CN105462675B - 一种环保型浓缩液及其制备方法 - Google Patents

一种环保型浓缩液及其制备方法 Download PDF

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CN105462675B
CN105462675B CN201510961186.1A CN201510961186A CN105462675B CN 105462675 B CN105462675 B CN 105462675B CN 201510961186 A CN201510961186 A CN 201510961186A CN 105462675 B CN105462675 B CN 105462675B
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张烈香
刘春雷
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Zizhou Xinrun Biotechnology Co Ltd
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Abstract

本发明公开了一种环保型浓缩液及其制备方法，浓缩液由以下质量百分数的原料制备而成：氢氧化钠为1.5％‑2.0％，EDTA为3.5％‑5％，蓖麻油钾皂20％‑30％，三乙醇胺油酸皂为3.5％‑5％，亚硝酸钠1.5％‑3％，苯甲酸钠为2.5％‑4％，乳化剂TX‑10为0.5％‑1.5％，苯姘三氮唑为0.1％‑1％，甘油为10％‑15％，水余量。本发明解决了现有技术中的生产工艺流程复杂，用料种类又多，气味较大的不足，降低了生产成本，原料的选择使龙输液质量有了提高，并且整个配方有机溶剂使用量减少，满足环保要求。

Description

一种环保型浓缩液及其制备方法
【技术领域】
本发明涉及煤炭行业浓缩液领域，涉及一种环保型浓缩液及其制备方法。
【背景技术】
液压支架是综合机械化和采煤面用于支撑顶板的重要机械设备，与其采煤机械配套使用。它的支撑、升降、移动和过载保护等，都是借助压力液体在一定结构的管路和控制元件组成的系统中，通过流动来实现能量的传递和转化。这种压力液体就是传动介质。因此，目前普遍试用的浓缩液，应用于液压支架中。然而现有的技术中，浓缩液在生产和配方上都有着复杂的过程，所需要原材料种类多，程序较多，步骤繁琐，气味较大；不满足绿色环保的要求。
【发明内容】
本发明的目的是提供一种环保型浓缩液及其制备方法，改进的配方解决了现有的生产工艺流程复杂，用料种类多的问题，新工艺的配方使用原材料少，成本低，制备方法简单。
为实现上述目的，本发明所采用一下技术方案：
一种环保型液压支架用乳化油，由以下质量百分数的原料制备而成：氢氧化钠为1.5％-2.0％，EDTA为3.5％-5％，蓖麻油钾皂20％-30％，三乙醇胺油酸皂为3.5％-5％，亚硝酸钠1.5％-3％，苯甲酸钠为2.5％-4％，乳化剂TX-10为0.5％-1.5％，苯姘三氮唑为0.1％-1％，甘油为10％-15％，水余量。
一种环保型浓缩液，由以下质量百分数的原料制备而成：氢氧化钠为2.0％，EDTA为4％，蓖麻油钾皂24％，三乙醇胺油酸皂为4％，亚硝酸钠2％，苯甲酸钠为3％，乳化剂TX-10为1％，苯姘三氮唑为0.1％，甘油为12％，水为47.9％。
浓缩液的制备方法，包括以下步骤：
1)在温度不低于20℃、搅拌速率不低于45r/min条件下，先把氢氧化钠放入水中，搅拌3分钟；
2)加入EDTA，搅拌10分钟；
3)加入适量的蓖麻油钾皂，搅拌10分钟，再加入三乙醇胺油酸皂，再搅拌10分钟；
4)加入亚硝酸钠，搅拌15分钟；再加入苯甲酸钠，搅拌15分钟；再加入乳化剂TX-10，搅拌10分钟；
5)加入苯姘三氮唑，搅拌5分钟，再加入甘油，搅拌1小时；静置反应48小时；
6)调节PH值至碱性；
7)经过过滤，灌装即成；
8)最后进行出厂检验。
步骤5)中用氢氧化钠调节至PH值至9～10。
相对于现有技术，本发明具有以下优点：
本发明解决了现有技术中的生产工艺流程复杂，用料种类有多，气味较大的不足，降低了生产成本；本发明的配方中采用了蓖麻油钾皂，原料的选择使浓缩液质量有了提高，并且整个配方有机溶剂使用量减少，满足环保要求。本发明产品不分层、不飘油、不污染、环保节能；而且有很好的清洗性、润滑性、防锈性、极压性；具有良好的防锈、冷却、清洗、润滑等多种功能，能够大大降低机械磨损量和刀具在切削中的磨损，适用于煤矿配有电液阀的液压支架用液力传动介质，也可以用于普通的综合机械化采煤液压支架及单体支柱以及普通切削设备，解决了机械化采煤过程中机械使用周期短的问题，使切削量增加，大大提高了生产效率。
本发明的制备方法简单，适合常温条件进行，无需加热等条件，原料按照步骤加入即得到乳化性能好，稳定性高的乳化剂。出厂检验产率性能良好，各项指标均合格。适合工业化批量生产。
【附图说明】
图1是本发明的浓缩液生产工艺流程图。
【具体实施方式】
下面结合附图和具体实施例对本发明做进一步说明，本发明不限于以下实施例。
实施例1
本发明配制1吨浓缩液所用原料配方如下：
成分 用量(KG) 成分 用量(KG)
水 479 氢氧化钠 20
EDTA 40 蓖麻油钾皂 240
三乙醇胺油酸皂 40 亚硝酸钠 20
苯甲酸钠 30 乳化剂TX-10 10
苯姘三氮唑 1 甘油 120
如图1所示，本发明方法制备方法的完整步骤：
1)在温度不低于20℃、搅拌速率不低于45r/min条件下，先把氢氧化钠、EDTA、蓖麻油钾皂，按比例分别加入反应釜中搅拌均匀，起乳化和稳定的作用；具体的先加入氢氧化钠，搅拌3分钟；再加入EDTA，搅拌10分钟；再加入蓖麻油钾皂，搅拌10分钟；
2)再加入三乙醇胺油酸皂，再搅拌10分钟；加入亚硝酸钠，搅拌15分钟；(起到抗硬水的作用)；
3)再加入苯甲酸钠，搅拌15分钟；再加入乳化剂TX-10，搅拌10分钟；
4)加入苯姘三氮唑，搅拌5分钟，再加入甘油，搅拌1小时；静置反应48小时；
5)调节PH值至碱性；
6)经过过滤，灌装即成；
7)最后进行出厂检验。
此方法在生产工艺过程中比较简单，使用的原材料有少，降低了成本，新的工艺流程比较简化，气味小了。经反复化验对比，本发明针对浓缩液的配方和技术改进的方法使用且可行。
实施例2
本发明配制1吨浓缩液所用原料配方如下：
成分 用量(KG) 成分 用量(KG)
水 339 氢氧化钠 16
EDTA 50 蓖麻油钾皂 300
三乙醇胺油酸皂 50 亚硝酸钠 30
苯甲酸钠 40 乳化剂TX-10 15
苯姘三氮唑 10 甘油 150
本实施例的制备方法和实施例1相同。
实施例3
本发明配制1吨浓缩液所用原料配方如下：
成分 用量(KG) 成分 用量(KG)
水 560 氢氧化钠 15
EDTA 35 蓖麻油钾皂 200
三乙醇胺油酸皂 35 亚硝酸钠 15
苯甲酸钠 25 乳化剂TX-10 5
苯姘三氮唑 10 甘油 100
本实施例的制备方法和实施例1相同。
实施例4
本发明配制1吨浓缩液所用原料配方如下：
成分 用量(KG) 成分 用量(KG)
水 467 氢氧化钠 20
EDTA 50 蓖麻油钾皂 240
三乙醇胺油酸皂 40 亚硝酸钠 18
苯甲酸钠 30 乳化剂TX-10 10
苯姘三氮唑 5 甘油 120
本实施例的制备方法和实施例1相同。
对本发明的各个实施例配方制备的环保型液压支架用乳化油抽样进行出厂检验；按照以下项目进行检测，结果见表1。
表1
由上表可以看出，本发明制备的浓缩液产品各项指标均合格，适用于煤矿配有电液阀的液压支架用液力传动介质，也可以用于普通综合机械化采煤液压支架及单体支柱以及普通切削设备，解决了机械化采煤过程中的机械使用周期短的问题，使切削量增大，大大提高了生产效率。
本发明解决了现有技术中的生产工艺流程复杂，用料种类又多，气味较大的不足，降低了生产成本，原料的选择使龙输液质量有了提高，并且整个配方有机溶剂使用量减少，满足环保要求。
以上所述，仅是本发明夹具实施例，上述实施例并非对本发明做任何限制，凡是根据本发明技术方案所给出的范围和对以上实施例所做的任何简单修改、变更以及等效结构变化，均属于本发明技术方案的保护范围。

Claims (4)

1.一种环保型浓缩液，其特征在于，由以下质量百分数的原料制备而成：氢氧化钠为1.5％-2.0％，EDTA为3.5％-5％，蓖麻油钾皂20％-30％，三乙醇胺油酸皂为3.5％-5％，亚硝酸钠1.5％-3％，苯甲酸钠为2.5％-4％，乳化剂TX-10为0.5％-1.5％，苯骈 三氮唑为0.1％-1％，甘油为10％-15％，水余量；
浓缩液的制备方法，包括以下步骤：
1)在温度不低于20℃、搅拌速率不低于45r/min条件下，先把氢氧化钠放入水中，搅拌完全溶解；
2)加入EDTA，搅拌10分钟；
3)加入适量的蓖麻油钾皂，搅拌10分钟，再加入三乙醇胺油酸皂，再搅拌10分钟；
4)加入亚硝酸钠，搅拌15分钟；再加入苯甲酸钠，搅拌15分钟；再加入乳化剂TX-10，搅拌10分钟；
5)加入苯骈 三氮唑，搅拌5分钟，再加入甘油，搅拌1小时；静置反应至反应完全；
6)调节pH 值至9～10；
7)经过过滤，灌装即成；
8)最后进行出厂检验。
2.根据权利要求1所述的一种环保型浓缩液，其特征在于，由以下质量百分数的原料制备而成：氢氧化钠为2.0％，EDTA为4％，蓖麻油钾皂24％，三乙醇胺油酸皂为4％，亚硝酸钠2％，苯甲酸钠为3％，乳化剂TX-10为1％，苯骈 三氮唑为0.1％，甘油为12％，水为47.9％。
3.权利要求1或2所述的一种浓缩液的制备方法，其特征在于，包括以下步骤：
1)在温度不低于20℃、搅拌速率不低于45r/min条件下，先把氢氧化钠放入水中，搅拌完全溶解；
2)加入EDTA，搅拌10分钟；
3)加入适量的蓖麻油钾皂，搅拌10分钟，再加入三乙醇胺油酸皂，再搅拌10分钟；
4)加入亚硝酸钠，搅拌15分钟；再加入苯甲酸钠，搅拌15分钟；再加入乳化剂TX-10，搅拌10分钟；
5)加入苯骈 三氮唑，搅拌5分钟，再加入甘油，搅拌1小时；静置反应至反应完全；
6)调节pH 值至碱性；
7)经过过滤，灌装即成；
8)最后进行出厂检验。
4.根据权利要求3所述的一种浓缩液的制备方法，其特征在于，步骤5)中用氢氧化钠调节至pH 值至9～10。
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