CN105541463A - Kang polyphenol-containing organic water soluble fertilizer and preparation method thereof - Google Patents
Kang polyphenol-containing organic water soluble fertilizer and preparation method thereof Download PDFInfo
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- CN105541463A CN105541463A CN201510940420.2A CN201510940420A CN105541463A CN 105541463 A CN105541463 A CN 105541463A CN 201510940420 A CN201510940420 A CN 201510940420A CN 105541463 A CN105541463 A CN 105541463A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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Abstract
The invention discloses Kang polyphenol-containing organic water soluble fertilizer and a preparation method thereof. The Kang polyphenol-containing organic water soluble fertilizer is prepared from 10-15% by mass of a waste liquid of molasses, 6-8% by mass of soluble nitrogenous fertilizer, 20-22% by mass of potassium dihydrogen phosphate, 5.1-10.2% by mass of a soluble trace metal salt, 6-8% by mass of boric acid, 5-8% by mass of an organic acid, 0.5-0.8% by mass of Kang polyphenol, 2-5% by mass of a surfactant, 0.5-1% by mass of an organic solvent and the balance water. The Kang polyphenol-containing organic water soluble fertilizer belongs to novel eco-friendly high-efficiency organic water soluble fertilizer, effectively improves disease resistance of wheat crops, reduces dry hot air-caused wheat damage, prevents wheat premature senility, improves wheat quality and improves a yield.
Description
Technical field
The present invention relates to agricultural fertilizer production technical field, particularly relate to a kind of organic water-soluble fertilizer containing health polyphenol and preparation method thereof.
Background technology
Along with the mankind increase day by day to the demand of wheat, and cultivated area presents the trend reduced year by year, and therefore wheat has vital meaning for China's agriculture production.Wheat needs fertile more crop, and the required nutritive element of Growth of Wheat has 16 kinds, and per forms 1 ton of dry-matter, needs absorption 232 grams of iron, 18 grams of boron, 26 grams of manganese, 8 grams of copper, 21 grams of zinc, 0.87 gram of molybdenum.Wheat has the fertilizer practice in corresponding period in different growing, and bulk application before general sowing, execute seed manure during sowing, turn green to the jointing stage and see that seedling topdresses, jointing stage to heading stage executes booting fertilizer, and the filling stage sprays foliage fertilizer.In the watery stage, during wheat root receptivity difference, foliage spray more directly effectively, can reduce hot dry wind to the harm of wheat with prevent the harm such as wheat early ageing simultaneously.
Hot dry wind is a kind of high temperature in Growth of Wheat later stage, low humidity with the agrometeorological hazard weather of certain wind-force.Wheat in hot dry wind process, Transpiration Intensity increase, moisture supply-demand imbalance, normal physiological activity is suppressed or destroys, and impels Wheat in Grain Filling Stage to shorten, thousand seed weight decline, can make time serious wheat green grass or young crops dry force ripe.Early ageing is one of major casualty of Wheat Production, and the phenomenon of wheat early ageing in recent years occurs again and again.Research shows, early ageing is caused by reasons such as later stage fertility deficiency, disease and pest, hot dry wind, bacterial wilts.Continuous high temperature and hot dry wind harm, cause plant lack of moisture, chlorophyll declines, and then plant early ageing, reduces output.Therefore, find a kind of volume increase foliage fertilizer preventing and treating Dry-hot winds, anti-early ageing, become a problem in the urgent need to address.
Summary of the invention
The object of the invention is to the shortcoming and defect overcoming above-mentioned prior art, there is provided a kind of and can improve the disease-resistant of wheat and resistance, prevent hot dry wind and early ageing to the harm of wheat, reach the organic water-soluble fertilizer containing health polyphenol increasing wheat yield and improve wheat quality.
Another object of the present invention is, provides a kind of preparation method that can be equipped with the above-mentioned organic water-soluble fertilizer containing health polyphenol simply, easily.
For reaching this object, the present invention by the following technical solutions:
Containing an organic water-soluble fertilizer for health polyphenol, be that raw material is prepared from by following mass percent: molasses waste liquid is 10% ~ 15%; Solubility nitrogenous fertilizer is 6% ~ 8%; Potassium primary phosphate is 20% ~ 22%; Solubility micro-metals salt is 5.1% ~ 10.2%; Boric acid is 6% ~ 8%; Organic acid is 5% ~ 8%; Health polyphenol is 0.5% ~ 0.8%; Tensio-active agent is 2% ~ 5%; Organic solvent is 0.5% ~ 1%; Surplus is water.
Described solubility nitrogenous fertilizer is urea.Urea is a kind of easily preservation, easy to use, little to the destruction of soil, is applicable to the neutral fertilizer of various soil and plant, and urea is that usage quantity is comparatively large at present, the nitrogenous fertilizer that nitrogen content is the highest.
Described molasses waste liquid is cane molasses alcohol slops.Containing large amount of organic compositions such as () sugar, crude protein, colloids in cane molasses alcohol slops, use cane molasses alcohol slops, as mother liquor, can provide required nutrient to farm crop.
Described solubility micro-metals salt is cupric nitrate, manganous nitrate, zinc nitrate and ammonium molybdate.Copper is that plant normal growth breeds necessary micronutrient element, is multiple oxidasic moiety in plant materials.It goes back the respiration of involved in plant, and have influence on the utilization of crop to iron, therefore copper and chlorophyll formation have close relationship.
The physiological action of trace element manganese to plant is many-sided, and it can participate in photolysis, improves the respiratory intensity of plant, promotes the hydrolysis of carbohydrate; Control agent internal oxidition reduction process; Promote the early growth of seed germination and seedling; Can also accelerate to sprout and maturation, increase the validity of phosphorus and calcium.In nitrogen metabolism, trace element zinc can change the ratio of organonitrogen and inorganic nitrogen in plant materials well, greatly improves drought-resistant, cryophylactic ability, promotes branches and leaves healthy growth.Trace element molybdenum all contains in the nitrate reductase of higher plant and the nitrogenase of biological nitrogen fixation, and the fertilizer abundance containing molybdenum element can improve nitrogen fixing capacity greatly, improves protein content; The toxic action can also urged nearly photosynthetic intensity simultaneously and eliminate active aluminum in acid soil to accumulate in plant materials and produce.
Described organic acid be citric acid, acetic acid and grape acid one or more.Organic acid can carry out sequestering action with trace element, improves plant to fertilizer absorption rate.
Described health polyphenol is the crude benzene phenols plant-growth regulator contained in plant materials, and described health polyphenol has significant degeneration-resistant induction usefulness in wheat growth, growth, maturation, old and feeble period.When wheat runs into hot dry wind, health polyphenol can induce the expression of drought resisting and heat resistanceheat resistant gene, suppresses transpiration, keeps the moisture content in wheat body, thus reduces hot dry wind to the harm of wheat; Described health polyphenol, as a kind of growth stimulant, also has remarkable effect to wheat Senescence manipulation, uses, can effectively prevent wheat early ageing in period boot stage to filling stage.
Described tensio-active agent is one or more in Tween-60, OP-10 and peregal O-9.As long as tensio-active agent a kind ofly significantly can change superficiality tensio-active agent matter or the material of character that is related to this, that derive from thus under low concentration.
Described organic solvent is one or more of ethanol, glycerine and dimethylformamide.Organic solvent is a class organic compound that can dissolve some water-fast materials.
The pH value of regulator solution is 3 ~ 7, and construction acidity or neutral chemical environment prepare fertilizer.
Prepare a method for the organic water-soluble fertilizer containing health polyphenol, comprise the following steps:
A, molasses waste liquid, solubility micro-metals salt, boric acid and organic acid added in suitable quantity of water be heated to 40 DEG C ~ 60 DEG C, be stirred well to and dissolve completely, be mixed with mother liquor;
B, described mother liquor add urea and potassium primary phosphate and are stirred to and dissolve completely at 40 DEG C ~ 60 DEG C, obtain mixed liquid B 1;
The mixed liquid B 1 that C, step B obtain adds tensio-active agent at 45 DEG C ~ 60 DEG C, and abundant stirring and adjusting, to appropriate pH, obtains mixed solution C1;
D, health polyphenol to be mixed with organic solvent, be stirred to after fully dissolving, add the mixed solution C1 that step C obtains, after stirring, obtain the organic water-soluble fertilizer containing health polyphenol.
The present invention adopts liquid molasses to be raw material, and various trace elements and organic acid complex role can promote the growth of little wheat crops, ratio science, comprehensive nutrition, can meet the various nutritive elements needed for wheat preferably.Add health polyphenol and effectively improve the disease-resistant of wheat and resistance, reduction hot dry wind is to the harm of wheat and prevent wheat early ageing.Add urea and potassium primary phosphate, wherein nitrogen, phosphorus and potassium content are high, with low cost.Under trace element and organic acid sequestering action, good stability, improves wheat to fertilizer absorption rate.This component and ratio are the problems for the little wheat crops of China ubiquitous nutritive element ratio serious unbalance, select suitable component and proportioning, effectively avoid the strain fringe quality causing wheat class due to the disappearance of some nutritive element low, the series of problems such as production declining.
Preparation method of the present invention, simple to operate, do not need to use special instrument and equipment, the above-mentioned organic water-soluble fertilizer containing health polyphenol can be produced.
Embodiment
Technical scheme of the present invention is further illustrated below by embodiment.
Embodiment 1
The organic water-soluble fertilizer containing health polyphenol of preparation 1000 kilograms of the present embodiment, comprises the following steps:
A, 110 kilograms of liquid molasses (11%), 20 kilograms of cupric nitrates (2%), 30 kilograms of manganous nitrates (3%), 30 kilograms of zinc nitrates (3%), 70 kilograms of boric acid (7%), 2 kilograms of ammonium molybdates (0.2%) and 60 kilograms of citric acids (6%) are added in 358 kg of water (35.8%) be heated to 40 DEG C ~ 60 DEG C, be stirred well to and dissolve completely, be mixed with mother liquor;
At 40 DEG C ~ 60 DEG C, add 70 kilograms of urea (7%) and 210 kg of phosphoric acid potassium dihydrogens (21%) in B, described mother liquor be stirred to and dissolve completely, obtain mixed liquid B 1;
C, described mixed solution add 30 kilograms of OP-10 (3%) at 45 DEG C ~ 60 DEG C, and abundant stirring and adjusting, to appropriate pH, obtains mixed solution C1;
D, 5 kilograms of health polyphenol (0.5%) to be mixed with 5 kg ethanol (0.5%), be stirred to after fully dissolving, add the mixed solution C1 that step C obtains, after stirring, obtain the organic water-soluble fertilizer containing health polyphenol.
Wherein, the number such as copper, manganese, zinc, molybdenum the adding of several trace element, for farm crop provide the various trace elements needed for growth, fertilizer is balanced, has vital role to short root strong sprout, activating soil, increasing of quality and production.Described urea and potassium primary phosphate are the source of macroelement N, P and K in the present invention; Trace element and organic acid sequestering action, improve wheat greatly to fertilizer absorption rate; Described health polyphenol is the crude benzene phenols plant-growth regulator contained in plant materials, in wheat growth, growth, maturation, old and feeble period, there is significant degeneration-resistant induction usefulness, reduction hot dry wind is to the harm of wheat and prevent wheat early ageing, thus significantly improves the crop yield of wheat class and improves crop quality.
The organic water-soluble fertilizer containing health polyphenol of the present embodiment is tested wheat increase yield effect at the wheat paddock in Xi Chang village of great Ying township, Weizhi County, Henan Province.
Experimental field physical features is smooth, and soil fertility is even, and great soil group is sand soil, and quality is sandy loam, and fertility is low.This field basis soil sample result of laboratory test is: organic 8.8g/kg, full nitrogen 0.83g/kg, available phosphorus 10.6mg/kg, available potassium 82.5mg/kg, and pH value 8.2 is wheat for studying thing, and kind is short anti-58 (a kind of common wheat breeds).Test period is year May in April, 2015 to 2015, and 3 process are established in test altogether.Process 1 is conventional fertilizer application contrast (not spraying any fertilizer); Process 2 is for conventional fertilizer application and spray the organic water-soluble fertilizer containing health polyphenol prepared by the present embodiment, spraying concentration be 1:1500 doubly, spray 3 times altogether, plot area 40m
2.Spray April 18 (blooming stage) in 2015, April 28 (filling stage) and May 11 (filling stage); Process 3 is for conventional fertilizer application and spray equivalent clear water the same period with process 2.Investigate the impact of organic water-soluble fertilizer of the present invention on wheat grains per spike, thousand seed weight and output, concrete data are in table 1 and table 2.
The organic water-soluble fertilizer containing health polyphenol of table 1, the present embodiment mainly becomes to produce the impact of factor on wheat
The organic water-soluble fertilizer containing health polyphenol of table 2, the present embodiment is on the impact of wheat yield
As can be seen from Table 1, on the basis that mu number of productive ear is identical, the process 2 spraying the organic water-soluble fertilizer of the present embodiment all increases by 1.8 than the wheat grains per spike of process 1, process 3, and process 2 increases 1.8g, 1.7g respectively than the thousand grain weight of wheat of process 1, process 3.Illustrate on the basis of conventional fertilizer application, the organic water-soluble fertilizer spraying the present embodiment adds grain number per spike and the thousand seed weight of wheat.
As can be seen from Table 2, spray the process 2 of the organic water-soluble fertilizer of the present embodiment respectively than process 1, process 3 mu volume increase 41.7kg, 40.0kg, stimulation ratio is respectively 9.1%, 8.7%, between process, volume variance all reaches conspicuous level, illustrates that the organic water-soluble fertilizer spraying the present embodiment has remarkable production-increasing function to wheat.
Embodiment 2
The organic water-soluble fertilizer containing health polyphenol of preparation 1000 kilograms of the present embodiment, comprises the following steps:
A, 120 kg liquid molasses (12%), 20 kilograms of cupric nitrates (2%), 30 kilograms of manganous nitrates (3%), 30 kilograms of zinc nitrates (3%), 60 kilograms of boric acid (6%), 2 kilograms of ammonium molybdates (0.2%) and 50 kilograms of citric acids (5%) are added in 362 kg of water (36.2%) be heated to 40 DEG C ~ 60 DEG C, be stirred well to and dissolve completely, be mixed with mother liquor;
B, described mother liquor add 60 kilograms of urea (6%) and 200 kg of phosphoric acid potassium dihydrogens (20%) and are stirred to and dissolve completely at 40 DEG C ~ 60 DEG C, obtain mixed liquid B 1;
C, described mixed solution add 25 kilograms of OP-10 (2.5%) and 25 kilograms of paregal Os-9 (2.5%) at 45 DEG C ~ 60 DEG C, and abundant stirring and adjusting, to appropriate pH, obtains mixed solution C1;
D, 8 kilograms of health polyphenol (0.8%) to be mixed with 8 kg of glycerin (0.8%), be stirred to after fully dissolving, add the mixed solution C1 that step C obtains, after stirring, obtain the organic water-soluble fertilizer containing health polyphenol.
The organic water-soluble fertilizer containing health polyphenol of the present embodiment is tested wheat increase yield effect at the wheat paddock in Shi Fo village of village township, position, Huojia County, Henan Province.
Supply examination soil to be moisture soil, physical features is smooth, and fertility is even.This field basis soil sample result of laboratory test is: organic 28.2g/kg, full nitrogen 1.27g/kg, and available phosphorus 31.9mg/kg, available potassium 183.0mg/kg, pH value 8.21, be wheat for studying thing, kind is all wheats 22 (a kind of common wheat breed).Test period is year May in April, 2015 to 2015, and 3 process are established in test altogether.Process 1 is conventional fertilizer application contrast (not spraying any fertilizer); Process 2 is for conventional fertilizer application and spray the organic water-soluble fertilizer containing health polyphenol prepared by the present embodiment, spraying concentration be 1:1500 doubly, spray 3 times altogether, plot area 40m
2.Spray April 26 (blooming stage) in 2015, May 5 (filling stage) and May 13 (filling stage); Process 3 is for conventional fertilizer application and spray equivalent clear water the same period with process 2.Each process on May 28 community is randomly drawed 20 strains and is carried out biological character investigation, and June 2, maturation was gathered in the crops, and meter product received by results Shi Ge community list.Investigate the impact of organic water-soluble fertilizer of the present invention on wheat grains per spike, thousand seed weight and output, concrete data are in table 3 and table 4.
The organic water-soluble fertilizer containing health polyphenol of table 3, the present embodiment is on wheat Growth Character and the impact becoming product factor
The organic water-soluble fertilizer containing health polyphenol of table 4, the present embodiment is on the impact of wheat yield
As shown in Table 3, spray the process 2 of the organic water-soluble fertilizer of the present embodiment with process 1, process compared with in the of 3, plant height increases 1.8cm, 1.6cm respectively, spike length increases 0.8cm, 0.7cm respectively, grain number per spike increases by 1.8,1.6 respectively, and thousand seed weight increases 2.3g, 2.2g respectively, and this illustrates on the basis of conventional fertilizer application, wheat sprays the organic water-soluble fertilizer energy wheat growth-promoting of the present embodiment, increases plant height, spike length, grain number per spike and thousand seed weight.
As shown in Table 4, spray the process 2 of the organic water-soluble fertilizer of the present embodiment with process 1, process compared with in the of 3, the volume increase of average mu 43.3kg, 37.8kg, stimulation ratio is 8.5%, 7.3%, and between process, volume variance all reaches pole conspicuous level.Illustrate that organic water-soluble fertilizer that wheat sprays the present embodiment significantly can increase the output of wheat.
In sum, spraying organic water-soluble fertilizer of the present invention not only can increase Plant Height in Wheat, significantly improves the quality of wheat, but also increases the output of wheat, thus increases substantially economic benefit.。
Wherein a kind of tensio-active agent Tween60 of the present invention is polyoxyethylene sorbitan ether stearate; Wherein a kind of tensio-active agent paregal O-9 of the present invention is fatty alcohol-polyoxyethylene ether O-9; Wherein a kind of Surfactant OP-10 of the present invention is alkylphenol-polyethenoxy (10) ether.
Compared with the existing technology, tool has the following advantages in the present invention:
This kind of organic water-soluble fertilizer is obtained under organic acid sequestering action by liquid molasses, various trace elements, and trace element is complete, stable performance.It, except having multiple nutritional components required in wheat class crop growth process, also adds tensio-active agent especially, reduces the surface tension of fertilizer and wheat leaf blade wax layer, improves Crop utilization ratio; The health polyphenol added has significant degeneration-resistant induction usefulness in wheat growth, growth, maturation, old and feeble period, on the one hand, when wheat runs into hot dry wind, health polyphenol can induce the expression of drought resisting and heat resistanceheat resistant gene, suppress transpiration, keep the moisture content in wheat body, thus reduce hot dry wind to the harm of wheat; On the other hand, health polyphenol, as a kind of growth stimulant, also has remarkable effect to wheat Senescence manipulation, use in period boot stage to filling stage, can effectively prevent wheat early ageing, thus the health polyphenol added effectively improves the quality of wheat and improves output, realizes wheat increase yield and increases income; The compatibility of macroelement N, P, K and various trace elements, proportioning science and balanced in nutrition, the active high crop utilization ratio of fertilizer nutrient is high, can meet the various nutritive elements needed for wheat preferably, promote the growth of wheat and the growth of particle, strengthen the cold tolerance of plant.Because this kind of fertilizer possesses above-mentioned multiple advantage, and reasonable price, the market competitiveness is strong, and its market outlook are very wide.
Below know-why of the present invention is described in conjunction with specific embodiments.These describe just in order to explain principle of the present invention, and can not be interpreted as limiting the scope of the invention by any way.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other embodiment of the present invention, and these modes all will fall within protection scope of the present invention.
Claims (9)
1. containing the organic water-soluble fertilizer of health polyphenol, it is characterized in that: be that raw material is prepared from by following mass percent: molasses waste liquid is 10% ~ 15%; Solubility nitrogenous fertilizer is 6% ~ 8%; Potassium primary phosphate is 20% ~ 22%; Solubility micro-metals salt is 5.1% ~ 10.2%; Boric acid is 6% ~ 8%; Organic acid is 5% ~ 8%; Health polyphenol is 0.5% ~ 0.8%; Tensio-active agent is 2% ~ 5%; Organic solvent is 0.5% ~ 1%; Surplus is water.
2. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described solubility nitrogenous fertilizer is urea.
3. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described molasses waste liquid is cane molasses alcohol slops.
4. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described solubility micro-metals salt is cupric nitrate, manganous nitrate, zinc nitrate and ammonium molybdate.
5. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described organic acid be citric acid, acetic acid and grape acid one or more.
6. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described tensio-active agent is one or more in Tween-60, OP-10 and peregal O-9.
7. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: described organic solvent is one or more of ethanol, glycerine and dimethylformamide.
8. a kind of organic water-soluble fertilizer containing health polyphenol according to claim 1, is characterized in that: its pH value is 3 ~ 7.
9. prepare a method for the organic water-soluble fertilizer containing health polyphenol, it is characterized in that: comprise the following steps:
A, molasses waste liquid, solubility micro-metals salt, boric acid and organic acid added in suitable quantity of water be heated to 40 DEG C ~ 60 DEG C, be stirred well to and dissolve completely, be mixed with mother liquor;
B, described mother liquor add urea and potassium primary phosphate and are stirred to and dissolve completely at 40 DEG C ~ 60 DEG C, obtain mixed liquid B 1;
The mixed liquid B 1 that C, step B obtain adds tensio-active agent at 45 DEG C ~ 60 DEG C, and abundant stirring and adjusting, to appropriate pH, obtains mixed solution C1;
D, health polyphenol to be mixed with organic solvent, be stirred to after fully dissolving, add the mixed solution C1 that step C obtains, after stirring, obtain the organic water-soluble fertilizer containing health polyphenol.
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Cited By (1)
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| CN109180344A (en) * | 2018-10-22 | 2019-01-11 | 德州市农业科学研究院 | A kind of mix preparation that resisting wheat cold spell in later spring and its preparation and spraying method |
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Application publication date: 20160504 |
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| RJ01 | Rejection of invention patent application after publication |