CN105420093B - Biological surfactant microemulsion production system for cosmetics - Google Patents

Biological surfactant microemulsion production system for cosmetics Download PDF

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CN105420093B
CN105420093B CN201610014953.2A CN201610014953A CN105420093B CN 105420093 B CN105420093 B CN 105420093B CN 201610014953 A CN201610014953 A CN 201610014953A CN 105420093 B CN105420093 B CN 105420093B
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fermentation
connecting rod
storage tank
stirring rod
distribution plate
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CN105420093A (en
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程叶红
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Perfect (Guangdong) Commodity Co., Ltd.
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Three Huamai Chemical Products Co Ltd
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Abstract

The present invention relates to a kind of biological surfactant microemulsion production systems for cosmetics, the fermentation cauldron for microbial fermentation production biosurfactant；Second agitating shaft is set in fermentation cauldron, the radial setting connecting rod in the lower end of second agitating shaft, shape is found respectively, stirring rod is set in the end of connecting rod, the agitating paddle of stirring feed liquid is respectively set in connecting rod and/or stirring rod, the length of stirring rod is twice of connecting rod, and connecting rod includes the first, second and third connecting rod, and stirring rod includes the first, second and third stirring rod, agitating paddle is respectively set in the upper section of first connecting rod, the lower section of the second stirring rod and third stirring rod, and agitating paddle is that a plate is constituted.The biological surfactant microemulsion production system for cosmetics provided in above-mentioned technical proposal, by carrying out purifying and microemulsified processing to fermentation liquid, so that the micro emulsion of biosurfactant quickly be made.

Description

Biological surfactant microemulsion production system for cosmetics
It is on November 14th, 2014 that the present invention, which is the applying date, application No. is 201410650537.2, entitled " makeup The divisional application of the patent of invention of the biological surfactant microemulsion production system of product, food, chemical industry and agricultural ".
Technical field
The present invention relates to emulsifier production fields, and in particular to a kind of cosmetics, food, chemical industry and agricultural are living with biological table Agent microemulsion production system.
Background technique
Micro emulsion is the transparent or semitransparent thermodynamic stable system spontaneously formed, there is oil-in-water and two kinds of Water-In-Oil Type.The formation of micro emulsion be it is spontaneous, do not need it is extraneous energy is provided, be a kind of system that thermodynamics is highly stable, because This is widely used in fields such as petrochemical industry, cosmetics, food.Wherein, the microemulsion prepared by biosurfactant Liquid is usually used in the cosmetics of super quality, more stable, highly-safe, skin absorption is good.Such micro emulsion the preparation method comprises the following steps: will Biosurfactant (Lipopeptide Biosurfactants), cosurfactant (C3~C5 alcohol) are mixed with alkali (sodium hydroxide) Forming surfactants mixed liquor is prepared, is prepared water phase (generally salt water), liquefaction phase (generally alkane, cycloalkane, fragrance are matched Hydrocarbon)；Prepared surfactant mixed liquor is added in water phase and is uniformly mixed, then mutually instills above-mentioned solution dropwise for oily In, and constantly stir evenly, until solution by muddiness to clarifying, obtain the micro emulsion being made of biosurfactant, Due to needing using oily phase is added dropwise dropwise, so that the throughput rate bottom of micro emulsion, seriously affects production rate.
Summary of the invention
It is an object of the invention to provide a kind of biological surfactant microemulsion production systems for cosmetics.
To achieve the above object, the invention adopts the following technical scheme:
A kind of biological surfactant microemulsion production system for cosmetics, which is characterized in that including following production equipment:
Fermentation cauldron for microbial fermentation production biosurfactant；
For in fermentation cauldron fermentation liquid carry out purifies and separates processing fermentation liquid purifier apparatus and for storing it is pure The biosurfactant storage tank of biosurfactant after change；
It is respectively used to cosurfactant storage tank, the lye storage of storage cosurfactant, lye, water phase and oily phase Tank, water phase storage tank and oily phase storage tank；
And surfactant Compound mixed solution kettle and micro emulsion reaction kettle；Fermentation cauldron, fermentation liquid purifier apparatus and life Object surfactant storage tank is successively attached, biosurfactant storage tank, cosurfactant storage tank and alkali liquor storage tank Liquid outlet be connected with surfactant Compound mixed solution kettle, surfactant Compound mixed solution kettle and water phase storage tank go out Liquid mouth is connected with micro emulsion reaction kettle；
The second rabbling mechanism is provided in fermentation cauldron, the top of fermentation cauldron is provided with material input port, the lower part of fermentation cauldron Discharge port is set, and the second rabbling mechanism includes the second agitating shaft of vertical shape arrangement, and the periphery of the second agitating shaft is uniformly arranged vertical shape The snorkel of arrangement is arranged at intervals with gas distribution plate on the pipe shaft of snorkel, offers in the middle part of each gas distribution plate and stir for second The through-hole that axis passes through is mixed, the inside of gas distribution plate is arranged to uniformly open up qi-emitting hole in the plate face of cavity-like and gas distribution plate, respectively Strainer is provided at qi-emitting hole, the lumen of each snorkel is connected with the inner cavity of a gas distribution plate respectively to be connect, each snorkel Upper end is connected after passing through fermentation cauldron autoclave body with air-blowing device, and temperature sensor and PH measurement component are additionally provided in fermentation cauldron；
The radial setting connecting rod in the lower end of second agitating shaft, the end of connecting rod found shape respectively and stirring rod, connection are arranged The agitating paddle of stirring feed liquid is respectively set on bar and/or stirring rod, the length of stirring rod is twice of connecting rod, and connecting rod includes First, second and third connecting rod, stirring rod include the first, second and third stirring rod, first connecting rod, the lower section of the second stirring rod and the Agitating paddle is respectively set in the upper section of three stirring rods, and agitating paddle is that a plate is constituted.
The biological surfactant microemulsion production system of cosmetics, food, chemical industry and the agricultural provided in above-mentioned technical proposal, By carrying out purifying and microemulsified processing to fermentation liquid, so that the micro emulsion of biosurfactant quickly be made.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is the structural schematic diagram of fermentation liquid purifier apparatus；
Fig. 3 is the structural schematic diagram of the second rabbling mechanism, gas distribution plate and snorkel；
Fig. 4 is the structural schematic diagram of the first rabbling mechanism, liquid distribution plate part and oily phase inlet tube；
Fig. 5 is the structural schematic diagram of gas distribution plate；
Fig. 6 is the structural schematic diagram of liquid distribution plate part；
Fig. 7 is the structural schematic diagram of shedding mechanism；
Fig. 8 is the structural schematic diagram of plate face on the downside of the first stripper.
Specific embodiment
In order to which objects and advantages of the present invention are more clearly understood, the present invention is carried out specifically with reference to embodiments It is bright.It should be appreciated that following text is only used to describe one or more of specific embodiments of the invention, not to the present invention The protection scope specifically requested carries out considered critical.
The technical solution that the present invention takes is as shown in Figure 1, 2, and a kind of cosmetics, food, chemical industry and agricultural are living with biological table Agent microemulsion production system, which is characterized in that including following production equipment:
Fermentation cauldron 40 for microbial fermentation production biosurfactant；
For carrying out the fermentation liquid purifier apparatus 90 of purifies and separates processing to the fermentation liquid in fermentation cauldron 40 and for storing up Put the biosurfactant storage tank 10 of biosurfactant after purification；
It is respectively used to cosurfactant storage tank 80, the lye storage of storage cosurfactant, lye, water phase and oily phase Tank 50, water phase storage tank 60 and oily phase storage tank 70；
And surfactant Compound mixed solution kettle 20 and micro emulsion reaction kettle 30；Fermentation cauldron, fermentation liquid purifier apparatus It is successively attached with biosurfactant storage tank, biosurfactant storage tank, cosurfactant storage tank and lye The liquid outlet of storage tank is connected with surfactant Compound mixed solution kettle, surfactant Compound mixed solution kettle and water phase storage tank Liquid outlet be connected with micro emulsion reaction kettle.
The biological surfactant microemulsion production system of cosmetics, food, chemical industry and the agricultural provided in above-mentioned technical proposal, By carrying out purifying and microemulsified processing to fermentation liquid, so that the micro emulsion of biosurfactant quickly be made.Due to The period of fermentation is longer, and in order to guarantee the continuity of production, multiple fermentation cauldrons, the fermentation liquid outlet of multiple fermentation cauldrons can be set It is connected respectively with purification devices.
Due to fermentation broth contents complexity, including thallus, the solid medium not being fermented is not fully utilized by microorganism Carbohydrate, inorganic salts, protein and the various metabolites of microorganism, fermentation broth viscosity is big, for fermentation liquid purifier apparatus, It specifically can be as shown in Fig. 2, including latter linked dilution device 91, rough filtering device 92, micro-filtration 93, decontamination before setting gradually Albumen device 94, decontamination ion unit 95 and salinization device 96.Dilution device is mainly diluted and adjusts to fermentation liquid PH is generally constituted using groove body；Rough filtering device mainly by fermentation liquid thallus, the solid medium that is not fermented and other Spin-on filter device or other filter plants can be used to getting rid of in biggish solid impurity, and multiple filterings can also be used and set Standby to be used in conjunction, the fermentation liquid after thick worry can be diluted and adjust again PH；Micro-filtration mainly removes the small molecular weight impurity in fermentation liquid, Such as pigment is generally carried out using film filter, and the aperture of used filter membrane should be according to purpose biosurfactant Molecular size chosen, should filter membrane be retained to biosurfactant, ceramic membrane generally can be used；Micro-filtration Later it can be diluted and adjust herein PH；Decontamination albumen device can be isoelectric precipitation device, decontamination ion unit Predominantly resin adsorption device, by eluting to the MICROBIAL SURFACTANT after absorption, eluent and lye are in salinization Reaction is carried out in device generates salt.It can not certainly for purifier apparatus used by different types of biosurfactant Together, the specific purifier apparatus that this law provides is primarily adapted for use in the purification process of Lipopeptide Biosurfactants.For other The purifying of the biosurfactant (such as carbohydrate, lipoprotein) of type, general process are also dilution, thick worry, micro-filtration, removal Impurity protein and ion.
Since fermentation broth viscosity is big in fermentation cauldron, conventionally employed tracheae is passed through air it is difficult to ensure that filtrated air is being sent out Being uniformly distributed in fermentation tank.Therefore, the present invention is implemented using the technical side such as Fig. 3,5 shown in: the of setting in fermentation cauldron Two rabbling mechanisms, the top of fermentation cauldron are provided with material input port, and discharge port, the second rabbling mechanism packet is arranged in the lower part of fermentation cauldron The second agitating shaft 41 of vertical shape arrangement is included, the periphery of the second agitating shaft 41 is uniformly arranged the snorkel 45 of vertical shape arrangement, snorkel Gas distribution plate 46 is arranged at intervals on 45 pipe shaft, the middle part of each gas distribution plate 46 is offered to be led to for what the second agitating shaft 41 passed through Hole, the inside of gas distribution plate 46 are arranged to uniformly open up qi-emitting hole 461 in the plate face of cavity-like and gas distribution plate 46, each qi-emitting hole Strainer is provided at 461, the lumen of each snorkel is connected with the inner cavity of a gas distribution plate 46 respectively to be connect, each snorkel 45 Upper end is connected after passing through autoclave body with air-blowing device, and temperature sensor and PH measurement component are additionally provided in fermentation cauldron.Stratiform row The gas distribution plate 46 of cloth can supplement air from each layer phase fermentation liquid, so that air in fermentation liquid when blasting filtrated air Uniformly, guarantee the fermentation of biosurfactant.
Preferred scheme are as follows: gas distribution plate can be constituted using a cone-shaped hood that Open Side Down, be opened up in the middle part of cone-shaped hood Through-hole is arranged to cavity-like inside the cover of cone-shaped hood, qi-emitting hole 461 is uniformly arranged in the outer cover of cone-shaped hood.Such gas distribution Uniformity and horizontal covering surface it is maximum, as shown in Figure 5.There are three the gas distribution plate stratiform settings, snorkel setting There are three, the upper end of snorkel passes through four-pass connecting joint and tracheae and drum after the motor mount on fermentation cauldron autoclave body top Device of air is connected.
It is further as shown in Figure 7,8, shedding mechanism is provided at discharge port, shedding mechanism includes at fermentor discharge port Circular first and second stripper 42,43 being arranged in parallel above and below, the first stripper 42 are fixed with one with fermentor, and second unloads Offer annular groove on the side of flitch 43, the second stripper 43 by the steel ball component 48 that is arranged in annular groove and fermentor around Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of the first and second stripper 42,43 is located on same plumb line, the first and second discharging Open up first and second discharge port 42a, 43a, the lower face setting of the first stripper 42 on plate at the circumference of same radius size respectively Step-like, the upper face in second step face 422 and the second stripper 43 is constituted at by the combination of the first and second step surface 421,422 It fits, forms cavity between 43 upper face of First terrace 421 and the second stripper, the first discharge port 42a is provided with first On step surface 421, sealing element 423, the shape of sealing element 423 and first and second are provided at the step that the first and second step surface is joined The step shape of step surface junction is consistent, and the second stripper 43 is connected with driving mechanism, preferred scheme are as follows: first and second The outer profile of step surface junction is arc, sets arc for sealing element in this way, and sealing element can be used O-ring seals, first The height that the upper face of stripper is arranged at cone cell and the first discharge port is minimum.By driving mechanism adjust the second stripper into Row rotation, so that the first and second discharge port on the first and second stripper is corresponding and different, to realize to the quick of fermentor The closure of discharging and discharge port realizes quickly discharging material, to save the time, improves extraction efficiency.
In order to improve the rate of microemulsified, the present invention is implemented using the technical side as shown in Fig. 4,6: micro emulsion is anti- Kettle is answered, including the first rabbling mechanism being arranged in autoclave body and autoclave body, the first rabbling mechanism includes the first stirring of vertical shape arrangement Axis 31, the periphery of the first agitating shaft 31 are uniformly arranged the oily phase inlet tube 35 of vertical shape arrangement, on the pipe shaft of oily phase inlet tube 35 between Every being provided with liquid distribution plate part 36, the middle part of each liquid distribution plate part 36 offers the through-hole passed through for the first agitating shaft 31, liquid distribution plate part 36 inside is arranged to cavity-like and the lower face of liquid distribution plate part 36 uniformly opens up liquid distributing hole, the lumen difference of each oil phase inlet tube It is connected with the inner cavity of a liquid distribution plate part 36 and connect, the upper end of each oil phase inlet tube is connected after passing through autoclave body with oily phase storage tank, Surfactant mixed liquor feed liquor nozzle and water phase feed liquor nozzle are additionally provided on autoclave body.The liquid distribution plate part 36 of stratiform arrangement, When oily phase is added dropwise, oil is mutually instilled in the mixed liquor in reaction kettle from each liquid distributing hole on liquid distribution plate part 36, relative to traditional One after another drop of instillation significantly improves production efficiency.Certain spacing should be kept between each liquid distributing hole, when specific operation, liquid distributing hole is The needle tubing plugged on liquid distribution plate part 36 is constituted, and the length of adjacent needle tubing is different.
Preferred scheme are as follows: liquid distribution plate part 36 is that the cone-shaped hood of an opening upwards is constituted, and opens up through-hole in the middle part of cone-shaped hood, It is arranged to cavity-like inside the cover of cone-shaped hood, the needle tubing 361 for constituting qi-emitting hole is uniformly arranged in the outer cover of cone-shaped hood, The length direction of needle tubing 361 and the perpendicular arrangement of the cover of cone-shaped hood, needle tubing is arranged on the cover of cone-shaped hood in round, and needle The length of pipe increases with the radius of cone-shaped hood and is increased, and the effect for instilling oily phase in this way is best.The liquid distribution plate part stratiform is set There are three setting, oily phase inlet tube is provided with three, and the upper end of oily phase inlet tube passes through four-pass connecting joint and material after passing through autoclave body Liquid conveyance conduit is connected with oily phase storage tank.
Due to being respectively provided with distribution device and liquid distributor, the first and second agitating shaft axle body on the first and second agitating shaft On agitating paddle can not be set, therefore the first and second rabbling mechanism is implemented using identical technical solution in the present invention, Yi Jiru Fig. 3, shown in 4, the radial setting connecting rod in lower end of the first and second agitating shaft 31,41, the end of connecting rod is stood shape setting respectively and is stirred Bar is mixed, the agitating paddle 34 of stirring feed liquid is respectively set in connecting rod and/or stirring rod.The length for being specifically stirring rod is connection Twice of bar, connecting rod include the first, second and third connecting rod 324,322,323, stirring rod include the first, second and third stirring rod 334, 332,333, stirring is respectively set in the upper section of first connecting rod 324, the lower section of the second stirring rod 332 and third stirring rod 333 Paddle 34, agitating paddle 34 are that a plate is constituted, and such rabbling mechanism can from different directions be stirred solution, improve mixed The uniformity of conjunction.Stirring rod and connecting rod are that angle steel is constituted, and such intensity is big, installation and blender convenient for agitating paddle 34 The stability of structure.
In addition, the kettle wall of fermentation cauldron is sandwich, and the clip cavity that sandwich is formed is for accommodating hot-fluid for fermentation cauldron Body.Hot fluid meets the needs of microbial fermentation for adjusting fermentation temperature in the kettle.For micro emulsion reaction kettle, autoclave body Flow-interfering bar is provided on inner sidewall, the side wall of autoclave body is sandwich composition, and the clip cavity that sandwich is formed is for accommodating hot-fluid Body.Hot fluid adapts to the production of different micro emulsions for adjusting temperature in the kettle.
Third rabbling mechanism and ultrasound emission component, surfactant are provided in surfactant Compound mixed solution kettle The kettle wall for preparing kettle is sandwich, the clip cavity of sandwich formation for accommodating heating fluid.Ultrasound emission component is to material It is vibrated, so that surfactant, cosurfactant quickly mix.
In short, the present invention can effectively improve the production efficiency of micro emulsion.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, in knowing the present invention after contents, without departing from the principle of the present invention, it can also be made several Same transformation and substitution, these convert and substitute on an equal basis and also should be regarded as belonging to the scope of protection of the present invention.

Claims (2)

1. a kind of biological surfactant microemulsion production system for cosmetics, which is characterized in that including following production equipment:
Fermentation cauldron for microbial fermentation production biosurfactant；
For carrying out the fermentation liquid purifier apparatus of purifies and separates processing to the fermentation liquid in fermentation cauldron and for storing after purification Biosurfactant biosurfactant storage tank；
Be respectively used to storage cosurfactant, lye, water phase and oily phase cosurfactant storage tank, alkali liquor storage tank, water Phase storage tank and oily phase storage tank；
And surfactant Compound mixed solution kettle and micro emulsion reaction kettle；Fermentation cauldron, fermentation liquid purifier apparatus and biological table Face activating agent storage tank is successively attached, and biosurfactant storage tank, cosurfactant storage tank and alkali liquor storage tank go out Liquid mouth is connected with surfactant Compound mixed solution kettle, the liquid outlet of surfactant Compound mixed solution kettle and water phase storage tank It is connected with micro emulsion reaction kettle；
The second rabbling mechanism is provided in fermentation cauldron, the top of fermentation cauldron is provided with material input port, the lower part setting of fermentation cauldron Discharge port, the second rabbling mechanism include the second agitating shaft of vertical shape arrangement, and the periphery of the second agitating shaft is uniformly arranged vertical shape arrangement Snorkel, be arranged at intervals with gas distribution plate on the pipe shaft of snorkel, offer in the middle part of each gas distribution plate for the second agitating shaft By through-hole, the inside of gas distribution plate is arranged to uniformly open up qi-emitting hole, each gas distribution in the plate face of cavity-like and gas distribution plate Strainer is provided at hole, the lumen of each snorkel is connected with the inner cavity of a gas distribution plate respectively to be connect, the upper end of each snorkel It is connected after fermentation cauldron autoclave body with air-blowing device, temperature sensor and PH measurement component is additionally provided in fermentation cauldron；
The radial setting connecting rod in the lower end of second agitating shaft, the end of connecting rod respectively stand shape be arranged stirring rod, connecting rod and/ Or the agitating paddle of stirring feed liquid is respectively set on stirring rod, the length of stirring rod is twice of connecting rod, connecting rod includes first, Two, three connecting rod, stirring rod include the first, second and third stirring rod, and first connecting rod, the lower section of the second stirring rod and third are stirred Agitating paddle is respectively set in the upper section for mixing bar, and agitating paddle is that a plate is constituted.
2. the biological surfactant microemulsion production system according to claim 1 for cosmetics, it is characterised in that: gas distribution Plate is that first cone-shaped hood that Open Side Down is constituted, and opens up through-hole in the middle part of the first cone-shaped hood, in the cover of the first cone-shaped hood Portion is arranged to cavity-like, is uniformly arranged qi-emitting hole in the outer cover of the first cone-shaped hood.
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CN201610015551.4A Active CN105505748B (en) 2014-11-14 2014-11-14 A kind of biological surfactant microemulsion production system for chemical industry
CN201610017018.1A Active CN105543076B (en) 2014-11-14 2014-11-14 The biological surfactant microemulsion production system of food
CN201610015251.6A Active CN105543074B (en) 2014-11-14 2014-11-14 A kind of fermentation cauldron for microbial fermentation production biosurfactant
CN201610017019.6A Expired - Fee Related CN105879816B (en) 2014-11-14 2014-11-14 Cosmetics biology surfactant microemulsion production micro emulsion reaction kettle
CN201410650537.2A Active CN104450510B (en) 2014-11-14 2014-11-14 Cosmetics, food, chemical industry and agricultural biology surfactant microemulsion production system
CN201610015244.6A Active CN105420094B (en) 2014-11-14 2014-11-14 Biological surfactant microemulsion production system for food
CN201610016980.3A Active CN105505757B (en) 2014-11-14 2014-11-14 A kind of biological surfactant microemulsion production system of chemical industry
CN201610017016.2A Active CN105543075B (en) 2014-11-14 2014-11-14 The biological surfactant microemulsion production system of agricultural
CN201610017026.6A Active CN105543077B (en) 2014-11-14 2014-11-14 Biological food surfactant microemulsion production fermentation cauldron
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