CN103355295A - Emulsion bird repellent and preparation method and use thereof - Google Patents
Emulsion bird repellent and preparation method and use thereof Download PDFInfo
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- CN103355295A CN103355295A CN2013103149742A CN201310314974A CN103355295A CN 103355295 A CN103355295 A CN 103355295A CN 2013103149742 A CN2013103149742 A CN 2013103149742A CN 201310314974 A CN201310314974 A CN 201310314974A CN 103355295 A CN103355295 A CN 103355295A
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Abstract
The invention provides an emulsion bird repellent and a preparation method and use thereof. The emulsion bird repellent is a composition including 20-40 parts by weight of a bird repellent spice, 10-40 parts by weight of an organic solvent, 10-40 parts by weight of carbomer resin, 40-80 parts by weight of pure water, 0.1-5 parts by weight of a stabilizer, 0.1-5 parts by weight of an antioxidant and 0.1-5 parts by weight of an emulsifier. The emulsion bird repellent combined with the preparation method and the use thereof overcomes the problems of difficult emulsification, short bird repellent time, and high cost.
Description
Technical field
The present invention relates to technological field of biochemistry, particularly a kind of emulsion-type bird repellent and its production and use.
Background technology
In recent years, because people's environmental consciousness strengthens, so that the birds life condition improves, it is many that the kind of bird becomes.And the good greening environment in airport and abundant physical resources be so that birds are gathered in this, and " bird is hit " upgraded to category-A aviation disaster by federation of international air service.Knock away aspect the preventing and treating of machine bird, generally adopt shotgun, clapnet, drive the bird viscose, Colour wind-wheel, coal gas big gun, drive physics or the means such as ammoniacal liquor poison mist, agricultural chemicals poisoning such as bird special-purpose vehicle.Shoot to death and agricultural chemicals poisoning with shotgun, though obvious effect on driving birds is arranged, cost is also low, but the environment of having violated " People's Republic of China's wild animal conservation law " and serious pollution.Clapnet to the flock of birds activity that surpasses the trammel net height without control efficiency.The sound such as pipe of horrible cry sound when driving bird special-purpose vehicle and voice scarecrow device and adopting the simulation birds frightened or the bird of prey drives bird, but birds have adapted to the rear effect on driving birds that just lost.The coal gas big gun is for the birds of the huge noisy environment in long-term custom airport, and its effect on driving birds is also very limited.
At present, occurred several bird products that drive on the market, concluded and mainly contain following a few class: (1) with the bird driving composition of chemical raw material preparation, as: tmtd, carbosulfan, anthraquinone, aluminum sulfate are pressed etc.This class mostly has very strong toxicity, so driving the bird active constituent content cannot join very high, so just caused effect on driving birds bad, and its formulation all is aqua, emulsifiable concentrate or pulvis, all not can be made into slowly-releasing or controlled release preparation, otherwise cause more residue of pesticide, it is ageing also poor to drive bird.(2) utilize the bitter taste of plant extracts and the bird driving composition of toxicity preparation, as: kuh-seng, Celastrus angulatus, the tuber of stemona, the root of langdu etc.This class mainly is to utilize bitter taste and toxicity to reach the purpose of driving bird, if long-term use also can work the mischief to birds.(3) utilize the bird driving composition of the fragrance preparation of plant extracts, such as artificial neroli oil, Moschus, cordate houttuynia essential oil etc.This class be relatively environmental protection drive the bird product, less to the injury effect of birds, the harm of environment is also little.But there is an emulsification difficulty in existing product, drives the problem that the bird timeliness is short, use cost is high.
And also do not have at present a kind of birds that can not injure, can long-actingly drive again bird, convenient that use and the nontoxic bird product that drives.
Summary of the invention
The invention provides a kind of emulsion-type bird repellent and its production and use, the emulsion-type bird repellent, comprise and drive bird spices, organic solvent, the carbomer resin, pure water, stabilizing agent, the formed composition of antioxidant and emulsifier, the wherein said parts by weight of bird spices in composition that drive are 20-40 part, the parts by weight of described organic solvent in composition are 10-40 part, the parts by weight of described carbomer resin in composition are 0.1-10 part, the parts by weight of described pure water in composition are 40-80 part, the parts by weight of described stabilizing agent in composition are 0.1-5 part, the parts by weight of described antioxidant in composition are 0.1-5 part, and the parts by weight of described emulsifier in composition are 0.1-5 part.And just overcome the emulsification difficulty, driven the problem that the bird timeliness is short, use cost is high in conjunction with Preparation Method And The Use.
For achieving the above object, technical scheme of the present invention is:
A kind of emulsion-type bird repellent, comprise and drive bird spices, organic solvent, the carbomer resin, pure water, stabilizing agent, the formed composition of antioxidant and emulsifier, the wherein said parts by weight of bird spices in composition that drive are 20-40 part, the parts by weight of described organic solvent in composition are 10-40 part, the parts by weight of described carbomer resin in composition are 0.1-10 part, the parts by weight of described pure water in composition are 40-80 part, the parts by weight of described stabilizing agent in composition are 0.1-5 part, the parts by weight of described antioxidant in composition are 0.1-5 part, and the parts by weight of described emulsifier in composition are 0.1-5 part.
The described bird spices that drives is made of any one or any two kinds in methyl anthranilate, mesitylenic acid or the cinnamic acid.
Described organic solvent is the terpene hydrocarbon.
Described terpene hydrocarbon is alkene, dipentene, australene, nopinene or (R)-4-isopropenyl-1-methyl-1-cyclohexene.
Described carbomer resin is made of any one or any two kinds in the carbomer resin series.
Described stabilizing agent is made of in citric acid or the Sodium Benzoate one or both.
Described antioxidant is made of in butylhydroxy anisole or the dibutyl hydroxy toluene one or both.
Described emulsifier is made of any one or any two kinds in the emulsifier of TX series.
Described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
The preparation method of described emulsion-type bird repellent, step is as follows:
Step 1: the standard that according to the parts by weight of described carbomer resin in composition is 0.1-10 part is that the pure water of the standard of 40-80 part is poured into and mixed the mixture that forms carbomer resin and pure water in the container with the carbomer resin with according to the parts by weight of described pure water in composition;
Step 2: be the mark of 20-40 part according to the described parts by weight of bird spices in composition that drive
The brigadier drives to mix in the mixture that bird spices adds described carbomer resin and pure water and forms the mixture that drives bird spices, carbomer resin and pure water;
Step 3: be the standard of 10-40 part according to the parts by weight of described organic solvent in composition
Organic solvent added in the described mixture that drives bird spices, carbomer resin and pure water mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: be that 0.1-5 part is with emulsifier according to the parts by weight of described emulsifier in composition
Add described organic solvent, drive and mix the mixture that forms emulsifier, organic solvent, drives bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water;
Step 5: be 0.1-5 part and described according to the parts by weight of described stabilizing agent in composition
The parts by weight of antioxidant in composition are that the standard of 0.1-5 part adds described emulsifier, organic solvent with stabilizing agent and antioxidant respectively, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill.
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
The preparation method's of described emulsion-type bird repellent operating temperature is normal temperature.
Difference with the prior art of the present invention is that the bird repellent emulsion evenly is difficult for layering, has good effect on driving birds, environment is not polluted, to not injury of birds, to the person poultry safety.
Embodiment
The present invention will be further described below by specific embodiment:
Embodiment 1
Described emulsion-type bird repellent comprises the emulsifier of TX-7 of butylhydroxy anisole, the 1g of citric acid, the 1g of D-citrene, the 1g of pure water, the 150g of carbomer resin 941, the 577g of methyl anthranilate, the 2g of 250g.
Described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
The preparation method of described emulsion-type bird repellent, step is as follows:
Step 1: pour the carbomer resin 941 of 2g and the pure water of 577g into mix formation carbomer resin and pure water in the container by high speed disperser mixture;
Step 2: the methyl anthranilate of 250g is added mix in the mixture of described carbomer resin and pure water and form the mixture that drives bird spices, carbomer resin and pure water;
Step 3: the D-citrene of 150g is added described bird spices, carbomer resin and the pure water of driving
Mixture in mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: the TX-7 emulsifier of 1g is added described organic solvent, drives bird spices, carbomer
Stir in the mixture of resin and pure water and close the mixture that 30min mixes formation emulsifier, organic solvent, drives bird spices, carbomer resin and pure water;
Step 5: the butylhydroxy anisole with the citric acid of 1g and 1g adds described emulsifier, organic solvent, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water respectively, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill.
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
The preparation method's of described emulsion-type bird repellent operating temperature is normal temperature.
Embodiment 2
Described emulsion-type bird repellent comprises the emulsifier of TX-7 of butylhydroxy anisole, the 1g of citric acid, the 1g of D-citrene, the 1g of pure water, the 150g of carbomer resin 941, the 577g of cinnamic acid, the 5g of methyl anthranilate, the 20g of 230g.
Described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
The preparation method of described emulsion-type bird repellent, step is as follows:
Step 1: pour the carbomer resin 941 of 2g and the pure water of 577g into mix formation carbomer resin and pure water in the container by high speed disperser mixture;
Step 2: the cinnamic acid of the methyl anthranilate of 230g and 20g is added mix in the mixture of described carbomer resin and pure water and form the mixture that drives bird spices, carbomer resin and pure water;
Step 3: the D-citrene of 150g is added described bird spices, carbomer resin and the pure water of driving
Mixture in mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: the TX-7 emulsifier of 1g is added described organic solvent, drives bird spices, carbomer
Stir in the mixture of resin and pure water and close the mixture that 30min mixes formation emulsifier, organic solvent, drives bird spices, carbomer resin and pure water;
Step 5: the butylhydroxy anisole with the citric acid of 1g and 1g adds described emulsifier, organic solvent, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water respectively, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill.
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
The preparation method's of described emulsion-type bird repellent operating temperature is normal temperature.
Embodiment 3
Described emulsion-type bird repellent comprises the emulsifier of TX-9 of butylhydroxy anisole, the 1g of citric acid, the 1g of D-citrene, the 1g of pure water, the 100g of carbomer resin 934, the 587g of mesitylenic acid, the 10g of 300g.
Described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
The preparation method of described emulsion-type bird repellent, step is as follows:
Step 1: pour the carbomer resin 934 of 10g and the pure water of 587g into mix formation carbomer resin and pure water in the container by high speed disperser mixture;
Step 2: the mesitylenic acid of 300g is added mix in the mixture of described carbomer resin and pure water and form the mixture that drives bird spices, carbomer resin and pure water;
Step 3: the D-citrene of 100g is added described bird spices, carbomer resin and the pure water of driving
Mixture in mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: the TX-9 emulsifier of 1g is added described organic solvent, drives bird spices, carbomer
Stir in the mixture of resin and pure water and close the mixture that 30min mixes formation emulsifier, organic solvent, drives bird spices, carbomer resin and pure water;
Step 5: the butylhydroxy anisole with the citric acid of 1g and 1g adds described emulsifier, organic solvent, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water respectively, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill.
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
The preparation method's of described emulsion-type bird repellent operating temperature is normal temperature.
Embodiment 4
Described emulsion-type bird repellent comprises the emulsifier of TX-9 of butylhydroxy anisole, the 1g of citric acid, the 1g of D-citrene, the 1g of pure water, the 100g of carbomer resin 934, the 587g of cinnamic acid, the 10g of mesitylenic acid, the 20g of 280g.
Described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
The preparation method of described emulsion-type bird repellent, step is as follows:
Step 1: pour the carbomer resin 934 of 10g and the pure water of 587g into mix formation carbomer resin and pure water in the container by high speed disperser mixture;
Step 2: the cinnamic acid of the mesitylenic acid of 280g and 20g is added mix in the mixture of described carbomer resin and pure water and form the mixture that drives bird spices, carbomer resin and pure water;
Step 3: the D-citrene of 100g is added described bird spices, carbomer resin and the pure water of driving
Mixture in mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: the TX-9 emulsifier of 1g is added described organic solvent, drives bird spices, carbomer
Stir in the mixture of resin and pure water and close the mixture that 30min mixes formation emulsifier, organic solvent, drives bird spices, carbomer resin and pure water;
Step 5: the butylhydroxy anisole with the citric acid of 1g and 1g adds described emulsifier, organic solvent, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water respectively, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill.
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
The preparation method's of described emulsion-type bird repellent operating temperature is normal temperature.
Then embodiment 1-embodiment 4 prepared emulsion-type bird repellents are carried out the effect observation of airport bird scaring, observation ground is western certain airport, the emulsion-type bird repellent time that sprays embodiment 1-embodiment 4 is respectively in March, 2013, in May, 2013, in July, 2013, spraying the place is lawns, runway both sides, spraying time is 12 noon, every day tracking observation, the duration was two weeks, the emulsion-type bird repellent experimental result of embodiment 1-embodiment 4 is as shown in table 1:
Can find out that from above-mentioned experimental result behind the emulsion-type bird repellent of use embodiment 1-embodiment 4, birds obviously reduce, repellent effect is good, is to be fit to the ideal product that use on the airport.
Also embodiment 1-embodiment 4 prepared emulsion-type bird repellents have been carried out experiment to the repellent effect of pigeon in addition, experimental subjects is 8 pigeons, test method be with 2 one group of circles of pigeon in wire mesh cage, making them adapt to corn in several days raises, then processing corn feed with embodiment 1-embodiment 4 prepared emulsion-type bird repellents is placed in the pigeon cage, wherein one group, the two groups feeds of feeding are undressed, three groups, four groups is to process with embodiment 1-embodiment 4 prepared emulsion-type bird repellents, and it is as shown in table 2 to observe the pigeon reaction:
The above; only be the embodiment that the present invention is directed to the inventive method; above-described embodiment is not that the present invention is done any restriction; everyly change according to the given scope of technical solution of the present invention and any simple modification that above embodiment is done, change and equivalent structure, all still belong to the protection domain of technical solution of the present invention.
Claims (9)
1. emulsion-type bird repellent, it is characterized in that comprising and drive bird spices, organic solvent, the carbomer resin, pure water, stabilizing agent, the formed composition of antioxidant and emulsifier, the wherein said parts by weight of bird spices in composition that drive are 20-40 part, the parts by weight of described organic solvent in composition are 10-40 part, the parts by weight of described carbomer resin in composition are 0.1-10 part, the parts by weight of described pure water in composition are 40-80 part, the parts by weight of described stabilizing agent in composition are 0.1-5 part, the parts by weight of described antioxidant in composition are 0.1-5 part, and the parts by weight of described emulsifier in composition are 0.1-5 part.
2. emulsion-type bird repellent according to claim 1 is characterized in that the described bird spices that drives is made of any one or any two kinds in methyl anthranilate, mesitylenic acid or the cinnamic acid.
3. according to claim 1 or emulsion-type bird repellent claimed in claim 2, it is characterized in that described organic solvent is the terpene hydrocarbon.
4. emulsion-type bird repellent according to claim 3 is characterized in that described terpene hydrocarbon is alkene, dipentene, australene, nopinene or (R)-4-isopropenyl-1-methyl-1-cyclohexene.
5. according to claim 1 or emulsion-type bird repellent claimed in claim 2, it is characterized in that described carbomer resin is made of any one or any two kinds in the carbomer resin series.
6. according to claim 1 or emulsion-type bird repellent claimed in claim 2, it is characterized in that described stabilizing agent is made of in citric acid or the Sodium Benzoate one or both; Described antioxidant is made of in butylhydroxy anisole or the dibutyl hydroxy toluene one or both; Described emulsifier is made of any one or any two kinds in the emulsifier of TX series.
7. emulsion-type bird repellent according to claim 1 is characterized in that described emulsion-type bird repellent is to realize by spraying after with the dilution of emulsion-type bird repellent driving purposes aspect the bird.
8. the preparation method of emulsion-type bird repellent according to claim 1 is characterized in that, step is as follows:
Step 1: the standard that according to the parts by weight of described carbomer resin in composition is 0.1-10 part is that the pure water of the standard of 40-80 part is poured into and mixed the mixture that forms carbomer resin and pure water in the container with the carbomer resin with according to the parts by weight of described pure water in composition;
Step 2: be the mark of 20-40 part according to the described parts by weight of bird spices in composition that drive
The brigadier drives to mix in the mixture that bird spices adds described carbomer resin and pure water and forms the mixture that drives bird spices, carbomer resin and pure water;
Step 3: be the standard of 10-40 part according to the parts by weight of described organic solvent in composition
Organic solvent added in the described mixture that drives bird spices, carbomer resin and pure water mix the mixture that forms organic solvent, drives bird spices, carbomer resin and pure water;
Step 4: be that 0.1-5 part is with emulsifier according to the parts by weight of described emulsifier in composition
Add described organic solvent, drive and mix the mixture that forms emulsifier, organic solvent, drives bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water;
Step 5: be 0.1-5 part and described according to the parts by weight of described stabilizing agent in composition
The parts by weight of antioxidant in composition are that the standard of 0.1-5 part adds described emulsifier, organic solvent with stabilizing agent and antioxidant respectively, drives the mixture that stirs and form stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in the mixture of bird spices, carbomer resin and pure water, the stable finished product that obtains described emulsion-type bird repellent behind the 24h that leaves standstill;
The mode of stirring in the described step 5 be the pH value scope of mixture that stirs 60min above until described stabilizing agent, antioxidant, emulsifier, organic solvent, drive bird spices, carbomer resin and pure water in 6.5-7.5 and specific gravity range between 1.000～1.006.
9. the preparation method of emulsion-type bird repellent according to claim 8, the operating temperature that it is characterized in that the preparation method of described emulsion-type bird repellent is normal temperature.
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| CN105594753A (en) * | 2015-11-17 | 2016-05-25 | 梅庆波 | Method for preparing spraying agent used in orchards for dispelling birds |
| CN107947014A (en) * | 2017-11-30 | 2018-04-20 | 国网山东省电力公司滨州市滨城区供电公司 | New occupying device |
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| US20060189690A1 (en) * | 2003-11-14 | 2006-08-24 | Dunham Charles F | Compounds to affect insect behavior and/or bird behavior |
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| CN107947014A (en) * | 2017-11-30 | 2018-04-20 | 国网山东省电力公司滨州市滨城区供电公司 | New occupying device |
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| CN103355295B (en) | 2014-10-15 |
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