CN104737860B - A kind of method of preventing and treating honey peach dichocrocis punctiferalis - Google Patents
A kind of method of preventing and treating honey peach dichocrocis punctiferalis Download PDFInfo
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- CN104737860B CN104737860B CN201510104781.3A CN201510104781A CN104737860B CN 104737860 B CN104737860 B CN 104737860B CN 201510104781 A CN201510104781 A CN 201510104781A CN 104737860 B CN104737860 B CN 104737860B
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Abstract
The application is related to a kind of method of preventing and treating honey peach dichocrocis punctiferalis, adopts the microemulsion being prepared from as active component using plant source extracting solution to be prevented and treated, and wherein, the microemulsion is prepared by mass percentage by following raw material：Plant source extracting solution：10 20%, methyl oleate：15 25%, styrylphenol polyoxyethylene ether：15 20%, polyoxyethylene lauryl ether 3 8%, balance of water, the mass percent summation of raw material is 100%；The application has considered the monarch relation between vegetable material, can significantly improve the prevention effect to honey peach dichocrocis punctiferalis.
Description
Technical field
The present invention relates to the pest control of honey peach, and in particular to a kind of method of preventing and treating honey peach dichocrocis punctiferalis.
Background technology
Compare with traditional chemical pesticide, botanical pesticide has raw material to be easy to get, action site is more, harmful organism be not likely to produce anti-
The property of medicine, degradable, low-residual, to natural enemy insect harm less and environmentally safe the advantages of.Height is filtered out from natural product
Active substance, is templated synthesis new chemical pesticide with which, or directly developed into efficient, low toxicity, low-residual and environment and
Humorous natural source pesticidal preparations, it has also become one of New pesticides discovery important and one of effective approach, is sending out for pesticide in future
Exhibition direction.China soil is vast, and plant resourceses enrich, and the condition for developing plant insecticide is richly endowed by nature, and prospect is very wide.
According to statistics, the whole world there are about more than 50 ten thousand kinds of plant, and higher plant is nearly more than 30 ten thousand kinds, existing 470 section of higher plant of China, and more than 3700
Category, occupies third place in the world by about 30,000 kinds.《Chinese poisonous plantss》List China poisonous plantss kind more than 1300 in, wherein great majority have
Insecticidal activity, numerous species are utilized as botanical pesticide.
But the medicine based on herbs in for currently available technology, is mostly random group of the effect according to each composition
Close, not the relation of the monarch between consideration various composition, not only the effect after causing to combine does not increase, and on the contrary can
Affect the effect after combination.
Medicine based on herbs is not adopted in prior art dedicated for the report of preventing and treating honey peach dichocrocis punctiferalis yet.
Content of the invention
The present invention is closed for some problems in currently available technology, the monarch considered between vegetable material
System, there is provided the prevention and controls of the honey peach dichocrocis punctiferalis of drug effect can be significantly improved after a kind of combination.
For solving above-mentioned technical problem, one aspect of the present invention is：A kind of preventing and treating juicy peach moth is provided
The method of snout moth's larva, adopts the microemulsion being prepared from as active component using plant source extracting solution to be prevented and treated, wherein, the microemulsion
Agent is prepared by mass percentage by following raw material：Plant source extracting solution：10-20%, methyl oleate：15-25%, styryl benzene
Phenol polyethenoxy ether：15-20%, polyoxyethylene lauryl ether 3-8%, balance of water, the mass percent summation of raw material is
100%；Described plant source extracting solution is prepared by following methods：Semen Abutili 8-10kg, Fructus Aristolochiae 7-9kg, Herba Senecionis Scandentiss 1- are taken respectively
3kg, Cynanchum Komarovii 0.5-1.5kg, Rhizoma Cibotii 0.1-0.3kg, the coarse powder for being crushed to 1mm～3mm with plant tissue pulverizer mince
After mix, the coarse powder of gained is minced with conventional solvent method extraction, Extracting temperature is 60～70 DEG C, and extraction time is 15～20
Hour obtains extract, and extract obtains plant source extracting solution through being concentrated in vacuo to equivalent to 0.8kg dry powder/kg concentrated solutions.
Described microemulsion prepares preferred plant source extracting solution 15%, methyl oleate by mass percentage by following raw material
20%, styrylphenol polyoxyethylene ether 18%, polyoxyethylene lauryl ether 5%, balance of water, the mass percent of raw material
Summation is 100%.
The solvent is ethyl acetate, chloroform, any one or a few in petroleum ether.
In the plant extraction liquid, the composition of plant is preferably：Semen Abutili 9g, Fructus Aristolochiae 8kg, Herba Senecionis Scandentiss 2kg, Cynanchum Komarovii
1kg, Rhizoma Cibotii 0.2kg.
The plant compatibility of the application is the interaction of the state of an illness according to honey peach dichocrocis punctiferalis and plant, selects Semen Abutili, horse
The method that Semen Oroxyli, Herba Senecionis Scandentiss, Cynanchum Komarovii, Rhizoma Cibotii are used cooperatively, wherein Semen Abutili, Fructus Aristolochiae are monarch, and Herba Senecionis Scandentiss are minister, and Rhizoma Cibotii is
Assistant, Cynanchum Komarovii is for making, it is therefore intended that adapt to the state of an illness of complicated honey peach dichocrocis punctiferalis, and prophylactic agent is poisoned, the formula be
On the basis of differential diagnosis in tcm opinion is controlled, according to the performance of Four Plants parasite killing and mutual relation compatibility, therefore, the application is whole
Body compatibility, noted righting turn round and look at stomach, distinguished based on Semen Abutili, Fructus Aristolochiae, Herba Senecionis Scandentiss, Rhizoma Cibotii, Cynanchum Komarovii be secondary, though between main points
Emphasize particularly on different fields, but connect each other, be a unified entirety, only organically combine four during concrete application,
The promising result of medicine Synergistic insecticidal can be reached.
Specific embodiment
Below presently preferred embodiments of the present invention is described in detail so that advantages and features of the invention can be easier to by
It will be appreciated by those skilled in the art that apparent clearly defining so as to make to protection scope of the present invention.
The embodiment of the present invention includes：
Embodiment 1
The method of preventing and treating honey peach dichocrocis punctiferalis, adopts the microemulsion being prepared from using plant source extracting solution as active component
Prevented and treated, wherein, the microemulsion is prepared by mass percentage by following raw material：Plant source extracting solution：10%, Oleic acid first
Ester：15%, styrylphenol polyoxyethylene ether：15%, polyoxyethylene lauryl ether 3%, balance of water, the quality hundred of raw material
It is 100% to divide than summation；Described plant source extracting solution is prepared by following methods：Semen Abutili 8kg, Fructus Aristolochiae 7kg, a thousand li are taken respectively
Light 1kg, Cynanchum Komarovii 0.5kg, Rhizoma Cibotii 0.1kg, the coarse powder for being crushed to 3mm with plant tissue pulverizer mix after mincing, by institute
The coarse powder for obtaining minces and is extracted with chloroform, and Extracting temperature is 60 DEG C, and extraction time is to obtain extract in 15 hours, and extract is dense through vacuum
It is reduced to equivalent to 0.8kg dry powder/kg concentrated solutions, that is, obtains plant source extracting solution.
Embodiment 2
The method of preventing and treating honey peach dichocrocis punctiferalis, adopts the microemulsion being prepared from using plant source extracting solution as active component
Prevented and treated, wherein, the microemulsion is prepared by mass percentage by following raw material：Plant source extracting solution 20%, methyl oleate
25%, styrylphenol polyoxyethylene ether 20%, polyoxyethylene lauryl ether 3-8%, balance of water, the quality percentage of raw material
It is 100% than summation；Described plant source extracting solution is prepared by following methods：Semen Abutili 10kg, Fructus Aristolochiae 9kg, a thousand li are taken respectively
Light 3kg, Cynanchum Komarovii 1.5kg, Rhizoma Cibotii 0.3kg, the coarse powder for being crushed to 2mm with plant tissue pulverizer mix after mincing, by institute
The coarse powder for obtaining minces and is extracted with petroleum ether, and Extracting temperature is 65 DEG C, and extraction time is to obtain extract in 18 hours, and extract is through vacuum
It is concentrated into equivalent to 0.8kg dry powder/kg concentrated solutions, that is, obtains plant source extracting solution.
Embodiment 3
The method of preventing and treating honey peach dichocrocis punctiferalis, adopts the microemulsion being prepared from using plant source extracting solution as active component
Prevented and treated, wherein, the microemulsion is prepared by mass percentage by following raw material：Plant source extracting solution 15%, methyl oleate
20%, styrylphenol polyoxyethylene ether 18%, polyoxyethylene lauryl ether 5%, balance of water, the mass percent of raw material
Summation is 100%；Described plant source extracting solution is prepared by following methods：Semen Abutili 9g, Fructus Aristolochiae 8kg, Herba Senecionis Scandentiss are taken respectively
2kg, Cynanchum Komarovii 1kg, Rhizoma Cibotii 0.2kg, the coarse powder for being crushed to 1mm with plant tissue pulverizer mix after mincing, by gained
Coarse powder minces and is extracted with ethyl acetate, and Extracting temperature is 70 DEG C, and extraction time is to obtain extract in 20 hours, and extract is dense through vacuum
It is reduced to equivalent to 0.8kg dry powder/kg concentrated solutions, that is, obtains plant source extracting solution.
By the plant source extracting solution of embodiment 1-3 gained, according to formula ratio with solvent and surfactant in mixture kettle,
Mixture kettle temperature degree is 45 DEG C -55 DEG C, and mixing time is 40 minutes, obtains final product microemulsion after stirring.
1000 times of liquid measures of the microemulsion prepared by embodiment 1-3 carry out blade face conventional spray, chlorpyrifos micro emulsion 1000
Times liquid carries out blade face conventional spray for comparison medicament, and sets clear water control, as a result shows, the application microemulsion is with chlopyrifos microemulsion
Agent has preferable prevention effect relative to control to honey peach dichocrocis punctiferalis, and the application microemulsion is with chlorpyrifos micro emulsion phase
Than insecticidal effect improves 20%.
Embodiments of the invention are the foregoing is only, the scope of the claims of the present invention is not thereby limited, every using this
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, is included within the scope of the present invention.
Claims (4)
1. a kind of preventing and treating honey peach dichocrocis punctiferalis method, it is characterised in that adopt using plant source extracting solution as active component system
Standby microemulsion is prevented and treated, and wherein, the microemulsion is prepared by mass percentage by following raw material：Plant source is extracted
Liquid：10-20%, methyl oleate：15-25%, styrylphenol polyoxyethylene ether：15-20%, polyoxyethylene lauryl ether 3-
8%, balance of water, the mass percent summation of raw material is 100%；Described plant source extracting solution is prepared by following methods：Point
Semen Abutili 8-10kg, Fructus Aristolochiae 7-9kg, Herba Senecionis Scandentiss 1-3kg, Cynanchum Komarovii 0.5-1.5kg, Rhizoma Cibotii 0.1-0.3kg is not taken, plant is used
Tissue pulverizer is crushed to after the coarse powder of 1mm～3mm minces and mixes, the conventional solvent of the mixture that the coarse powder of gained is minced
Method is extracted, and Extracting temperature is 60～70 DEG C, and extraction time is to obtain within 15～20 hours extract, and extract is through being concentrated in vacuo to quite
In 0.8kg dry powder/kg concentrated solutions, that is, obtain plant source extracting solution.
2. according to claim 1 preventing and treating honey peach dichocrocis punctiferalis method, it is characterised in that described microemulsion is by following
Raw material is prepared by mass percentage：Plant source extracting solution 15%, methyl oleate 20%, styrylphenol polyoxyethylene ether
18%, polyoxyethylene lauryl ether 5%, balance of water, the mass percent summation of raw material is 100%.
3. according to claim 1 preventing and treating honey peach dichocrocis punctiferalis method, it is characterised in that used in the solvent method
Solvent is ethyl acetate, chloroform, any one or a few in petroleum ether.
4. according to claim 1 preventing and treating honey peach dichocrocis punctiferalis method, it is characterised in that in the plant source extracting solution
Plant consists of：Semen Abutili 9g, Fructus Aristolochiae 8kg, Herba Senecionis Scandentiss 2kg, Cynanchum Komarovii 1kg, Rhizoma Cibotii 0.2kg.
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| CN201510104781.3A CN104737860B (en) | 2015-03-11 | 2015-03-11 | A kind of method of preventing and treating honey peach dichocrocis punctiferalis |
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| CN201510104781.3A CN104737860B (en) | 2015-03-11 | 2015-03-11 | A kind of method of preventing and treating honey peach dichocrocis punctiferalis |
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| CN104737860A CN104737860A (en) | 2015-07-01 |
| CN104737860B true CN104737860B (en) | 2017-03-15 |
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| CN105410052A (en) * | 2015-11-26 | 2016-03-23 | 全椒县桃花湾果蔬种植专业合作社 | Dichocrocis punctiferalis attractive toxicant |
| CN105410072A (en) * | 2015-11-26 | 2016-03-23 | 全椒县桃花湾果蔬种植专业合作社 | Method for preventing and treating yellow peach dichocrocis punctiferalis |
| CN105613619B (en) * | 2016-03-25 | 2018-09-07 | 镇远县醉美果业有限公司 | A kind of reagent and application method of prevention heart dichocrocis punctiferalis |
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| CN1077339A (en) * | 1993-05-27 | 1993-10-20 | 广东省江门市农药厂 | To the composition of insecticide tool synergistic effect and the application on insecticide thereof |
| CN1301060C (en) * | 2003-07-29 | 2007-02-21 | 王丽华 | Plant Source non-public hazard biological insect repellant and preparing process |
| KR20110064606A (en) * | 2009-12-08 | 2011-06-15 | 주식회사 엘지생활건강 | Mosquito control composition containing farnesene or ingredients of flower scent of cestrum nocturnum |
| CN102487953A (en) * | 2011-12-12 | 2012-06-13 | 张金林 | Buffalobur extract insecticide and preparation method thereof |
| CN103141523A (en) * | 2013-02-06 | 2013-06-12 | 杨凌农科大无公害农药研究服务中心 | Acanthopanax gracilistylus insecticide and its preparation method |
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