CN105544191A - Textile finishing agent prepared by taking flower and fruit of sweet osmanthus as raw material and preparation method of textile finishing agent - Google Patents
Textile finishing agent prepared by taking flower and fruit of sweet osmanthus as raw material and preparation method of textile finishing agent Download PDFInfo
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- D—TEXTILES; PAPER
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- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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Abstract
The invention provides a textile finishing agent prepared by taking flower and fruit of sweet osmanthus as the raw material and a preparation method of the textile finishing agent. The preparation method particularly comprises the following steps: after removing dirt of the petals and the fruit of picked sweet osmanthus, placing the petals and the fruit in the shade to be naturally dried, sealing the dried petals and fruit, preserving at the ordinary temperature, then washing the petals of sweet osmanthus with distilled water, after that, distilling with steam to obtain a distillation liquid, and extracting and drying the distillation liquid to obtain a sweet osmanthus flavoring agent and sweet osmanthus petal residues; placing the sweet osmanthus petal residues and the fruit of sweet osmanthus into a crusher to be crushed, sieving and screening to obtain sweet osmanthus powder; performing constant-temperature water bathing and reflux extraction on the sweet osmanthus powder, adding an organic solution, performing ultrasonic oscillation, filtering, repeating 2-3 times, merging the filtrates to obtain a sweet osmanthus natural pigment and a sweet osmanthus antibacterial agent, namely sweet osmanthus extracts; performing evaporation and concentration on the sweet osmanthus extracts, purifying via macroporous resin, concentrating, adding the sweet osmanthus flavoring agent, uniformly stirring, finally, adding an additive, and then uniformly mixing to obtain the textile finishing agent prepared by taking flower and fruit of sweet osmanthus as the raw material.
Description
Technical field:
The invention belongs to textile material technical field, be specifically related to a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus and preparation method thereof.
Background technology:
Sweet osmanthus is one of China ten great tradition famous flower, also referred to as sweet-scented osmanthus, rock osmanthus, kamuning and Jin Li, belongs to Oleaceae osmanthus, is distributed widely in the provinces such as Sichuan, Yunnan, Guangdong, Guangxi, Hubei, Jiangsu, Jiangxi, is the preciousness fragrance flower of China's special product.Sweet osmanthus is rich in protein, fat, carbohydrate, carrotene, aromatic oil, anthocyanidin, amino acid, vitamin, trace element, hormone, enzyme, sweet osmanthus alkane etc., therefore sweet osmanthus is famous spice berry, can be used as again medicinal material, dyestuff, and its flower, really, root all can be used as medicine, because Osmanthus Fragrans resources is limited, raw material is precious, is called as in the world " wholefood ", has very high economic worth.
At present, the osmanthus concrete prepared based on sweet osmanthus is the precious spices of China's special product, and it stays long and very popular because of pure and fresh elegance, gracefulness, outlet countries in the world.But the limited starting material of sweet osmanthus, florescence is extremely short, flower is more weak, fragrance very easily loses, timely process is needed after harvesting, and a large amount of discarded sweet osmanthus residues produced in the production process of osmanthus concrete, and still containing a considerable amount of active ingredient in these residues, as flavones, polyphenol and natural colouring matter, cause the great wasting of resources.Therefore be necessary to utilize fully Osmanthus Fragrans resources, to improve its economic worth.
The disclosed a kind of hydrolysis technology of Chinese patent CN102206550B (publication date 2011.10.5) prepares the method for osmanthus concrete and sweet osmanthus general flavone, fresh sweet osmanthus is coagulated after water collection through vacuumize, pulverize, with the sweet enzyme hydrolysis of β-D-Glucose, then extract osmanthus concrete with benzinum, methanol solvate extracts and coordinates ultrasonic assistant to obtain refining sweet osmanthus general flavone.The osmanthus concrete product yield that the method adopts enzyme hydrolysis to extract improves more than 20%, the yield of the sweet osmanthus general flavone product adopting ultrasonic assistant to extract improves 10%, extraction conditions milder, be conducive to keeping biologically active, be applicable to general plant extract producer and production of flavor producer, easy and simple to handle, invest little, practical.Disclosed haematochrome, the Its Preparation Method And Use extracted from fragrans seed peel of Chinese patent CN10999614B (publication date 2007.7.18), fragrans seed peel is put in acid polar solvent, extract and filter, evaporant obtains the haematochrome in fragrans seed peel, and this haematochrome can be used as food coloring, cosmetic additive agent and coloring agent.The haematochrome good water solubility that the method is extracted from fragrans seed peel, strong coloring force, has good heat endurance, non-oxidizability and reducibility, resistance to sugared salt tolerance etc., and safety non-toxic, of many uses.
From above-mentioned prior art, with the spices, antiseptic, natural colouring matter etc. that the flowers and fruits skin of sweet osmanthus is prepared for raw material, all there is quite high economic worth, but the comprehensive utilization ratio of sweet osmanthus is still lower at present, cause with the product category of sweet osmanthus raw material rare, and it is expensive, be unfavorable for its marketing, be more difficult to large batch of in field uses such as weavings.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus and preparation method thereof, select the petal of the sweet osmanthus of fresh harvesting and fruit as raw material, sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter and sweet osmanthus antiseptic is obtained after purifying respectively through steam distillation, pulverizer pulverizing, backflow lixiviate, solvent extraction, sonic oscillation, resin, three mixed and adds auxiliary agent, obtaining the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus.Active ingredient in sweet osmanthus flowers and fruits is extracted by one-step method by the present invention respectively, by the value maximization of sweet osmanthus flowers and fruits, and containing natural colouring matter, flavouring agent and antiseptic in the fabric finishing agent of preparation, fabric is after this finishing agent arranges, its color, the sense of taste and function all improve, Be very effective, economic worth is high, is conducive to marketing.
For solving the problems of the technologies described above, technical scheme of the present invention is:
A kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, it is characterized in that, the main raw material of the described fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus is sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, described sweet osmanthus flavouring agent is sweet osmanthus petal extract, and described sweet osmanthus natural colouring matter and sweet osmanthus antiseptic are sweet osmanthus petal and fruit extract.
The present invention also provides a kind of preparation method of the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, comprises the following steps:
(1) petal of sweet osmanthus after plucking and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit;
(2), after the sweet osmanthus petal distilled water washing prepared by step (1), through steam distillation 2-4h, obtain distillating liquid after extracting drying, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue;
(3) sweet osmanthus fruit prepared by sweet osmanthus petal residue step (2) prepared and step (1) is placed in pulverizer and pulverizes, and filtration of sieving, obtains sweet osmanthus powder;
(4) sweet osmanthus powder step (3) prepared to reflux lixiviate through water bath with thermostatic control, then adds organic solution, sonic oscillation, filter, repeat 2-3 time, merging filtrate obtain, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, be Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration prepared by step (4), through macroporous absorbent resin purification 1-2 time, concentrated, add sweet osmanthus flavouring agent prepared by step (2) again, stir, finally add auxiliary agent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus.
Preferred as technique scheme, in described step (1), the petal of sweet osmanthus and fruit are the fresh feed won under the kind of golden osmanthus.
Preferred as technique scheme, in described step (2), the extract of extraction is ether, and the volume ratio of distillating liquid and extract is 1:0.5-0.8.
Preferred as technique scheme, in described step (2), the recovery rate of sweet osmanthus flavouring agent is 0.12-0.17%.
Preferred as technique scheme, in described step (3), the particle diameter of sweet osmanthus powder is 1-2 μm.
Preferred as technique scheme, in described step (4), organic solvent is one or more in ethyl acetate, benzinum, ethanolic solution.
Preferred as technique scheme, in described step (4), the materials of sweet osmanthus powder and organic solution are than being 1:8-10.
Preferred as technique scheme, in described step (5), auxiliary agent is one or more in film forming agent, preservative agent, dispersant, surfactant and solvent.
Preferred as technique scheme, in described step (5), in the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is higher than 12%.
Compared with prior art, the present invention has following beneficial effect:
(1) raw material of the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus prepared of the present invention is for sweet osmanthus flowers and fruits, by rational selective extraction technique and means, plurality of active ingredients is extracted respectively from sweet osmanthus flowers and fruits, as flavouring agent, pigment, antioxidant and antiseptic, improve the comprehensive utilization ratio of Osmanthus Fragrans resources, prevent the waste of Osmanthus Fragrans resources, improve its economic worth.
(2) in the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus prepared of the present invention containing active ingredients such as linalool oxide, irisone, red pigments, general flavone, polyphenol and triterpenes, therefore there is the fragrance of sweet osmanthus, red color and luster, and there is anti-oxidant, antibacterial effect.
Detailed description of the invention:
Describe the present invention in detail below in conjunction with specific embodiment, be used for explaining the present invention in this illustrative examples of the present invention and explanation, but not as a limitation of the invention.
Embodiment 1:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 2h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.5 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.12%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 1 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add ethyl acetate solution, materials are than being 1:8, sonic oscillation 20min, filters, repeats 2 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 1 time through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add film forming agent, preservative agent, dispersant, surfactant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 12%.
Embodiment 2:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 4h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.8 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.17%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 2 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add petroleum ether solution, materials are than being 1:10, sonic oscillation 30min, filters, repeats 3 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 2 times through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add film forming agent, preservative agent, dispersant, surfactant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 19%.
Embodiment 3:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 3h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.6 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.14%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 1.5 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add ethyl acetate solution, materials are than being 1:9, sonic oscillation 25min, filters, repeats 2 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 2 times through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add preservative agent, dispersant, surfactant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 16%.
Embodiment 4:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 2.5h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.7 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.15%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 1.6 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add petroleum ether solution, materials are than being 1:8, sonic oscillation 30min, filters, repeats 3 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 1 time through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add film forming agent, preservative agent, dispersant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 15%.
Embodiment 5:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 4h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.5 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.16%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 1.2 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add ethyl acetate solution, materials are than being 1:10, sonic oscillation 25min, filters, repeats 3 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 2 times through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add film forming agent, preservative agent, surfactant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 18%.
Embodiment 6:
(1) petal of fresh sweet osmanthus won under the kind of golden osmanthus and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit.
(2) after sweet osmanthus petal being washed with distilled water, through steam distillation 4h, obtain distillating liquid, by the distillating liquid of 1 parts by volume after the extracted with diethyl ether drying of 0.6 part, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue, wherein the recovery rate of sweet osmanthus flavouring agent is 0.13%.
(3) sweet osmanthus petal residue and sweet osmanthus fruit are placed in pulverizer to pulverize, filtration of sieving, obtain the sweet osmanthus powder that particle diameter is 1.4 μm.
(4) to be refluxed lixiviate through water bath with thermostatic control by sweet osmanthus powder, then add ethanolic solution, materials are than being 1:8, sonic oscillation 20min, filters, repeats 3 times, merging filtrate obtains, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, is Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration, purify 2 times through macroporous absorbent resin, concentrated, add sweet osmanthus flavouring agent again, stir, finally add film forming agent, preservative agent, dispersant, surfactant and solvent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, wherein the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic is 17%.
After testing, the result of the smell of the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus prepared of embodiment 1-6, absorbance, non-oxidizability, antibiotic property is as follows:
As seen from the above table, the smell delicate fragrance of the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus prepared by the present invention, absorbance is good, and possesses good non-oxidizability and anti-microbial property, good combination property.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, it is characterized in that, the main raw material of the described fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus is sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, described sweet osmanthus flavouring agent is sweet osmanthus petal extract, and described sweet osmanthus natural colouring matter and sweet osmanthus antiseptic are sweet osmanthus petal and fruit extract.
2. a preparation method for the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, is characterized in that, comprise the following steps:
(1) petal of sweet osmanthus after plucking and fruit are removed dirt, In Shadely naturally to dry in the shade, sealing normal temperature is preserved, the sweet osmanthus petal sealed up for safekeeping in advance and fruit;
(2), after the sweet osmanthus petal distilled water washing prepared by step (1), through steam distillation 2-4h, obtain distillating liquid after extracting drying, obtain sweet osmanthus flavouring agent and sweet osmanthus petal residue;
(3) sweet osmanthus fruit prepared by sweet osmanthus petal residue step (2) prepared and step (1) is placed in pulverizer and pulverizes, and filtration of sieving, obtains sweet osmanthus powder;
(4) sweet osmanthus powder step (3) prepared to reflux lixiviate through water bath with thermostatic control, then adds organic solution, sonic oscillation, filter, repeat 2-3 time, merging filtrate obtain, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant and sweet osmanthus antiseptic, be Flos Osmanthi Fragrantis extract;
(5) by Flos Osmanthi Fragrantis extract evaporation and concentration prepared by step (4), through macroporous absorbent resin purification 1-2 time, concentrated, add sweet osmanthus flavouring agent prepared by step (2) again, stir, finally add auxiliary agent, mix, obtain the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus.
3. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (1), the petal of sweet osmanthus and fruit are the fresh feed won under the kind of golden osmanthus.
4. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (2), the extract of extraction is ether, and the volume ratio of distillating liquid and extract is 1:0.5-0.8.
5. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (2), the recovery rate of sweet osmanthus flavouring agent is 0.12-0.17%.
6. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (3), the particle diameter of sweet osmanthus powder is 1-2 μm.
7. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (4), organic solvent is one or more in ethyl acetate, benzinum, ethanolic solution.
8. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, is characterized in that: in described step (4), and the materials of sweet osmanthus powder and organic solution are than being 1:8-10.
9. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (5), auxiliary agent is one or more in film forming agent, preservative agent, dispersant, surfactant and solvent.
10. the preparation method of a kind of fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus according to claim 2, it is characterized in that: in described step (5), in the fabric finishing agent prepared for raw material with the flowers and fruits of sweet osmanthus, the total content of sweet osmanthus flavouring agent, sweet osmanthus natural colouring matter, sweet osmanthus antioxidant, sweet osmanthus antioxidant and sweet osmanthus antiseptic is higher than 12%.
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Effective date of registration: 20201218 Address after: No.18-91, Gongye Road, South Taihu high tech Industrial Park, Wuxing District, Huzhou City, Zhejiang Province Patentee after: Zhejiang julibao Textile Technology Co., Ltd Address before: 215000 2 Taishan Road, high tech Zone, Suzhou, Jiangsu (Room 101 and 201, zone A, test center, Poji science and Technology Pioneer Park) Patentee before: SUZHOU INSILK Co.,Ltd. |