CN105462349A - Completely-renewable, green and environment-friendly offset printing ink - Google Patents
Completely-renewable, green and environment-friendly offset printing ink Download PDFInfo
- Publication number
- CN105462349A CN105462349A CN201610019842.0A CN201610019842A CN105462349A CN 105462349 A CN105462349 A CN 105462349A CN 201610019842 A CN201610019842 A CN 201610019842A CN 105462349 A CN105462349 A CN 105462349A
- Authority
- CN
- China
- Prior art keywords
- oil
- environmental protection
- vegetable
- phenolic resin
- flexographic ink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/103—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds of aldehydes, e.g. phenol-formaldehyde resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/06—Printing inks based on fatty oils
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
- C09D11/105—Alkyd resins
Abstract
The invention discloses completely-renewable, green and environment-friendly offset printing ink. The offset printing ink is prepared from, by mass, 55-75% of a connecting material, 10-25% of plant pigment, 0-5% of alkyd resin, 0-5% of vegetable oil, 0-2% of wax and 5-10% of a vegetable oil derivative. The connecting material is prepared from, by mass, 35-45% of rosin modified phenolic resin, 20-35% of vegetable oil and 10-40% of a vegetable oil derivative. The offset printing ink is close to common offset printing ink in adhesion and drying speed and excellent in glossiness and rub resistance and contains no petroleum solvent, and constituents are totally renewable resources.
Description
Technical field
The present invention relates to technical field of ink, particularly relate to a kind of regeneration composition flexographic ink.
Background technology
Today of rapid economic development, Nonrenewable resources have been more and more valuable, because it is non-renewable, it is more aobvious that it is precious, in order to respond the call of energy-saving and emission-reduction, under the policy of national sustainable development is guided, reduce the dependence of printing industry for Nonrenewable resources, reduce the discharge of VOC, sustainable environment-friendly and green printing has been instant developing direction.But in high renewable composition environmental protection ink, still the material of some is Nonrenewable resources, therefore studies a kind of 100% renewable resources environmental protection flexographic ink very urgent.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of complete renewable environmental protection flexographic ink, possess the set close with common flexographic ink and rate of drying, have excellent glossiness and crocking resistance, without petroleum solvent, composition is the renewable resources of 100%.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is:
Thering is provided a kind of complete renewable environmental protection flexographic ink, is be prepared from by the composition of following massfraction: binder 55 ~ 75%, vegetable pigment 10 ~ 25%, Synolac 0 ~ 5%, vegetables oil 0 ~ 5%, wax 0 ~ 2%, vegetable oil derivatives 5 ~ 10%;
Described binder is prepared from by the composition of following massfraction: the rosin modified phenolic resin of 35 ~ 45%, the vegetables oil of 20 ~ 35% and 10 ~ 40% vegetable oil derivatives be prepared from.
In a preferred embodiment of the present invention, described rosin modified phenolic resin comprises the first rosin modified phenolic resin and the second rosin modified phenolic resin, described first rosin modified phenolic resin is made up of rosin, maleficent acid, dimeracid and glycerol polymerization modification, and described second rosin modified phenolic resin is prepared from by rosin, maleficent acid and glycerin modification.
In a preferred embodiment of the present invention, described Synolac is long oil alkyd, and described Synolac adopts one or more modified alkyd resins obtained with maleficent acid, glycerine reaction in oleum lini, soya-bean oil, Oleum Cocois, rapeseed oil, rosin, dimeracid.
In a preferred embodiment of the present invention, described vegetables oil is that dry vegetable oil and semi-drying vegetable oils mix, and described dry vegetable oil comprises oleum lini, tung oil, perilla oil and Chinese catalpa oil, and described semi-drying oil comprises soya-bean oil, rapeseed oil and Viscotrol C.
In a preferred embodiment of the present invention, described vegetable oil derivatives is the cut cut substrate of soybean oil methyl ester, soya-bean oil ethyl ester, soya-bean oil isobutyl ester, palm oil methyl ester, plam oil ethyl ester, plam oil isobutyl ester, rapeseed methylester, rapeseed oil ethyl ester or rapeseed oil isobutyl ester.
In a preferred embodiment of the present invention, the boiling range of described cut cut substrate between 260 ~ 320 DEG C, pour point below 0 DEG C, cold filter clogging temperature is below 0 DEG C.
In a preferred embodiment of the present invention, described vegetable pigment comprises the red extracting from safflower, lignum sappan or madder and obtain, the yellow pigment extracted from cape jasmine, turmeric or sophora flower, the blue pigment extracted from bluegrass, the mineral black extracted from walnut tree, persimmon tree or robur.
In a preferred embodiment of the present invention, the described cured animals and plants for obtaining from animal or plant are cured.
The invention has the beneficial effects as follows: a kind of complete renewable environmental protection flexographic ink of the present invention, its composition is 100% renewable, possesses the set close with common flexographic ink and rate of drying, has excellent glossiness and crocking resistance, without petroleum solvent, there is the remarkable feature of environmental protection.
Embodiment
Below preferred embodiment of the present invention is described in detail, can be easier to make advantages and features of the invention be readily appreciated by one skilled in the art, thus more explicit defining is made to protection scope of the present invention.
Embodiment 1:
A kind of complete renewable environmental protection flexographic ink is be prepared from by the composition of following massfraction: binder 65%, vegetable pigment 20%, Synolac 2.5%, vegetables oil 2.5%, wax 1.5%, vegetable oil derivatives 8.5%;
Described binder is prepared from by the composition of following massfraction: the rosin modified phenolic resin of 40%, the vegetables oil of 28% and 32% vegetable oil derivatives be prepared from.
Described rosin modified phenolic resin comprises the first rosin modified phenolic resin and the second rosin modified phenolic resin, described first rosin modified phenolic resin is made up of rosin, maleficent acid, dimeracid and glycerol polymerization modification, it is the resin of high structure, low-solubility, for ink provides body bone, and anti-fly performance of ink, excellent wear resistance, sharpness of dots, print gloss and ink-water balance; Described second rosin modified phenolic resin is prepared from by rosin, maleficent acid and glycerin modification, and this resin is low viscosity, low structure, moderate solubility resin, for ink provides excellent gloss, levelling property and pigment wettability.。
Described Synolac is long oil alkyd, and described Synolac adopts one or more modified alkyd resins obtained with maleficent acid, glycerine reaction in oleum lini, soya-bean oil, Oleum Cocois, rapeseed oil, rosin, dimeracid.
Described vegetables oil is that dry vegetable oil and semi-drying vegetable oils mix, and described dry vegetable oil comprises oleum lini, tung oil, perilla oil and Chinese catalpa oil, and described semi-drying oil comprises soya-bean oil, rapeseed oil and Viscotrol C.Be auxiliary with tung oil, select remaining any vegetables oil to be main, utilize the conjugated double bond of tung oil to improve the rate of drying of ink.
Described vegetable oil derivatives is the cut cut substrate of soybean oil methyl ester, soya-bean oil ethyl ester, soya-bean oil isobutyl ester, palm oil methyl ester, plam oil ethyl ester, plam oil isobutyl ester, rapeseed methylester, rapeseed oil ethyl ester or rapeseed oil isobutyl ester.
The boiling range of described cut cut substrate between 260 ~ 320 DEG C, pour point below 0 DEG C, cold filter clogging temperature is below 0 DEG C.
Described vegetable pigment comprises the red extracting from safflower, lignum sappan or madder and obtain, the yellow pigment extracted from cape jasmine, turmeric or sophora flower, the blue pigment extracted from bluegrass, the mineral black extracted from walnut tree, persimmon tree or robur.
The described cured animals and plants for obtaining from animal or plant are cured.
Embodiment 2:
A kind of complete renewable environmental protection flexographic ink is be prepared from by the composition of following massfraction: binder 70%, vegetable pigment 15%, Synolac 2.5%, vegetables oil 2.5%, wax 1.0%, vegetable oil derivatives 9%;
Described binder is prepared from by the composition of following massfraction: the rosin modified phenolic resin of 38 ~ 40%, the vegetables oil of 28 ~ 32% and 20 ~ 38% vegetable oil derivatives be prepared from.
All the other moietys are with embodiment 1.
Embodiment 3:
A kind of complete renewable environmental protection flexographic ink is be prepared from by the composition of following massfraction: binder 60%, vegetable pigment 25%, Synolac 3%, vegetables oil 3%, wax 1.0%, vegetable oil derivatives 8%;
Described binder is prepared from by the composition of following massfraction: the rosin modified phenolic resin of 42%, the vegetables oil of 27% and 31% vegetable oil derivatives be prepared from.
All the other moietys are with embodiment 1.
The preparation method of above-mentioned three embodiments, comprises the steps:
1) prepare burden, get out the material of the mass fraction of being correlated with according to ink formulations;
2) binder is prepared, vegetables oil and rosin modified phenolic resin is added in reactor, heat up and stir, temperature adds 85% of the total consumption of vegetable oil derivatives after reaching 180 ~ 210 DEG C of insulation for some time, all the other vegetable oil derivatives of 15% are for adjusting viscosity, it is stand-by that viscosity filters rear discharging, prepares binder;
3) pre-dispersed, vegetable pigment, Synolac, vegetables oil are added in binder and carries out dispersion and stir;
4) grinding and stirring, is ground to fineness by the material obtained pre-dispersed in step 3) and reaches less than 7.5 microns, then add wax and vegetable oil derivatives stirs;
5) aftertreatment, by warehouse-in after carrying out through the material of step 4) process detecting, packing.
Following table is the performance comparison data sheet of complete renewable environmental protection flexographic ink that in embodiment 1 ~ 3, any embodiment prepares and common flexographic ink, high renewable composition environment-friendly ink (ink prepared by the renewable composition of non-fully).
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every utilize description of the present invention to do equivalent structure or equivalent flow process conversion; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.
Claims (8)
1. a complete renewable environmental protection flexographic ink, it is characterized in that, be prepared from by the composition of following massfraction: binder 55 ~ 75%, vegetable pigment 10 ~ 25%, Synolac 0 ~ 5%, vegetables oil 0 ~ 5%, wax 0 ~ 2%, vegetable oil derivatives 5 ~ 10%;
Described binder is prepared from by the composition of following massfraction: the rosin modified phenolic resin of 35 ~ 45%, the vegetables oil of 20 ~ 35% and 10 ~ 40% vegetable oil derivatives be prepared from.
2. complete renewable environmental protection flexographic ink according to claim 1, it is characterized in that, described rosin modified phenolic resin comprises the first rosin modified phenolic resin and the second rosin modified phenolic resin, described first rosin modified phenolic resin is made up of rosin, maleficent acid, dimeracid and glycerol polymerization modification, and described second rosin modified phenolic resin is prepared from by rosin, maleficent acid and glycerin modification.
3. complete renewable environmental protection flexographic ink according to claim 1, it is characterized in that, described Synolac is long oil alkyd, and described Synolac adopts one or more modified alkyd resins obtained with maleficent acid, glycerine reaction in oleum lini, soya-bean oil, Oleum Cocois, rapeseed oil, rosin, dimeracid.
4. complete renewable environmental protection flexographic ink according to claim 1, it is characterized in that, described vegetables oil is that dry vegetable oil and semi-drying vegetable oils mix, described dry vegetable oil comprises oleum lini, tung oil, perilla oil and Chinese catalpa oil, and described semi-drying oil comprises soya-bean oil, rapeseed oil and Viscotrol C.
5. complete renewable environmental protection flexographic ink according to claim 1, it is characterized in that, described vegetable oil derivatives is the cut cut substrate of soybean oil methyl ester, soya-bean oil ethyl ester, soya-bean oil isobutyl ester, palm oil methyl ester, plam oil ethyl ester, plam oil isobutyl ester, rapeseed methylester, rapeseed oil ethyl ester or rapeseed oil isobutyl ester.
6. complete renewable environmental protection flexographic ink according to claim 5, is characterized in that, the boiling range of described cut cut substrate between 260 ~ 320 DEG C, pour point below 0 DEG C, cold filter clogging temperature is below 0 DEG C.
7. complete renewable environmental protection flexographic ink according to claim 1, it is characterized in that, described vegetable pigment comprises the red extracting from safflower, lignum sappan or madder and obtain, the yellow pigment extracted from cape jasmine, turmeric or sophora flower, the blue pigment extracted from bluegrass, the mineral black extracted from walnut tree, persimmon tree or robur.
8. complete renewable environmental protection flexographic ink according to claim 1, is characterized in that, the described cured animals and plants for obtaining from animal or plant are cured.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610019842.0A CN105462349A (en) | 2016-01-13 | 2016-01-13 | Completely-renewable, green and environment-friendly offset printing ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610019842.0A CN105462349A (en) | 2016-01-13 | 2016-01-13 | Completely-renewable, green and environment-friendly offset printing ink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105462349A true CN105462349A (en) | 2016-04-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610019842.0A Pending CN105462349A (en) | 2016-01-13 | 2016-01-13 | Completely-renewable, green and environment-friendly offset printing ink |
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| CN (1) | CN105462349A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106118229A (en) * | 2016-08-29 | 2016-11-16 | 苏州安洁科技股份有限公司 | A kind of environment-friendly ink |
| CN106497216A (en) * | 2016-10-26 | 2017-03-15 | 上海数印网络科技有限公司 | A kind of low dry move back the special wide colour gamut fluorescent ink of 10 microns of modulating nets |
| CN106833120A (en) * | 2017-03-03 | 2017-06-13 | 苏州市博来特油墨有限公司 | The stainless coloring agent printing ink of high osmosis wearable environment protection |
| CN107722717A (en) * | 2017-10-12 | 2018-02-23 | 山东丽鹏股份有限公司 | A kind of offset metal ink and preparation method thereof and offset metal ink are applied to the typography of aluminium sheet |
| CN107793834A (en) * | 2017-11-20 | 2018-03-13 | 武汉红金龙印务股份有限公司 | A kind of preparation method and application of the single-sheet offset printing ink of low VOC content |
| CN107793833A (en) * | 2016-08-31 | 2018-03-13 | 天津天女化工集团股份有限公司 | A kind of Water-free environment-friendlyurinal offset ink |
| CN108342925A (en) * | 2017-12-30 | 2018-07-31 | 苏州丰倍生物科技有限公司 | A kind of carbonless paper environmentally friendly solvent oil and preparation method thereof from fixation |
| CN113234348A (en) * | 2021-04-30 | 2021-08-10 | 新华社印务有限责任公司 | Green and environment-friendly printing ink |
| CN113637353A (en) * | 2021-09-03 | 2021-11-12 | 杭华油墨股份有限公司 | Ink binder and preparation method and application thereof |
| CN114854244A (en) * | 2022-04-27 | 2022-08-05 | 北京金印联国际供应链管理有限公司 | Environment-friendly offset printing ink and preparation method thereof |
| CN115505290A (en) * | 2021-06-23 | 2022-12-23 | 上海深日化工有限公司 | Full vegetable oil high-gloss environment-friendly offset printing ink |
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| CN102643577A (en) * | 2012-05-03 | 2012-08-22 | 中钞油墨有限公司 | Environment-friendly printing ink suitable for high speed rotary printing |
| CN102796419A (en) * | 2012-08-20 | 2012-11-28 | 中钞油墨有限公司 | Offset ink for improving polyester film binding fastness |
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| CN101250353A (en) * | 2008-03-26 | 2008-08-27 | 中国印钞造币总公司 | Soybean oil based hectographic ink and bonding material thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106118229A (en) * | 2016-08-29 | 2016-11-16 | 苏州安洁科技股份有限公司 | A kind of environment-friendly ink |
| CN107793833A (en) * | 2016-08-31 | 2018-03-13 | 天津天女化工集团股份有限公司 | A kind of Water-free environment-friendlyurinal offset ink |
| CN106497216A (en) * | 2016-10-26 | 2017-03-15 | 上海数印网络科技有限公司 | A kind of low dry move back the special wide colour gamut fluorescent ink of 10 microns of modulating nets |
| CN106497216B (en) * | 2016-10-26 | 2019-06-18 | 上海数印网络科技股份有限公司 | It is a kind of low dry to move back the dedicated wide colour gamut fluorescent ink of 10 microns of modulating nets |
| CN106833120A (en) * | 2017-03-03 | 2017-06-13 | 苏州市博来特油墨有限公司 | The stainless coloring agent printing ink of high osmosis wearable environment protection |
| CN107722717A (en) * | 2017-10-12 | 2018-02-23 | 山东丽鹏股份有限公司 | A kind of offset metal ink and preparation method thereof and offset metal ink are applied to the typography of aluminium sheet |
| CN107793834B (en) * | 2017-11-20 | 2021-05-04 | 武汉红金龙印务股份有限公司 | Preparation method and application of single-sheet paper offset printing ink with low VOC content |
| CN107793834A (en) * | 2017-11-20 | 2018-03-13 | 武汉红金龙印务股份有限公司 | A kind of preparation method and application of the single-sheet offset printing ink of low VOC content |
| CN108342925A (en) * | 2017-12-30 | 2018-07-31 | 苏州丰倍生物科技有限公司 | A kind of carbonless paper environmentally friendly solvent oil and preparation method thereof from fixation |
| CN113234348A (en) * | 2021-04-30 | 2021-08-10 | 新华社印务有限责任公司 | Green and environment-friendly printing ink |
| CN115505290A (en) * | 2021-06-23 | 2022-12-23 | 上海深日化工有限公司 | Full vegetable oil high-gloss environment-friendly offset printing ink |
| CN113637353A (en) * | 2021-09-03 | 2021-11-12 | 杭华油墨股份有限公司 | Ink binder and preparation method and application thereof |
| CN113637353B (en) * | 2021-09-03 | 2023-10-24 | 杭华油墨股份有限公司 | Printing ink binder and preparation method and application thereof |
| CN114854244A (en) * | 2022-04-27 | 2022-08-05 | 北京金印联国际供应链管理有限公司 | Environment-friendly offset printing ink and preparation method thereof |
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Application publication date: 20160406 |