CN105560360B - A kind of deodorant - Google Patents
A kind of deodorant Download PDFInfo
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- CN105560360B CN105560360B CN201511034525.8A CN201511034525A CN105560360B CN 105560360 B CN105560360 B CN 105560360B CN 201511034525 A CN201511034525 A CN 201511034525A CN 105560360 B CN105560360 B CN 105560360B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/715—Polysaccharides, i.e. having more than five saccharide radicals attached to each other by glycosidic linkages; Derivatives thereof, e.g. ethers, esters
- A61K31/716—Glucans
- A61K31/722—Chitin, chitosan
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- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
- A61K47/10—Alcohols; Phenols; Salts thereof, e.g. glycerol; Polyethylene glycols [PEG]; Poloxamers; PEG/POE alkyl ethers
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
- A61K9/7015—Drug-containing film-forming compositions, e.g. spray-on
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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Abstract
The invention provides a kind of deodorant, the deodorant includes following raw material：Chitosan and lavender.Deodorant of the present invention has good deodorizing effect, and adverse reaction non-stimulated to human body, will not cause dry skin, blackening, can repair skin.
Description
Technical field
The present invention relates to a kind of deodorant.
Background technology
The generation of body odor (body odour)：Contain excessive thick lipid, the opposite sex in the sweat of human body axillary apocrine secretion
Albumen etc. and bacterium collective effect, unrighted acid is produced, release a kind of unpleasant stink.Body odor people's ratio：Chinese account for
20%, westerner (American-European, Africa) accounts for 80%.
Human body deodorant type has on the market：Antiperspirant (or antiperspirant/deodorant body spray) and deodorant body spray, also have containing Chinese herbal medicine
The medicine preparation for curing bromhidrosis of extract.
For antiperspirant, it is acted on：The amount of sweat for flowing to skin surface is reduced, and suppresses the bacterial reproduction for causing body odour.Its
Main component：Aluminium salt (aluminium chloride, alum (alum), aluminium hydroxide), zirconates.Its submember：Tannic acid, preservative, breast
Agent, soothing oil, essence etc..Its hidroschesis mechanism：Antiperspirant applies spray position in oxter, and formation is solidifying after aluminium salt runs into sweat dissolving
Glue, an interim spile is formed in sweat gland near top, greatly reduces the amount of sweat for being secreted into skin surface, Reusability can subtract
It is few to perspire, reach refreshing body effect.Its objective shortcoming：(1) because bathing etc. acts, the aluminium salt composition of absorbing sweat divides from skin surface
From sweating can recover normal.(2) antiperspirant can only act on skin surface, and depth is no more than subcutaneous cuticula, due to cuticula
Metabolism, hidroschesis function limitation system.(3) it cannot be used at skin injury, infection can be caused.(4) excessive use, sweat mistake is subtracted
Degree can influence human body metabolic balance, not notice that sweat stain, red swelling of the skin, itch occurs in cleaning, and serious causes epifolliculitis, for a long time
Use, dry skin, blackening, be damaged.(5) aluminium salt is harmful, State Planning Commission's bulletin：Flour product must not add alum (sulphur
Sour aluminium potassium).
Antiperspirant/refreshing body perfume (or spice) body has more than 100 years history in America and Europe.Scientists both domestic and external are made great efforts to seek gentle
Absorbing sweat composition adds moisturizing composition, improves meat flavor formulating technology etc., improves state of the art, such as Mentholatum, in antiperspirant
Plant essence aloe, peppermint etc. and moisturizing composition are added, increases the product of different flavor, to adapt to needed for market.But antiperspirant
Main component or aluminium salt.
For deodorant body spray (generally ball-type), it is acted on：Suppress bacterium, deodorization, perfuming taste masking.Its main component：Contain
Sterilization or antiseptic, such as alcohol.Its submember：Soothing oil, essence, silica etc., not aluminium containing salt.Its objective shortcoming：Nothing
Antiperspirancy performance, perfuming are intended merely to cover stink, can only respite 8 hours or so, sweat and essence are mutually reciprocal as mismatched
It should can produce more unpleasant stink.
For Chinese medicine medicine preparation for curing bromhidrosis (external application), its advantage：Pure Chinese medicine composition, safe and non-toxic, processing is simple, composition is low, and pair is made
With less.Its shortcoming：In-convenience in use being not suitable with the requirement of the modernization of Chinese medicine, there is patent without market.Its existing patent application is such as
A kind of Chinese medicine (number of patent application 201410288134.8) for treating body odour, a kind of effective ingredient in Chinese for being used to treat body odour
Composition and preparation method thereof (number of patent application 201310336341.1), a kind of Chinese medicine preparation (patent Shen for treating body odour
Please be number for 201410296781.3), three of the above preparation is all using Chinese Traditional Medicine as theory, with the coordination of a variety of primitive components
Effect reaches deodorizing effect.
It is modernization of Chinese medicine technology that certain deodorization composition is extracted from Chinese medicine, and medicine preparation for curing bromhidrosis is various in style on the market, but into
Code insurance is close, false propaganda it is more, real patented product is few.Its existing patent application for example it is a kind of remove underarm odor face cream and
Its preparation method (number of patent application 2014104001361), existing product such as name dew No. 1 (state adornment spy word G20090093), with
Based on aluminium salt, add Chinese medicine witch hazel extract, product introduction, which has, repairs sweat gland function, but the effect such as aluminium salt injury skin according to
So exist.Existing product such as fox despot is solely smelly net (state adornment spy word G20130307), product introduction fully natural green extraction elite, but
Without component identification.The lonely enlightening dew (state adornment spy word G20090592) in existing product such as essence side, main component are hamamelis, Jin He
Joyous to wait extract, product packaging only indicates main component, and other are unknown.
The content of the invention
A kind of deodorant is provided it is an object of the invention to overcome the shortcomings of the prior art part.
To achieve the above object, the technical scheme taken：A kind of deodorant, the deodorant include following raw material：Shell
Glycan and lavender.
Preferably, the deodorant includes the raw material of following parts by weight：The parts by weight of chitosan 1.8~2.2 and lavender 4.5
~5.5 parts by weight.
Preferably, the deodorant also includes following raw material：Menthol, glacial acetic acid, alcohol, emulsifying agent and water.
Preferably, the deodorant also includes the raw material of following parts by weight：The parts by weight of menthol 0.27~0.33, glacial acetic acid
0.9~1.1 parts by weight, the parts by weight of alcohol 1.8~2.2, the parts by weight of emulsifying agent 0.9~1.1, and the parts by weight of water 152~208.
Preferably, the deodorant includes the raw material of following parts by weight：The parts by weight of chitosan 2, the parts by weight of lavender 5 are thin
The parts by weight of lotus alcohol 0.3, the parts by weight of glacial acetic acid 1, the parts by weight of alcohol 2, the parts by weight of emulsifying agent 1, and the parts by weight of water 180.
The invention provides the preparation method of deodorant described above, it is characterised in that methods described includes following step
Suddenly：
(1) chitosan, acetic acid and water are mixed, chitosan is dissolved in aqueous acetic acid, be uniformly mixing to obtain shell and gather
Sugar juice；
(2) lavender is extracted at 60 DEG C with water, leaching liquor is separated with lavender, the leaching liquor after separation is smokes clothing
Careless low temperature extract, by the water air-distillation at 100 DEG C of the lavender after separation, steam cooling, collect oil mixing with water distillation
Liquid, as lavender high temperature extract；
(3) chitosan solution that step (1) obtains is mixed with the lavender low temperature extract prepared in step (2)
Even, sealed storage, then degraded under sunshine or ultraviolet irradiation；
(4) menthol is dissolved in alcohol, adds the lavender high temperature extract prepared in emulsifying agent and step (2),
Stir；
(5) mixed liquor that step (3) obtains is mixed with the mixed liquor that step (4) obtains, obtains the deodorant.
Preferably, the weight of chitosan and water ratio is 1 in the step (1):40；Step (2) extraction time is 8 small
When.
Preferably, the step (2) is：Lavender is extracted with the water of 10 times of weight at 60 DEG C, by leaching liquor with smoking
Clothing grass separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of weight 100
Air-distillation at DEG C, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract.
Preferably, degradation time is at least 5 days in the step (3).
Preferably, after the mixed liquor that step (3) obtains is mixed with the mixed liquor that step (4) obtains in the step (5)
Place 1~6 month, obtain the deodorant.The inventors discovered that effect can be more preferable after deodorant is placed into a period of time, preferably
Ground is 1~6 month.
The present invention adds minimal amount of additive using Nantural non-toxic material chitosan and lavender etc., using microemulsified skill
Art, a kind of film forming agent of chitosan-containing and herbal plant is mixed and made into, applies and is sprayed on human body oxter, had lasting sterilization, repair sweat
Gland cell, remove body odour effect.
The characteristic of deodorant of the present invention
1st, outward appearance：The transparent slightly slime body of brownish red, soluble in water, fragrant grass is fragrant, nontoxic, non-stimulated to skin.
2nd, principle active component：Natural organic polysaccharide class chitosan (molecular weight about 1-2 ten thousand) and herbaceous plant lavender carry
Take thing, menthol etc..
3rd, cationic, pH=6 or so.
4th, not putrid and deteriorated under normal temperature, no floccule is not muddy.Molecular weight and viscosity progressively have on a small quantity with the resting period
Decline, drug effect is more preferable.
5th, film forming：Naturally dry forms the ventilative medicine film of layer of transparent after spray is applied in oxter, and meeting water or sweat has sustained release
Function.
6th, bioactivity is antibacterial, absorption, flocculation, degraded, moisture absorption, moisturizing, repair skin, sweat gland, remove bed body smell.
Chitosan, chemical name：Poly- N-Acetyl-D-glucosamine, chitosan are chitins (or chitin) after deacetylated
Convert and obtain.Chitin is the only naturally nontoxic, good biocompatibility alkaline polysaccharide in nature, is deposited extensively in nature
.Typically handled with shrimp shell, crab shell by soda acid, decalcification and protein, obtain chitin.Again deacetylation is heated with highly basic
Convert to obtain chitosan.The characteristic of chitosan：Translucent sheet is colourless or slightly yellow solid, can also process powdering, tasteless, nothing
Smelly, nontoxic, molecular weight 1-10 ten thousand is not soluble in water, is soluble in diluted acid (formic acid, acetic acid) and positively charged.Chitosan molecule has
Complicated double-spiral structure, containing substantial amounts of hydroxyl and amino, also N- acetamidos, special in structure has it
Unique physico-chemical property, there is good biocompatibility, degradability, film forming, adsorptivity, antibiotic property.Thus in agricultural, doctor
The aspects such as medicine, food, cosmetics, environmental protection are widely used.
Chitosan has bacteriostasis, and the bioactivity and cationic that chitosan is held have to various bacteria and fungi
The anti-microbial property of wide spectrum, such as have to Escherichia coli, black-koji mould, staphylococcus aureus and acted on compared with high inhibition.It is main to positive bacteria
Will be in phage surface film forming, by preventing nutriment from entering to reach bacteriostasis.For negative bacterium, it is cloudy mainly to neutralize it
Ionic charge, infilter into the cell, adsorpting anion material, interference cell is metabolized to reach antibacterial.
Chitosan has adsorption-flocculation effect, is rich in lipid, protein, iron etc. in human body apocrine secretion thing and has and becomes sour
The smelly composition of cause of rotten taste, chitosan can decompose lipid, protein floculation, complexing heavy metal, Adsorption these cause it is smelly into
Point, cut off the nutrient source of bacterium.
Chitosan has a filming function, the component units composition Glucosamine and human epidermal adipose membrane of chitosan it is important into
Divide the structure of ceramide closely similar, it can produce one layer of chitosan adipose membrane layer with epidermal lipid membrane interaction, have good
Permeability, breathe freely, moisturizing.This tunic forms one of natural cover for defense on armpit skin, can block or weaken extraneous thin
Infringement of the bacterium to skin.The active ingredient of chitosan and herbal composition composite membrane can also infilter skin follicle hole, suppress and kill
The harmful microorganisms such as the dead mould wherein concealed, bacterium.This tunic also has slow releasing function, and deodorization is lasting.
Chitosan has sweat gland effect of repairing, and chitosan has stimulation cytothesis and repairs subcutaneous tissue function, chitosan
Penetration it is extremely strong, have adjustment effect to the subcutaneous profuse sweating gland cell of armpit, reduce gap, repair sweat gland, lipid, albumen can be reduced
Matter etc. causes smelly composition to solve body odor from source in the discharge of oxter.
Lavender is savoury herb, natural antibacterial agent.Mainly it is applied to clinical and cosmetic conduct in the form of dry product or essential oil
Industry.The pure and fresh gracefulness of its fragrance, property is gentle, have it is calm, releive, syngignoscism, can healing of wound, it is anti-inflammation and sterilization, antimycotic, go
Scar, oil-control, Regeneration and Repair skin.Lavender low temperature (60 DEG C) extract component of the present invention：Bergamio, acetic acid lavender
Ester, linalool, geraniol, cumarin etc..Its high temperature distillation extract is a variety of tannins, albumen in Lavender and lavender
The water soluble ingredients such as matter, plant sugar.Essential oil is the complex mixture of many different types of aromatic compound compositions again, mainly
Composition is linalool, acetic acid linalool, cineole, B- ocimenums (including cis and trans) to, acetic acid lavender ester, lavender
Alcohol, terpene -4- alcohol and camphor etc..Herba Lysimachiae foenumgraeci extract eliminates the part composition invalid to deodorization, improves purity, and chitosan
Solution is mixed with cooperative effect, forms film forming agent-medicine film, greatly strengthen sterilization, deodorization.
Menthol is the extract of natural plants peppermint, there is anesthesia, refrigerant and antiinflammatory action, and its alcoholic solution has anti-corrosion work
With being mixed to form the medicine film of cooperative effect with chitosan, lavender, give full play to the complementation between composition.
The beneficial effects of the present invention are：The invention provides a kind of deodorant, compared with prior art, has following excellent
Point：
(1) deodorant principle active component chitosan, herbaceous plant lavender and menthol of the present invention are natural
Antiseptic, auxiliary element glacial acetic acid and alcohol are also antiseptic, and lavender and menthol are natural perfume material again, need not in structure
Any chemical preservative and essence are added again, it is safe and non-toxic, it is more healthy than prior art, environmentally friendly.
(2) present invention uses micro-emulsion technology, and the chitosan with positive electricity and negatively charged herbal extract are mixed
The film forming agent with slow-release function of transparent no floccule is made, is the external application Chinese medicine process technology of modernization.
(3) film forming deodorization is the breakthrough of human body deodorization technology, unprecedented.Spray is made in deodorant of the present invention,
I.e. spray is film forming, easy to use, and lasting medicine is low-consuming.And the bioactivity of chitosan is extremely strong to Cutaneous permeation, antibacterial,
Skin care, the function of repairing apocrine sweat gland cell membrane, are all that the medicine preparation for curing bromhidrosis based on other aluminium salts can not compare.
(4) present invention is that discarded chitin is applied in health, is gone back to nature again after degraded, realizes life
State circulates, and is an environment-friendly products.Raw material used is common, and cost is low, and technique is brief, small investment, easily realizes, economic benefits
It is good.
Embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
A kind of embodiment of deodorant of the present invention, the deodorant include the raw material of following parts by weight：Chitosan 1.8
Parts by weight, the parts by weight of lavender 5.5, the parts by weight of menthol 0.27, the parts by weight of glacial acetic acid 0.9, the parts by weight of alcohol 1.8, emulsifying agent
0.9 parts by weight, and the parts by weight of pure water 182.The emulsifying agent is emulsifier op-10.
Chitosan of the present invention：Cosmetic grade, powdery, deacetylation ＞ 90%, low molecule amount 1-5 ten thousand.
Lavender of the present invention：Pale reddish brown flower bud, fragrance is pure, no-sundries, no design of scattered small flowers and plants, high-class product.
Menthol of the present invention：Natural raw peppermint oil purification, content >=99.5%.
Glacial acetic acid of the present invention：Meet national standard GB/T1628-2008, acetic acid content 98%.
Alcohol of the present invention：Food-grade, national standard GB103432008,95%.
Emulsifier op-10 of the present invention:APES, cosmetic grade.
Pure water of the present invention：Meet《2000 Chinese Pharmacopoeias》The purifying water quality standard recorded.
The preparation method of deodorant of the present invention：
(1) 1.8 parts by weight chitosans, 0.9 parts by weight acetic acid and 72 parts by weight water are mixed at 35 DEG C, gathers shell
Sugar is dissolved in aqueous acetic acid, 60 revs/min of mixing speed, and mixing time is 2 hours, filters off except a small amount of insoluble matter, obtains
Chitosan solution；
(2) lavender of 5.5 parts by weight is extracted 8 hours at 60 DEG C with the water of 55 parts by weight, by leaching liquor and smokes clothing
Grass separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of parts by weight 100
Air-distillation at DEG C, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract；
(3) chitosan solution for obtaining step (1) mixes with the lavender low temperature extract prepared in step (2)
Uniformly, 60 revs/min of speed of agitator, 0.5 hour time, sealed storage, then sunshine or ultraviolet irradiation under degrade, at least according to
Penetrate 5 days, solution colour is progressively deepened, by pale brown turn of reddish brown, hyalomucoid；
(4) by 0.27 parts by weight menthol stirring and dissolving in 1.8 parts by weight alcohol, speed of agitator is 30 revs/min, stirring
Time is 0.5 hour；The lavender high temperature extract prepared in 0.9 parts by weight Emulsifier and step (2) is added, is stirred,
Speed of agitator is 1000 revs/min, 0.5 hour time；
(5) in rotating speed it is 1000 revs/min after the mixing of mixed liquor that the mixed liquor and step (4) obtained step (3) obtains
Lower stirring 0.5 hour, sealed storage, color is further deepened, the transparent slightly slime body of deep maroon, haze-free, no flocculate or
Precipitated impurities, storage time are 1-6 months.
Embodiment 2
A kind of embodiment of deodorant of the present invention, the deodorant include the raw material of following parts by weight：The weight of chitosan 2
Amount part, the parts by weight of lavender 5, the parts by weight of menthol 0.3, the parts by weight of glacial acetic acid 1, the parts by weight of alcohol 2, the parts by weight of emulsifying agent 1, and
The parts by weight of pure water 180.The emulsifying agent is emulsifier op-10.
Chitosan of the present invention：Cosmetic grade, powdery, deacetylation ＞ 90%, low molecule amount 1-5 ten thousand.
Lavender of the present invention：Pale reddish brown flower bud, fragrance is pure, no-sundries, no design of scattered small flowers and plants, high-class product.
Menthol of the present invention：Natural raw peppermint oil purification, content >=99.5%.
Glacial acetic acid of the present invention：Meet national standard GB/T1628-2008, acetic acid content 98%.
Alcohol of the present invention：Food-grade, national standard GB103432008,95%.
Emulsifier op-10 of the present invention:APES, cosmetic grade.
Pure water of the present invention：Meet《2000 Chinese Pharmacopoeias》The purifying water quality standard recorded.
The preparation method of deodorant of the present invention：
(1) 2 parts by weight chitosans, 1 parts by weight acetic acid and 80 parts by weight water are mixed at 35 DEG C, makes chitosan molten
Solution is in aqueous acetic acid, 60 revs/min of mixing speed, and mixing time is 2 hours, filters off except a small amount of insoluble matter, obtains shell and gather
Sugar juice；
(2) lavender of 5 parts by weight is extracted 8 hours at 60 DEG C with the water of 50 parts by weight, by leaching liquor and lavender
Separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of parts by weight at 100 DEG C
Lower air-distillation, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract；
(3) chitosan solution for obtaining step (1) mixes with the lavender low temperature extract prepared in step (2)
Uniformly, 60 revs/min of speed of agitator, 0.5 hour time, sealed storage, then sunshine or ultraviolet irradiation under degrade, at least according to
Penetrate 5 days, solution colour is progressively deepened, by pale brown turn of reddish brown, hyalomucoid；
(4) by 0.3 parts by weight menthol stirring and dissolving in 2 parts by weight alcohol, speed of agitator is 30 revs/min, during stirring
Between be 0.5 hour；The lavender high temperature extract prepared in 1 parts by weight Emulsifier and step (2) is added, is stirred, is stirred
Rotating speed is 1000 revs/min, 0.5 hour time；
(5) in rotating speed it is 1000 revs/min after the mixing of mixed liquor that the mixed liquor and step (4) obtained step (3) obtains
Lower stirring 0.5 hour, sealed storage, color is further deepened, the transparent slightly slime body of deep maroon, haze-free, no flocculate or
Precipitated impurities, storage time are 1-6 months.
Embodiment 3
A kind of embodiment of deodorant of the present invention, the deodorant include the raw material of following parts by weight：Chitosan 2.2
Parts by weight, the parts by weight of lavender 4.5, the parts by weight of menthol 0.33, the parts by weight of glacial acetic acid 1.1, the parts by weight of alcohol 2.2, emulsifying agent
1.1 parts by weight, and the parts by weight of pure water 178.The emulsifying agent is emulsifier op-10.
Chitosan of the present invention：Cosmetic grade, powdery, deacetylation ＞ 90%, low molecule amount 1-5 ten thousand.
Lavender of the present invention：Pale reddish brown flower bud, fragrance is pure, no-sundries, no design of scattered small flowers and plants, high-class product.
Menthol of the present invention：Natural raw peppermint oil purification, content >=99.5%.
Glacial acetic acid of the present invention：Meet national standard GB/T1628-2008, acetic acid content 98%.
Alcohol of the present invention：Food-grade, national standard GB103432008,95%.
Emulsifier op-10 of the present invention:APES, cosmetic grade.
Pure water of the present invention：Meet《2000 Chinese Pharmacopoeias》The purifying water quality standard recorded.
The preparation method of deodorant of the present invention：
(1) 2.2 parts by weight chitosans, 1.1 parts by weight acetic acid and 88 parts by weight water are mixed at 35 DEG C, gathers shell
Sugar is dissolved in aqueous acetic acid, 60 revs/min of mixing speed, and mixing time is 2 hours, filters off except a small amount of insoluble matter, obtains
Chitosan solution；
(2) lavender of 4.5 parts by weight is extracted 8 hours at 60 DEG C with the water of 45 parts by weight, by leaching liquor and smokes clothing
Grass separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of parts by weight 100
Air-distillation at DEG C, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract；
(3) chitosan solution for obtaining step (1) mixes with the lavender low temperature extract prepared in step (2)
Uniformly, 60 revs/min of speed of agitator, 0.5 hour time, sealed storage, then sunshine or ultraviolet irradiation under degrade, at least according to
Penetrate 5 days, solution colour is progressively deepened, by pale brown turn of reddish brown, hyalomucoid；
(4) by 0.33 parts by weight menthol stirring and dissolving in 2.2 parts by weight alcohol, speed of agitator is 30 revs/min, stirring
Time is 0.5 hour；The lavender high temperature extract prepared in 1.1 parts by weight Emulsifier and step (2) is added, is stirred,
Speed of agitator is 1000 revs/min, 0.5 hour time；
(5) in rotating speed it is 1000 revs/min after the mixing of mixed liquor that the mixed liquor and step (4) obtained step (3) obtains
Lower stirring 0.5 hour, sealed storage, color is further deepened, the transparent slightly slime body of deep maroon, haze-free, no flocculate or
Precipitated impurities, storage time are 1-6 months.
Embodiment 4
A kind of embodiment of deodorant of the present invention, the deodorant include the raw material of following parts by weight：Chitosan 1.8
Parts by weight, the parts by weight of lavender 5.5, the parts by weight of menthol 0.33, the parts by weight of glacial acetic acid 0.9, the parts by weight of alcohol 1.8, emulsifying agent
0.9 parts by weight, and the parts by weight of pure water 182.The emulsifying agent is emulsifier op-10.
Chitosan of the present invention：Cosmetic grade, powdery, deacetylation ＞ 90%, low molecule amount 1-5 ten thousand.
Lavender of the present invention：Pale reddish brown flower bud, fragrance is pure, no-sundries, no design of scattered small flowers and plants, high-class product.
Menthol of the present invention：Natural raw peppermint oil purification, content >=99.5%.
Glacial acetic acid of the present invention：Meet national standard GB/T1628-2008, acetic acid content 98%.
Alcohol of the present invention：Food-grade, national standard GB103432008,95%.
Emulsifier op-10 of the present invention:APES, cosmetic grade.
Pure water of the present invention：Meet《2000 Chinese Pharmacopoeias》The purifying water quality standard recorded.
The preparation method of deodorant of the present invention：
(1) 1.8 parts by weight chitosans, 0.9 parts by weight acetic acid and 72 parts by weight water are mixed at 35 DEG C, gathers shell
Sugar is dissolved in aqueous acetic acid, 60 revs/min of mixing speed, and mixing time is 2 hours, filters off except a small amount of insoluble matter, obtains
Chitosan solution；
(2) lavender of 5.5 parts by weight is extracted 8 hours at 60 DEG C with the water of 55 parts by weight, by leaching liquor and smokes clothing
Grass separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of parts by weight 100
Air-distillation at DEG C, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract；
(3) chitosan solution for obtaining step (1) mixes with the lavender low temperature extract prepared in step (2)
Uniformly, 60 revs/min of speed of agitator, 0.5 hour time, sealed storage, then sunshine or ultraviolet irradiation under degrade, at least according to
Penetrate 5 days, solution colour is progressively deepened, by pale brown turn of reddish brown, hyalomucoid；
(4) by 0.27 parts by weight menthol stirring and dissolving in 1.8 parts by weight alcohol, speed of agitator is 30 revs/min, stirring
Time is 0.5 hour；The lavender high temperature extract prepared in 0.9 parts by weight Emulsifier and step (2) is added, is stirred,
Speed of agitator is 1000 revs/min, 0.5 hour time；
(5) in rotating speed it is 1000 revs/min after the mixing of mixed liquor that the mixed liquor and step (4) obtained step (3) obtains
Lower stirring 0.5 hour, sealed storage, color is further deepened, the transparent slightly slime body of deep maroon, haze-free, no flocculate or
Precipitated impurities, storage time are 1-6 months.
Embodiment 5
A kind of embodiment of deodorant of the present invention, the deodorant include the raw material of following parts by weight：Chitosan 2.2
Parts by weight, the parts by weight of lavender 4.5, the parts by weight of menthol 0.27, the parts by weight of glacial acetic acid 1.1, the parts by weight of alcohol 2.2, emulsifying agent
1.1 parts by weight, and the parts by weight of pure water 178.The emulsifying agent is emulsifier op-10.
Chitosan of the present invention：Cosmetic grade, powdery, deacetylation ＞ 90%, low molecule amount 1-5 ten thousand.
Lavender of the present invention：Pale reddish brown flower bud, fragrance is pure, no-sundries, no design of scattered small flowers and plants, high-class product.
Menthol of the present invention：Natural raw peppermint oil purification, content >=99.5%.
Glacial acetic acid of the present invention：Meet national standard GB/T1628-2008, acetic acid content 98%.
Alcohol of the present invention：Food-grade, national standard GB103432008,95%.
Emulsifier op-10 of the present invention:APES, cosmetic grade.
Pure water of the present invention：Meet《2000 Chinese Pharmacopoeias》The purifying water quality standard recorded.
The preparation method of deodorant of the present invention：
(1) 2.2 parts by weight chitosans, 1.1 parts by weight acetic acid and 88 parts by weight water are mixed at 35 DEG C, gathers shell
Sugar is dissolved in aqueous acetic acid, 60 revs/min of mixing speed, and mixing time is 2 hours, filters off except a small amount of insoluble matter, obtains
Chitosan solution；
(2) lavender of 4.5 parts by weight is extracted 8 hours at 60 DEG C with the water of 45 parts by weight, by leaching liquor and smokes clothing
Grass separation, the leaching liquor after separation is lavender low temperature extract, by the lavender after separation with the water of 10 times of parts by weight 100
Air-distillation at DEG C, steam cooling, collects oil mixing with water distillate, as lavender high temperature extract；
(3) chitosan solution for obtaining step (1) mixes with the lavender low temperature extract prepared in step (2)
Uniformly, 60 revs/min of speed of agitator, 0.5 hour time, sealed storage, then sunshine or ultraviolet irradiation under degrade, at least according to
Penetrate 5 days, solution colour is progressively deepened, by pale brown turn of reddish brown, hyalomucoid；
(4) by 0.33 parts by weight menthol stirring and dissolving in 2.2 parts by weight alcohol, speed of agitator is 30 revs/min, stirring
Time is 0.5 hour；The lavender high temperature extract prepared in 1.1 parts by weight Emulsifier and step (2) is added, is stirred,
Speed of agitator is 1000 revs/min, 0.5 hour time；
(5) in rotating speed it is 1000 revs/min after the mixing of mixed liquor that the mixed liquor and step (4) obtained step (3) obtains
Lower stirring 0.5 hour, sealed storage, color is further deepened, the transparent slightly slime body of deep maroon, haze-free, no flocculate or
Precipitated impurities, storage time are 1-6 months.
Embodiment 6
Deodorant of the present invention is packaged into finished product, to pass through secondary filter before packaging, is sprayed with clear, colorless glass
Bottle, 20-40ml/ branch, make-up room sanitary condition will meet Cosmetic Manufacture health license requirement.
The operation instruction of deodorant of the present invention：
Before being slept after body odor person's evening bathing under double oxters respectively spray two, once a day.Rear body odor is dried to remove.Disease after five days
Shape takes a turn for the better, once every other day.After ten days once three days.The lighter recovers normal body odour after one month, and weight patient can proper extension use
Time.This product lasting medicine, it can use as needed, it is not necessary to use everyday, body odour can be transferred to defects liability period after recovering normal.
The maintenance of body odour：Bathing lotion is replaced with this product during bathing, under oxter spray two, then with warm water cleaning skin, sheet
Product are also extraordinary body cleanser, and decontamination is deoiled deodorizing, moisturizing, skin care.
According to relevant statistics, body odor person Chinese account for 20%, and the foreigner (including west, the Middle East, Africa) accounts for 80%, with
Women and young man are in the majority, and the foreigner is more serious than Chinese, and this product is mainly women using object, take into account home and abroad personage.
1st, it is grouped
A groups：The domestic people of personage's body odour patient 4
B groups：The people of Black African (Zambia) severe body odor person 4
2nd, deodorant agent granting amount：Everyone 1 bottle (50ml)
3rd, validity period：2015.8.30-2015.10.30,2 totally months
4th, using front and rear comparing result such as table 1
Comparing result before and after the use of table 1
As can be seen from the above data, deodorant of the present invention has good deodorizing effect, it is non-stimulated to human body and
Adverse reaction, dry skin, blackening will not be caused, skin can be repaired.
Embodiment 7：The clinical test of deodorant of the present invention
Someone, male, 74 years old, retired employee, Italian Tula spy people from city.First visit：On September 21st, 2015.
Main suit:Smelly more than 40 years of skin.
Present illness history:Smelly more than 40 years of skin, runs into inconvenience, trouble, comes upon somebody's introduction in public places《Milan benevolence Ji
Traditional Chinese and western medicine clinic》Seek medical advice.
Past medical history：There is allergic history.
The four methods of diagnosis:Body is big and tall, and healthy and strong, talk is freely；Patient has just enter into clinic, just allows people to feel that its skin is smelly and assails the nostrils, is full of
Clinic.Readme：It is unmarried, make Plot Work in municipal government, there is single office；Although knowing has bad smell of perspiration, colleague does not exist
Handle official business together, it is few to the people of the smelly complaint of skin；After retirement in 65 years old, together with the old man of leisure, often hear that others complains
Bad smell of perspiration, it is ashamed endlessly；Then try every possible means in place of having bought deodorant spray oxter and the hidrosis with it of some in the markets, can change sometimes
It is kind, but it is smelly as before to occur skin again soon.Usually, dry is bitter, drinking a lot of water, receives kind, and eating meat, two is just without exception, sleeps.Arteries and veins
Slightly chord number, red tongue with thin fur are white.Blood pressure：140/85, heart rate：74 beats/min.
Pathology：Containing excessive thick lipid in human sweat, unrighted acid is produced through putrefactive fermentation, is sent unpleasant
Stink.
It is dialectical:Liver and gall excess heat, smoke excessive skin.
The rules for the treatment of：Local application's removing skin is smelly, bland diet.
Face card analysis：Patient is unmarried, and happiness is carnivorous, veins string bitter taste, illustrates that liver and gall have heat, and heat toxin accumulates hair, fumigates skin and dissipates
Stink.Clinical syndrome differentiation is liver and gall excess heat, smokes excessive skin.Because patient body is uncomfortable without other, therefore it treats suitable external application deodorant,
Deodorant as described herein, then change diet, eats that meat etc. is higher fatty acid, food of high protein less.See how the offender behaves.
Treatment:
(1) deodorant of the present invention is used.
Application method：Before being slept after evening bathing under the sweat such as double oxters, groin multiple location respectively spray two, once a day.
The maintenance of body odour：Bathing lotion is replaced with this product during bathing, under oxter, groin spray two, then with warm water cleaning skin
Skin.
(2) higher fatty acid, high protein and pungent product are eaten less, eat green vegetables fruit more.
Further consultation：On the day of the first visit on the 21st of September in 2015 at night, start to use deodorant of the present invention by doctor's advice.
September 26 days, after patient uses deodorant of the present invention, start there is a skin to itch, just all went well later, skin is smelly to be had
Significantly reduce, in public places unmanned complaint, into clinic, the also no longer smelly smoked day of skin.
October 3, after two weeks use deodorant of the present invention, the substantially smelly disappearance of skin.
Curative effect:Announcement is cured.
Through the clinic Clinical practice deodorant treatment smelly patient of skin of the present invention, positive effect, disease can be substantially eliminated
People's skin is smelly, has no discomfort.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent substitution, without departing from the essence of technical solution of the present invention
And scope.
Claims (7)
1. a kind of deodorant, it is characterised in that the deodorant includes the raw material of following parts by weight：The weight of chitosan 1.8~2.2
Part and the parts by weight of lavender 4.5~5.5；The deodorant also includes the raw material of following parts by weight：The weight of menthol 0.27~0.33
Amount part, the parts by weight of glacial acetic acid 0.9~1.1, the parts by weight of alcohol 1.8~2.2, the parts by weight of emulsifying agent 0.9~1.1, and water 152~
208 parts by weight；
The preparation method of the deodorant comprises the following steps：
(1) chitosan, acetic acid and water are mixed, chitosan is dissolved in aqueous acetic acid, it is molten to be uniformly mixing to obtain chitosan
Liquid；
(2) lavender is extracted at 60 DEG C with water, leaching liquor is separated with lavender, the leaching liquor after separation is that lavender is low
Warm extract, by the water air-distillation at 100 DEG C of the lavender after separation, steam cooling, oil mixing with water distillate is collected, i.e.,
For lavender high temperature extract；
(3) chitosan solution that step (1) obtains is well mixed with the lavender low temperature extract prepared in step (2), is close
Envelope storage, then degraded under sunshine or ultraviolet irradiation；
(4) menthol is dissolved in alcohol, adds the lavender high temperature extract prepared in emulsifying agent and step (2), stirring
Uniformly；
(5) mixed liquor that step (3) obtains is mixed with the mixed liquor that step (4) obtains, obtains the deodorant.
2. deodorant according to claim 1, it is characterised in that the deodorant includes the raw material of following parts by weight：Shell
The parts by weight of glycan 2, the parts by weight of lavender 5, the parts by weight of menthol 0.3, the parts by weight of glacial acetic acid 1, the parts by weight of alcohol 2, the weight of emulsifying agent 1
Measure part, and the parts by weight of water 180.
3. the preparation method of a kind of deodorant as described in claim 1-2 is any, it is characterised in that methods described includes following
Step：
(1) chitosan, acetic acid and water are mixed, chitosan is dissolved in aqueous acetic acid, it is molten to be uniformly mixing to obtain chitosan
Liquid；
(2) lavender is extracted at 60 DEG C with water, leaching liquor is separated with lavender, the leaching liquor after separation is that lavender is low
Warm extract, by the water air-distillation at 100 DEG C of the lavender after separation, steam cooling, oil mixing with water distillate is collected, i.e.,
For lavender high temperature extract；
(3) chitosan solution that step (1) obtains is well mixed with the lavender low temperature extract prepared in step (2), is close
Envelope storage, then degraded under sunshine or ultraviolet irradiation；
(4) menthol is dissolved in alcohol, adds the lavender high temperature extract prepared in emulsifying agent and step (2), stirring
Uniformly；
(5) mixed liquor that step (3) obtains is mixed with the mixed liquor that step (4) obtains, obtains the deodorant.
4. preparation method according to claim 3, it is characterised in that the weight of chitosan and water ratio in the step (1)
For 1:40；Step (2) extraction time is 8 hours.
5. preparation method according to claim 3, it is characterised in that the step (2) is：By lavender with 10 times of weight
Water extracted at 60 DEG C, leaching liquor is separated with lavender, the leaching liquor after separation is lavender low temperature extract, will be separated
Water air-distillation at 100 DEG C of 10 times of weight of lavender afterwards, steam cooling, collects oil mixing with water distillate, as smokes
Clothing natural plant height temperature extract.
6. preparation method according to claim 3, it is characterised in that degradation time is at least 5 days in the step (3).
7. preparation method according to claim 3, it is characterised in that the mixing for obtaining step (3) in the step (5)
Liquid is placed 1~6 month after being mixed with the mixed liquor that step (4) obtains, and obtains the deodorant.
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