CN102058081B - Device for preparing black pepper oil resin - Google Patents
Device for preparing black pepper oil resin Download PDFInfo
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- CN102058081B CN102058081B CN2010105574841A CN201010557484A CN102058081B CN 102058081 B CN102058081 B CN 102058081B CN 2010105574841 A CN2010105574841 A CN 2010105574841A CN 201010557484 A CN201010557484 A CN 201010557484A CN 102058081 B CN102058081 B CN 102058081B
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Abstract
The invention relates to a method for preparing black pepper oil resin, which comprises a flaking and crushing machine, a supercritical extraction kettle, a separation kettle, a molecular distillation device and a black pepper oil resin blending device, wherein the flaking and crushing machine is used for crushing flaked black pepper with water content being below 13 percent, and the crushed flaked black pepper enters the supercritical extraction kettle; the supercritical extraction kettle is used for extracting the black pepper powder, the extraction solvent is carbon dioxide of good grade, the total time of the extraction is 3-4h; the separation kettle is used for separating fluid with extract to obtain a crude extract, wherein the fluid with the extract enters the separation kettle; the molecular distillation device is used for separating and removing impurities of water and the like from the crude extract and separating into light components and heavy components, the light components are mainly black pepper oil and account for more than 70 percent, the heavy components are mainly piperine and account for more than 50 percent; and the black pepper oil resin blending device comprises an edible plant oil metering valve, a black pepper essential oil metering valve and a piperine metering valve, and the black pepper oil resins with different specifications are blended from the black pepper essential oil, the piperine and the edible plant oil according to a certain proportion. The device has the advantages of simple structure and high efficiency and can be used for preparing sensoner with top-grade catering industry.
Description
Technical field
The present invention relates to a kind of device for making of pepper oleoresin.
Background technology
Pepper is dry near maturation or the ripening fruits of Piperaceae plant pepper (Piper nigrum L.).When autumn to next year, be dirty-green spring, when the fruit of fruit ear base portion begins to redden, cut fruit ear and dry or dry, fruit is pitchy, claims black pepper.Gather in the time of also can waiting whole fruits to redden, the water logging a few days, wipe crust, to dry, the surface is canescence, claims white pepper.Containing volatile oil, pipering, crude fat, crude protein, starch, each biostearin, trace element etc. in the pepper fruit, is the flavouring that people like.Pepper is mainly as flavouring industry, can be used as peptic, antipyretic, diuretics and tunica mucosa bronchiorum stimulant etc. in pepper pharmaceutically, can treat indigestion, cold phlegm, cough, enteritis, bronchitis, flu and rheumatism etc., clinical act as with white pepper good.In food industry, according to 2003 No. four file of Ministry of Health of the People's Republic of China, pepper oleoresin, papper oil are approved for the food additives new varieties.Pepper oleoresin is that the natural extract of white pepper or black pepper forms with the allotment of plant wet goods auxiliary material, and cost is low, be easy to store, transport, and be the development trend of pepper series products application and development.
At present, vegetable oil lixiviate or solvent-extracted mode are mainly still adopted in the extraction of pepper fragrance and pungency component.The vegetable oil lixiviate can obtain the flavouring hot pepper oil of taste good, but the active ingredient extracting efficiency is low, and waste is serious.Solvent-extracted product has dissolvent residual, and product appearance is bad, and oil-soluble is relatively poor, is unfavorable for using.At present domestic aspect the development and application of pepper class flavoring products, still be in the starting stage.
Summary of the invention:
In order to overcome the shortcoming of prior art, the invention provides a kind of device of preparing black pepper oil resin, it is simple in structure, and efficient is high.
The present invention solves the technical scheme that its technical problem takes: it comprises:
Roll the embryo pulverizer: water content is pulverized, entered supercritical extraction reactor after the pepper compressing tablet below 13%;
Supercritical extraction reactor: pepper powder is extracted, extractant is the carbon dioxide of food-grade, extraction first half term pressure is 15-18Mpa, temperature 40-45 ℃, the second half extracting pressure is 26-30Mpa, temperature 55-60 ℃, carbon dioxide flow remains at 1200-1400L/h, the total time 3-4h of extraction; Enter separating still;
Separating still: enter in separating still with the fluid of extract and separate, the time is 20-40 minute; Get crude extract, main component is pipering and pepper essential oil;
Molecular still: crude extract is separated impurity such as removing moisture, and be separated into heavy constituent and light component; Light component is mainly the pepper essential oil, and content is greater than 70%; Heavy constituent is mainly pipering, and content is greater than 50%;
With the pepper oleoresin tuner: comprise edible vegetable oil metering valve, pepper essential oil metering valve and pipering metering valve; With pepper essential oil, pipering and the edible vegetable oil pepper oleoresin of furnishing different size according to a certain ratio.
The present invention is simple in structure, and extractant used is pollution-free, noresidue, and product yield is high, and quality better is convenient to allocate in edible oil, and has kept the natural flavour mountaineous and functional component of pepper, has higher use value.The gained pepper oleoresin can be used as the flavoring of high-grade catering industry, also can use as flavoring agent in instant noodles and meat products processing.
Description of drawings
The present invention is further described below in conjunction with drawings and Examples.
Accompanying drawing is structural representation of the present invention.
The specific embodiment
As shown in drawings, the present invention includes and roll embryo pulverizer 1, supercritical extraction reactor 2, separating still 3, molecular still 4 and pepper oleoresin tuner 10.
Roll embryo pulverizer 1: water content is pulverized, entered supercritical extraction reactor 2 after the pepper compressing tablet below 13%.The described compressing tablet thickness that rolls embryo pulverizer 1 is that grinding particle size is 2-3mm less than 1.5mm.
Supercritical extraction reactor 2: choose 300Lx2 technical grade supercritical extraction reactor, single still charge is 80kg.To the pepper powder extraction, extractant is the carbon dioxide of food-grade, the extraction conditions setting: front 2 hours extracting pressure 15Mpa, 40 ℃ of extraction temperature were adjusted to extracting pressure 28Mpa after 2 hours, 55 ℃ of extraction temperature, carbon dioxide flow remains 1200-1400L/h, extraction total time 4h.
Separating still 3: enter in separating still 3 with the fluid of extract and separate, the pressure 5.5Mpa of separation, temperature is 30 ℃.Get crude extract after separation, main component is pipering and pepper essential oil.
Molecular still 4: crude extract is separated impurity such as removing moisture, and be separated into heavy constituent and light component, enter respectively heavy constituent tank 5 and light component tank 6.Light component is mainly the pepper essential oil, and content is greater than 70%; Heavy constituent is mainly pipering, and content is greater than 50%.Light component obtains 2.64kg, and the pepper essential oil content is 75%; Heavy constituent obtains 2.32kg, and content of piperine is 55%.
Pepper oleoresin tuner 10: comprise edible vegetable oil metering valve 7, pepper essential oil metering valve 9 and pipering metering valve 8.Pepper essential oil, pipering and edible vegetable oil are by the pepper oleoresin of proportioning furnishing 36/18 specification of 21.6: 65.5: 12.9.
Described embryo pulverizer 1, supercritical extraction reactor 2, separating still 3, molecular still 4 and the pepper oleoresin tuner 10 of rolling seals connection successively by pipeline.
Pepper oleoresin can be used as the flavoring of high-grade catering industry, also can use as flavoring agent in instant noodles and meat products processing.
Claims (4)
1. the method for a preparing black pepper oil resin, it is characterized in that: it comprises:
Roll embryo pulverizer (1): water content is pulverized, entered supercritical extraction reactor (2) after the pepper compressing tablet below 13%;
Supercritical extraction reactor (2): pepper powder is extracted, extractant is the carbon dioxide of food-grade, extraction first half term pressure is 15-18Mpa, temperature 40-45 ℃, the second half extracting pressure is 26-30Mpa, temperature 55-60 ℃, carbon dioxide flow remains at 1200-1400L/h, the total time 3-4h of extraction; Enter separating still (3);
Separating still (3): enter with the fluid of extract and separate to get crude extract in separating still, main component is pipering and pepper essential oil;
Molecular still (4): crude extract is separated impurity such as removing moisture, and be separated into heavy constituent and light component; Light component is mainly the pepper essential oil, and content is greater than 70%; Heavy constituent is mainly pipering, and content is greater than 50%;
Pepper oleoresin tuner (10): comprise edible vegetable oil metering valve (7), pepper essential oil metering valve (9) and pipering metering valve (8); With pepper essential oil, pipering and the edible vegetable oil pepper oleoresin of furnishing different size according to a certain ratio.
2. the method for preparing black pepper oil resin according to claim 1 is characterized in that: the described compressing tablet thickness that rolls the embryo pulverizer is for less than 1.5mm; Grinding particle size is 2-3mm.
3. the method for preparing black pepper oil resin according to claim 1, it is characterized in that: the pressure of described separating still is 5-6Mpa, temperature is 22-30 ℃.
4. the method for preparing black pepper oil resin according to claim 1, it is characterized in that: described embryo pulverizer (1), supercritical extraction reactor (2), separating still (3), molecular still (4) and the pepper oleoresin tuner (10) of rolling seals connection successively by pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2010105574841A CN102058081B (en) | 2010-11-22 | 2010-11-22 | Device for preparing black pepper oil resin |
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| CN2010105574841A CN102058081B (en) | 2010-11-22 | 2010-11-22 | Device for preparing black pepper oil resin |
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| CN102058081A CN102058081A (en) | 2011-05-18 |
| CN102058081B true CN102058081B (en) | 2013-06-26 |
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| CN2010105574841A Active CN102058081B (en) | 2010-11-22 | 2010-11-22 | Device for preparing black pepper oil resin |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102260594B (en) * | 2011-08-01 | 2013-02-13 | 晨光生物科技集团股份有限公司 | Method for extracting black pepper essence oil and black pepper essence oil resin from black paper |
| CN103396885B (en) * | 2013-07-24 | 2015-06-10 | 郑州雪麦龙食品香料有限公司 | Method for preparing pepper aromatic oil |
| CN104026538B (en) * | 2014-05-19 | 2016-02-24 | 郑州雪麦龙食品香料有限公司 | A kind of preparation method of high-purity numb-taste component of zanthoxylum |
| CN105176674B (en) * | 2015-10-22 | 2020-08-25 | 陕西为康食品科技股份有限公司 | Preparation method of pepper seed edible oil |
| CN107927696A (en) * | 2017-11-20 | 2018-04-20 | 广东聿津食品有限公司 | A kind of preparation method of black pepper essential oil |
| CN108464483B (en) * | 2018-01-08 | 2020-12-08 | 晨光生物科技集团股份有限公司 | Industrial method for preparing pepper extract by using fresh pepper as raw material |
| CN111011814A (en) * | 2019-12-19 | 2020-04-17 | 韩城市宏达花椒香料有限公司 | Method for extracting composite spice for marinating meat products |
| CN112293726B (en) * | 2020-10-29 | 2022-11-25 | 晨光生物科技集团股份有限公司 | A method for preparing decolorized black pepper oleoresin and black pepper oleoresin with low piperine content |
| CN115806859A (en) * | 2022-12-23 | 2023-03-17 | 晨光生物科技集团股份有限公司 | Method for extracting pepper essential oil and pepper essential oil prepared by same |
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