CN105341847A - A preparing method of a seasoned toona sinensis instant powder - Google Patents
A preparing method of a seasoned toona sinensis instant powder Download PDFInfo
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- CN105341847A CN105341847A CN201510645586.1A CN201510645586A CN105341847A CN 105341847 A CN105341847 A CN 105341847A CN 201510645586 A CN201510645586 A CN 201510645586A CN 105341847 A CN105341847 A CN 105341847A
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- chinese toon
- parts
- leaves
- paste
- instant powder
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- 241000425037 Toona sinensis Species 0.000 title claims abstract description 76
- 239000000843 powder Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 20
- 235000011783 Cedrela sinensis Nutrition 0.000 title abstract 8
- 238000000605 extraction Methods 0.000 claims abstract description 16
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 235000013305 food Nutrition 0.000 claims abstract description 6
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 claims abstract description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
- 235000011194 food seasoning agent Nutrition 0.000 claims description 15
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000001569 carbon dioxide Substances 0.000 claims description 10
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 10
- 239000002674 ointment Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 240000004160 Capsicum annuum Species 0.000 claims description 9
- 238000000889 atomisation Methods 0.000 claims description 6
- 240000005528 Arctium lappa Species 0.000 claims description 3
- 235000003130 Arctium lappa Nutrition 0.000 claims description 3
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 3
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 3
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 3
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 3
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 3
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 3
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 3
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 3
- 240000000171 Crataegus monogyna Species 0.000 claims description 3
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 3
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 3
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 239000004375 Dextrin Substances 0.000 claims description 3
- 240000002853 Nelumbo nucifera Species 0.000 claims description 3
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims description 3
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 239000006071 cream Substances 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 235000013923 monosodium glutamate Nutrition 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 229940073490 sodium glutamate Drugs 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000004575 stone Substances 0.000 claims description 3
- 239000006228 supernatant Substances 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 4
- COBBNRKBTCBWQP-UHFFFAOYSA-N Graveoline Chemical compound C1=C2OCOC2=CC(C=2N(C3=CC=CC=C3C(=O)C=2)C)=C1 COBBNRKBTCBWQP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- 239000003053 toxin Substances 0.000 abstract 1
- 231100000765 toxin Toxicity 0.000 abstract 1
- 108700012359 toxins Proteins 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 17
- 235000019198 oils Nutrition 0.000 description 17
- 239000003814 drug Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000036449 good health Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention relates to a preparing method of seasoned toona sinensis instant powder and the preparing method comprises the following steps: (1) preparing toona sinensis leaf paste; (2) extracting toona sinensis leaf oil; (3) preparing mixed materials; and (4) preparing the toona sinensis instant powder. The provided toona sinensis instant powder preparation method uses a supercritical carbon dioxide extraction technology to extract the toona sinensis leaf oil, can prevent the volatilization loss of toona sinensis foliosine, is free of toxins and residues, and is a green and environmentally protective food processing technology with an extraction rate not less than 92.4%.
Description
Technical field
The invention belongs to field of food, be specifically related to a kind of preparation method of seasoning Chinese toon instant powder.
Background technology
Chinese toon is a kind of top grade spice, is mostly the tender shoots in the edible early spring at present.The Chinese Toon Leaves suboutput entered after autumn is large, and be rich in more Chinese toon foline, economic worth and edibility are very high, are not developed for a long time owing to not being familiar with by people, more utilize without industrialization.
Summary of the invention
The object of this invention is to provide a kind of preparation method of seasoning Chinese toon instant powder, the Chinese toon leaf oil be extracted in Chinese Toon Leaves is after autumn prepared into flavouring, adds the economic worth into Chinese Toon Leaves after autumn.
The present invention is achieved through the following technical solutions:
A preparation method for seasoning Chinese toon instant powder, comprises the following steps:
(1), choose the Chinese toon leaf of early autumn, clean up, drain the moisture on surface, choose cleaned Chinese Toon Leaves 100 parts by weight, use stone mill to grind, in process of lapping, add the water with the weight such as Chinese Toon Leaves, obtaining Chinese Toon Leaves sticks with paste for subsequent use;
(2) Chinese Toon Leaves, by step (1) obtained is stuck with paste and is used supercritical carbon dioxide extraction method to extract, and extraction temperature is 32-33 DEG C, and extracting pressure is 42-45Mpa, and separating carbon dioxide obtains Chinese toon leaf oil;
(3), baking oven is used by chilli to be dried to micro-Huang, fragmentation obtains 600 object chilli powders, take food salt 10 parts by weight, sodium glutamate 5 parts, chilli powder 3 powder, starch 20 parts, 25 parts, dextrin be uniformly mixed, then carry out ultramicro grinding, obtain mixed accessories;
(4), by the Chinese toon leaf oil that step (2) obtains use ultrasonic atomization technique to be atomized under anaerobic, then the Chinese toon leaf oil after atomization is evenly sprayed on mixed accessories, obtain seasoning Chinese toon instant powder.
Preferably, in step (2), in Chinese Toon Leaves, supercritical carbon dioxide extracting comprises the following steps:
A, Chinese Toon Leaves to be stuck with paste and add extractive reaction still with liquid carbon dioxide by weight 1:3.25, extracting pressure is 42-45MPa, temperature is 32-33 DEG C, and in extraction process, use the process of 215MHz ultrasonic wave, extraction time is 1-1.5h, obtains thick Chinese toon leaf oil;
B, thick Chinese Toon Leaves oil is refrigerated to-20 DEG C, then uses high speed freezing centrifuge centrifugal treating 20min under the condition of rotating speed 12000-15000r/min, removing impurity, obtains Chinese toon leaf oil.
Preferably, in mixed accessories, add 0.5 part of traditional Chinese medicinal ointment, traditional Chinese medicinal ointment is prepared as follows: get leaves of Hawthorn 10 parts, fructus choerospondiatis 5 parts, great burdock achene 1.5 parts, Sculellaria barbata 1.2 parts, 3 parts, lotus seeds by weight, clean up, 60-70 part soak by water 1-2h is added after mixing, filter, obtain first-time filtrate, in filter residue, add 40-50 part water continue to decoct 2-3h, filter, obtain secondary filtrate, merge first-time filtrate and secondary filtrate, being concentrated into 25 DEG C of lower densities is 1.20-1.25g/cm
3paste; In paste, add paste weight 3-5 times mass fraction is the ethanolic solution of 75%, stirs 10-15min, then ultrasonic process 5-10min, and then leave standstill and insoluble matter is sunk, get supernatant, being concentrated into 25 DEG C of lower densities is 1.28-1.32g/cm
3clear cream, be traditional Chinese medicinal ointment.
Eating method: namely rush i.e. use, with the boiling water of 10 times by dissolved for seasoning Chinese toon instant powder one-tenth pasty state, instills appropriate sesame oil, aromatic flavour, namely can be used as high-grade instant seasoning product.
Beneficial effect of the present invention: the preparation method of seasoning Chinese toon instant powder provided by the invention uses carbon dioxide supercritical extraction technology to extract Chinese toon leaf oil, can prevent Chinese toon foline volatile flow from losing, and nontoxic residue-free, it is a kind of green environmental protection technique of food processing, recovery rate can reach 7-9%, can more than 99.2% be reached through its purity of Extraction and isolation, the seasoning Chinese toon instant powder mouthfeel of preparation is good, instant, there is good health value, simultaneously often edible also have good help pregnant function.
Through orthogonal experiment checking, use condition Chinese toon of the present invention also oil extraction rate reached to more than 7%, can more than 1% be promoted relative to other conditions, there is obvious lifting.
Traditional Chinese medicinal ointment is added in mixed accessories, reasonable compatibility through between medicine, eliminate the toxic and side effect of medicine, improve the health value of medicine further, have and good help pregnant function, also there is the effect of beautifying face and moistering lotion, maintenance taste simultaneously, can not also need to use other anticorrisive agents to extend the holding time of instant powder, old Chinese Toon Leaves can be used to be prepared, and to avoid Chinese Toon Leaves Sodium Nitrite and exceed standard.
The quality * 100% of the Chinese Toon Leaves quality amount/Chinese Toon Leaves of Chinese toon leaf oil recovery rate (%)=extraction.
Detailed description of the invention
A preparation method for seasoning Chinese toon instant powder, comprises the following steps:
(1), choose the Chinese toon leaf of early autumn, clean up, drain the moisture on surface, choose cleaned Chinese Toon Leaves 100 parts by weight, use stone mill to grind, in process of lapping, add the water with the weight such as Chinese Toon Leaves, obtaining Chinese Toon Leaves sticks with paste for subsequent use;
(2) Chinese Toon Leaves, by step (1) obtained is stuck with paste and is used supercritical carbon dioxide extraction method to extract, and extraction temperature is 32-33 DEG C, and extracting pressure is 42-45Mpa, and separating carbon dioxide obtains Chinese toon leaf oil;
(3), baking oven is used by chilli to be dried to micro-Huang, fragmentation obtains 600 object chilli powders, take food salt 10 parts by weight, sodium glutamate 5 parts, chilli powder 3 powder, starch 20 parts, 25 parts, dextrin be uniformly mixed, then carry out ultramicro grinding, obtain mixed accessories;
(4), by the Chinese toon leaf oil that step (2) obtains use ultrasonic atomization technique to be atomized under anaerobic, then the Chinese toon leaf oil after atomization is evenly sprayed on mixed accessories, obtain seasoning Chinese toon instant powder.
Preferably, in step (2), in Chinese Toon Leaves, supercritical carbon dioxide extracting comprises the following steps:
A, Chinese Toon Leaves stuck with paste add extractive reaction still with liquid carbon dioxide by weight 1:3.25, extracting pressure is 42-45MPa, temperature is 32-33 DEG C, further, when extracting pressure is 43.25MPa, temperature is 32.5 DEG C, extraction yield is more than 95%, the process of 215MHz ultrasonic wave is used in extraction process, extraction time is 1-1.5h, obtains thick Chinese toon leaf oil;
B, thick Chinese Toon Leaves oil is refrigerated to-20 DEG C, then uses high speed freezing centrifuge centrifugal treating 20min under the condition of rotating speed 12000-15000r/min, removing impurity, obtains Chinese toon leaf oil.
Preferably, in mixed accessories, add 0.5 part of traditional Chinese medicinal ointment, traditional Chinese medicinal ointment is prepared as follows: get leaves of Hawthorn 10 parts, fructus choerospondiatis 5 parts, great burdock achene 1.5 parts, Sculellaria barbata 1.2 parts, 3 parts, lotus seeds by weight, clean up, 60-70 part soak by water 1-2h is added after mixing, filter, obtain first-time filtrate, in filter residue, add 40-50 part water continue to decoct 2-3h, filter, obtain secondary filtrate, merge first-time filtrate and secondary filtrate, being concentrated into 25 DEG C of lower densities is 1.20-1.25g/cm
3paste; In paste, add paste weight 3-5 times mass fraction is the ethanolic solution of 75%, stirs 10-15min, then ultrasonic process 5-10min, and then leave standstill and insoluble matter is sunk, get supernatant, being concentrated into 25 DEG C of lower densities is 1.28-1.32g/cm
3clear cream, be traditional Chinese medicinal ointment.
The extraction yield of Chinese toon leaf oil significantly can be promoted under extraction conditions of the present invention.
Claims (3)
1. a preparation method for seasoning Chinese toon instant powder, is characterized in that, comprises the following steps:
(1), choose the Chinese toon leaf of early autumn, clean up, drain the moisture on surface, choose cleaned Chinese Toon Leaves 100 parts by weight, use stone mill to grind, in process of lapping, add the water with the weight such as Chinese Toon Leaves, obtaining Chinese Toon Leaves sticks with paste for subsequent use;
(2) Chinese Toon Leaves, by step (1) obtained is stuck with paste and is used supercritical carbon dioxide extraction method to extract, and extraction temperature is 32-33 DEG C, and extracting pressure is 42-45Mpa, and separating carbon dioxide obtains Chinese toon leaf oil;
(3), baking oven is used by chilli to be dried to micro-Huang, fragmentation obtains 600 object chilli powders, take food salt 10 parts by weight, sodium glutamate 5 parts, chilli powder 3 powder, starch 20 parts, 25 parts, dextrin be uniformly mixed, then carry out ultramicro grinding, obtain mixed accessories;
(4), by the Chinese toon leaf oil that step (2) obtains use ultrasonic atomization technique to be atomized under anaerobic, then the Chinese toon leaf oil after atomization is evenly sprayed on mixed accessories, obtain seasoning Chinese toon instant powder.
2. the preparation method of a kind of seasoning Chinese toon instant powder according to claim 1, is characterized in that: in step (2), in Chinese Toon Leaves, supercritical carbon dioxide extracting comprises the following steps:
A, Chinese Toon Leaves to be stuck with paste and add extractive reaction still with liquid carbon dioxide by weight 1:3.25, extracting pressure is 42-45MPa, temperature is 32-33 DEG C, and in extraction process, use the process of 215MHz ultrasonic wave, extraction time is 1-1.5h, obtains thick Chinese toon leaf oil;
B, thick Chinese Toon Leaves oil is refrigerated to-20 DEG C, then uses high speed freezing centrifuge centrifugal treating 20min under the condition of rotating speed 12000-15000r/min, removing impurity, obtains Chinese toon leaf oil.
3. the preparation method of a kind of seasoning Chinese toon instant powder according to claim 1, it is characterized in that: in mixed accessories, add 0.5 part of traditional Chinese medicinal ointment, traditional Chinese medicinal ointment is prepared as follows: get leaves of Hawthorn 10 parts, fructus choerospondiatis 5 parts, great burdock achene 1.5 parts, Sculellaria barbata 1.2 parts, 3 parts, lotus seeds by weight, clean up, 60-70 part soak by water 1-2h is added after mixing, filter, obtain first-time filtrate, in filter residue, add 40-50 part water continue to decoct 2-3h, filter, obtain secondary filtrate, merge first-time filtrate and secondary filtrate, being concentrated into 25 DEG C of lower densities is 1.20-1.25g/cm
3paste; In paste, add paste weight 3-5 times mass fraction is the ethanolic solution of 75%, stirs 10-15min, then ultrasonic process 5-10min, and then leave standstill and insoluble matter is sunk, get supernatant, being concentrated into 25 DEG C of lower densities is 1.28-1.32g/cm
3clear cream, be traditional Chinese medicinal ointment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510645586.1A CN105341847A (en) | 2015-10-09 | 2015-10-09 | A preparing method of a seasoned toona sinensis instant powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510645586.1A CN105341847A (en) | 2015-10-09 | 2015-10-09 | A preparing method of a seasoned toona sinensis instant powder |
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| Publication Number | Publication Date |
|---|---|
| CN105341847A true CN105341847A (en) | 2016-02-24 |
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| CN201510645586.1A Pending CN105341847A (en) | 2015-10-09 | 2015-10-09 | A preparing method of a seasoned toona sinensis instant powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108967959A (en) * | 2018-09-24 | 2018-12-11 | 罗炜欣 | Technique based on wall breaking technology Yu molecule technique for packing processing and seasoning food |
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| CN1568786A (en) * | 2004-05-08 | 2005-01-26 | 西南农业大学 | Production technique for extracting pepper essence by supercritical carbon dioxide process |
| CN102987277A (en) * | 2011-09-09 | 2013-03-27 | 李从勇 | Instant Chinese toon powder, and its processing technology |
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-
2015
- 2015-10-09 CN CN201510645586.1A patent/CN105341847A/en active Pending
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| CN108967959A (en) * | 2018-09-24 | 2018-12-11 | 罗炜欣 | Technique based on wall breaking technology Yu molecule technique for packing processing and seasoning food |
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Application publication date: 20160224 |
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