CN105524697A - 一种汽车座椅滑轨润滑脂及其制备方法 - Google Patents

一种汽车座椅滑轨润滑脂及其制备方法 Download PDF

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CN105524697A
CN105524697A CN201610037978.4A CN201610037978A CN105524697A CN 105524697 A CN105524697 A CN 105524697A CN 201610037978 A CN201610037978 A CN 201610037978A CN 105524697 A CN105524697 A CN 105524697A
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sliding rail
automobile seat
acid
sulfonate
base oil
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严冲
谢刚
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NATOR LUBRICATION TECHNOLOGY JIANGSU CO., LTD.
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Abstract

本发明公开了一种汽车座椅滑轨润滑脂,该润滑脂由如下重量百分数的组分组成:基础油52%~65%;磺酸盐26%~33%;结构改善剂6%~10%;稠化剂3%~5%。本发明的润滑脂采用食品级的基础油,无气味、对人体无伤害,高低温性能优越,能满足汽车座椅滑轨在极端环境下使用;高碱值合成磺酸钙具有优异的极压抗磨性能,对人体无伤害,无需再添加高成本的固体润滑剂即可起到抗磨、减摩以及降噪的效果;结构改善剂能有效改善产品的稠化能力,并缩短生产时间;稠化剂能进一步提高产品的抗磨、减摩性能,并具有良好的泵送性;原料便宜易得,制备方法简单易控,极大地提高了产品的生产效率。

Description

一种汽车座椅滑轨润滑脂及其制备方法
技术领域
本发明属于润滑与密封材料领域,涉及一种润滑脂,更具体而言,涉及一种汽车座椅滑轨润滑脂及其制备方法。
背景技术
随着汽车工业的快速发展,汽车零部件产业也正处于高速发展阶段。汽车座椅是汽车内饰中比较重要的零部件,现代化汽车越来越要求其多功能性、舒适性和可调节性,这就要求汽车座椅的集成度越来越高,对润滑的要求也越来越高。驾驶员需要前后调整座椅位置时,要求座椅在滑轨上的运动平滑,顺畅,力矩小于100N·m,不会产生吱吱的噪音,能够保证在调整座椅前后位置时滑轨上的低摩擦系数、低磨损及低噪音。滑槽内为金属与金属之间的摩擦,当座椅完全的前推和后移时,会有一部分裸露在外面,传统的润滑脂在该部分裸露时气味较大,且润滑的长效性不是很好,一段时间后部件磨损严重;同时,在高温环境下容易渗油,污染布料和地毯,影响车内的整洁和美观度。
发明内容
本发明所要解决的技术问题是提供一种具有优异极压抗磨性能、高低温性能和润滑性能,对人体无伤害的汽车座椅滑轨润滑脂及其制备方法。
为解决上述技术问题,本发明采用的技术方案是:
一种汽车座椅滑轨润滑脂,该润滑脂由如下重量百分数的组分组成:
基础油52%~65%;
磺酸盐26%~33%;
结构改善剂6%~10%;
稠化剂3%~5%;
其中,基础油为食品级的癸二酸酯、壬二酸酯、聚α烯烃中的一种或多种的混合物。
上述磺酸盐为直链型高碱值烷基苯磺酸钙、支链型高碱值烷基苯磺酸钙、高碱值合成二烷基苯磺酸钙中的一种或多种的混合物。
上述结构改善剂为水、乙醇、正丁醇、磷酸、12-羟基硬脂酸、醋酸、十二烷基苯磺酸中的一种或多种的混合物。
上述稠化剂为氢氧化钙、癸二酸、壬二酸、硼酸、硬脂酸、12-羟基硬脂酸中的一种或多种的混合物。
上述汽车座椅滑轨润滑脂的制备方法,包括以下步骤:
将基础油总量的50~70%和磺酸盐投入反应釜内,搅拌加热至60~70℃,混合均匀后加入结构改善剂,在60~70℃的温度下密闭搅拌60-70min,然后升温至90~100℃,再加入剩余基础油和稠化剂,继续升温至180~190℃,最后降温至85~90℃均质取样检测。
与现有技术相比,本发明的优点是:本发明的润滑脂采用食品级的基础油,无气味、对人体无伤害,高低温性能优越,能满足汽车座椅滑轨在极端环境下使用;磺酸盐采用高碱值合成磺酸钙,具有优异的极压抗磨性能,对人体无伤害,无需再添加高成本的固体润滑剂即可起到抗磨、减摩以及降噪的效果;采用的结构改善剂能有效改善产品的稠化能力,并缩短生产时间;采用的稠化剂能进一步提高产品的抗磨、减摩性能,并具有良好的泵送性;原料便宜易得,制备方法简单易控,极大地提高了产品的生产效率。
具体实施方式:
下面结合具体实施例对本发明进行详细描述,但这些实施例并不是对对本发明的限定。
实施例1
将35kg聚α烯烃、30kg直链型高碱值烷基苯磺酸钙投入反应釜内,搅拌加热至60℃,混合均匀后加入2kg十二烷基苯磺酸、5kg水和1kg磷酸混合液,在60℃的温度下密闭搅拌60min,然后升温至90℃,再分别加入22.1kg聚α烯烃、1.5kg硼酸、2kg12-羟基硬脂酸、1.4kg氢氧化钙,继续升温至180℃,最后降温至90℃均质取样检测。
实施例2
将33kg癸二酸酯、32kg直链型高碱值烷基苯磺酸钙投入反应釜内,搅拌加热至60℃,混合均匀后加入2kg十二烷基苯磺酸、5kg水和3kg乙醇混合液,在70℃的温度下密闭搅拌60min,然后升温至90℃,再分别加入20kg癸二酸酯、1.6kg癸二酸、2.2kg12-羟基硬脂酸、1.2kg氢氧化钙,继续升温至180℃,最后降温至90℃均质取样检测。
实施例3
将34kg聚α烯烃、31kg支链型高碱值烷基苯磺酸钙投入反应釜内,搅拌加热至63℃,混合均匀后加入2kg磷酸、1kg醋酸、5kg水和1kg正丁醇混合液,在70℃的温度下密闭搅拌60min,然后升温至100℃,再分别加入21.1kg聚α烯烃、1.6kg硼酸、2kg硬脂酸、1.3kg氢氧化钙,继续升温至180℃,最后降温至90℃均质取样检测。
实施例4
将33kg壬二酸酯、32kg高碱值合成二烷基苯磺酸钙投入反应釜内,搅拌加热至68℃,混合均匀后加入2kg磷酸、1kg醋酸、5kg水和1kg正丁醇混合液,在68℃的温度下密闭搅拌65min,然后升温至95℃,再分别加入21.1kg壬二酸酯、1.6kg壬二酸、2.1kg12-羟基硬脂酸、1.2kg氢氧化钙,继续升温至180℃,最后降温至90℃均质取样检测。
实施例5
将32kg聚α烯烃、31kg支链型高碱值烷基苯磺酸钙投入反应釜内,搅拌加热至70℃,混合均匀后加入2kg12-羟基硬脂酸、4kg水和1.3kg正丁醇混合液,在70℃的温度下密闭搅拌70min,然后升温至100℃,再分别加入25.8kg聚α烯烃、1.4kg硼酸、1.0kg硬脂酸、1.5kg氢氧化钙,继续升温至180℃,最后降温至90℃均质取样检测。
上述各实施例所制备得到的润滑脂根据测量方法所得的各种性能参数如下表所示:
从上表可知,本发明所制备的产品具有优异的极压抗磨性能,无气味、对人体无伤害,高低温性能优越,能满足汽车座椅滑轨在极端环境下使用。

Claims (5)

1.一种汽车座椅滑轨润滑脂,其特征在于,该润滑脂由如下重量百分数的组分组成:
基础油52%~65%;
磺酸盐26%~33%;
结构改善剂6%~10%;
稠化剂3%~5%;
其中,所述基础油为食品级的癸二酸酯、壬二酸酯、聚α烯烃中的一种或多种的混合物。
2.根据权利要求1所述的一种汽车座椅滑轨润滑脂,其特征在于:所述磺酸盐为直链型高碱值烷基苯磺酸钙、支链型高碱值烷基苯磺酸钙、高碱值合成二烷基苯磺酸钙中的一种或多种的混合物。
3.根据权利要求1所述的一种汽车座椅滑轨润滑脂,其特征在于:所述结构改善剂为水、乙醇、正丁醇、磷酸、12-羟基硬脂酸、醋酸、十二烷基苯磺酸中的一种或多种的混合物。
4.根据权利要求1所述的一种汽车座椅滑轨润滑脂,其特征在于:所述稠化剂为氢氧化钙、癸二酸、壬二酸、硼酸、硬脂酸、12-羟基硬脂酸中的一种或多种的混合物。
5.一种如权利要求1至4中任一项所述的汽车座椅滑轨润滑脂的制备方法,其特征在于,包括以下步骤:
将基础油总量的50~70%和磺酸盐投入反应釜内,搅拌加热至60~70℃,混合均匀后加入结构改善剂,在60~70℃的温度下密闭搅拌60-70min,然后升温至90~100℃,再加入剩余基础油和稠化剂,继续升温至180~190℃,最后降温至85~90℃均质取样检测。
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