CN105505089A - Durable interior wall moldproof coating and preparation method thereof - Google Patents
Durable interior wall moldproof coating and preparation method thereof Download PDFInfo
- Publication number
- CN105505089A CN105505089A CN201511026956.XA CN201511026956A CN105505089A CN 105505089 A CN105505089 A CN 105505089A CN 201511026956 A CN201511026956 A CN 201511026956A CN 105505089 A CN105505089 A CN 105505089A
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- ethyl
- ergosterol
- rosin
- deionized water
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D145/00—Coating compositions based on homopolymers or copolymers of compounds having no unsaturated aliphatic radicals in a side chain, and having one or more carbon-to-carbon double bonds in a carbocyclic or in a heterocyclic system; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a durable interior wall moldproof coating. The durable interior wall moldproof coating is prepared from the following raw materials in parts by weight: 4-8 parts of ergosterol, 2.5-6.4 parts of rosin, 5-10 parts of terpene resin, 2.5-6.4 parts of ethyl chrysanthemate, 6.4-7.4 parts of deionized water, 1.5-4.6 parts of 2-ethyl-1,3-hexanediol, 1.4-2.8 parts of ethyl vanillin, 3.7-6.2 parts of phenethyl phenylpropylphenol polyoxyethylene ether, 2.5-5 parts of acrylic resin modified casein film forming agent and 1.5-3.6 parts of tetraisopropyl orthotitanate. Compared with an existing product, the durable interior wall moldproof coating has the advantages that ergosterol and ethyl vanillin are added, the emulsion paint finished product has good antibacterial effect and strong mildew resistance after the ergosterol and ethyl vanillin are mixed, and raw material ingredients such as terpene resin, 2-ethyl-1,3-hexanediol and tetraisopropyl orthotitanate are low in cost, so that the emulsion paint finished product is low in cost; and meanwhile, the raw materials do not contain ingredients such as formaldehyde and VOC, thereby being energy-saving and environment-friendly.
Description
Technical field
The present invention relates to a kind of durable inner wall mold-proof paint and preparation method thereof, belong to building material field.
Background technology
Emulsion paint is also called synthetic resin emulsion coating, is the one of organic coating, is be that base-material adds the formulated class water-borne coatings of pigment, filler and various auxiliary agent with synthetic resin emulsion.Prior art in environmental protection, improve opacifying power, improve in color and luster etc. and all achieve certain progress, but also Shortcomings: the most anti-microbial property of emulsion paint is poor, and production cost is higher simultaneously.
Summary of the invention
For the deficiency that prior art exists, technical problem to be solved by this invention is, provides a kind of durable inner wall mold-proof paint and preparation method thereof, good anti-bacterial effect, with low cost, energy-conserving and environment-protective.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of durable inner wall mold-proof paint, be made up of the raw material of following parts by weight: ergosterol 4-8 part, rosin 2.5-6.4 part, terpine resin 5-10 part, ethyl chrysanthemate 2.5-6.4 part, deionized water 6.4-7.4 part, 2-ethyl-1,3-hexylene glycol 1.5-4.6 part, vanirone 1.4-2.8 part, styroyl hydrocinnamyl phenol polyethenoxy ether 3.7-6.2 part, acrylic resin modification casein filming agent 2.5-5 part and original four-isopropyl titanate 1.5-3.6 part.
Optimize, above-mentioned durable inner wall mold-proof paint, be made up of the raw material of following parts by weight: ergosterol 6 parts, rosin 4.8 parts, terpine resin 7 parts, ethyl chrysanthemate 5.2 parts, deionized water 6.7 parts, 2-ethyl-1,3-hexylene glycol 3.6 parts, vanirone 1.8 parts, styroyl hydrocinnamyl phenol polyethenoxy ether 4.8 parts, acrylic resin modification casein filming agent 3.7 parts and original four-isopropyl titanate 2.8 parts.
A preparation method for durable inner wall mold-proof paint, comprises the following steps:
1) take ergosterol, rosin and terpine resin by above-mentioned formula ratio, after adding deionized water, one piece is placed in stirring tank, after the high-speed stirring of 1-2 hour, be cooled to room temperature;
2) ethyl chrysanthemate of formula ratio and 2-ethyl-1,3-hexylene glycol are added stirring tank, carry out dispersion with 600-700r/min and stir 25-30min, be then heated to 45-50 DEG C;
3) take vanirone and styroyl hydrocinnamyl phenol polyethenoxy ether by formula ratio, add in the mixture in previous step;
4) mixture in previous step is placed in ultrasonic extractor, open ultrasonic generator, adjustment ultrasonic frequency vibratory is 35KHz, delivering vapor heating in ultrasonic extractor, temperature of charge in ultrasonic extractor is made to rise to 100 DEG C, maintain this temperature and continue heating after 40 minutes to 50 minutes, steam off valve stops heating;
5) take acrylic resin modification casein filming agent and original four-isopropyl titanate, put into the mixture that previous step is crossed through ultrasonication, be heated to 45-48 DEG C, after insulation 10-20min, be cooled to room temperature.
The present invention is compared with existing product, owing to adding ergosterol and vanirone, emulsion paint finished product good anti-bacterial effect is made after both and mixing, resistance to performance of going mouldy is strong, the component materials such as terpine resin, 2-ethyl-1,3-hexylene glycol and original four-isopropyl titanate are with low cost, make emulsion paint product cost low, and owing to not containing the composition such as formaldehyde and VOC in raw material, energy-conserving and environment-protective.
Embodiment
Embodiment 1
The present invention is a kind of durable inner wall mold-proof paint, be made up of the raw material of following parts by weight: ergosterol 4 parts, rosin 2.5 parts, terpine resin 5 parts, ethyl chrysanthemate 2.5 parts, deionized water 6.4 parts, 2-ethyl-1,3-hexylene glycol 1.5 parts, vanirone 1.4 parts, styroyl hydrocinnamyl phenol polyethenoxy ether 3.7 parts, acrylic resin modification casein filming agent 2.5 parts and original four-isopropyl titanate 1.5 parts.
A preparation method for durable inner wall mold-proof paint, comprises the following steps:
1) take ergosterol, rosin and terpine resin by above-mentioned formula ratio, after adding deionized water, one piece is placed in stirring tank, after the high-speed stirring of 1 hour, be cooled to room temperature;
2) ethyl chrysanthemate of formula ratio and 2-ethyl-1,3-hexylene glycol are added stirring tank, carry out dispersion with 600r/min and stir 25min, be then heated to 45 DEG C;
3) take vanirone and styroyl hydrocinnamyl phenol polyethenoxy ether by formula ratio, add in the mixture in previous step;
4) mixture in previous step is placed in ultrasonic extractor, open ultrasonic generator, adjustment ultrasonic frequency vibratory is 35KHz, delivering vapor heating in ultrasonic extractor, temperature of charge in ultrasonic extractor is made to rise to 100 DEG C, maintain this temperature and continue heating after 40 minutes, steam off valve stops heating;
5) take acrylic resin modification casein filming agent and original four-isopropyl titanate, put into the mixture that previous step is crossed through ultrasonication, be heated to 45 DEG C, after insulation 10min, be cooled to room temperature.
Embodiment 2
The present invention is a kind of durable inner wall mold-proof paint, be made up of the raw material of following parts by weight: ergosterol 8 parts, rosin 6.4 parts, terpine resin 10 parts, ethyl chrysanthemate 6.4 parts, deionized water 7.4 parts, 2-ethyl-1,3-hexylene glycol 4.6 parts, vanirone 2.8 parts, styroyl hydrocinnamyl phenol polyethenoxy ether 6.2 parts, acrylic resin modification casein filming agent 5 parts and original four-isopropyl titanate 3.6 parts.
A preparation method for durable inner wall mold-proof paint, comprises the following steps:
1) take ergosterol, rosin and terpine resin by above-mentioned formula ratio, after adding deionized water, one piece is placed in stirring tank, after the high-speed stirring of 2 hours, be cooled to room temperature;
2) ethyl chrysanthemate of formula ratio and 2-ethyl-1,3-hexylene glycol are added stirring tank, carry out dispersion with 700r/min and stir 30min, be then heated to 50 DEG C;
3) take vanirone and styroyl hydrocinnamyl phenol polyethenoxy ether by formula ratio, add in the mixture in previous step;
4) mixture in previous step is placed in ultrasonic extractor, open ultrasonic generator, adjustment ultrasonic frequency vibratory is 35KHz, delivering vapor heating in ultrasonic extractor, temperature of charge in ultrasonic extractor is made to rise to 100 DEG C, maintain this temperature and continue heating after 50 minutes, steam off valve stops heating;
5) take acrylic resin modification casein filming agent and original four-isopropyl titanate, put into the mixture that previous step is crossed through ultrasonication, be heated to 48 DEG C, after insulation 20min, be cooled to room temperature.
Embodiment 3
The present invention is a kind of durable inner wall mold-proof paint, be made up of the raw material of following parts by weight: ergosterol 6 parts, rosin 4.8 parts, terpine resin 7 parts, ethyl chrysanthemate 5.2 parts, deionized water 6.7 parts, 2-ethyl-1,3-hexylene glycol 3.6 parts, vanirone 1.8 parts, styroyl hydrocinnamyl phenol polyethenoxy ether 4.8 parts, acrylic resin modification casein filming agent 3.7 parts and original four-isopropyl titanate 2.8 parts.
A preparation method for durable inner wall mold-proof paint, comprises the following steps:
1) take ergosterol, rosin and terpine resin by above-mentioned formula ratio, after adding deionized water, one piece is placed in stirring tank, after the high-speed stirring of 1.5 hours, be cooled to room temperature;
2) ethyl chrysanthemate of formula ratio and 2-ethyl-1,3-hexylene glycol are added stirring tank, carry out dispersion with 650r/min and stir 28min, be then heated to 47 DEG C;
3) take vanirone and styroyl hydrocinnamyl phenol polyethenoxy ether by formula ratio, add in the mixture in previous step;
4) mixture in previous step is placed in ultrasonic extractor, open ultrasonic generator, adjustment ultrasonic frequency vibratory is 35KHz, delivering vapor heating in ultrasonic extractor, temperature of charge in ultrasonic extractor is made to rise to 100 DEG C, maintain this temperature and continue heating after 45 minutes, steam off valve stops heating;
5) take acrylic resin modification casein filming agent and original four-isopropyl titanate, put into the mixture that previous step is crossed through ultrasonication, be heated to 46 DEG C, after insulation 15min, be cooled to room temperature.
The finished product prepared by embodiment 1-3 carries out the test of following table properties, the results are shown in Table 1:
Can find out, indices all conformance with standard of coating of the present invention, have very strong abrasion resistance and wear resistance etc.Compared with existing product, owing to adding ergosterol and vanirone, emulsion paint finished product good anti-bacterial effect is made after both and mixing, resistance to performance of going mouldy is strong, the component materials such as terpine resin, 2-ethyl-1,3-hexylene glycol and original four-isopropyl titanate are with low cost, make emulsion paint product cost low, and owing to not containing the composition such as formaldehyde and VOC in raw material, energy-conserving and environment-protective.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (3)
1. a durable inner wall mold-proof paint, it is characterized in that: be made up of the raw material of following parts by weight: ergosterol 4-8 part, rosin 2.5-6.4 part, terpine resin 5-10 part, ethyl chrysanthemate 2.5-6.4 part, deionized water 6.4-7.4 part, 2-ethyl-1,3-hexylene glycol 1.5-4.6 part, vanirone 1.4-2.8 part, styroyl hydrocinnamyl phenol polyethenoxy ether 3.7-6.2 part, acrylic resin modification casein filming agent 2.5-5 part and original four-isopropyl titanate 1.5-3.6 part.
2. durable inner wall mold-proof paint according to claim 1, it is characterized in that: be made up of the raw material of following parts by weight: ergosterol 6 parts, rosin 4.8 parts, terpine resin 7 parts, ethyl chrysanthemate 5.2 parts, deionized water 6.7 parts, 2-ethyl-1,3-hexylene glycol 3.6 parts, vanirone 1.8 parts, styroyl hydrocinnamyl phenol polyethenoxy ether 4.8 parts, acrylic resin modification casein filming agent 3.7 parts and original four-isopropyl titanate 2.8 parts.
3. the preparation method of the durable inner wall mold-proof paint according to claims 1 or 2, comprises the following steps:
1) take ergosterol, rosin and terpine resin by above-mentioned formula ratio, after adding deionized water, one piece is placed in stirring tank, after the high-speed stirring of 1-2 hour, be cooled to room temperature;
2) ethyl chrysanthemate of formula ratio and 2-ethyl-1,3-hexylene glycol are added stirring tank, carry out dispersion with 600-700r/min and stir 25-30min, be then heated to 45-50 DEG C;
3) take vanirone and styroyl hydrocinnamyl phenol polyethenoxy ether by formula ratio, add in the mixture in previous step;
4) mixture in previous step is placed in ultrasonic extractor, open ultrasonic generator, adjustment ultrasonic frequency vibratory is 35KHz, delivering vapor heating in ultrasonic extractor, temperature of charge in ultrasonic extractor is made to rise to 100 DEG C, maintain this temperature and continue heating after 40 minutes to 50 minutes, steam off valve stops heating;
5) take acrylic resin modification casein filming agent and original four-isopropyl titanate, put into the mixture that previous step is crossed through ultrasonication, be heated to 45-48 DEG C, after insulation 10-20min, be cooled to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511026956.XA CN105505089A (en) | 2015-12-31 | 2015-12-31 | Durable interior wall moldproof coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511026956.XA CN105505089A (en) | 2015-12-31 | 2015-12-31 | Durable interior wall moldproof coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105505089A true CN105505089A (en) | 2016-04-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201511026956.XA Pending CN105505089A (en) | 2015-12-31 | 2015-12-31 | Durable interior wall moldproof coating and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103122160A (en) * | 2012-12-22 | 2013-05-29 | 桑达化工（南通）有限公司 | Exterior wall emulsion paint |
| CN104592849A (en) * | 2015-02-03 | 2015-05-06 | 安徽工业大学 | Multifunctional composite coating for lithium aluminate nanosheets |
| CN104927522A (en) * | 2015-06-15 | 2015-09-23 | 张家港市山牧新材料技术开发有限公司 | Fireproof oil paint |
-
2015
- 2015-12-31 CN CN201511026956.XA patent/CN105505089A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103122160A (en) * | 2012-12-22 | 2013-05-29 | 桑达化工（南通）有限公司 | Exterior wall emulsion paint |
| CN104592849A (en) * | 2015-02-03 | 2015-05-06 | 安徽工业大学 | Multifunctional composite coating for lithium aluminate nanosheets |
| CN104927522A (en) * | 2015-06-15 | 2015-09-23 | 张家港市山牧新材料技术开发有限公司 | Fireproof oil paint |
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Application publication date: 20160420 |