CN103146474A - Method for preparing anise resin and seasoning oil thereof - Google Patents
Method for preparing anise resin and seasoning oil thereof Download PDFInfo
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- CN103146474A CN103146474A CN2013101037992A CN201310103799A CN103146474A CN 103146474 A CN103146474 A CN 103146474A CN 2013101037992 A CN2013101037992 A CN 2013101037992A CN 201310103799 A CN201310103799 A CN 201310103799A CN 103146474 A CN103146474 A CN 103146474A
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- anise
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- oil resin
- oil
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Abstract
The invention relates to a method for preparing an anise resin and seasoning oil of the anise resin. The method comprises the following steps of: a. crushing, namely, taking dry anise seeds, crushing by using a medicine crusher, and screening by using a #2 sieve so as to obtain the anise powder; b. drying in vacuum drying oven, namely, drying the anise powder obtained in the step a for 0.5-1 hour under the condition that the vacuum degree is 0.05Mpa-0.1Mpa and the temperature is 70-80 DEG C, so as to obtain the anise powder of which the moisture content is 5-20%; and c. extracting so as to obtain an anise oil resin product. By utilizing the method, an oil resin which has the typical spicy and sweet anise flavor is obtained, and moreover the product is free of solvent residue, and the defects that a few types of anise oil resin products are available in market and the flavor is not adequate are made up, so that the anise resin has wide market development application prospect.
Description
Technical field
The present invention relates to food processing technology field, particularly a kind of deep processing with soy sauce braising star aniseed oil resin and flavor oil thereof.Particularly, the present invention relates to a kind of CO of utilization
2Supercritical extraction unit preparation has that typical suffering is sweet, star anise, the star aniseed oil resin of soy sauce braising and the method for flavor oil thereof.
Background technology
Star anise is little sweet, slightly bitter like the Radix Glycyrrhizae flavor, and strong hot fragrant and sweet gas is arranged.Mainly directly for Cooking Seasoning, also being the important source material of preparation spice mixture, can removing raw meat, increase meat perfume, is the essential spice of meat product, is the major ingredient as soy sauce braising.
The utilization of star anise mainly contains the forms such as direct pulverizing, wet distillation essential oil, supercritical extraction oleo-resinous.Conventional extracting process yield is lower, and local flavor is dull.The present invention is by adopting special extracting process, and concocting method, and the star aniseed oil resin that obtains and flavor oil's fragrance thereof, aromatic flavour have the fragrant and sweet gas fragrance of obvious suffering, can use widely in seasonings.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, provide a kind of and utilize the supercritical extraction unit preparation typical hot sweet, the star aniseed oil resin of star anise local flavor and the method for flavor oil thereof.
The technical solution used in the present invention is:
A kind of method of utilizing supercritical extraction unit to prepare the star aniseed oil resin comprises following steps:
A. pulverize: get dry star anise fruit, pulverize with medicinal herb grinder, cross sieve No. two, obtain the star anise powder;
B. vacuum drying oven is dry: the star anise powder that step a is obtained, and at vacuum tightness (Absolute truth reciprocal of duty cycle) 0.05Mpa-0.1Mpa, under the condition of temperature 70 C-80 ℃, dry 0.5-1h obtains water content at the star anise powder of 5%-20%, as the raw material of extraction;
C. extraction: the star anise powder of step b gained is added supercritical CO
2In fluid extraction device (extraction kettle), the temperature that extraction kettle is set is 50 ℃-60 ℃, and pressure is 25-30Mpa, and the separating still temperature is 40 ℃-50 ℃, and pressure is 3Mpa-8Mpa, opens CO
2Pump passes into CO
2As extraction solvent, adjust CO
2Flow velocity be 10g/min-20g/min, during in settings, CO is closed in the beginning timing after 2-3h until the extraction kettle pressure-stabilisation
2Gas, CO
2Gas recycles through high-pressure pump, opens separating still, collects the star aniseed oil resin, is the star aniseed oil rosin products.
Preferably, the CO in described step c
2Be the CO of the food grade of 99.5%-99.9% for purity
2
The present invention also provides a kind of star aniseed oil resin for preparing by aforesaid method.
The present invention also provides a kind of star aniseed oil resin flavor oil, and this flavor oil is allocated by above-mentioned star aniseed oil resin and Glycerin, mixed triester with caprylic acid capric acid and salad oil and obtains.
Preferably, described star aniseed oil resin, Glycerin, mixed triester with caprylic acid capric acid, salad oil allotment ratio of quality and the number of copies are: 1 part: 10-20 part: 10-20 part.
Supercritical carbon dioxide extraction can well be protected volatile matter and extracting effective components cmpletely.And CO
2Supercritical extraction has following advantage, and the solvent of utilization is nontoxic CO
2Gas, in product without hazardous and noxious substances; CO
2Critical temperature low, the loss of volatile component in the thermo-sensitivity spice is little, and oxidizing reaction can be controlled in bottom line, can pass through the selection operation condition, obtains desired local flavor and fragrance.Separating of solute and extraction solvent can under reduced pressure complete, and avoided the decomposition of the heat-sensitive substance that heating brings in concentrated to change, murder by poisoning problem that also can residual solvent.
The beneficial effect that the present invention has:
The present invention adopts CO
2Supercritical extraction technique extracts the star aniseed oil resin, by selecting suitable extracting pressure and temperature, and fluid flow rate, separation temperature and pressure, thus the effective constituent of star anise is dissolved in fluid, it is extracted.The CO that this process using is nontoxic, cheap, be easy to get
2As solvent, and can recycle, pollution-free to product, environmentally safe.Simple to operate, be applicable to suitability for industrialized production, can obtain having typical suffering sweet, the oleo-resinous of star anise local flavor, and product no solvent residue have been filled up the shortcoming that on market, star aniseed oil resene product is less, local flavor is not enough.Has wide market development application prospect.
Embodiment
Below the present invention will be further described by specific embodiment, but do not limit protection scope of the present invention.
Embodiment 1:
A kind ofly utilize supercritical extraction unit preparation typical hot sweet, the method for the star aniseed oil resin flavor oil of star anise local flavor comprises following steps:
Get dry star anise fruit 10kg, pulverize with medicinal herb grinder, cross sieve No. two, obtain the star anise powder; With the star anise powder that obtains, at vacuum tightness 0.07Mpa, temperature 70 C, dry 0.5h obtains water content at 10% star anise powder, and the raw material as extraction stops drying.Take out dried star anise powder, put in (Huaan, Nantong supercritical extraction company, HA221-50-03 type), the temperature that sets extraction kettle is 50 ℃, and pressure is 30Mpa, and the separating still temperature is 40 ℃, and pressure is 5Mpa, opens CO
2Pump passes into purity and is 99.9% food-class CO
2As extraction solvent, adjust CO
2Flow velocity be 15g/min, treat the extraction kettle pressure-stabilisation at 30Mpa, the beginning timing, close CO after 2h
2Gas, CO
2Gas recycles through high-pressure pump, opens separating still, collects the star aniseed oil resin, is the star aniseed oil rosin products.
Embodiment 2:
A kind ofly utilize supercritical extraction unit preparation typical hot sweet, the method for the star aniseed oil resin flavor oil of star anise local flavor comprises following steps:
Get dry star anise fruit 10kg, pulverize with medicinal herb grinder, cross sieve No. two, obtain the star anise powder; With the star anise powder that obtains, at vacuum tightness 0.07Mpa, temperature 70 C, dry 0.5h obtains water content at 10% star anise powder, and the raw material as extraction stops drying.Take out dried star anise powder, put in (Huaan, Nantong supercritical extraction company, HA221-50-03 type), the temperature that sets extraction kettle is 50 ℃, and pressure is 30Mpa, and the separating still temperature is 40 ℃, and pressure is 5Mpa, opens CO
2Pump passes into purity and is 99.9% food-class CO
2As extraction solvent, adjust CO
2Flow velocity be 15g/min, treat the extraction kettle pressure-stabilisation at 30Mpa, the beginning timing, close CO after 2h
2Gas, CO
2Gas recycles through high-pressure pump, opens separating still, collects the star aniseed oil resin, and star aniseed oil resin, Glycerin, mixed triester with caprylic acid capric acid, salad oil are mixed to get star aniseed oil resin flavor oil according to weight ratio 1:10:10.
Embodiment 3
A kind ofly utilize supercritical extraction unit preparation typical hot sweet, the method for the star aniseed oil resin flavor oil of star anise local flavor comprises following steps:
Get dry star anise fruit 15kg, pulverize with medicinal herb grinder, cross sieve No. two, obtain the star anise powder; With the star anise powder that obtains, at vacuum tightness 0.06Mpa, 80 ℃ of temperature, dry 0.5h obtains water content at 12% star anise powder, and the raw material as extraction stops drying.Take out dried star anise powder, put in (Huaan, Nantong supercritical extraction company, HA221-50-03 type), the temperature that sets extraction kettle is 60 ℃, and pressure is 25Mpa, and the separating still temperature is 50 ℃, and pressure is 6Mpa, opens CO
2Pump passes into purity and is 99.9% food-class CO
2As extraction solvent, adjust CO
2Flow velocity be 15g/min, treat the extraction kettle pressure-stabilisation at 25Mpa, the beginning timing, close CO after 2h
2Gas, CO
2Gas recycles through high-pressure pump, opens separating still, collects the star aniseed oil resin, and star aniseed oil resin, Glycerin, mixed triester with caprylic acid capric acid, salad oil are mixed to get star aniseed oil resin flavor oil according to weight ratio 1:20:20.
The above is only preferred embodiment of the present invention, is not technical scheme of the present invention is done any pro forma restriction.Every foundation technical spirit of the present invention all still belongs in the scope of technical scheme of the present invention any simple modification, equivalent variations and modification that above embodiment does.
Claims (5)
1. method of utilizing supercritical extraction unit to prepare the star aniseed oil resin is characterized in that: comprise following steps:
A. pulverize: get dry star anise fruit, pulverize with medicinal herb grinder, cross sieve No. two, obtain the star anise powder;
B. vacuum drying oven is dry: the star anise powder that step a is obtained, at vacuum tightness 0.05Mpa-0.1Mpa, under the condition of temperature 70 C-80 ℃, dry 0.5-1h obtains water content at the star anise powder of 5%-20%, as the raw material of extraction.
C. extraction: the star anise powder of step b gained is added supercritical CO
2In the fluid extraction device, the temperature that extraction kettle is set is 50 ℃-60 ℃, and pressure is 25-30Mpa, and the separating still temperature is 40 ℃-50 ℃, and pressure is 3Mpa-8Mpa, opens CO
2Pump passes into CO
2As extraction solvent, adjust CO
2Flow velocity be 10g/min-20g/min, during in settings, CO is closed in the beginning timing after 2-3h until the extraction kettle pressure-stabilisation
2Gas, CO
2Gas recycles through high-pressure pump, opens separating still, collects the star aniseed oil resin, is the star aniseed oil rosin products.
2. a kind of method of utilizing supercritical extraction unit to prepare the star aniseed oil resin according to claim 1, is characterized in that: the CO in described step c
2Be the CO of the food grade of 99.5%-99.9% for purity
2
3. star aniseed oil resin, it is characterized in that: this star aniseed oil resin is prepared by the described method of claim 1 or 2.
4. star aniseed oil resin flavor oil is characterized in that: this flavor oil is allocated by the described star aniseed oil resin of claim 3 and Glycerin, mixed triester with caprylic acid capric acid and salad oil and obtains.
5. a kind of star aniseed oil resin according to claim 4 flavor oil, it is characterized in that: described star aniseed oil resin, Glycerin, mixed triester with caprylic acid capric acid, salad oil allotment ratio of quality and the number of copies are: 1 part: 10-20 part: 10-20 part.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2013101037992A CN103146474A (en) | 2013-03-28 | 2013-03-28 | Method for preparing anise resin and seasoning oil thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2013101037992A CN103146474A (en) | 2013-03-28 | 2013-03-28 | Method for preparing anise resin and seasoning oil thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103749743A (en) * | 2013-10-12 | 2014-04-30 | 晨光生物科技集团股份有限公司 | Spicy flavor seasoning oil and preparation method thereof |
| CN104140881A (en) * | 2014-07-31 | 2014-11-12 | 叶新 | Method for extracting anise seed oil |
| CN105038989A (en) * | 2015-07-13 | 2015-11-11 | 湖北中烟工业有限责任公司 | Method for preparing tobacco flavor by taking glycerol triacetate as extractant |
| CN109593609A (en) * | 2018-12-20 | 2019-04-09 | 天津春宇食品配料有限公司 | A method of extraction composite aromatic condiment oleoresin |
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| GB2337528A (en) * | 1998-05-19 | 1999-11-24 | St Giles Foods Ltd | Alcohol free vegetable oil composition comprising a medium chain triglyceride |
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| CN101664076A (en) * | 2009-08-24 | 2010-03-10 | 天津春发食品配料有限公司 | Condiment oil containing sesame oil and oleoresin |
| CN101690527A (en) * | 2009-09-23 | 2010-04-07 | 北京市科威华食品工程技术有限公司 | Nutritional walnut blending oil |
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2013
- 2013-03-28 CN CN2013101037992A patent/CN103146474A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2337528A (en) * | 1998-05-19 | 1999-11-24 | St Giles Foods Ltd | Alcohol free vegetable oil composition comprising a medium chain triglyceride |
| CN101530137A (en) * | 2008-03-12 | 2009-09-16 | 李建成 | Novel edible oil for rice and method for preparing same |
| CN101664076A (en) * | 2009-08-24 | 2010-03-10 | 天津春发食品配料有限公司 | Condiment oil containing sesame oil and oleoresin |
| CN101690527A (en) * | 2009-09-23 | 2010-04-07 | 北京市科威华食品工程技术有限公司 | Nutritional walnut blending oil |
Non-Patent Citations (3)
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| 李建成: "辛癸酸甘油酯的应用及系列产品的开发保健", 《中国食品添加剂》 * |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103749743A (en) * | 2013-10-12 | 2014-04-30 | 晨光生物科技集团股份有限公司 | Spicy flavor seasoning oil and preparation method thereof |
| CN103749743B (en) * | 2013-10-12 | 2015-05-13 | 晨光生物科技集团股份有限公司 | Spicy flavor seasoning oil and preparation method thereof |
| CN104140881A (en) * | 2014-07-31 | 2014-11-12 | 叶新 | Method for extracting anise seed oil |
| CN105038989A (en) * | 2015-07-13 | 2015-11-11 | 湖北中烟工业有限责任公司 | Method for preparing tobacco flavor by taking glycerol triacetate as extractant |
| CN109593609A (en) * | 2018-12-20 | 2019-04-09 | 天津春宇食品配料有限公司 | A method of extraction composite aromatic condiment oleoresin |
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