CN105385207A - New type interior wall paint and preparation method thereof - Google Patents

New type interior wall paint and preparation method thereof Download PDF

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Publication number
CN105385207A
CN105385207A CN201511015734.8A CN201511015734A CN105385207A CN 105385207 A CN105385207 A CN 105385207A CN 201511015734 A CN201511015734 A CN 201511015734A CN 105385207 A CN105385207 A CN 105385207A
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CN
China
Prior art keywords
parts
interior wall
latex
ethylene
titanium dioxide
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Pending
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CN201511015734.8A
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Chinese (zh)
Inventor
曲少春
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Individual
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Individual
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Priority to CN201511015734.8A priority Critical patent/CN105385207A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D4/00Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
    • C09D4/06Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Plant Pathology (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses new type interior wall paint, which is prepared from the following raw materials in parts by weight: 3.5 to 7.5 parts of acrylic ester, 5 to 10 parts of polyving akohol, 20 to 30 parts of latex, 10 to 15 parts of titanium dioxide, 5 to 8 parts of benzyl alcohol, 2.5 to 6.8 parts of capraldehyde, 8.5 to 9.8 parts of deionized water, 3.5 to 6.9 parts of octylphenol polyoxyethylene ether, 2.5 to 7.5 parts of butadiene resin film-forming agent and 1.5 to 4 parts of ethylene-vinyl acetate copolymer. Compared with the existing products, the antibacterial effect of a finished product of the emulsion paint is good due to the fact that the benzyl alcohol and the octylphenol polyoxyethylene ether are added and mixed, the mildew-resistant performance is strong, the cost of raw materials of ingredients such as the ethylene-vinyl acetate copolymer, the latex, the titanium dioxide and the like is low, so that the cost of the finished product of the emulsion paint is low, and energy conservation and environment protection are realized due to the fact that the raw materials do not contain ingredients such as formaldehyde, VOC and the like.

Description

A kind of Novel interior wall paint and preparation method thereof
Technical field
The present invention relates to a kind of Novel interior wall paint and preparation method thereof, belong to building material field.
Background technology
Emulsion paint is also called synthetic resin emulsion coating, is the one of organic coating, is be that base-material adds the formulated class water-borne coatings of pigment, filler and various auxiliary agent with synthetic resin emulsion.Prior art in environmental protection, improve opacifying power, improve in color and luster etc. and all achieve certain progress, but also Shortcomings: the most anti-microbial property of emulsion paint is poor, and production cost is higher simultaneously.
Summary of the invention
For the deficiency that prior art exists, technical problem to be solved by this invention is, provides a kind of Novel interior wall paint and preparation method thereof, good anti-bacterial effect, with low cost, energy-conserving and environment-protective.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of Novel interior wall paint, is made up of the raw material of following parts by weight: acrylate 3.5-7.5 part, polyvinyl alcohol 5-10 part, latex 20-30 part, titanium dioxide 10-15 part, phenylcarbinol 5-8 part, capraldehyde 2.5-6.8 part, deionized water 8.5-9.8 part, polyoxyethylene octylphenol ether 3.5-6.9 part, butadiene resin membrane-forming agent 2.5-7.5 part and ethylene-vinyl acetate copolymer 1.5-4 part.
Optimize, above-mentioned Novel interior wall paint, is made up of the raw material of following parts by weight: acrylate 5.8 parts, polyvinyl alcohol 7 parts, latex 25 parts, titanium dioxide 11.6 parts, phenylcarbinol 6.8 parts, capraldehyde 4.7 parts, deionized water 8.9 parts, polyoxyethylene octylphenol ether 4.8 parts, butadiene resin membrane-forming agent 5.1 parts and ethylene-vinyl acetate copolymer 2.8 parts.
A preparation method for Novel interior wall paint, comprises the following steps:
1) take acrylate and polyvinyl alcohol by above-mentioned formula ratio, after adding deionized water, one piece is placed in reactor, is heated to 70-80 DEG C, is incubated and leaves standstill 3-5 hour after 2-3 hour stirs;
2) latex of formula ratio and titanium dioxide are added reactor, carry out dispersion with 600-700r/min and stir 15-20min, be then heated to 55-60 DEG C;
3) mixed emulsion is cooled to 12-15 DEG C, takes phenylcarbinol and capraldehyde by formula ratio, add in the mixture in previous step, carry out dispersion with 500-600r/min and stir 20-25min;
4) take polyoxyethylene octylphenol ether and the butadiene resin membrane-forming agent of formula ratio, carry out dispersion with 600-700r/min and stir 15-20min, mixed emulsion is put into the sealed vessel that safety valve is housed and carry out ageing, leave standstill 4-5 days;
5) take ethylene-vinyl acetate copolymer, put into the mixture of previous step through ripening, be heated to 40-48 DEG C, be cooled to room temperature after insulation 20-30min, then pack, stamp, inspection, gets product.
The present invention is compared with existing product, owing to adding phenylcarbinol and polyoxyethylene octylphenol ether, emulsion paint finished product good anti-bacterial effect is made after both and mixing, resistance to performance of going mouldy is strong, the component materials such as ethylene-vinyl acetate copolymer, latex and titanium dioxide are with low cost, make emulsion paint product cost low, and owing to not containing the composition such as formaldehyde and VOC in raw material, energy-conserving and environment-protective.
Embodiment
embodiment 1
The present invention is a kind of Novel interior wall paint, is made up of the raw material of following parts by weight: acrylate 3.5 parts, polyvinyl alcohol 5 parts, latex 20 parts, titanium dioxide 10 parts, phenylcarbinol 5 parts, capraldehyde 2.5 parts, deionized water 8.5 parts, polyoxyethylene octylphenol ether 3.5 parts, butadiene resin membrane-forming agent 2.5 parts and ethylene-vinyl acetate copolymer 1.5 parts.
A preparation method for Novel interior wall paint, comprises the following steps:
1) take acrylate and polyvinyl alcohol by above-mentioned formula ratio, after adding deionized water, one piece is placed in reactor, is heated to 70 DEG C, is incubated and leaves standstill 3 hours after 2 hours stir;
2) latex of formula ratio and titanium dioxide are added reactor, carry out dispersion with 600r/min and stir 15min, be then heated to 55 DEG C;
3) mixed emulsion is cooled to 12 DEG C, takes phenylcarbinol and capraldehyde by formula ratio, add in the mixture in previous step, carry out dispersion with 500r/min and stir 20min;
4) take polyoxyethylene octylphenol ether and the butadiene resin membrane-forming agent of formula ratio, carry out dispersion with 600r/min and stir 15min, mixed emulsion is put into the sealed vessel that safety valve is housed and carry out ageing, leave standstill 4 days;
5) take ethylene-vinyl acetate copolymer, put into the mixture of previous step through ripening, be heated to 40 DEG C, be cooled to room temperature after insulation 20min, then pack, stamp, inspection, gets product.
embodiment 2
The present invention is a kind of Novel interior wall paint, is made up of the raw material of following parts by weight: acrylate 7.5 parts, polyvinyl alcohol 10 parts, latex 30 parts, titanium dioxide 15 parts, phenylcarbinol 8 parts, capraldehyde 6.8 parts, deionized water 9.8 parts, polyoxyethylene octylphenol ether 6.9 parts, butadiene resin membrane-forming agent 7.5 parts and ethylene-vinyl acetate copolymer 4 parts.
A preparation method for Novel interior wall paint, comprises the following steps:
1) take acrylate and polyvinyl alcohol by above-mentioned formula ratio, after adding deionized water, one piece is placed in reactor, is heated to 80 DEG C, is incubated and leaves standstill 5 hours after 3 hours stir;
2) latex of formula ratio and titanium dioxide are added reactor, carry out dispersion with 700r/min and stir 20min, be then heated to 60 DEG C;
3) mixed emulsion is cooled to 15 DEG C, takes phenylcarbinol and capraldehyde by formula ratio, add in the mixture in previous step, carry out dispersion with 600r/min and stir 25min;
4) take polyoxyethylene octylphenol ether and the butadiene resin membrane-forming agent of formula ratio, carry out dispersion with 700r/min and stir 20min, mixed emulsion is put into the sealed vessel that safety valve is housed and carry out ageing, leave standstill 5 days;
5) take ethylene-vinyl acetate copolymer, put into the mixture of previous step through ripening, be heated to 48 DEG C, be cooled to room temperature after insulation 30min, then pack, stamp, inspection, gets product.
embodiment 3
The present invention is a kind of Novel interior wall paint, is made up of the raw material of following parts by weight: acrylate 5.8 parts, polyvinyl alcohol 7 parts, latex 25 parts, titanium dioxide 11.6 parts, phenylcarbinol 6.8 parts, capraldehyde 4.7 parts, deionized water 8.9 parts, polyoxyethylene octylphenol ether 4.8 parts, butadiene resin membrane-forming agent 5.1 parts and ethylene-vinyl acetate copolymer 2.8 parts.
A preparation method for Novel interior wall paint, comprises the following steps:
1) take acrylate and polyvinyl alcohol by above-mentioned formula ratio, after adding deionized water, one piece is placed in reactor, is heated to 75 DEG C, is incubated and leaves standstill 4 hours after 2.5 hours stir;
2) latex of formula ratio and titanium dioxide are added reactor, carry out dispersion with 650r/min and stir 18min, be then heated to 58 DEG C;
3) mixed emulsion is cooled to 13 DEG C, takes phenylcarbinol and capraldehyde by formula ratio, add in the mixture in previous step, carry out dispersion with 550r/min and stir 22min;
4) take polyoxyethylene octylphenol ether and the butadiene resin membrane-forming agent of formula ratio, carry out dispersion with 650r/min and stir 17min, mixed emulsion is put into the sealed vessel that safety valve is housed and carry out ageing, leave standstill 4.5 days;
5) take ethylene-vinyl acetate copolymer, put into the mixture of previous step through ripening, be heated to 45 DEG C, be cooled to room temperature after insulation 25min, then pack, stamp, inspection, gets product.
The finished product prepared by embodiment 1-3 carries out the test of following table properties, the results are shown in Table 1:
Can find out, indices all conformance with standard of coating of the present invention, have very strong abrasion resistance and wear resistance etc.Compared with existing product, owing to adding phenylcarbinol and polyoxyethylene octylphenol ether, emulsion paint finished product good anti-bacterial effect is made after both and mixing, resistance to performance of going mouldy is strong, the component materials such as ethylene-vinyl acetate copolymer, latex and titanium dioxide are with low cost, make emulsion paint product cost low, and owing to not containing the composition such as formaldehyde and VOC in raw material, energy-conserving and environment-protective.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.

Claims (3)

1. a Novel interior wall paint, is characterized in that: be made up of the raw material of following parts by weight: acrylate 3.5-7.5 part, polyvinyl alcohol 5-10 part, latex 20-30 part, titanium dioxide 10-15 part, phenylcarbinol 5-8 part, capraldehyde 2.5-6.8 part, deionized water 8.5-9.8 part, polyoxyethylene octylphenol ether 3.5-6.9 part, butadiene resin membrane-forming agent 2.5-7.5 part and ethylene-vinyl acetate copolymer 1.5-4 part.
2. Novel interior wall paint according to claim 1, is characterized in that: be made up of the raw material of following parts by weight: acrylate 5.8 parts, polyvinyl alcohol 7 parts, latex 25 parts, titanium dioxide 11.6 parts, phenylcarbinol 6.8 parts, capraldehyde 4.7 parts, deionized water 8.9 parts, polyoxyethylene octylphenol ether 4.8 parts, butadiene resin membrane-forming agent 5.1 parts and ethylene-vinyl acetate copolymer 2.8 parts.
3. the preparation method of the Novel interior wall paint according to claims 1 or 2, comprises the following steps:
1) take acrylate and polyvinyl alcohol by above-mentioned formula ratio, after adding deionized water, one piece is placed in reactor, is heated to 70-80 DEG C, is incubated and leaves standstill 3-5 hour after 2-3 hour stirs;
2) latex of formula ratio and titanium dioxide are added reactor, carry out dispersion with 600-700r/min and stir 15-20min, be then heated to 55-60 DEG C;
3) mixed emulsion is cooled to 12-15 DEG C, takes phenylcarbinol and capraldehyde by formula ratio, add in the mixture in previous step, carry out dispersion with 500-600r/min and stir 20-25min;
4) take polyoxyethylene octylphenol ether and the butadiene resin membrane-forming agent of formula ratio, carry out dispersion with 600-700r/min and stir 15-20min, mixed emulsion is put into the sealed vessel that safety valve is housed and carry out ageing, leave standstill 4-5 days;
5) take ethylene-vinyl acetate copolymer, put into the mixture of previous step through ripening, be heated to 40-48 DEG C, be cooled to room temperature after insulation 20-30min, then pack, stamp, inspection, gets product.
CN201511015734.8A 2015-12-31 2015-12-31 New type interior wall paint and preparation method thereof Pending CN105385207A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201511015734.8A CN105385207A (en) 2015-12-31 2015-12-31 New type interior wall paint and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201511015734.8A CN105385207A (en) 2015-12-31 2015-12-31 New type interior wall paint and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105385207A true CN105385207A (en) 2016-03-09

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106189582A (en) * 2016-07-14 2016-12-07 安徽恒兴装饰工程有限公司 A kind of environmental protection emulsion paint and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53105536A (en) * 1977-02-28 1978-09-13 Showa Electric Wire & Cable Co Ltd Fire proofing paint
CN101113265A (en) * 2006-07-28 2008-01-30 中宏(天津)实业有限公司 Single-component cold-construction water-based waterproofing paint
CN102391733A (en) * 2011-12-20 2012-03-28 袁文君 Multifunctional green environment-friendly interior wall emulsion paint
CN102816489A (en) * 2012-08-21 2012-12-12 江苏紫石化工科技有限公司 Interior wall stain resistant emulsion paint and preparation method thereof
CN102936442A (en) * 2012-03-12 2013-02-20 洛阳市科隆涂料有限公司 Pure water paint
CN104804560A (en) * 2015-04-08 2015-07-29 田福东 Scrubbing-resistant environment-friendly interior-wall latex paint

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53105536A (en) * 1977-02-28 1978-09-13 Showa Electric Wire & Cable Co Ltd Fire proofing paint
CN101113265A (en) * 2006-07-28 2008-01-30 中宏(天津)实业有限公司 Single-component cold-construction water-based waterproofing paint
CN102391733A (en) * 2011-12-20 2012-03-28 袁文君 Multifunctional green environment-friendly interior wall emulsion paint
CN102936442A (en) * 2012-03-12 2013-02-20 洛阳市科隆涂料有限公司 Pure water paint
CN102816489A (en) * 2012-08-21 2012-12-12 江苏紫石化工科技有限公司 Interior wall stain resistant emulsion paint and preparation method thereof
CN104804560A (en) * 2015-04-08 2015-07-29 田福东 Scrubbing-resistant environment-friendly interior-wall latex paint

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106189582A (en) * 2016-07-14 2016-12-07 安徽恒兴装饰工程有限公司 A kind of environmental protection emulsion paint and preparation method thereof

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Application publication date: 20160309