CN105369593A - 超高分子量聚乙烯原丝的制备方法 - Google Patents

超高分子量聚乙烯原丝的制备方法 Download PDF

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CN105369593A
CN105369593A CN201510938503.8A CN201510938503A CN105369593A CN 105369593 A CN105369593 A CN 105369593A CN 201510938503 A CN201510938503 A CN 201510938503A CN 105369593 A CN105369593 A CN 105369593A
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李振国
蔡建南
刘兆峰
丁洪昌
陆红星
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Changshu Super Fibers Co Ltd
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Abstract

本发明公开了一种超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：1）在34质量份去离子水中投入1～2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。本发明超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。

Description

超高分子量聚乙烯原丝的制备方法
技术领域
本发明涉及超高分子量聚乙烯原丝的制备方法。
背景技术
现有羟乙基纤维素纤维的抗菌、阻燃、抗静电性能都有待提高。
发明内容
本发明的目的在于提供一种超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。
为实现上述目的，本发明的技术方案是设计一种超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1～2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
优选的，超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
优选的，超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
本发明的优点和有益效果在于：提供一种超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。
具体实施方式
下面结合实施例，对本发明的具体实施方式作进一步描述。以下实施例仅用于更加清楚地说明本发明的技术方案，而不能以此来限制本发明的保护范围。
本发明具体实施的技术方案是：
实施例1
一种超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1～2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
实施例2
超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
实施例3
超高分子量聚乙烯原丝的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。

Claims (3)

1.超高分子量聚乙烯原丝的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1～2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
2.根据权利要求1所述的超高分子量聚乙烯原丝的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入1质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
3.根据权利要求1所述的超高分子量聚乙烯原丝的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在34质量份去离子水中投入2质量份十二烷基三甲基硫酸铵、2.6质量份偶氮二异丁腈、3.5质量份羧甲基淀粉钠、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入4.2质量份烷基芳基磺酸钠、1.7质量份石棉灰、3.6质量份硫氰酸钾、2.8质量份N-甲基吡咯烷酮，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
CN201510938503.8A 2015-12-16 2015-12-16 超高分子量聚乙烯原丝的制备方法 Pending CN105369593A (zh)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935946A (zh) * 2010-09-02 2011-01-05 荣盛石化股份有限公司 一种阻燃纤维的制备方法
CN103306130A (zh) * 2013-07-05 2013-09-18 吴江龙纺纺织有限公司 一种阻燃涤纶面料的制备方法
CN103790006A (zh) * 2013-11-30 2014-05-14 常熟市亚欧进出口贸易有限公司 织物阻燃整理剂的制备方法
CN104894868A (zh) * 2015-06-15 2015-09-09 湖州厉华妤婕联合纺织有限公司 一种用于织物的新型抗静电整理剂

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101935946A (zh) * 2010-09-02 2011-01-05 荣盛石化股份有限公司 一种阻燃纤维的制备方法
CN103306130A (zh) * 2013-07-05 2013-09-18 吴江龙纺纺织有限公司 一种阻燃涤纶面料的制备方法
CN103790006A (zh) * 2013-11-30 2014-05-14 常熟市亚欧进出口贸易有限公司 织物阻燃整理剂的制备方法
CN104894868A (zh) * 2015-06-15 2015-09-09 湖州厉华妤婕联合纺织有限公司 一种用于织物的新型抗静电整理剂

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Application publication date: 20160302