CN105348893A - Two-component efficient and light internal wall insulation putty and preparation method thereof - Google Patents
Two-component efficient and light internal wall insulation putty and preparation method thereof Download PDFInfo
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- CN105348893A CN105348893A CN201510901273.8A CN201510901273A CN105348893A CN 105348893 A CN105348893 A CN 105348893A CN 201510901273 A CN201510901273 A CN 201510901273A CN 105348893 A CN105348893 A CN 105348893A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
Abstract
The invention belongs to the field of insulation building materials and discloses two-component efficient and light internal wall insulation putty and a preparation method thereof. The insulation putty comprises a component 1 and a component 2, wherein the component 1 is gypsum which takes up 40-70 mass parts; the component 2 is prepared from, by mass, 0.3-1 part of coalescing agent, 0.4-0.8 part of cellulose, 10-20 parts of hydrophobic aluminum-magnesium silicate, 5-10 parts of hydrophobic SiO2 aerogel, 10-20 parts of rock wool, 0.05-0.4 part of retarder, 3-8 parts of bentonite and 3-10 parts of synthetic resin emulsion. The insulation putty is low in heat conductivity coefficient, good in insulation effect, high in fire resistance rating and convenient to construct.
Description
Technical field
The invention belongs to heat-insulating construction material field, be specifically related to a kind of double-component efficient light internal wall heat preservation putty and preparation method thereof.
Background technology
In building field, buildings heat-insulation and heat-preservation is the Important Action realizing China's sustainable development target.Consider the factors such as the occupying of area, heat bridge, apply the most widely or interior wall outer heat preservation system to buildings heat-insulation and heat-preservation at present, the heat-insulating heat-preserving material of application is usually the organic polymer polymeric plate such as extruded polystyrene board (XPS plate), expansion polyphenyl plate (EPS plate), hard-foam polyurethane (PU) plate.Organic polymer polymeric plate has the advantages such as thermal conductivity is low, water-fast, but also there are the problems such as fire safety poor-performing, ageing resistance are not good, construction inconvenience; And although conventional inorganic heat insulation material has higher fire-protection rating, security is good. but it is poor also to there is heat-insulating property, the deficiency that thermal conductivity is high, therefore development physical strength is high, stability good, the inorganic heat insulation material of low thermal conductivity is the needs of social development.
At present, some researchists also have developed some novel inorganic heat insulation materials pointedly, but its thermal conductivity is still larger, heat insulation effect is poor, such as: Chinese invention patent CN103708794A discloses the waterproof thermal insulation mortar that a kind of external wall uses, by weight, this thermal insulation mortar is obtained by following raw material: ordinary Portland cement 80-90 part, white lime 3-5 part, granular polystyrene 20-30 part, 9mm long polypropylene fibre 2-4 part, yttrium oxide 1-2 part, cenosphere 5-10 part, urea 1-2 part, coarse colza meal 0.01-0.02 part, butadiene-styrene latex 4-6 part, Syzygium aromaticum stem oil 1-2 part, vitamins C 3-4 part, MNC-C frostproofer 1.3-2.4 part, compounded mix 4-6 part.Use glass bead as one of main lagging material in the program, glass bead more easily breaks in whipping process, and yttrium oxide belongs to rare-earth substance in addition, resource-constrained, and final thermal conductivity is 0.07W/ (mk) left and right, bigger than normal.
Summary of the invention
The technical problem to be solved in the present invention is to provide that a kind of thermal conductivity is low, high insulating effect, fire resistance rating are high and efficient light heat insulating inner wall putty of easy construction and preparation method thereof.
In order to solve the problems of the technologies described above, the invention provides following technical scheme: double-component efficient light internal wall heat preservation putty, comprise component 1 and component 2, described component 1 is gypsum, and the mass fraction of gypsum is 40-70 part; Composition and the mass fraction of described component 2 are: film coalescence aid 0.3-1 part, Mierocrystalline cellulose 0.4-0.8 part, hydrophobicity neusilin 10-20 part, hydrophobicity SiO
2aerogel 5-10 part, rock wool 10-20 part, retardant 0.05-0.4 part, wilkinite 3-8 part, synthetic resin emulsion 3-10 part.
Adopt a kind of double-component efficient light internal wall heat preservation putty in this programme, compared with prior art, its technique effect is:
(1) thermal conductivity is low, and fire resistance rating is high, and its thermal conductivity is suitable with conventional organic polymer heat insulating board, but fire resistance rating is apparently higher than the latter, belongs to grade A product;
(2) bonding strength is high;
(3) easy construction, the thermal insulation layer of formation is not easy to crack.
Below the preferred version based on such scheme:
Preferred version one: composition and the mass fraction of described component 2 are: film coalescence aid 0.4 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 18 parts, hydrophobicity SiO
2aerogel 8 parts, rock wool 18 parts, retardant 0.08 part, wilkinite 5 parts, synthetic resin emulsion 5 parts.
Preferred version two: composition and the mass fraction of described component 2 are: film coalescence aid 0.3 part, Mierocrystalline cellulose 0.6 part, hydrophobicity neusilin 16 parts, hydrophobicity SiO
2aerogel 8 parts, rock wool 16 parts, retardant 0.15 part, wilkinite 6 parts, synthetic resin emulsion 4 parts.
Preferred version three: composition and the mass fraction of described component 2 are: film coalescence aid 0.3 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 15 parts, hydrophobicity SiO
2aerogel 10 parts, rock wool 18 parts, retardant 0.1 part, wilkinite 5 parts, synthetic resin emulsion 3 parts.
Preferred version four: composition and the mass fraction of described component 2 are: film coalescence aid 0.6 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 18 parts, hydrophobicity SiO
2aerogel 10 parts, rock wool 18 parts, retardant 0.05 part, wilkinite 7 parts, synthetic resin emulsion 4 parts.
Preferred version five: based on any one in such scheme,
Described gypsum is one or both in grey gypsum, white gypsum, and granularity is 300-500 order;
Described film coalescence aid is ten diester alcohol film coalescence aid;
Described Mierocrystalline cellulose is one or both in Vltra tears, alkyl ethers;
Described hydrophobicity neusilin is the hydrophobicity neusilin of ionic surfactant modification, and its granularity is 200-400 order;
Described rock wool is with Black Warrior stone, gabbro, rhombspar for raw material, and through high temperature melting, fibrosis and the inorganic fibre made, its granularity is 200-300 order;
Described retardant is one or both in citric acid or Trisodium Citrate;
Described wilkinite is sodium bentonite, and its granularity is 300-500 order;
Described synthetic resin emulsion is one or more in acetate emulsion, VAE emulsion, benzene emulsion, ACRYLIC EMULSION, pure-acrylic emulsion.
Preferred version six: based on preferred version five, described positive ion promoting agent is one or more in cetyl trimethylammonium bromide, bromination tetramethyl-amine, cetylpyridinium chloride.
In addition, the invention provides another technical scheme is: the preparation method of double-component efficient light internal wall heat preservation putty, comprises the following steps successively:
1) get the water of 35-50 part, under the stirring of 300-400rpm, in water, add film coalescence aid and the Mierocrystalline cellulose of respective quality number successively, then stir 5-10min under 300-400rpm after, under 800-1000rpm, stir 20-30min;
2) hydrophobicity neusilin, the hydrophobicity SiO of respective quality number is added successively
2aerogel, rock wool, retardant and wilkinite, after stirring 30-60min, then add the synthetic resin emulsion of respective quality number under 800-1000rpm under 300-400rpm stirs, and continues to stir 5-10min, obtain component 2;
3) component 1 gypsum is under agitation added in component 2, stirs into paste, get product.
Embodiment
Below by embodiment, the present invention is further detailed explanation:
The quality of each composition of the embodiment of the present invention one to embodiment six with and preparation method thereof in processing parameter as shown in table 1, unit is kg:
Table 1
For above-described embodiment three, preparation method of the present invention is described, wherein, gypsum is granularity is 300-500 object ash gypsum; Film coalescence aid is ten diester alcohol film coalescence aid; Mierocrystalline cellulose is Vltra tears; Hydrophobicity neusilin is the hydrophobicity neusilin of cetyl trimethylammonium bromide modification, and its granularity is 200-400 order; Hydrophobicity SiO
2aerogel is the light porous amorphous solid material of a kind of nano level; Rock wool is with Black Warrior stone, gabbro, rhombspar for raw material, through high temperature melting, fibrosis and the inorganic fibre made; Retardant is citric acid; Wilkinite is sodium bentonite, and its granularity is 300-500 order; Synthetic resin emulsion is acetate emulsion.
Preparation method comprises the following steps:
1) get the water of 35kg, under the stirring of 300rpm, in water, add the film coalescence aid of 0.3kg and the Mierocrystalline cellulose of 0.5kg successively, then after stirring 10min at 300 rpm, stir 30min at 800 rpm;
2) the hydrophobicity neusilin of 15kg, the hydrophobicity SiO of 10kg is added successively
2the wilkinite of the rock wool of aerogel, 18kg, the retardant of 0.1kg and 5kg, after stirring 60min at 800 rpm, then adds the synthetic resin emulsion of 3kg under 300rpm stirs, and continues to stir 10min, obtains component 2;
3), when using, component 1 gypsum getting 48kg is under agitation added in component 2, stirs into paste, gets product.
Embodiment one, embodiment two, the step of embodiment four, embodiment five and the preparation method of embodiment six is except each composition quality of table 1 is different, and all the other are all consistent with embodiment three.
Comparative example one:
Be with the difference of embodiment three, its composition and quality are: gypsum 45kg, water 35kg, film coalescence aid 0.2kg, Mierocrystalline cellulose 0.3kg, hydrophobicity neusilin 9kg, hydrophobicity SiO
2aerogel 4kg, rock wool 9kg, retardant 0.04kg, wilkinite 2kg, synthetic resin emulsion 2kg.
Comparative example two:
Be with the difference of embodiment three, its composition and quality are: gypsum 35kg, water 50kg, film coalescence aid 1.1kg, Mierocrystalline cellulose 0.9kg, hydrophobicity neusilin 21kg, hydrophobicity SiO
2aerogel 11kg, rock wool 21kg, retardant 0.41kg, wilkinite 9kg, synthetic resin emulsion 5kg.
Comparative example one is all consistent with embodiment three with the preparation method of comparative example two.
Experiment one: heat conductivility
By the finished product of embodiment one ~ embodiment six, comparative example one and comparative example two, make the sample of Φ 10mm × 1mm, after maintenance 7d, dry to constant weight, under 25 DEG C of conditions, carry out Measured Results of Thermal Conductivity with laser method heat transfer analysis instrument LFA457, measurement result is as shown in table 2:
Table 2
Wherein, the finished product in comparative example two there occurs cracking in experimentation, consequently leads to thermal conductivity and increases.
As seen from Table 2, the thermal conductivity of heat insulating inner wall putty finished product prepared by double-component efficient light internal wall heat preservation putty of the present invention and preparation method thereof each embodiment is all less than the thermal conductivity of the documents mentioned in background technology and the thermal conductivity of comparative example, therefore, the thermal conductivity of double-component efficient light internal wall heat preservation putty prepared by the present invention is low, high insulating effect.
Experiment two: bonding strength
Carry out bonding strength detection according to national standard JG/T242000 the 6.14th article to the finished product in each embodiment and comparative example, its detected result is as shown in table 3:
Table 3
As seen from Table 3, the bonding strength of each embodiment of double-component efficient light internal wall heat preservation putty of the present invention and preparation method thereof is all better than comparative example.
In addition, the finished product of embodiments of the invention one to embodiment six is when constructing, and thermal insulation layer is without cracking phenomena, and fire resistance rating is A level, belongs to highest ranking.
Certainly, in the present invention, the gypsum in component is the mixture of the white gypsum of 300-500 object or grey gypsum, in vain gypsum;
Mierocrystalline cellulose is Vltra tears, or alkyl ethers, or Vltra tears, alkyl ethers mixture;
Hydrophobicity neusilin is bromination tetramethyl-amine, or cetylpyridinium chloride, or cetyl trimethylammonium bromide, bromination tetramethyl-amine mixture, or cetyl trimethylammonium bromide, cetylpyridinium chloride mixture, or bromination tetramethyl-amine, cetylpyridinium chloride mixture, or cetyl trimethylammonium bromide, bromination tetramethyl-amine, cetylpyridinium chloride the neusilin of mixture modification, the granularity of the neusilin of this modification is 200-400 order;
Retardant is the mixture of Trisodium Citrate or citric acid, Trisodium Citrate;
Synthetic resin emulsion is the mixture of one or more in acetate emulsion, VAE emulsion, benzene emulsion, ACRYLIC EMULSION, pure-acrylic emulsion;
Only the selection of material, all consistent with the effect of embodiment one to embodiment six.
In addition; in preparation method of the present invention; the effect that processing parameter wherein gets other numerical value in its protection domain is consistent with the effect of embodiment one to embodiment six; difference is that stirring velocity is fast; its corresponding churning time will shorten; stirring velocity is slow, and its corresponding churning time will increase.
For a person skilled in the art, under the prerequisite not departing from structure of the present invention, can also make some distortion and improvement, these also should be considered as protection scope of the present invention, and these all can not affect effect of the invention process and practical applicability.
Claims (8)
1. a double-component efficient light internal wall heat preservation putty, is characterized in that, comprises component 1 and component 2, and described component 1 is gypsum, and the mass fraction of gypsum is 40-70 part; Composition and the mass fraction of described component 2 are: film coalescence aid 0.3-1 part, Mierocrystalline cellulose 0.4-0.8 part, hydrophobicity neusilin 10-20 part, hydrophobicity SiO
2aerogel 5-10 part, rock wool 10-20 part, retardant 0.05-0.4 part, wilkinite 3-8 part, synthetic resin emulsion 3-10 part.
2. a kind of double-component efficient light internal wall heat preservation putty according to claim 1, is characterized in that, composition and the mass fraction of described component 2 are: film coalescence aid 0.4 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 18 parts, hydrophobicity SiO
2aerogel 8 parts, rock wool 18 parts, retardant 0.08 part, wilkinite 5 parts, synthetic resin emulsion 5 parts.
3. a kind of double-component efficient light internal wall heat preservation putty according to claim 1, is characterized in that, composition and the mass fraction of described component 2 are: film coalescence aid 0.3 part, Mierocrystalline cellulose 0.6 part, hydrophobicity neusilin 16 parts, hydrophobicity SiO
2aerogel 8 parts, rock wool 16 parts, retardant 0.15 part, wilkinite 6 parts, synthetic resin emulsion 4 parts.
4. a kind of double-component efficient light internal wall heat preservation putty according to claim 1, is characterized in that, composition and the mass fraction of described component 2 are: film coalescence aid 0.3 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 15 parts, hydrophobicity SiO
2aerogel 10 parts, rock wool 18 parts, retardant 0.1 part, wilkinite 5 parts, synthetic resin emulsion 3 parts.
5. a kind of double-component efficient light internal wall heat preservation putty according to claim 1, is characterized in that, composition and the mass fraction of described component 2 are: film coalescence aid 0.6 part, Mierocrystalline cellulose 0.5 part, hydrophobicity neusilin 18 parts, hydrophobicity SiO
2aerogel 10 parts, rock wool 18 parts, retardant 0.05 part, wilkinite 7 parts, synthetic resin emulsion 4 parts.
6., according to a kind of double-component efficient light internal wall heat preservation putty in claim 1-5 described in any one, it is characterized in that,
Described gypsum is one or both in grey gypsum, white gypsum, and granularity is 300-500 order;
Described film coalescence aid is ten diester alcohol film coalescence aid;
Described Mierocrystalline cellulose is one or both in Vltra tears, alkyl ethers;
Described hydrophobicity neusilin is the hydrophobicity neusilin of ionic surfactant modification, and its granularity is 200-400 order;
Described rock wool is with Black Warrior stone, gabbro, rhombspar for raw material, and through high temperature melting, fibrosis and the inorganic fibre made, its granularity is 200-300 order;
Described retardant is one or both in citric acid, Trisodium Citrate;
Described wilkinite is sodium bentonite, and its granularity is 300-500 order;
Described synthetic resin emulsion is one or more in acetate emulsion, VAE emulsion, benzene emulsion, ACRYLIC EMULSION, pure-acrylic emulsion.
7. a kind of double-component efficient light internal wall heat preservation putty according to claim 6, is characterized in that, described positive ion promoting agent is one or more in cetyl trimethylammonium bromide, bromination tetramethyl-amine, cetylpyridinium chloride.
8., according to the preparation method of the double-component efficient light internal wall heat preservation putty in claim 1-5 described in any one, it is characterized in that, comprise the following steps successively:
1) get the water of 35-50 part, under the stirring of 300-400rpm, in water, add film coalescence aid and the Mierocrystalline cellulose of respective quality number successively, then stir 5-10min under 300-400rpm after, under 800-1000rpm, stir 20-30min;
2) hydrophobicity neusilin, the hydrophobicity SiO of respective quality number is added successively
2aerogel, rock wool, retardant and wilkinite, after stirring 30-60min, then add the synthetic resin emulsion of respective quality number under 800-1000rpm under 300-400rpm stirs, and continues to stir 5-10min, obtain component 2;
3) component 1 gypsum is under agitation added in component 2, stirs into paste, get product.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108129901A (en) * | 2017-12-26 | 2018-06-08 | 重庆兴渝新材料研究院有限公司 | A kind of two-component heat insulating inner wall putty and preparation method thereof |
CN108529990A (en) * | 2018-06-29 | 2018-09-14 | 深圳市嘉达高科产业发展有限公司 | A kind of Thermal insulating putty for exterior wall of building and preparation method thereof |
CN109956732A (en) * | 2017-12-26 | 2019-07-02 | 上海泛亚生命科技有限公司 | A kind of Novel interior wall energy-saving heat preserving base and its preparation and application |
CN110408253A (en) * | 2018-04-26 | 2019-11-05 | 公安部四川消防研究所 | A kind of water-proof fire-retardant coating and preparation method thereof |
CN111995896A (en) * | 2020-09-21 | 2020-11-27 | 重庆兴渝新材料研究院有限公司 | Bi-component interior wall heat-insulating leveling putty |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN108129901A (en) * | 2017-12-26 | 2018-06-08 | 重庆兴渝新材料研究院有限公司 | A kind of two-component heat insulating inner wall putty and preparation method thereof |
CN109956732A (en) * | 2017-12-26 | 2019-07-02 | 上海泛亚生命科技有限公司 | A kind of Novel interior wall energy-saving heat preserving base and its preparation and application |
CN109956732B (en) * | 2017-12-26 | 2022-03-25 | 上海泛亚生命科技有限公司 | Novel inner wall energy-saving heat-insulating base layer and preparation and application thereof |
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CN111995896A (en) * | 2020-09-21 | 2020-11-27 | 重庆兴渝新材料研究院有限公司 | Bi-component interior wall heat-insulating leveling putty |
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Effective date of registration: 20190626 Address after: 402760 No. 13, Second Road, Longqing Branch, Qingba Street, Bishan District, Chongqing Patentee after: Chongqing Xingcheng New Material Research Institute Co., Ltd. Address before: 401329 Baohong Fourth Society, Hangu Town, Jiulongpo District, Chongqing Patentee before: CHONGQING XINGYU PAINT CO., LTD. |