CN105495411A - Preparation method of sea cucumber ultramicro pure powder tablets - Google Patents
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Abstract
The invention relates to a preparation method of sea cucumber ultramicro pure powder tablets. The preparation method comprises the steps of (1) increasing the water content of sea cucumber ultramicro pure powder of which the particle size is 1 to 100mum to 25 to 33 percent; (2) preparing the mixed sea cucumber ultramicro pure powder into sea cucumber particles of which the particle sizes are 25 to 40-mesh; (3) drying the sea cucumber particles at 60 to 70 DEG C until the water content is 10 to 20 percent; (4) sieving the dried sea cucumber particles with a 25 to 40-mesh screen; (5) tabletting the sieved sea cucumber particles in the step 4; (6) drying the tableted sea cucumber tablets under the condition that the temperature is 70 to 75 DEG C, and the vacuum pressure is 25 to 40 KPa until the water content is 5 percent, and obtaining the tablets. According to the tablets provided by the invention, no excipient is added, meanwhile parameters such as water content, tabletting pressure, temperature and the like are controlled to change the characteristic of sea cucumber powder, moisture is mixed with pure powder through a spray mixing technology, and the tablets are obtained by processes of pelletizing, drying, sieving, tabletting and the like, effective components of the sea cucumber can not be reduced or destroyed, and active nutritional ingredients of the sea cucumber can be kept to maximum limit.
Description
Technical field
The present invention relates to aquatic products field of deep, particularly the deep processing of sea cucumber, i.e. a kind of preparation method of sea cucumber ultramicro pure powder sheet.
Background technology
The history of Chinese's beche-de-mer is of long standing and well established, and sea cucumber is gained the name because of the similar ginseng of benefiting action.Record according in supplementary Amplifications of the Compendium of Materia Medica: sea cucumber, sweet-salty, kidney tonifying, beneficial marrow, takes the photograph urine, and impotence is treated in establishing-Yang, its benefit warm in nature, sufficient enemy's ginseng, therefore named sea cucumber.Modern study shows, the active ingredients such as the distinctive sea cucumber polysaccharide of sea cucumber, Sea Cucumber Glycosides, sea cucumber chondroitin have and improve memory, benefiting qi and nourishing blood, raising immunity, delay sexual gland aging, prevent artery sclerosis, diabetes and the effect such as antitumor.And meat quality of sea cucumber is soft tender, nutritious, be typical high protein, low fat food, flavour fat is beautiful, and local flavor is graceful, is the name food delicacies had long enjoyed a good reputation, ranks first of seafood delights " eight delicacies ".So sea cucumber is not only precious food, it is also famous and precious medicinal material.
For a long time, the conventional edible way of sea cucumber is sent out with dried sea-cucumber bubble, the mode of boiling is processed, the effect that this traditional handicraft reaches on the surface " delicious and nourishing ".But in Holothurian machining process, high temperature, high pressure, sugaring salt adding etc. cause a large amount of nutrition leak.And consumer eats in process and wastes time and energy, boiling causes nutrition leak further.The sea cucumber that this mode is processed simultaneously is unfavorable for absorption of human body, and tonic effect is not obvious.Along with the development in epoch, a kind of new beche-de-mer products of the fast pace of modern, high-quality living needs meets their daily demand, has both required to reach natural, the effect of nutritious tonifying, the again object of realistic existing instant, efficiency utilization.And sea cucumber tablet can well reach this requirement.
When inventor finds that in research process sea cucumber is ground into the micro mist scaled powders of 1-30 μm, its dissolution rate is very high, and powder particle diameter is less, and dissolution time is shorter, can ensure within the shortest time, and sea cucumber active component is fully absorbed in time.But it is short to there is the holding time in sea cucumber powder, edible inconvenient problem.On the basis of not adding any auxiliary material, if the pure powder of sea cucumber can make tablet, reach the assimilation effect the same with sea cucumber powder, that greatly will meet the life of modern fast pace to the demand of the beche-de-mer products of quick and easy, efficiency utilization.
Whether sea cucumber tablet meets the requirements directly related with the compression property of sea cucumber powder, and the latter is the comprehensive embodiment of sea cucumber powder multiple compression mechanism and multiple dry jet mixing pile.In usual the art preparation process, the compression property of sea cucumber powder and mobility directly affect its adaptability to production high speed compressing tablet, and desirable compressing tablet material will have fabulous mobility, cohesive and compressibility.Therefore need some technological means and technique to improve the performance of sea cucumber powder. as: change its particle size distribution, change form etc. and improved, as recrystallization method, spray drying process, moisture controls, temperature controls, Stress control, adds the factors such as auxiliary material.What generally adopt at present is mixed with a large amount of auxiliary material by sea cucumber micro mist with the moulding performance change sea cucumber powder characteristics by auxiliary material, and auxiliary material can account for very large ratio.
But people wish in sea cucumber tablet not containing any artificial additive.Be on the one hand because there is the problems such as the accessory substance containing Prof. Du Yucang that is difficult to avoid and organic solvent residual in auxiliary material, the pursuit of modern to all-natural product cannot be met.And add the sea cucumber lozenge of auxiliary material and also have that to there will be mixing uneven, hardness is too large, the problem of poorly soluble.Sea cucumber active ingredient dissolution time can be caused long, and concentration is low.And then affect human absorptivity, do not reach corresponding effect.
But if adopt the pure powder compressing tablet of sea cucumber, because sea cucumber micro mist surface tension is large, powder voids is large, causes powder compressibility, cohesive, illiquidity.Usual those skilled in the art are difficult to pure for sea cucumber powder direct tablet compressing, and therefore the enforcement of this technique has many difficulties and less application in actual production.
Summary of the invention
For the defect existed in prior art, the object of the present invention is to provide one only containing sea cucumber ultramicro pure powder, the tablet be prepared from when controlling moisture, temperature, pressure and other parameters, can not reduce or destroy the active ingredient of sea cucumber in preparation process.
For reaching above object, the technical scheme that the present invention takes is:
A preparation method for sea cucumber ultramicro pure powder sheet, concrete steps are as follows:
(1) be that the sea cucumber Ultramicro-powder increase water content of 1-100 μm is to 25-33% by particle diameter;
(2) the sea cucumber Ultramicro-powder mixed being obtained particle diameter is 25-40 object sea cucumber granules;
(3) sea cucumber granules is dried to water content 10-20% under the condition of 60-70 DEG C;
(4) sea cucumber granules after oven dry is crossed 25-40 mesh sieve;
(5) the sea cucumber granules compressing tablet after step (4) being sieved;
(6) sea cucumber slice pressed is at 70-75 DEG C, and vacuum pressure is under 25-40KPa condition, and drying to water content is 5%, obtains in flakes.
On the basis of such scheme, the method increasing water content in step (1) is in airtight space, sea cucumber powder is at the uniform velocity stirred and with the pure water Homogeneous phase mixing of mist, thus increase sea cucumber powder water content.
On the basis of such scheme, the compressing tablet in step (5) carries out in tablet press machine, preload pressure 5-12KN, principal pressure 6-12KN.
On the basis of such scheme, a kind of preparation method of sea cucumber ultramicro pure powder sheet, concrete steps are as follows:
(1) by particle diameter be 25 μm sea cucumber Ultramicro-powder increase water content to 30%;
(2) the sea cucumber Ultramicro-powder mixed being obtained particle diameter is 31 object sea cucumber granules;
(3) sea cucumber granules is dried to water content 15% under the condition of 65 DEG C;
(4) sea cucumber granules after oven dry is crossed 30 mesh sieves;
(5) the sea cucumber granules compressing tablet after step (4) being sieved;
(6) sea cucumber slice pressed is at 72 DEG C, and vacuum pressure is under 34KPa condition, and drying to water content is 5%, obtains in flakes.
On the basis of such scheme, the compressing tablet in step (5) carries out in tablet press machine, preload pressure 8KN, principal pressure 10KN.
Sea cucumber Ultramicro-powder is prepared from by following methods:
(1) fresh sea cucumber is pulled the rear environment being placed in rapidly 0-6 DEG C out and carries out fresh-keeping and alive-keeping; And cleaned in 1 hour;
(2) cut open to tone place along the back side from sea cucumber anus with scissors always, gill, time controling is in 5 seconds;
(3) rinsed by the flowing clear water of sea cucumber 10-12 DEG C cutd open, scavenging period is in 10 seconds;
(4) sea cucumber after cleaning, be placed on cold fresh storage in the pure water of 5 DEG C immediately, the holding time is no more than 30 minutes;
(5) microwave system is ripe; Sea cucumber is put neatly, not overlapping, the outside of belly upwards, under the microwave intensity of 8kw/kg, temperature controls at 70-80 DEG C, and through the microwave treatment of 1-2 minute, in microwave processing process, pallet rotated with the speed of 7.5r/min, after microwave treatment terminates, rapidly sea cucumber is placed in 0 DEG C of frozen water to lower the temperature, the sea cucumber after cooling removes the calcium carbonate of mouth, by clean water;
(6) vacuum freeze drying, the sea cucumber after microwave system is ripe is put successively neatly on pallet, not overlapping, and the downward outside of belly in the back side is upwards; At-10 DEG C freeze settled 2 hours, keep 6 hours under proceeding to-40 DEG C of environment; Proceed to pressure 10-100Pa afterwards, initial temperature is distil in the environment of 45 DEG C, the temperature that controls environment in sublimation process is between ± 5 DEG C; After 40 hours, the temperature that controls environment is at 55 DEG C, and the time is 8 hours;
(7) low-temperature submicron powder is broken, will be ground into the first powder particulate that particle diameter is 1-5mm through the ripe sea cucumber of dried system; Just 1.5-2 hour is frozen at afterwards first powder particulate being placed in-5 DEG C ~-10 DEG C; Drop in pulverizer rapidly afterwards and pulverize; During pulverizing, pulverize built-in temperature and control at 0 DEG C ~-20 DEG C; Be crushed to diameter 1-100 μm.
The present invention has the following advantages and beneficial effect:
(1) tablet of the present invention does not add other any auxiliary material, control the parameters such as moisture, tableting pressure, temperature simultaneously, by spraying mixing technology, moisture is mixed with pure powder, and through granulating, drying, sieve, the compacting of the technique such as compressing tablet forms, can not reduce or destroy the active ingredient of sea cucumber, retain the active nutrient component of sea cucumber to greatest extent.
(2) the present invention selects the sea cucumber Ultramicro-powder of 1-100 μm, and especially the sea cucumber Ultramicro-powder of 1-30 μm reaches cytoclastic specification, and the powder grinding particle size of this particle size range is evenly distributed, and active material of sea cucumber is discharged completely.Research shows, the dissolution rate of the active material (selenka, holothurian collagen, acid mucopolysaccharide, sea cucumber) of the pure powder of sea cucumber etc. is relevant with sea cucumber powder particle diameter.
(3) the present invention is first in airtight space, sea cucumber powder is at the uniform velocity stirred the pure water Homogeneous phase mixing with mist, makes sea cucumber Ultramicro-powder increase water content to 25-33%.Object is sea cucumber pure dry powder too dry mainly, normally adds water and is easy to be adhered and lump, mix uneven, can not get desirable powder state.And water content is inadequate, powder cohesive is not enough, therefore utilizes method of the present invention to significantly increase cohesive, the compressibility of sea cucumber powder.
(4) the present invention adopts granulating process that the sea cucumber powder after adding water is made 25-40 order particle, changes granular size, improves the compressibility of sea cucumber powder.
(5) the present invention is by pure for sea cucumber powder 60-70 DEG C of oven dry, dries moisture to 10%-20%.Adopt 60-70 DEG C to be that temperature low moisture is removed slow because temperature height can cause sea cucumber nutrient to run off and activity change, sea cucumber powder compressibility is not enough.Drying moisture to 10%-20% is because in moisture evaporation process, the mobility of sea cucumber powder, compressibility and cohesive all can change, because the number of moisture is shifting relations to these three features of powder, such as excess moisture cohesive is large, but poor fluidity, during compressing tablet, tablet caking phenomenon is obvious.How removing moisture fast, and guarantee that sea cucumber powder characteristics meets compressing tablet requirement, is a difficult point of this technology.We show through great many of experiments, and sea cucumber ultramicro pure powder powder fluidity, compressibility, cohesive when water content is 15% are in optimum balance state, and the tablet qualification rate extruded is the highest.
(6) the sea cucumber powder after the present invention's oven dry crosses 25-40 eye mesh screen, this is because the sea cucumber granules after drying has small part condensation situation, and skewness.Must again make the particle be evenly distributed, could uniform discharge during such compressing tablet, the tablet pressed out is also dense, is not easy to occur sliver situation.
(7) compressing tablet preload pressure of the present invention is 5 ~ 12KN, and principal pressure is 6 ~ 12KN, can ensure good tablet effect.If pressure conference causes sea cucumber tablet sliver, the little meeting of pressure causes sea cucumber tablet hardness inadequate.Adopt pressing step, be beneficial to the air of discharging in powder, reduce sliver, increase the hardness of tablet.
(8) compressing tablet of the present invention needs 70-75 DEG C of oven dry under vacuum conditions to water content 5-6%, adopt vacuum state that tablet can be made to keep the shape of the best, 70-75 DEG C of oven dry is adopted to be when ensureing that sea cucumber nutrient composition does not lose, not running off, the evaporation of uniform moisture is gone out, and ensures that the pure powder tablet of sea cucumber meets the requirements.The evaporation of sea cucumber tablet moisture is faster, can cause sliver.Moisture evaporation is slow, can affect the quality of sea cucumber tablet.How removing moisture fast, and ensure nutrient substance, is also a difficult point of this technology.The water content of 5% can ensure that sea cucumber stores for a long time, keeps best quality.
The method preparing sea cucumber ultramicro pure powder sheet of the present invention is a complete multi-parameter technique, this technique is a complete entirety, arbitrary parameter in this technique entirety all can affect its rate in blocks in various degree, in the present invention, each factor parameter cooperatively interacts, and reaches the optimal effectiveness of preparation sea cucumber ultramicro pure powder sheet.The pure powder of sea cucumber in the present invention, by controlling moisture, temperature, pressure and other parameters, changing the pure powder cohesive of sea cucumber, mobility, compressibility, meeting compressing tablet requirement.
When the pure powder sheet of sea cucumber of the present invention is with oral application, by the absorption features of oral mucosa in conjunction with oral stomach and intestine, active ingredient in sea cucumber ultramicro pure powder is entered rapidly in body, the first pass effect of liver can be overcome, improve assimilation effect, and dose minimizing can be made to reduce even at double, it has important using value for aquatic products field of deep.
The method utilizing fresh sea cucumber to prepare sea cucumber Ultramicro-powder of the present invention, in order to ensure that the nutrient content of sea cucumber does not run off, increase the absorption rate of human body to sea cucumber nutrient material, strict Controlling Technology step and step parameter, fish for, control temperature, time when cleaning, can effectively remove the impurity such as sea cucumber internal organ, the fresh-keeping of sea cucumber can be realized again to the full extent; Microwave cooking skill is the important step in present invention process entirety, this link strict temperature control, time and microwave intensity, the homogeneous heating system not only achieving sea cucumber is ripe, sterilizing deactivation, prevents again the hot-spot produced in traditional handicraft to make sea cucumber polysaccharide, sea cucumber peptide etc. that the defects such as sex change decomposition occur; At utmost remain sea cucumber nutrient to be worth and mouthfeel.
Detailed description of the invention
For better the present invention being described, be convenient to understand technical scheme of the present invention, below the present invention is described in more detail.But following embodiment is only simple case of the present invention, does not represent or limits the scope of the present invention, and protection scope of the present invention is as the criterion with claims.
In the present invention, inventor is creationary only to be added in moisture situation, and pure for sea cucumber powder is pressed into pure powder tablet truly, sea cucumber is the sole component of tablet.
A preparation method for sea cucumber ultramicro pure powder sheet, concrete steps are as follows:
1, the preparation of sea cucumber Ultramicro-powder
(1) in marine site, Xiao Wang family of Dalian Zhuanghe City island, fresh sea cucumber is pulled out the rear environment being placed in rapidly 5 DEG C and carry out fresh-keeping and alive-keeping; And cleaned 45 minutes time;
(2) upwards cut open to tone place along the back side from sea cucumber anus with scissors, gill, time controling was at 4 seconds;
(3) rinsed by the flowing clear water of the sea cucumber cutd open with 10 DEG C, scavenging period was at 9 seconds;
(4) sea cucumber after cleaning, is placed on cold fresh storage in the pure water of 5 DEG C, 25 minutes holding times;
(5) microwave system is ripe; Sea cucumber is put neatly, not overlapping, the outside of belly upwards, under the microwave intensity of 8kw/kg, temperature controls at 80 DEG C, and through the microwave treatment of 2 minutes, in microwave processing process, pallet rotated with the speed of 7.5r/min, after microwave treatment terminates, rapidly sea cucumber is placed in 0 DEG C of frozen water to lower the temperature, the sea cucumber after cooling removes the calcium carbonate of mouth, by clean water;
(6) vacuum freeze drying, the sea cucumber after microwave system is ripe is put successively neatly on pallet, not overlapping, and the downward outside of belly in the back side is upwards; At-10 DEG C freeze settled 2 hours, keep 6 hours under proceeding to-40 DEG C of environment; Proceed to pressure 10-100Pa afterwards, initial temperature is distil in the environment of 45 DEG C, the temperature that controls environment in sublimation process is between ± 5 DEG C; After 40 hours, the temperature that controls environment is at 55 DEG C, and the time is 8 hours;
(7) low-temperature submicron powder is broken, will be ground into the first powder particulate that particle diameter is 5mm through the ripe sea cucumber of dried system; At afterwards first powder particulate being placed in-10 DEG C freezing 2 hours; Drop in pulverizer rapidly afterwards and pulverize; During pulverizing, pulverize built-in temperature and control at-20 DEG C; Be crushed to diameter 1-100 μm.
2, the preparation of pure powder sheet
By particle diameter be 1-100 μm sea cucumber Ultramicro-powder blow out vaporific, blow out vaporific sea cucumber powder and mist pure water Homogeneous phase mixing, mixed sea cucumber powder water content is 25-33%; The sea cucumber Ultramicro-powder mixed being obtained particle diameter is 25-40 object sea cucumber granules; Sea cucumber granules is dried to water content 10-20% under the condition of 60-70 DEG C; Sea cucumber granules after drying is crossed 25-40 mesh sieve; Afterwards sea cucumber granules is inserted in tablet press machine, preload pressure 5-12KN, principal pressure 6-12KN, compressing tablet; The sea cucumber slice pressed is at 70-75 DEG C, and vacuum pressure is under 25-40KPa condition, and drying to water content is 5%, obtains in flakes; Employing blister package in blocks is preserved.
Table 1 different parameters coordinates the rate in blocks of lower sea cucumber pure powder sheet
Can be found out by table 1,
The sea cucumber powder footpath that making sea cucumber pure powder sheet uses has a significant impact sea cucumber pure powder sheet rate in blocks, under normal circumstances, sea cucumber pure powder footpath is less, the cohesive of sea cucumber powder is better, and when particle diameter reaches Ultracytochemical fragmentation standard, intracellular for sea cucumber active material can be discharged completely, namely effect in blocks is better, but finding that when making particle diameter is too low, hardness can be caused not enough, easy sliver.The in blocks rate of control to sea cucumber pure powder sheet of spraying mixing water content has a significant impact, and the interpolation of the pure powder moisture of sea cucumber is to change its powder characteristics, too high too low all improper.We within the scope of 25-33%, have investigated the tablet properties of adding sea cucumber pure powder tablet after different in moisture situation in the pure powder water content of sea cucumber.In equal compressing tablet mode situation, analyze its yield rate, finally find when 30% best.The in blocks rate of size to sea cucumber pure powder sheet of granulation particle has a significant impact, and granulation size determines the gap size between sea cucumber granules, and particle is large, and the tablet of extrusion is thin and have sliver situation.Particle is little, and gap is few, and the tablet hardness of extrusion is large, is not easy to separate out nutriment.Pellet moisture controls to have a significant impact the rate in blocks of sea cucumber pure powder sheet, in sea cucumber granules drying course, the water content of sea cucumber granules has a great impact its mobility, cohesive, compressibility, for this reason, the exploration of situation in blocks under inventors performed sea cucumber granules different in moisture content situation, find that mobility when sea cucumber granules water content is 15%, cohesive, compressibility reach optimum balance state, when in conjunction with other factor parameters, now sea cucumber rate in blocks is the highest.Finding in manufacturing process, there is very large impact equally on sea cucumber pure powder sheet rate in blocks in tableting pressure, if pressure is too small, occurs the situation that loose pieces, tablet hardness are low.Pressure is bigger than normal, and hardness is too large, occurs that active material of sea cucumber dissolution rate is low, the situation of sliver.Inventor is when studying tablet forming technique, and in conjunction with other factor parameters, find that precompression is at 5-12kN, principal pressure is be more suitable for the pure powder compressed tablets of sea cucumber at 6-12kN.This tablet yield rate of suppressing and obtaining is high, conforms to quality requirements.The tablet of preparation there will be the phenomenon such as sliver, crash when drying because of the impact of bake out temperature, pressure, have impact on rate in blocks, in tablet drying course, mainly remove moisture by temperature, tablet moisture is faster evenly distribute to rely on negative pressure of vacuum to ensure.Generally, temperature is low, and moisture evaporation is slow, and tablet hardness is not enough.Drying time is long, and tablet is also easily oxidized.And temperature is high, moisture evaporation easily causes sliver, crash soon, and high temperature can cause nutritive loss very much.Therefore, we have selected at 72 DEG C, and vacuum pressure is in 34KPa situation, and moisture evaporation is the most even, and tablet state is best.
The mensuration of the total leachable of sea cucumber pure powder tablet:
Research shows, the nutriment dissolution rate such as total leachable, holothurian collagen, acid mucopolysaccharide, selenka of the pure powder of sea cucumber is relevant with sea cucumber grinding particle size, and grinding particle size is less, and dissolution time is faster, and dissolution rate is larger.So we are by instantaneous Dissolution experiments, total material dissolution rate situation of obtained sea cucumber slice under comparing different-grain diameter situation.Pure for the sea cucumber of same particle size powder and tablet are contrasted simultaneously, check whether the sea cucumber powder of two kinds of forms exists the difference of total dissolution rate.
Below test powder particle diameter to be respectively: A1 group powder, the agent of particle diameter 100-200 μm, A2 pack, particle diameter 100-200 μm.B1 group powder, the agent of particle diameter 30-100 μm, B2 pack, particle diameter 30-100 μm.C1 group powder, particle diameter 1-30 μm of .C2 pack agent, particle diameter 1-30 μm. different active ingredient dissolution rate in time of pulverizing in the sea cucumber of rank is in Table:
Accurately take the pure powder of sea cucumber three groups of each 5g (often group establishes 3 Duplicate Samples, gets average) in conical flask, each adding distil water 100ml, be placed in 37 DEG C of thermostat water baths, respectively sampling in 1,5,10,20,30 minute, rock and mix, get filtrate 50ml, the results are shown in Table 2:
Total time dependent dissolution rate (g) of material in the sea cucumber powder of table 2 different-grain diameter and tablet
The measurement result of the total leachable of the pure powder of sea cucumber of different group shows, the dissolution rate of each group sea cucumber powder and sea cucumber tablet increases in time gradually, and dissolution rate is directly proportional to the pure powder footpath of sea cucumber simultaneously.As when 1 minute, the powder dissolution rate of C1 (1-30 μm) is more than 4 times of A1 (100-200 μm), and the Dissolution of Tablet of C2 (1-30 μm) is close to 6 times of A2 (100-200 μm).But under particle diameter condition of the same race, Dissolution of Tablet comparatively powder is slightly low, but does not have notable difference.Therefore sea cucumber powder is made tablet and can not be impacted nutrition stripping, and this is mainly because adopt pure powder compressing tablet, and tablet can dissolve rapidly.
Above-mentioned embodiment is the embodiment of the best of the present invention; but embodiment of the present invention are not by the restriction of above-mentioned embodiment; other any without prejudice under the condition of the principle of the invention; the embodiment that can be produced by the form changing parameter, is all contained within protection scope of the present invention.
Claims (6)
1. a preparation method for sea cucumber ultramicro pure powder sheet, it is characterized in that, concrete steps are as follows:
(1) be that the sea cucumber Ultramicro-powder increase water content of 1-100 μm is to 25-33% by particle diameter;
(2) the sea cucumber Ultramicro-powder mixed being obtained particle diameter is 25-40 object sea cucumber granules;
(3) sea cucumber granules is dried to water content 10-20% under the condition of 60-70 DEG C;
(4) sea cucumber granules after oven dry is crossed 25-40 mesh sieve;
(5) the sea cucumber granules compressing tablet after step (4) being sieved;
(6) sea cucumber slice pressed is at 70-75 DEG C, and vacuum pressure is under 25-40KPa condition, and drying to water content is 5%, obtains in flakes.
2. the preparation method of sea cucumber ultramicro pure powder sheet according to claim 1, it is characterized in that, on the basis of such scheme, the method increasing water content in step (1) is in airtight space, sea cucumber powder is at the uniform velocity stirred the pure water Homogeneous phase mixing with mist, thus increase sea cucumber powder water content.
3. the preparation method of sea cucumber ultramicro pure powder sheet according to claim 2, it is characterized in that, the compressing tablet in step (5) carries out in tablet press machine, tablet press machine preload pressure 5-12KN, principal pressure 6-12KN.
4. the preparation method of sea cucumber ultramicro pure powder sheet according to claim 1, it is characterized in that, concrete steps are as follows:
(1) by particle diameter be 25 μm sea cucumber Ultramicro-powder increase water content to 30%;
(2) the sea cucumber Ultramicro-powder mixed being obtained particle diameter is 31 object sea cucumber granules;
(3) sea cucumber granules is dried to water content 15% under the condition of 65 DEG C;
(4) sea cucumber granules after oven dry is crossed 30 mesh sieves;
(5) the sea cucumber granules compressing tablet after step (4) being sieved;
(6) sea cucumber slice pressed is at 72 DEG C, and vacuum pressure is under 34KPa condition, and drying to water content is 5%, obtains in flakes.
5. the preparation method of sea cucumber ultramicro pure powder sheet according to claim 3, it is characterized in that, the compressing tablet in step (5) carries out in tablet press machine, tablet press machine preload pressure 8KN, principal pressure 10KN.
6. the preparation method of the sea cucumber ultramicro pure powder sheet according to any one of claim 1-5, it is characterized in that, sea cucumber Ultramicro-powder is prepared from by following methods:
(1) fresh sea cucumber is pulled the rear environment being placed in rapidly 0-6 DEG C out and carries out fresh-keeping and alive-keeping; And cleaned in 1 hour;
(2) cut open to tone place along the back side from sea cucumber anus with scissors always, gill, time controling is in 5 seconds;
(3) rinsed by the flowing clear water of sea cucumber 10-12 DEG C cutd open, scavenging period is in 10 seconds;
(4) sea cucumber after cleaning, be placed on cold fresh storage in the pure water of 5 DEG C immediately, the holding time is no more than 30 minutes;
(5) microwave system is ripe; Sea cucumber is put neatly, not overlapping, the outside of belly upwards, under the microwave intensity of 8kw/kg, temperature controls at 70-80 DEG C, and through the microwave treatment of 1-2 minute, in microwave processing process, pallet rotated with the speed of 7.5r/min, after microwave treatment terminates, rapidly sea cucumber is placed in 0 DEG C of frozen water to lower the temperature, the sea cucumber after cooling removes the calcium carbonate of mouth, by clean water;
(6) vacuum freeze drying, the sea cucumber after microwave system is ripe is put successively neatly on pallet, not overlapping, and the downward outside of belly in the back side is upwards; At-10 DEG C freeze settled 2 hours, keep 6 hours under proceeding to-40 DEG C of environment; Proceed to pressure 10-100Pa afterwards, initial temperature is distil in the environment of 45 DEG C, the temperature that controls environment in sublimation process is between ± 5 DEG C; After 40 hours, the temperature that controls environment is at 55 DEG C, and the time is 8 hours;
(7) low-temperature submicron powder is broken, will be ground into the first powder particulate that particle diameter is 1-5mm through the ripe sea cucumber of dried system; Just 1.5-2 hour is frozen at afterwards first powder particulate being placed in-5 DEG C ~-10 DEG C; Drop in pulverizer rapidly afterwards and pulverize; During pulverizing, pulverize built-in temperature and control at 0 DEG C ~-20 DEG C; Be crushed to diameter 1-100 μm.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106509694A (en) * | 2016-11-09 | 2017-03-22 | 天津贝罗尼生物科技有限公司 | Preparation method of ultrafine sea cucumber powder convenient to eat and easy to digest |
| CN112352934A (en) * | 2020-11-02 | 2021-02-12 | 谢沛鸿 | Preparation method of pure sea cucumber freeze-dried superfine powder tablet for secondary freeze-drying |
| CN112385798A (en) * | 2020-11-22 | 2021-02-23 | 福建御蓝记水产食品有限公司 | Sea cucumber chewable tablet and preparation method thereof |
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| CN115399474A (en) * | 2022-08-29 | 2022-11-29 | 广西壮族自治区农业科学院 | Processing method of selenium-rich moringa oleifera leaf raw powder tablets |
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| CN113080291A (en) * | 2019-12-23 | 2021-07-09 | 福建御蓝记水产食品有限公司 | Preparation method of solid sea cucumber tablet candy |
| CN112352934A (en) * | 2020-11-02 | 2021-02-12 | 谢沛鸿 | Preparation method of pure sea cucumber freeze-dried superfine powder tablet for secondary freeze-drying |
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| CN115399474A (en) * | 2022-08-29 | 2022-11-29 | 广西壮族自治区农业科学院 | Processing method of selenium-rich moringa oleifera leaf raw powder tablets |
| CN115399474B (en) * | 2022-08-29 | 2024-03-26 | 广西壮族自治区农业科学院 | Processing method of selenium-enriched moringa oleifera leaf raw powder tablet |
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