CN105582858B - 一种树脂催化剂在工业列管反应器上的装填方法 - Google Patents
一种树脂催化剂在工业列管反应器上的装填方法 Download PDFInfo
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- CN105582858B CN105582858B CN201410563465.8A CN201410563465A CN105582858B CN 105582858 B CN105582858 B CN 105582858B CN 201410563465 A CN201410563465 A CN 201410563465A CN 105582858 B CN105582858 B CN 105582858B
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- Prior art keywords
- catalyst
- solvent
- tubulation
- pipe
- shell
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- 239000003054 catalyst Substances 0.000 title claims abstract description 90
- 238000000034 method Methods 0.000 title claims abstract description 46
- 238000012856 packing Methods 0.000 title claims abstract description 19
- 239000011347 resin Substances 0.000 title claims abstract description 11
- 229920005989 resin Polymers 0.000 title claims abstract description 11
- 239000002904 solvent Substances 0.000 claims abstract description 40
- 238000011049 filling Methods 0.000 claims abstract description 20
- 239000000945 filler Substances 0.000 claims abstract description 12
- 238000007654 immersion Methods 0.000 claims abstract description 3
- 230000008961 swelling Effects 0.000 claims abstract description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 4
- -1 methyl-isobutyl Chemical group 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- SHOJXDKTYKFBRD-UHFFFAOYSA-N 4-Methyl-3-penten-2-one, 9CI Chemical compound CC(C)=CC(C)=O SHOJXDKTYKFBRD-UHFFFAOYSA-N 0.000 claims description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N iso-butyl alcohol Natural products CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 2
- 229940035429 isobutyl alcohol Drugs 0.000 claims description 2
- 150000002576 ketones Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 230000001427 coherent effect Effects 0.000 abstract description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 13
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 13
- 229940043265 methyl isobutyl ketone Drugs 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000013459 approach Methods 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000003475 lamination Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- ZZMVLMVFYMGSMY-UHFFFAOYSA-N 4-n-(4-methylpentan-2-yl)-1-n-phenylbenzene-1,4-diamine Chemical compound C1=CC(NC(C)CC(C)C)=CC=C1NC1=CC=CC=C1 ZZMVLMVFYMGSMY-UHFFFAOYSA-N 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000004916 vomit Anatomy 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
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CN201410563465.8A CN105582858B (zh) | 2014-10-22 | 2014-10-22 | 一种树脂催化剂在工业列管反应器上的装填方法 |
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CN201410563465.8A CN105582858B (zh) | 2014-10-22 | 2014-10-22 | 一种树脂催化剂在工业列管反应器上的装填方法 |
Publications (2)
Publication Number | Publication Date |
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CN105582858A CN105582858A (zh) | 2016-05-18 |
CN105582858B true CN105582858B (zh) | 2018-03-16 |
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CN201410563465.8A Active CN105582858B (zh) | 2014-10-22 | 2014-10-22 | 一种树脂催化剂在工业列管反应器上的装填方法 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4257171A (en) * | 1979-07-16 | 1981-03-24 | Stone & Webster Engineering Corp. | Fluidized bed gas distributor system |
US5607893A (en) * | 1993-12-02 | 1997-03-04 | Haldor Tops.o slashed.e A/S | Method for uniform loading of catalyst tubes |
CN101137431A (zh) * | 2005-03-08 | 2008-03-05 | 巴斯福股份公司 | 填充反应器的方法 |
CN101829526A (zh) * | 2010-05-10 | 2010-09-15 | 南京蓝星化工新材料有限公司 | 催化剂更换系统、催化剂更换方法及具有该系统的精馏塔 |
CN102989375A (zh) * | 2011-09-08 | 2013-03-27 | 中国石油化工股份有限公司 | 一种列管反应器催化剂装填方法 |
-
2014
- 2014-10-22 CN CN201410563465.8A patent/CN105582858B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4257171A (en) * | 1979-07-16 | 1981-03-24 | Stone & Webster Engineering Corp. | Fluidized bed gas distributor system |
US5607893A (en) * | 1993-12-02 | 1997-03-04 | Haldor Tops.o slashed.e A/S | Method for uniform loading of catalyst tubes |
CN101137431A (zh) * | 2005-03-08 | 2008-03-05 | 巴斯福股份公司 | 填充反应器的方法 |
CN101829526A (zh) * | 2010-05-10 | 2010-09-15 | 南京蓝星化工新材料有限公司 | 催化剂更换系统、催化剂更换方法及具有该系统的精馏塔 |
CN102989375A (zh) * | 2011-09-08 | 2013-03-27 | 中国石油化工股份有限公司 | 一种列管反应器催化剂装填方法 |
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CN105582858A (zh) | 2016-05-18 |
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Effective date of registration: 20240322 Address after: No. 96-1 Nankai Street, Lvshunkou District, Dalian City, Liaoning Province, 116045 Patentee after: Sinopec (Dalian) Petrochemical Research Institute Co.,Ltd. Country or region after: China Patentee after: CHINA PETROLEUM & CHEMICAL Corp. Address before: No. 213, No.1 Chuangxin Road, Tieshan Street, Lvshunkou District, Dalian City, Liaoning Province, 116045 Patentee before: DALIAN RESEARCH INSTITUTE OF PETROLEUM AND PETROCHEMICALS, SINOPEC Corp. Country or region before: China Patentee before: CHINA PETROLEUM & CHEMICAL Corp. |