CN108529990A - A kind of Thermal insulating putty for exterior wall of building and preparation method thereof - Google Patents
A kind of Thermal insulating putty for exterior wall of building and preparation method thereof Download PDFInfo
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- CN108529990A CN108529990A CN201810697368.6A CN201810697368A CN108529990A CN 108529990 A CN108529990 A CN 108529990A CN 201810697368 A CN201810697368 A CN 201810697368A CN 108529990 A CN108529990 A CN 108529990A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Sealing Material Composition (AREA)
- Paints Or Removers (AREA)
- Building Environments (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The present invention relates to a kind of Thermal insulating putty for exterior wall of building and preparation method thereof, wherein Thermal insulating putty for exterior wall of building includes that following parts by weight content prepares raw material：20 25 parts of inorganic material, 20 35 parts of inorganic expansive expanded material, 20 35 parts of composite aluminium-magnesium-silicate, 25 parts of modified aerogels material, 58 parts of phase-changing energy storage material, 0.2 0.6 parts of hydroxyethyl cellulose, 0.5 1 parts of ceramic fibre, 0.1 0.4 parts of wetting dispersing agent and Si modification polymerize 13 parts of rubber powder.The Thermal insulating putty for exterior wall of building of the present invention has good thermal and insulating performance, and water absorption rate is low, and can reach A grades of fire protection requirements.
Description
Technical field
The present invention relates to building thermal insulation material, more particularly to a kind of Thermal insulating putty for exterior wall of building and preparation method thereof.
Background technology
Thermal insulation material used in wall thermal insulating mainly has two major classes at present：One kind is existed based on organic foam plate
The problem of working procedure complexity and easily generation fire；Another kind of is the inorganic heat insulation mortar caking property based on inorganic heat insulation mortar
By force, there is good environmental protection, weather resistance, but its heat insulating effect is not so good as organic insulation material, and that there are unit weights is larger, inhales
The defect of water rate height and heat preservation and insulation difference.
Need heat-insulated region especially for summer, no matter organic or inorganic heat insulation material, all there is certain
Drawback, reflective heat-insulation paint are to use near-infrared reflection principle, and the near-infrared part that heat is generated in sunlight is directly reflected
It goes out, building for hot summer and warm winter region can be fully met to play heat-insulated effect by not forming accumulation of heat in surface of wall
Power conservation requirement is built, but the region in view of Winter protection is needed for some, then needs to coordinate thermal insulation material to meet building
It is energy saving.
Invention content
The technical problem to be solved by the present invention is to：A kind of Thermal insulating putty for exterior wall of building is provided, can be used for reflecting with building
Insulating moulding coating matches；Further, a kind of preparation method of above-mentioned Thermal insulating putty for exterior wall of building is provided.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is：
A kind of Thermal insulating putty for exterior wall of building, including following parts by weight content prepare raw material：Inorganic material 20-25
Part, 20-35 parts of inorganic expansive expanded material, 20-35 parts of composite aluminium-magnesium-silicate, 2-5 parts of modified aerogels material, phase-change accumulation energy material
5-8 parts of material, 0.2-0.6 parts of hydroxyethyl cellulose, 0.5-1 parts of ceramic fibre, 0.1-0.4 parts of wetting dispersing agent and Si modification polymerization
1-3 parts of rubber powder.
A kind of preparation method of Thermal insulating putty for exterior wall of building, includes the following steps：
(1) by the inorganic material of 20-25 parts by weight, the hydroxyethyl cellulose of 0.2-0.6 parts by weight, 0.1-0.4 weights
The ceramic fibre of the wetting dispersing agent and 0.5-1 parts by weight of measuring part is mixed and stirred for, and obtains the first blending ingredients；
(2) by the composite aluminium-magnesium-silicate of 20-35 parts by weight, the inorganic expansive expanded material of 20-35 parts by weight, 2-5 weight
The modified aerogels material of part is mixed and stirred for, and the Si modification polymerization rubber powder of 1-3 parts by weight is added in whipping process, is obtained
Second blending ingredients；
(3) the first blending ingredients and the second blending ingredients are mixed and stirred for, the phase transformation of 5-8 parts by weight is added while stirring
Energy storage material obtains the Thermal insulating putty for exterior wall of building after mixing.
The beneficial effects of the present invention are：
(1) Si modification polymerization rubber powder is used in product, good combination can be formed with modified aerogels material so that gas
Gel can form uniform and stable dispersion after heat preservation putty and subsequent construction, and inorganic modified rubber powder can be in phase-change accumulation energy
Material surface forms layer protecting film, avoids destruction of the alkaline matter of cement to phase-change material capsule material, ensure that material
Service life；
(2) heat preservation putty of the invention has good thermal and insulating performance, and water absorption rate is low, and can reach A grades of fire prevention
It is required that.
Specific implementation mode
To explain the technical content, the achieved purpose and the effect of the present invention in detail, it is explained below in conjunction with embodiment.
The design of most critical of the present invention is：Using Si modification polymerization rubber powder good knot is formed with modified aerogels material
It closes so that aeroge can form uniform and stable dispersion after heat preservation putty and subsequent construction.
The present invention provides a kind of Thermal insulating putty for exterior wall of building, including following parts by weight content prepares raw material：Inorganic gluing
20-25 parts of material, 20-35 parts of inorganic expansive expanded material, 20-35 parts of composite aluminium-magnesium-silicate, 2-5 parts of modified aerogels material,
5-8 parts of phase-changing energy storage material, 0.2-0.6 parts of hydroxyethyl cellulose, 0.5-1 parts of ceramic fibre, 0.1-0.4 parts of wetting dispersing agent and
Si modification polymerize 1-3 parts of rubber powder.
The present invention also provides a kind of preparation methods of Thermal insulating putty for exterior wall of building, include the following steps：
(1) by the inorganic material of 20-25 parts by weight, the hydroxyethyl cellulose of 0.2-0.6 parts by weight, 0.1-0.4 weights
The ceramic fibre of the wetting dispersing agent and 0.5-1 parts by weight of measuring part is mixed and stirred for, and obtains the first blending ingredients；
(2) by the composite aluminium-magnesium-silicate of 20-35 parts by weight, the inorganic expansive expanded material of 20-35 parts by weight, 2-5 weight
The modified aerogels material of part is mixed and stirred for, and the Si modification polymerization rubber powder of 1-3 parts by weight is added in whipping process, is obtained
Second blending ingredients；
(3) the first blending ingredients and the second blending ingredients are mixed and stirred for, the phase transformation of 5-8 parts by weight is added while stirring
Energy storage material obtains the Thermal insulating putty for exterior wall of building after mixing.
As can be seen from the above description, the beneficial effects of the present invention are：
(1) Si modification polymerization rubber powder is used in product, good combination can be formed with modified aerogels material so that gas
Gel can form uniform and stable dispersion after heat preservation putty and subsequent construction, and inorganic modified rubber powder can be in phase-change accumulation energy
Material surface forms layer protecting film, avoids destruction of the alkaline matter of cement to phase-change material capsule material, ensure that material
Service life；
(2) heat preservation putty of the invention has good thermal and insulating performance, and water absorption rate is low, and can reach A grades of fire prevention
It is required that.
Further, the inorganic material includes portland cement, aluminate cement, sulphate aluminium cement and fluorine aluminium
At least one of hydrochlorate quick-hardening cement mixes.
Further, inorganic expansive expanded material include closed pore glass bead, hollow glass microbead, hollow ceramic microballon and
At least one of hydrophobic modified perlite.
Further, composite aluminium-magnesium-silicate includes at least one of palygorskite, sepiolite, bentonite and sepiolite.
Further, modified aerogels material is the SiO modified by trim,ethylchlorosilane2Aeroge.
Further, wetting dispersing agent is the powder material for including at least one of polyphosphoric acid sodium salt and polyphosphoric acid ammonium salt
Material.
Further, Si modification polymerization rubber powder be using inorganic nano silicon materials to organic polymer resin graft modification after
Polymer powder.
The embodiment of the present invention one is：
By 25 parts of 42.5 Portland cements, 0.4 part of hydroxyethyl cellulose, 0.2 part of wetting dispersing agent and 1 part
Ceramic fibre sequentially add in blender, place for use after stirring evenly, be labeled as component A；It simultaneously will be compound by 35 parts
Aluminium-magnesium silicate powder, 28 parts of inorganic expansive glass bead, 5 parts of modified aerogels material stir evenly, and in whipping process
In 2.4 parts of Si modifications polymerization rubber powders are at the uniform velocity added, label is after stirring evenly, and component A and B component is mixed equal
After even, it is slowly added into 3 parts of phase-changing energy storage material under stirring at low speed, has obtained that there is incubation and thermal insulation function after mixing
Insulation putty for architectural exterior wall.
The embodiment of the present invention two is：
By 16.5 parts of 42.5 Portland cements, 5 parts of 42.5 sulphate aluminium cements, 0.3 part of hydroxy ethyl fiber
Element, 0.4 part of wetting dispersing agent and 0.8 part of ceramic fibre sequentially add in blender, and for use, label is placed after stirring evenly
For component A；It simultaneously will be by 30 parts of composite aluminium-magnesium-silicate powder, 35 parts of inorganic expansive glass bead, 3 parts of modified aerogels
Material stirs evenly, and 3 parts of Si modification polymerization rubber powders are at the uniform velocity added in whipping process, and label is after stirring evenly, will
After component A and B component are mixed evenly, it is slowly added into 6 parts of phase-changing energy storage material under stirring at low speed, is after mixing
The insulation putty for architectural exterior wall with incubation and thermal insulation function is obtained.
The embodiment of the present invention three is：
By 20 parts of 42.5 Portland cements, 5 parts of 42.5 sulphate aluminium cements, 0.3 part of hydroxyethyl cellulose,
0.3 part of wetting dispersing agent and 0.4 part of ceramic fibre sequentially add in blender, are placed after stirring evenly for use, are labeled as A
Component；It simultaneously will be by the modified aerogels material of the inorganic expansive glass bead of 35 parts of composite aluminium-magnesium-silicate powder, 23 parts, 5 parts
Material stirs evenly, and 3 parts of Si modification polymerization rubber powders are at the uniform velocity added in whipping process, and label is after stirring evenly, by A
After component and B component are mixed evenly, it is slowly added into 8 parts of phase-changing energy storage material under stirring at low speed, is after mixing
The insulation putty for architectural exterior wall with incubation and thermal insulation function is obtained.
The embodiment of the present invention four is：
The Thermal insulating putty for exterior wall of building of the present embodiment includes that following parts by weight content prepares raw material：Inorganic material 20
Part, 20 parts of inorganic expansive expanded material, 20 parts of composite aluminium-magnesium-silicate, 2 parts of modified aerogels material, 5 parts of phase-changing energy storage material, hydroxyl
0.2 part of ethyl cellulose, 0.5 part of ceramic fibre, 0.1 part of wetting dispersing agent and Si modification polymerize 1 part of rubber powder.
The embodiment of the present invention five is：
The Thermal insulating putty for exterior wall of building of the present embodiment includes that following parts by weight content prepares raw material：Inorganic material 25
Part, 35 parts of inorganic expansive expanded material, 35 parts of composite aluminium-magnesium-silicate, 5 parts of modified aerogels material, 8 parts of phase-changing energy storage material, hydroxyl
0.6 part of ethyl cellulose, 1 part of ceramic fibre, 0.4 part of wetting dispersing agent and Si modification polymerize 3 parts of rubber powder.
The embodiment of the present invention six is：
The Thermal insulating putty for exterior wall of building of the present embodiment includes that following parts by weight content prepares raw material：Inorganic material 23
Part, 33 parts of inorganic expansive expanded material, 33 parts of composite aluminium-magnesium-silicate, 3 parts of modified aerogels material, 7 parts of phase-changing energy storage material, hydroxyl
0.5 part of ethyl cellulose, 0.7 part of ceramic fibre, 0.3 part of wetting dispersing agent and Si modification polymerize 2.7 parts of rubber powder.
Performance test
The Thermal insulating putty for exterior wall of building that embodiment one to embodiment six obtains is subjected to thermal and insulating performance, water absorption rate respectively
It is tested with fire protection requirement (such as measurement of thermal coefficient).
Test result is referring to the following table 1.
Table 1
In conclusion Thermal insulating putty for exterior wall of building provided by the invention has good thermal and insulating performance, water absorption rate is low,
And A grades of fire protection requirements can be reached.
Example the above is only the implementation of the present invention is not intended to limit the scope of the invention, every to utilize this hair
Equivalents made by bright description are applied directly or indirectly in relevant technical field, are similarly included in this hair
In bright scope of patent protection.
Claims (10)
1. a kind of Thermal insulating putty for exterior wall of building, which is characterized in that prepare raw material including following parts by weight content：Inorganic gluing material
20-25 parts of material, 20-35 parts of inorganic expansive expanded material, 20-35 parts of composite aluminium-magnesium-silicate, 2-5 parts of modified aerogels material, phase
5-8 parts of change energy-storage material, 0.2-0.6 parts of hydroxyethyl cellulose, 0.5-1 parts of ceramic fibre, 0.1-0.4 parts of wetting dispersing agent and silicon
1-3 parts of modified polymer powder.
2. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that the inorganic material includes silicic acid
At least one of salt cement, aluminate cement, sulphate aluminium cement and fluoaluminate quick-hardening cement mix.
3. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that inorganic expansive expanded material includes closed pore
Glass bead, hollow glass microbead, hollow ceramic microballon and hydrophobic modified at least one of perlite.
4. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that composite aluminium-magnesium-silicate include palygorskite,
At least one of sepiolite, bentonite and sepiolite.
5. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that modified aerogels material is by front three
The SiO of base chlorosilane modification2Aeroge.
6. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that wetting dispersing agent includes polyphosphoric acid sodium salt
At least one of with polyphosphoric acid ammonium salt.
7. Thermal insulating putty for exterior wall of building according to claim 1, which is characterized in that it is using inorganic that Si modification, which polymerize rubber powder,
Nano silicon material is to the polymer powder after organic polymer resin graft modification.
8. a kind of preparation method of Thermal insulating putty for exterior wall of building, which is characterized in that include the following steps：
(1) by the inorganic material of 20-25 parts by weight, the hydroxyethyl cellulose of 0.2-0.6 parts by weight, 0.1-0.4 parts by weight
Wetting dispersing agent and the ceramic fibres of 0.5-1 parts by weight be mixed and stirred for, obtain the first blending ingredients；
(2) by the composite aluminium-magnesium-silicate of 20-35 parts by weight, the inorganic expansive expanded materials of 20-35 parts by weight, 2-5 parts by weight
Modified aerogels material is mixed and stirred for, and the Si modification polymerization rubber powder of 1-3 parts by weight is added in whipping process, obtains second
Blending ingredients；
(3) the first blending ingredients and the second blending ingredients are mixed and stirred for, the phase-change accumulation energy of 5-8 parts by weight is added while stirring
Material obtains the Thermal insulating putty for exterior wall of building after mixing.
9. the preparation method of Thermal insulating putty for exterior wall of building according to claim 8, which is characterized in that in step (2), stirring
During mixing, the Si modification polymerization rubber powder is at the uniform velocity added.
10. the preparation method of Thermal insulating putty for exterior wall of building according to claim 8, which is characterized in that in step (3), first
Mixing speed is reduced, the phase-changing energy storage material is added.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810697368.6A CN108529990B (en) | 2018-06-29 | 2018-06-29 | Building exterior wall heat-insulating putty and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810697368.6A CN108529990B (en) | 2018-06-29 | 2018-06-29 | Building exterior wall heat-insulating putty and preparation method thereof |
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| CN108529990B CN108529990B (en) | 2020-11-10 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109370292A (en) * | 2018-12-12 | 2019-02-22 | 河北晨阳工贸集团有限公司 | A kind of phase transformation exterior wall putty and preparation method thereof |
| CN112551938A (en) * | 2020-12-08 | 2021-03-26 | 苏州启创新材料科技有限公司 | Phase-change composite material for thermal insulation mortar and preparation method thereof |
| CN114014622A (en) * | 2021-11-12 | 2022-02-08 | 江苏恺曼斯节能科技有限公司 | Inorganic heat-insulating paste for nanogel floor and preparation method thereof |
| WO2022106641A1 (en) * | 2020-11-20 | 2022-05-27 | Franken Maxit Mauermörtel Gmbh & Co | Heat-insulating plaster system and method for producing same |
| EP4177231A1 (en) * | 2021-11-03 | 2023-05-10 | Evonik Operations GmbH | Thermal insulation systems with improved cost efficiency |
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| KR20110088626A (en) * | 2010-01-29 | 2011-08-04 | 이은용 | Manufacturing method for super light silica aerogel cerment mortar having insulating, water proofing, refractory characteristics |
| CN103214893A (en) * | 2013-04-07 | 2013-07-24 | 浙江大学宁波理工学院 | Phase-change thermal insulation putty |
| CN105348893A (en) * | 2015-12-09 | 2016-02-24 | 重庆兴渝涂料股份有限公司 | Two-component efficient and light internal wall insulation putty and preparation method thereof |
| CN105524507A (en) * | 2015-12-09 | 2016-04-27 | 重庆兴渝涂料股份有限公司 | Single-component high-efficiency lightweight interior-wall insulation putty and preparation method thereof |
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| CN101255039A (en) * | 2008-04-03 | 2008-09-03 | 武汉昂泰科技有限公司 | Polymer micro-sphere insulation heat-proof mortar |
| KR20110088626A (en) * | 2010-01-29 | 2011-08-04 | 이은용 | Manufacturing method for super light silica aerogel cerment mortar having insulating, water proofing, refractory characteristics |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109370292A (en) * | 2018-12-12 | 2019-02-22 | 河北晨阳工贸集团有限公司 | A kind of phase transformation exterior wall putty and preparation method thereof |
| WO2022106641A1 (en) * | 2020-11-20 | 2022-05-27 | Franken Maxit Mauermörtel Gmbh & Co | Heat-insulating plaster system and method for producing same |
| CN112551938A (en) * | 2020-12-08 | 2021-03-26 | 苏州启创新材料科技有限公司 | Phase-change composite material for thermal insulation mortar and preparation method thereof |
| EP4177231A1 (en) * | 2021-11-03 | 2023-05-10 | Evonik Operations GmbH | Thermal insulation systems with improved cost efficiency |
| CN114014622A (en) * | 2021-11-12 | 2022-02-08 | 江苏恺曼斯节能科技有限公司 | Inorganic heat-insulating paste for nanogel floor and preparation method thereof |
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| CN108529990B (en) | 2020-11-10 |
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