CN209108972U - A kind of FAU zeolite membrane circulation preparation facilities for CO2 capture - Google Patents
A kind of FAU zeolite membrane circulation preparation facilities for CO2 capture Download PDFInfo
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- CN209108972U CN209108972U CN201821679849.6U CN201821679849U CN209108972U CN 209108972 U CN209108972 U CN 209108972U CN 201821679849 U CN201821679849 U CN 201821679849U CN 209108972 U CN209108972 U CN 209108972U
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- zeolite membrane
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- liquid outlet
- perfusion tube
- rose box
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Abstract
The utility model discloses a kind of FAU zeolite membranes for CO2 capture to recycle preparation facilities, including zeolite membrane hydrothermal synthesis case, the bottom end of outer wall on the right side of the zeolite membrane hydrothermal synthesis case is communicated with Rose Box by the first liquid outlet, solvent recycling apparatus is provided on the right side of the filtering box outer wall, agitator tank is provided on the left of the solvent recycling apparatus, the intracavitary right side of the Rose Box is connected to by the first perfusion tube with agitator tank, the bottom of the stirring box outer wall is communicated with liquid storage chamber by the second liquid outlet, the bottom of the liquid storage chamber is communicated with separating tube, the lower end of the separating tube is communicated with liquid separation tank, the bottom of the liquid separation tank is communicated with the second perfusion tube by third liquid outlet, second perfusion tube is communicated with ion chromatograph far from one end of third liquid outlet, the utility model relates to zeolite membrane preparation technical fields.This recycles preparation facilities for the CO2 FAU zeolite membrane captured, has achieved the purpose that recycle solvent, has improved the utilization rate of raw material.
Description
Technical field
The utility model relates to zeolite membrane preparation technical field, specially a kind of FAU zeolite membrane circulation for CO2 capture
Preparation facilities.
Background technique
Zeolite membrane is a kind of with uniform micro, the absorption being mainly made of silicon, aluminium, oxygen and some other metal cation
Agent or film substance, aperture is suitable with general molecular size, and various fluid molecules are sieved according to its effective aperture.Zeolite membrane
Refer to those natural and artificial synthesized crystalline aluminosilicates with molecular sieve effect.Zeolite membrane due to its distinctive structure and
Performance, it has also become an independent subject, zeolite membrane application spread petrochemical industry, environmental protection, bioengineering, food industry,
The fields such as medication chemistry.With the development of national economy every profession and trade, the application prospect of zeolite membrane is increasingly wide.
The existing FAU zeolite membrane for CO2 capture after the completion of preparation facilities prepared each time, remaining solvent is direct
Discharge, not only pollutes environment, but also also remain a large amount of silicon ion, aluminium ion and sodium ion in solvent, causes the utilization of raw material
Rate is low, increases production cost.
Utility model content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the utility model provides a kind of FAU zeolite membrane circulation preparation for CO2 capture
Device solves the problems, such as that solvent cannot recycle.
(2) technical solution
In order to achieve the above object, the utility model is achieved by the following technical programs: it is a kind of for CO2 capture
FAU zeolite membrane recycles preparation facilities, including zeolite membrane hydrothermal synthesis case, the bottom of the outer wall on the right side of the zeolite membrane hydrothermal synthesis case
End is communicated with the first liquid outlet, and first liquid outlet is communicated with Rose Box far from one end of zeolite membrane hydrothermal synthesis case, described
The position on the intracavitary right side of Rose Box is provided with the first perfusion tube, and the upper end of first perfusion tube is through Rose Box and is communicated with the
One water pump is provided with solvent recycling apparatus on the right side of the filtering box outer wall, is provided with and stirs on the left of the solvent recycling apparatus
Case is mixed, the right end of first water pump is connected to by the first perfusion tube with the inside of agitator tank, the bottom of the stirring box outer wall
The position at middle part offers the second liquid outlet, and the lower end of second liquid outlet is communicated with liquid storage chamber, the bottom of the liquid storage chamber
It is arranged at intervals with separating tube, the upper end of the separating tube is connected to the inside of liquid storage chamber, and the lower end of the separating tube is communicated with point
Flow container, the bottom of the liquid separation tank offer third liquid outlet, and the lower end of the third liquid outlet is communicated with the second perfusion tube,
Second perfusion tube is communicated with ion chromatograph far from one end of third liquid outlet.
Preferably, the position in the intracavitary left side of the Rose Box is provided with the first strainer, the intracavitary middle part of the Rose Box
And the position of the first perfusion tube is provided with the second strainer, the upper and lower ends of first strainer and the second strainer with filtering
The inner wall of case is fixedly connected.
Preferably, the position at the intracavitary middle part of the agitator tank is provided with shaft, is fixedly connected at left and right sides of the shaft
There is stirring rod, the inside of the stirring rod is uniformly provided with through-hole.
Preferably, the position of the agitator tank upper surface middle part is equipped with motor, and agitator tank is run through on the top of the shaft
And it is rotatablely connected with motor.
Preferably, second perfusion tube is communicated with the second water pump, the ion chromatography close to one end of ion chromatograph
The position of instrument upper surface middle part offers sample inlet, and the right end of second water pump passes through the second perfusion tube and sample feed liquor
Mouth connection.
Preferably, the inner wall on the right side of the agitator tank is provided with return pipe, the upper end of the return pipe through agitator tank and
It is communicated with third water pump, the left end of the third water pump is connected to by return pipe with the upper end on the right side of zeolite membrane hydrothermal synthesis case.
(3) beneficial effect
The utility model provides a kind of FAU zeolite membrane circulation preparation facilities for CO2 capture.Have following beneficial to effect
Fruit:
(1), the FAU zeolite membrane circulation preparation facilities for being used for CO2 capture, zeolite membrane hydrothermal synthesis case pass through hydrothermal synthesis
Method for the first time preparation zeolite membrane after, open the first liquid outlet valve, remaining solvent enters in Rose Box, by first
Strainer and the second strainer filtering fall impurity, open the first water pump, and solvent is entered in agitator tank by the first perfusion tube, open electricity
Machine, motor drive shaft rotation, and shaft drives stirring rod rotation, and stirring rod carries out uniform stirring, the inside of stirring rod to solvent
It is uniformly provided with through-hole, makes stirring more evenly, is uniformly distributed the silicon ion in solvent, aluminium ion and sodium ion, is improved below
The precision of ion chromatograph detection after stirring, opens the valve of the second liquid outlet, and solvent enters in liquid storage chamber, then leads to
It crosses separating tube to respectively enter in three different liquid separation tanks, first opens the valve of the third liquid outlet of first liquid separation tank, open
Second water pump, the solvent in first liquid separation tank are entered in ion chromatograph by the second perfusion tube, drive ion chromatograph work
To make, ion chromatograph is analyzed and is detected to the content of silicon ion, aluminium ion and sodium ion in solvent, after detection,
The valve of the third liquid outlet of second liquid separation tank is opened, second is carried out and detects, then carry out third time detection again, repeatedly examine
The precision for improving detection is surveyed, the valve of third water pump and return pipe is then opened, the solvent in agitator tank comes back to zeolite membrane
In hydrothermal synthesis case, finally according to the testing result of ion chromatograph, supplement required siliceous, corresponding with containing sodium raw materials containing aluminium
Then amount carries out the preparation of second of zeolite membrane, repeat above step, carry out the preparation of multiple zeolite membrane, zeolite film water
Thermal synthesis case and ion chromatograph are the technologies of existing maturation, can directly buy, be pacified on the market according to installation instructions
Dress achieved the purpose that recycle solvent, improves the utilization rate of raw material.
Detailed description of the invention
Fig. 1 is that the FAU zeolite membrane for CO2 capture of the utility model recycles preparation facilities perspective view of the explosion；
Fig. 2 is the Rose Box structural schematic diagram of the utility model；
Fig. 3 is the solvent recycling apparatus structural schematic diagram of the utility model.
In figure: 1 zeolite membrane hydrothermal synthesis case, 2 first liquid outlets, 3 Rose Boxes, 4 first perfusion tubes, 5 first water pumps, 6 molten
Agent circulator, 7 agitator tanks, 8 second liquid outlets, 9 liquid storage chambers, 10 separating tubes, 11 liquid separation tanks, 12 third liquid outlets, 13 second
Perfusion tube, 14 ion chromatographs, 15 first strainers, 16 second strainers, 17 shafts, 18 stirring rods, 19 motors, 20 second water pumps,
21 sample inlets, 22 return pipes, 23 third water pumps.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, the utility model provides a kind of technical solution: a kind of FAU zeolite membrane circulation for CO2 capture
Preparation facilities, including zeolite membrane hydrothermal synthesis case 1, the bottom end of the outer wall on 1 right side of zeolite membrane hydrothermal synthesis case are communicated with first and go out
Liquid mouth 2, the first liquid outlet 2 are communicated with Rose Box 3, the position on the intracavitary right side of Rose Box 3 far from one end of zeolite membrane hydrothermal synthesis case 1
It installs and is equipped with the first perfusion tube 4, the upper end of the first perfusion tube 4 through Rose Box 3 and is communicated with the first water pump 5,3 outer wall of Rose Box
Right side be provided with solvent recycling apparatus 6, the left side of solvent recycling apparatus 6 is provided with agitator tank 7, and the right end of the first water pump 5 is logical
It crosses the first perfusion tube 4 to be connected to the inside of agitator tank 7, the position in the middle part of the bottom of 7 outer wall of agitator tank offers the second liquid outlet
8, the lower end of the second liquid outlet 8 is communicated with liquid storage chamber 9, and the bottom interval of liquid storage chamber 9 is provided with separating tube 10, separating tube 10 it is upper
End is connected to the inside of liquid storage chamber 9, and the lower end of separating tube 10 is communicated with liquid separation tank 11, and the bottom of liquid separation tank 11 offers third
Liquid outlet 12, the lower end of third liquid outlet 12 are communicated with the second perfusion tube 13, and the second perfusion tube 13 is far from third liquid outlet 12
One end is communicated with ion chromatograph 14.
The position in the intracavitary left side of Rose Box 3 is provided with the first strainer 15, the intracavitary middle part of Rose Box 3 and defeated close to first
The position of liquid pipe 4 is provided with the second strainer 16, inner wall of the upper and lower ends of the first strainer 15 and the second strainer 16 with Rose Box 3
It is fixedly connected.
The position at the intracavitary middle part of agitator tank 7 is provided with shaft 17, and the left and right sides of shaft 17 is fixedly connected with stirring rod 18,
The inside of stirring rod 18 is uniformly provided with through-hole.
The position of 7 upper surface middle part of agitator tank is equipped with motor 19, the top of shaft 17 through agitator tank 7 and with motor 19
Rotation connection.
Second perfusion tube 13 is communicated with the second water pump 20,14 upper surface of ion chromatograph close to one end of ion chromatograph 14
The position at middle part offers sample inlet 21, and the right end of the second water pump 20 is connected by the second perfusion tube 13 with sample inlet 21
It is logical.
The inner wall on 7 right side of agitator tank is provided with return pipe 22, and the upper end of return pipe 22 through agitator tank 7 and is communicated with third
The left end of water pump 23, third water pump 23 is connected to by return pipe 22 with the upper end on 1 right side of zeolite membrane hydrothermal synthesis case.
In use, opening first after zeolite membrane hydrothermal synthesis case 1 prepares zeolite membrane for the first time by the method for hydrothermal synthesis
The valve of liquid outlet 2, remaining solvent enter in Rose Box 3, filter out impurity by the first strainer 15 and the second strainer 16, beat
The first water pump 5 is opened, solvent is entered in agitator tank 7 by the first perfusion tube 4, opens motor 19, and motor 19 drives shaft 17 to rotate,
Shaft 17 drives stirring rod 18 to rotate, and stirring rod 18 carries out uniform stirring to solvent, and the inside of stirring rod 18 is uniformly provided with logical
Hole makes stirring more evenly, is uniformly distributed the silicon ion in solvent, aluminium ion and sodium ion, improves ion chromatograph 14 below
The precision of detection after stirring, opens the valve of the second liquid outlet 8, and solvent enters in liquid storage chamber 9, then passes through separating tube
10 respectively enter in three different liquid separation tanks 11, first open the valve of the third liquid outlet 12 of first liquid separation tank 11, open
Second water pump 20, the solvent in first liquid separation tank 11 are entered in ion chromatograph 14 by the second perfusion tube 13, drive ion
Chromatograph 14 works, and ion chromatograph 14 is analyzed and detected to the content of silicon ion, aluminium ion and sodium ion in solvent,
After detection, the valve of the third liquid outlet 12 of second liquid separation tank 11 is opened, carry out second and detect, then carry out the again
It detects three times, repeated detection improves the precision of detection, then the valve of opening third water pump 23 and return pipe 22, in agitator tank 7
Solvent come back in zeolite membrane hydrothermal synthesis case 1, finally according to the testing result of ion chromatograph 14, supplement required contain
Silicon contains aluminium amount corresponding with sodium raw materials are contained, and then carries out the preparation of second of zeolite membrane, repeats above step, repeatedly boiled
The preparation of stone film.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions.By sentence " element limited including one ..., it is not excluded that
There is also other identical elements in the process, method, article or apparatus that includes the element ".
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities, including zeolite membrane hydrothermal synthesis case (1), feature exists
In: the bottom end of the outer wall on the right side of the zeolite membrane hydrothermal synthesis case (1) is communicated with the first liquid outlet (2), first liquid outlet
(2) one end far from zeolite membrane hydrothermal synthesis case (1) is communicated with Rose Box (3), and the position on the intracavitary right side of the Rose Box (3) is set
It is equipped with the first perfusion tube (4), the upper end of first perfusion tube (4) through Rose Box (3) and is communicated with the first water pump (5), institute
It states and is provided with solvent recycling apparatus (6) on the right side of Rose Box (3) outer wall, be provided with and stir on the left of the solvent recycling apparatus (6)
It mixes case (7), the right end of first water pump (5) is connected to by the first perfusion tube (4) with the inside of agitator tank (7), the stirring
Position in the middle part of the bottom of case (7) outer wall offers the second liquid outlet (8), and the lower end of second liquid outlet (8) is communicated with storage
The bottom interval of sap cavity (9), the liquid storage chamber (9) is provided with separating tube (10), the upper end of the separating tube (10) and liquid storage chamber
(9) inside connection, the lower end of the separating tube (10) are communicated with liquid separation tank (11), and the bottom of the liquid separation tank (11) opens up
Have third liquid outlet (12), the lower end of the third liquid outlet (12) is communicated with the second perfusion tube (13), second perfusion tube
(13) one end far from third liquid outlet (12) is communicated with ion chromatograph (14).
2. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities according to claim 1, it is characterised in that: described
The position in the intracavitary left side of Rose Box (3) is provided with the first strainer (15), the intracavitary middle part of the Rose Box (3) and close first
The position of perfusion tube (4) is provided with the second strainer (16), and the upper and lower ends of first strainer (15) and the second strainer (16) are equal
It is fixedly connected with the inner wall of Rose Box (3).
3. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities according to claim 1, it is characterised in that: described
The position at agitator tank (7) intracavitary middle part is provided with shaft (17), is fixedly connected with stirring rod at left and right sides of the shaft (17)
(18), the inside of the stirring rod (18) is uniformly provided with through-hole.
4. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities according to claim 3, it is characterised in that: described
The position of agitator tank (7) upper surface middle part is equipped with motor (19), the top of the shaft (17) through agitator tank (7) and with electricity
Machine (19) rotation connection.
5. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities according to claim 1, it is characterised in that: described
Second perfusion tube (13) is communicated with the second water pump (20) close to the one end of ion chromatograph (14), on the ion chromatograph (14)
The position of surface middle part offers sample inlet (21), the right end of second water pump (20) by the second perfusion tube (13) with
Sample inlet (21) connection.
6. a kind of FAU zeolite membrane for CO2 capture recycles preparation facilities according to claim 1, it is characterised in that: described
Inner wall on the right side of agitator tank (7) is provided with return pipe (22), and the upper end of the return pipe (22) through agitator tank (7) and is communicated with
The left end of third water pump (23), the third water pump (23) passes through on the right side of return pipe (22) and zeolite membrane hydrothermal synthesis case (1)
Upper end connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821679849.6U CN209108972U (en) | 2018-10-17 | 2018-10-17 | A kind of FAU zeolite membrane circulation preparation facilities for CO2 capture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821679849.6U CN209108972U (en) | 2018-10-17 | 2018-10-17 | A kind of FAU zeolite membrane circulation preparation facilities for CO2 capture |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209108972U true CN209108972U (en) | 2019-07-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821679849.6U Active CN209108972U (en) | 2018-10-17 | 2018-10-17 | A kind of FAU zeolite membrane circulation preparation facilities for CO2 capture |
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| Country | Link |
|---|---|
| CN (1) | CN209108972U (en) |
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2018
- 2018-10-17 CN CN201821679849.6U patent/CN209108972U/en active Active
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