 50 ~ 60 DEG C, immersion mixture completely, and service property (quality) mark isIt is 6.0 ~ 6.5 that 15% hydrochloric acid solution regulates pH, keeps temperature 2 ~ 5h, and then filtration under diminished pressure while hot, puts the filtered fluid of gainedEnter in centrifuge and carry out centrifugation, collect supernatant;
(3) supernatant of gained is mixed with the phegma of step (1) gained, obtain mixed liquor, put into the reactor of 50LIn, the 1-methyl cyclopropene that the mass fraction that then adds wherein mixeding liquid volume 5 ~ 8% is 0.1%, uses nitrogen protection,Being warming up to 80 ~ 100 DEG C, is under 4000 ~ 6000r/min at rotating speed, stirs 5 ~ 10min;
(4) after above-mentioned stirring finishes, be cooled to 40 ~ 50 DEG C, add wherein 300 ~ 500mL dog saliva, stir, then toWherein 30 ~ 50g calcium propionate, 40 ~ 60g Sodium Benzoate, keeps temperature to stir 30 ~ 50min, and then discharging, by the discharging thing of gainedFilter, the filtered fluid of gained is put into Rotary Evaporators and concentrate, be concentrated into 1/3 of original volume, obtain concentrate;
(5) 1:1 in mass ratio, gets marigold petal and mixes with Ageratum conyzoides petal, then by the mixing petal of gained and upperState the concentrate of gained, by solid-to-liquid ratio 1:2, put into container, then add wherein the absolute ethyl alcohol of concentrate volume 5%, soAfter by container as in microwave device, keeping temperature is 40 ~ 60 DEG C, after microwave concussion 1 ~ 3h, filters, and the filtered fluid of gained is put intoIn centrifuge, carry out centrifugation, collect supernatant, can obtain dispersing birds spray.
Application process of the present invention is: when the fruit maturation of the fruit tree in orchard, and every 3 ~ 5 days, 1:2 by volume,The made the present invention birds spray of dispersing is mixed with water, then sprayed with fruit tree on, to obtain fruit by detectingGarden, because of the amount of the birds underproduction, has reduced by 70 ~ 80%.
The invention has the beneficial effects as follows:
(1) the present invention is by ecological relationship, and for preparing disperses birds spray, successful;
(2) cost of manufacture of the present invention is low, easy operating;
(3) what the present invention was made disperses birds spray, not only can disperse birds, and can keep fruit fresh.
Detailed description of the invention
Get 2 ~ 3kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture excrementJust mix with vulture hawk ight soil, get 1 ~ 2kg mixing ight soil and put into container, mix with minced meat, then add wherein qualityMark is 80 ~ 90% the complete immersion mixture of ethanolic solution, then adds wherein 500 ~ 700g aminophylline, is warming up to 70 ~ 80DEG C, refluxing 2 ~ 4 times, return time is 30 ~ 40min, collects phegma, for subsequent use; By solid matter remaining after above-mentioned backflowWith composite flavor protease in mass ratio 10:1 mix, then put it in container, adding wherein temperature is 50 ~ 60DEG C distilled water, completely immersion mixture, it is 6.0 ~ 6.5 that the hydrochloric acid solution that service property (quality) mark is 15% regulates pH, keeps temperatureDegree 2 ~ 5h, then filtration under diminished pressure while hot, puts into centrifuge by the filtered fluid of gained and carries out centrifugation, collects supernatant; WillThe supernatant of gained mixes with the phegma of gained, obtains mixed liquor, puts into the reactor of 50L, then adds whereinThe mass fraction of mixeding liquid volume 5 ~ 8% is 0.1% 1-methyl cyclopropene, uses nitrogen protection, is warming up to 80 ~ 100 DEG C,Rotating speed is under 4000 ~ 6000r/min, stirs 5 ~ 10min; After above-mentioned stirring finishes, be cooled to 40 ~ 50 DEG C, add wherein300 ~ 500mL dog saliva, stirs, then 30 ~ 50g calcium propionate wherein, 40 ~ 60g Sodium Benzoate, keep temperature stir 30 ~50min, then discharging, filters the discharging thing of gained, and the filtered fluid of gained is put into Rotary Evaporators and concentrate,Be concentrated into 1/3 of original volume, obtain concentrate; 1:1 in mass ratio, gets marigold petal and mixes with Ageratum conyzoides petal, thenBy the mixing petal of gained and the concentrate of above-mentioned gained, by solid-to-liquid ratio 1:2, put into container, then add concentrate whereinThe absolute ethyl alcohol of volume 5%, then by container as in microwave device, keeping temperature is 40 ~ 60 DEG C, mistake after microwave concussion 1 ~ 3hFilter, puts into centrifuge by the filtered fluid of gained and carries out centrifugation, collects supernatant, can obtain dispersing birds spray.
Example 1
Get 2kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture ight soil and vultureHawk ight soil mixes, and gets 1kg mixing ight soil and puts into container, mixes with minced meat, then adds wherein mass fraction to be80% the complete immersion mixture of ethanolic solution, then add wherein 500g aminophylline, be warming up to 70 DEG C, reflux 2 times, when backflowBetween be 30min, collect phegma, for subsequent use; Solid matter remaining after above-mentioned backflow and composite flavor protease are pressed to qualityMix than 10:1, then put it in container, adding wherein temperature is the distilled water of 50 DEG C, completely soaks and mixesThing, it is 6.0 that hydrochloric acid solution that service property (quality) mark is 15% regulates pH, keeps temperature 2h, then filtration under diminished pressure while hot, by instituteThe filtered fluid obtaining is put into centrifuge and is carried out centrifugation, collects supernatant; The phegma of the supernatant of gained and gained is mixedClose evenly, obtain mixed liquor, put into the reactor of 50L, then add wherein the mass fraction of mixeding liquid volume 5% to be0.1% 1-methyl cyclopropene, uses nitrogen protection, is warming up to 80 DEG C, is under 4000r/min at rotating speed, stirs 5min; TreatAfter stating and stirring and finish, be cooled to 40 DEG C, add wherein 300mL dog saliva, stir, then 30g calcium propionate wherein, 40gSodium Benzoate, keeps temperature to stir 30min, and then discharging, filters the discharging thing of gained, and the filtered fluid of gained is put intoIn Rotary Evaporators, concentrate, be concentrated into 1/3 of original volume, obtain concentrate; 1:1 in mass ratio, gets marigold petal and victoryRed thistle lobe mixes, and then, by the mixing petal of gained and the concentrate of above-mentioned gained, by solid-to-liquid ratio 1:2, puts into containerIn, then add wherein the absolute ethyl alcohol of concentrate volume 5%, then by container as in microwave device, keeping temperature is 40 DEG C,After microwave concussion 1h, filter, the filtered fluid of gained is put into centrifuge and carry out centrifugation, collect supernatant, can be drivenLoose birds spray.
When the fruit maturation of fruit tree in orchard, every 3 days, 1:2 by volume, by the made the present invention bird of dispersingClass spray is mixed with water, then sprayed with fruit tree on, by detect orchard because of the amount of the birds underproduction, reduced70％。
Example 2
Get 3kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture ight soil and vultureHawk ight soil mixes, and gets 2kg mixing ight soil and puts into container, mixes with minced meat, then adds wherein mass fraction to be90% the complete immersion mixture of ethanolic solution, then add wherein 700g aminophylline, be warming up to 80 DEG C, reflux 4 times, when backflowBetween be 40min, collect phegma, for subsequent use; Solid matter remaining after above-mentioned backflow and composite flavor protease are pressed to qualityMix than 10:1, then put it in container, adding wherein temperature is the distilled water of 60 DEG C, completely soaks and mixesThing, it is 6.5 that hydrochloric acid solution that service property (quality) mark is 15% regulates pH, keeps temperature 5h, then filtration under diminished pressure while hot, by instituteThe filtered fluid obtaining is put into centrifuge and is carried out centrifugation, collects supernatant; The phegma of the supernatant of gained and gained is mixedClose evenly, obtain mixed liquor, put into the reactor of 50L, then add wherein the mass fraction of mixeding liquid volume 8% to be0.1% 1-methyl cyclopropene, uses nitrogen protection, is warming up to 100 DEG C, is under 6000r/min at rotating speed, stirs 10min; TreatAfter above-mentioned stirring finishes, be cooled to 50 DEG C, add wherein 500mL dog saliva, stir, then 50g calcium propionate wherein,60g Sodium Benzoate, keeps temperature to stir 50min, and then discharging, filters the discharging thing of gained, by the filtered fluid of gainedPut into Rotary Evaporators and concentrate, be concentrated into 1/3 of original volume, obtain concentrate; 1:1 in mass ratio, gets marigold petalMix with Ageratum conyzoides petal, then, by the mixing petal of gained and the concentrate of above-mentioned gained, by solid-to-liquid ratio 1:2, put intoIn container, then add wherein the absolute ethyl alcohol of concentrate volume 5%, then by container as in microwave device, keep temperature to be60 DEG C, after microwave concussion 3h, filter, the filtered fluid of gained is put into centrifuge and carry out centrifugation, collect supernatant,Obtain dispersing birds spray.
When the fruit maturation of fruit tree in orchard, every 5 days, 1:2 by volume, by the made the present invention birds of dispersingSpray is mixed with water, then sprayed with fruit tree on, by detect orchard because of the amount of the birds underproduction, reduced80％。
Example 3
Get 3kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture ight soil and vultureHawk ight soil mixes, and gets 1kg mixing ight soil and puts into container, mixes with minced meat, then adds wherein mass fraction to be85% the complete immersion mixture of ethanolic solution, then add wherein 600g aminophylline, be warming up to 70 DEG C, reflux 3 times, when backflowBetween be 35min, collect phegma, for subsequent use; Solid matter remaining after above-mentioned backflow and composite flavor protease are pressed to qualityMix than 10:1, then put it in container, adding wherein temperature is the distilled water of 50 DEG C, completely soaks and mixesThing, it is 6.5 that hydrochloric acid solution that service property (quality) mark is 15% regulates pH, keeps temperature 3h, then filtration under diminished pressure while hot, by instituteThe filtered fluid obtaining is put into centrifuge and is carried out centrifugation, collects supernatant; The phegma of the supernatant of gained and gained is mixedClose evenly, obtain mixed liquor, put into the reactor of 50L, then add wherein the mass fraction of mixeding liquid volume 7% to be0.1% 1-methyl cyclopropene, uses nitrogen protection, is warming up to 90 DEG C, is under 5000r/min at rotating speed, stirs 8min; TreatAfter stating and stirring and finish, be cooled to 45 DEG C, add wherein 400mL dog saliva, stir, then 40g calcium propionate wherein, 50gSodium Benzoate, keeps temperature to stir 40min, and then discharging, filters the discharging thing of gained, and the filtered fluid of gained is put intoIn Rotary Evaporators, concentrate, be concentrated into 1/3 of original volume, obtain concentrate; 1:1 in mass ratio, gets marigold petal and victoryRed thistle lobe mixes, and then, by the mixing petal of gained and the concentrate of above-mentioned gained, by solid-to-liquid ratio 1:2, puts into containerIn, then add wherein the absolute ethyl alcohol of concentrate volume 5%, then by container as in microwave device, keeping temperature is 50 DEG C,After microwave concussion 2h, filter, the filtered fluid of gained is put into centrifuge and carry out centrifugation, collect supernatant, can be drivenLoose birds spray.
When the fruit maturation of fruit tree in orchard, every 4 days, 1:2 by volume, by the made the present invention bird of dispersingClass spray is mixed with water, then sprayed with fruit tree on, by detect orchard because of the amount of the birds underproduction, reduced76％。
Claims (1)
1. disperse a preparation method for birds spray for orchard, it is characterized in that concrete preparation process is:
(1) get 2 ~ 3kg hawk meat and put into meat grinder and be twisted into minced meat, put it in container, then 1:1 in mass ratio, by cinereous vulture excrementJust mix with vulture hawk ight soil, get 1 ~ 2kg mixing ight soil and put into container, mix with minced meat, then add wherein qualityMark is 80 ~ 90% the complete immersion mixture of ethanolic solution, then adds wherein 500 ~ 700g aminophylline, is warming up to 70 ~ 80DEG C, refluxing 2 ~ 4 times, return time is 30 ~ 40min, collects phegma, for subsequent use;
(2) by solid matter remaining after above-mentioned backflow and composite flavor protease in mass ratio 10:1 mix, thenPut it in container, adding wherein temperature is the distilled water of 50 ~ 60 DEG C, immersion mixture completely, and service property (quality) mark isIt is 6.0 ~ 6.5 that 15% hydrochloric acid solution regulates pH, keeps temperature 2 ~ 5h, and then filtration under diminished pressure while hot, puts the filtered fluid of gainedEnter in centrifuge and carry out centrifugation, collect supernatant;
(3) supernatant of gained is mixed with the phegma of step (1) gained, obtain mixed liquor, put into the reactor of 50LIn, the 1-methyl cyclopropene that the mass fraction that then adds wherein mixeding liquid volume 5 ~ 8% is 0.1%, uses nitrogen protection,Being warming up to 80 ~ 100 DEG C, is under 4000 ~ 6000r/min at rotating speed, stirs 5 ~ 10min;
(4) after above-mentioned stirring finishes, be cooled to 40 ~ 50 DEG C, add wherein 300 ~ 500mL dog saliva, stir, then toWherein 30 ~ 50g calcium propionate, 40 ~ 60g Sodium Benzoate, keeps temperature to stir 30 ~ 50min, and then discharging, by the discharging thing of gainedFilter, the filtered fluid of gained is put into Rotary Evaporators and concentrate, be concentrated into 1/3 of original volume, obtain concentrate;
(5) 1:1 in mass ratio, gets marigold petal and mixes with Ageratum conyzoides petal, then by the mixing petal of gained and upperState the concentrate of gained, by solid-to-liquid ratio 1:2, put into container, then add wherein the absolute ethyl alcohol of concentrate volume 5%, soAfter by container as in microwave device, keeping temperature is 40 ~ 60 DEG C, after microwave concussion 1 ~ 3h, filters, and the filtered fluid of gained is put intoIn centrifuge, carry out centrifugation, collect supernatant, can obtain dispersing birds spray.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510791743.XA CN105594753A (en) | 2015-11-17 | 2015-11-17 | Method for preparing spraying agent used in orchards for dispelling birds |
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| CN201510791743.XA CN105594753A (en) | 2015-11-17 | 2015-11-17 | Method for preparing spraying agent used in orchards for dispelling birds |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103355295A (en) * | 2013-07-25 | 2013-10-23 | 西安高科理化技术有限责任公司 | Emulsion bird repellent and preparation method and use thereof |
| CN103548864A (en) * | 2012-08-27 | 2014-02-05 | 安徽爱戈德生物科技有限公司 | Bird repellent composition, solid preparations and preparation method thereof |
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- 2015-11-17 CN CN201510791743.XA patent/CN105594753A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103548864A (en) * | 2012-08-27 | 2014-02-05 | 安徽爱戈德生物科技有限公司 | Bird repellent composition, solid preparations and preparation method thereof |
| CN103355295A (en) * | 2013-07-25 | 2013-10-23 | 西安高科理化技术有限责任公司 | Emulsion bird repellent and preparation method and use thereof |
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Application publication date: 20160525 |
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