CN105295492A - Putty powder and preparation method thereof - Google Patents
Putty powder and preparation method thereof Download PDFInfo
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- CN105295492A CN105295492A CN201510502531.5A CN201510502531A CN105295492A CN 105295492 A CN105295492 A CN 105295492A CN 201510502531 A CN201510502531 A CN 201510502531A CN 105295492 A CN105295492 A CN 105295492A
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Abstract
The invention discloses putty powder and a preparation method thereof. The putty powder comprises gelatination polymerization materials, a particle material and an additive, wherein the particle size of the particle material is 50 to 100 [Mu]m; the putty powder comprises the following materials by weight: 20 to 40 percent of the gelatination polymerization materials, 40 to 60 percent of the particle material and 10 to 30 percent of the additive; the gelatination polymerization materials comprise cellulose ether, styrene-type thermoplastic elastomer, polypropylene resin, macromolecular silicone oil, a polythene liquid, polypropylene, polyamide, pimaric acid, maleic anhydride, and propyl trititanate. The putty powder and the preparation method have the advantages that the preparation process is simple and convenient; the preparation cost is low; the operation is convenient; the preparation efficiency is high; the prepared putty powder is reliable in quality, anti-microbial, and bacteriostatic, and has an air-purifying function.
Description
Technical field
The invention belongs to and building material technical field, particularly relate to a kind of putty powder and preparation method thereof.
Background technology
In building industry, wall surface putty is supplementary material important in building coating coating process, tradition putty is for binding agent with organic high molecular polymer or inorganics, by certain or several hybrid modulation such as base-material and mass filler, pigment extender and a small amount of auxiliary agent with adhesive property, and add the soft paste building and ornament materials that thixotropic agent, defoamer, color stuffing etc. make.Be widely used in the places such as the inside and outside metope of all kinds of buildings in civil construction field, ground, roofing ceiling, the functional materials be a kind of wide application, being worth research and development and paying much attention to.
Chinese patent CN1796467 discloses a kind of name and is called lacquer putty paste, powder capable of for purifying air in use on inner wall and outer wall, be specially: a kind of lacquer putty paste, powder capable of for purifying air in use on inner wall and outer wall, following raw materials according is made according to following weight proportion: tourmalinite 10-20 part, talcum powder 800-1000 part, carboxymethyl cellulose 20-40 part, formaldehyde 0.4-0.8 part, 1.5 parts, whitening agent, water 300-500 part.But this putty paste, powder in use easily cause putty coating efflorescence, cracking, hollowing and come off.
Chinese patent CN201310251137.X discloses a kind of preparation method and using method of putty powder for exterior wall of antistripping, and described preparation method is: talcum powder 6-8 part, White Bentonite 2-4 part and white silicate water 12-14 part mud are added pulverizer and is crushed to and is less than 150 orders by S1; The powder that S1 obtains by S2 mixes with diatomite 40-44 part, high strength gypsum powder 7-9 part, titanium dioxide 6-8 part, then puts into after pulverizing mill carries out grinding 10-15 minute and adds Vltra tears 2-3 part again, then grind 5-10 minute; The powder that S2 obtains is crossed 320 eye mesh screens by S3, and minus mesh is described putty powder for exterior wall.Described using method is that the putty powder for exterior wall of preparation is put into container, be that 10:2-3 adds water in the ratio of putty powder for exterior wall and water, and need to add suitable pigment according to the color of exterior wall, infiltrate 40-60 minute, then adopt stirrer to stir and carry out knife-coat application in 5-10 minute.But the method complex manufacturing process, is unfavorable for that the marketization is promoted.
Therefore be badly in need of that a kind of preparation process is easy, the putty powder of reliable in quality and preparation method thereof, to meet the needs in market.
Summary of the invention
The present invention is directed to the problems referred to above, a kind of putty powder and preparation method thereof is provided.
The present invention's adopted technical scheme that solves the problem is: a kind of putty powder, comprise gel polymerization material, particulate material and admixture, the particle diameter of particulate material is 50 μm ~ 100 μm, putty powder granularity is little, there is color and luster exquisiteness, intensity is high, sticking power good, cohesive force is large and the feature of crack resistence, the later strength of putty powder for exterior wall can be strengthened, exterior wall can be avoided to produce and return white phenomenon.The weight percent of putty powder consists of: gel polymerization material 20% ~ 40%, particulate material 40% ~ 60%, admixture 10% ~ 30%; Cohesion condensation material comprises: ether of cellulose, styrene analog thermoplastic elastomer, acrylic resin, macromole silicone oil, polyethylene liquid, polypropylene, polymeric amide, pimaric acid, maleic anhydride, propyl group three titanic acid ester, and the weight part of cohesion condensation material consists of: ether of cellulose 1 part ~ 3 parts, styrene analog thermoplastic elastomer 10 parts ~ 13 parts, acrylic resin 1 part ~ 3 parts, macromole silicone oil 1 part ~ 3 parts, polyethylene liquid 1 part ~ 3 parts, polypropylene 1 part ~ 3 parts, polymeric amide 1 part ~ 3 parts, pimaric acid 1 part ~ 3 parts, maleic anhydride 1 part ~ 3 parts, propyl group acid esters 2 parts ~ 3 parts.Add excellent gel polymerization material, the putty powder of preparation has antibacterial, antibacterial effect, has the function purified air, and can dispel the multiple toxic gases such as indoor formaldehyde, ammonia, radon, benzene.
Further, styrene analog thermoplastic elastomer is made up of styrene-ethylene, butadiene-styrene, isoprene styrene.
Further, the weight percent of styrene analog thermoplastic elastomer consists of: styrene-ethylene 10% ~ 30%, butadiene-styrene 20% ~ 40%, isoprene styrene 40% ~ 60%.
Further, particulate material comprises: sierozem power, light calcium carbonate, gypsum, diatomite, White Bentonite, titanium dioxide.
Further, the weight part of particle consists of: sierozem power 8 parts ~ 10 parts, light calcium carbonate 8 parts ~ 10 parts, 2 parts ~ 10 parts, gypsum, 8 parts ~ 10 parts, diatomite, White Bentonite 8 parts ~ 10 parts, titanium dioxide 6 parts ~ 10 parts.
Further, admixture is: Tripotassium Citrate, lemon oil and macromole silicone oil.
Further, the weight part of admixture consists of: Tripotassium Citrate 4 parts ~ 10 parts, lemon oil 4 parts ~ 10 parts, macromole silicone oil 2 parts ~ 10 parts.
According to another object of the present invention, be the making method that a kind of putty powder is provided, adopt the shearing force under different mixing speed condition different, and then the size distribution of adjustment material, the time of processing and manufacturing is short, fits and produces at rapid, high volume, and can reach the effect reducing Production Time and manpower operation's cost, effectively can improve industrial competitiveness, concrete steps are:
Step S01, particulate material is pulverized: particulate material supper micron mill being crushed to particle diameter is 50 μm ~ 100 μm.
Step S02, batch mixing: the particulate material after pulverizing is added admixture under rotating speed stirs, stirs 10 minutes ~ 15 minutes, to completely even.
Step S03, dispersion: add gel polymerization material on batch mixing completely basis, high speed dispersion 20 minutes ~ 30 minutes, the particle diameter to material is 40 μm ~ 50 μm.Utilize the shearing force stirred to disperse material, obtain different dispersion effects by adjustment rotating speed, technique is advanced, and preparation cost is low, easy to operate, and the putty powder reliable in quality obtained, preparation efficiency is high.
Further, in step S02, the rotating speed of stirring is 1000r/min ~ 1200r/min.
Further, in step S03, the condition of high speed dispersion is: process under stirring pulverizing rotating speed is the condition of 3000r/min ~ 4000r/min.
Advantage of the present invention is:
1. the preparation method of the present invention's employing, utilizes the shearing force stirred to disperse material, and obtain different dispersion effects by adjustment rotating speed, technique is advanced, and preparation cost is low, easy to operate, the putty powder reliable in quality obtained, and preparation efficiency is high;
2. the preparation method that the present invention adopts can shorten the time of processing and manufacturing, fits and produces at rapid, high volume, and can reach the effect reducing Production Time and manpower operation's cost, and effectively can improve industrial competitiveness;
3. the present invention adds excellent gel polymerization material, and the putty powder of preparation has antibacterial, antibacterial effect, has the function purified air, and can dispel the multiple toxic gases such as indoor formaldehyde, ammonia, radon, benzene;
4. putty powder granularity of the present invention is little, has color and luster exquisiteness, intensity is high, sticking power good, cohesive force is large and the feature of crack resistence, can strengthen the later strength of putty powder for exterior wall, exterior wall can be avoided to produce and return white phenomenon.
Except object described above, feature and advantage, the present invention also has other object, feature and advantage.Below with reference to embodiment, the present invention is further detailed explanation.
Embodiment
Below in conjunction with embodiment, the present invention is described in detail, but the multitude of different ways that the present invention can be defined by the claims and cover is implemented.
Embodiment 1
A kind of putty powder and preparation method thereof
Putty powder starting material:
Cohesion condensation material:
Ether of cellulose 1kg, styrene-ethylene 1kg, butadiene-styrene 3kg, isoprene styrene 6kg, acrylic resin 1kg, macromole silicone oil 1kg, polyethylene liquid 1kg, polypropylene 1kg, polymeric amide 1kg, pimaric acid 1kg, maleic anhydride 1kg, propyl group acid esters 2kg.
Particulate material:
Sierozem power 10kg, light calcium carbonate 10kg, gypsum 10kg, diatomite 10kg, White Bentonite 10kg, titanium dioxide 10kg.
Admixture:
Tripotassium Citrate 6kg, lemon oil 6kg, macromole silicone oil 8kg.
Making method is:
(1) particulate material is pulverized: sierozem power 10kg, light calcium carbonate 10kg, gypsum 10kg, diatomite 10kg, White Bentonite 10kg, titanium dioxide 10kg supper micron mill are crushed to the particulate material that particle diameter is 50 μm.
(2) batch mixing: the particulate material after pulverizing is added Tripotassium Citrate 6kg, lemon oil 6kg, macromole silicone oil 8kg under 1000r/min rotating speed stirs, stirs 10 minutes, to completely even.
(3) disperse: on batch mixing completely basis, add ether of cellulose 1kg, styrene-ethylene 1kg, butadiene-styrene 3kg, isoprene styrene 6kg, acrylic resin 1kg, macromole silicone oil 1kg, polyethylene liquid 1kg, polypropylene 1kg, polymeric amide 1kg, pimaric acid 1kg, maleic anhydride 1kg, propyl group acid esters 2kg, high speed dispersion 20 minutes under 3000r/min condition, particle diameter to material is 40 μm, obtains putty powder finished product.
Embodiment 2
A kind of putty powder and preparation method thereof
Putty powder starting material:
Cohesion condensation material:
Ether of cellulose 3kg, styrene-ethylene 3.9kg, butadiene-styrene 2.6kg isoprene styrene 6.5kg, styrene analog thermoplastic elastomer 13kg, acrylic resin 3kg, macromole silicone oil 3kg, polyethylene liquid 3kg, polypropylene 3kg, kymene kg, pimaric acid 3kg, maleic anhydride 3kg, propyl group acid esters 3kg.
Particulate material:
Sierozem power 8kg, light calcium carbonate 8kg, gypsum 8kg, diatomite 8kg, White Bentonite 8kg, titanium dioxide 10kg.
Admixture:
Tripotassium Citrate 4kg, lemon oil 4kg, macromole silicone oil 2kg.
Making method is:
(1) particulate material is pulverized: sierozem power 8kg, light calcium carbonate 8kg, gypsum 8kg, diatomite 8kg, White Bentonite 8kg, titanium dioxide 10kg supper micron mill are crushed to the particulate material that particle diameter is 100 μm.
(2) batch mixing: the particulate material after pulverizing is added Tripotassium Citrate 4kg, lemon oil 4kg, macromole silicone oil 2kg under 1200r/min rotating speed stirs, stirs 15 minutes, to completely even.
(3) disperse: on batch mixing completely basis, add gel polymerization material, high speed dispersion 30 minutes under 4000r/min condition, the particle diameter to material is 50 μm, obtains putty powder finished product.
Embodiment 3
A kind of putty powder and preparation method thereof
Putty powder starting material:
Cohesion condensation material:
Ether of cellulose 2kg, styrene-ethylene 3kg, butadiene-styrene 3kg, isoprene styrene 6kg, acrylic resin 2kg, macromole silicone oil 2kg, polyethylene liquid 2kg, polypropylene 2kg, polymeric amide 2kg, pimaric acid 2kg, maleic anhydride 2kg, propyl group acid esters 2kg.
Particulate material:
Sierozem power 8kg, light calcium carbonate 8kg, gypsum 2kg, diatomite 8kg, White Bentonite 8kg, titanium dioxide 6kg.
Admixture:
Tripotassium Citrate 10kg, lemon oil 10kg, macromole silicone oil 10kg.
Making method is:
(1) particulate material is pulverized: sierozem power 8kg, light calcium carbonate 8kg, gypsum 2kg, diatomite 8kg, White Bentonite 8kg, titanium dioxide 6kg supper micron mill are crushed to the particulate material that particle diameter is 75 μm.
(2) batch mixing: the particulate material after pulverizing is added Tripotassium Citrate 10kg, lemon oil 10kg, macromole silicone oil 10kg under 1100r/min rotating speed stirs, stirs 12.5 minutes, to completely even.
(3) disperse: on batch mixing completely basis, add gel polymerization material, high speed dispersion 25 minutes under 3500r/min condition, the particle diameter to material is 45 μm, obtains putty powder finished product.
Experimental example
In this experimental example, test the performance of putty powder prepared by the present invention 1 ~ 3 by experiment.
1. test materials
Experimental group: putty powder prepared by the embodiment of the present invention 1 ~ 3;
Control group: common putty powder.
2. test method
The indices performance of the test embodiment of the present invention 1 ~ 3 putty powder, common putty powder.
3. test-results
Analyze after the indices performance test of the embodiment of the present invention 1 ~ 3 putty powder, common putty powder, experimental result is in table 1.
Table 1. test result
Experimental result shows, compared with common putty powder, the embodiment of the present invention 1 ~ 3 prepare the durable splitting resistance of putty powder under square one, cohesive strength, minimum tolerable temperature results of property measure be better than common putty powder, water-intake rate is lower than common putty powder, preparation method is applicable to promoting, and quality product is better.
These are only the preferred embodiments of the present invention and experimental example, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., within the protection domain that all should be included in invention.
Claims (10)
1. a putty powder, comprise gel polymerization material, particulate material and admixture, the particle diameter of described particulate material is 50 μm ~ 100 μm, and it is characterized in that, the weight percent of described putty powder consists of: gel polymerization material 20% ~ 40%, particulate material 40% ~ 60%, admixture 10% ~ 30%; Described cohesion condensation material comprises: ether of cellulose, styrene analog thermoplastic elastomer, acrylic resin, macromole silicone oil, polyethylene liquid, polypropylene, polymeric amide, pimaric acid, maleic anhydride, propyl group three titanic acid ester, and the weight part of described cohesion condensation material consists of: ether of cellulose 1 part ~ 3 parts, styrene analog thermoplastic elastomer 10 parts ~ 13 parts, acrylic resin 1 part ~ 3 parts, macromole silicone oil 1 part ~ 3 parts, polyethylene liquid 1 part ~ 3 parts, polypropylene 1 part ~ 3 parts, polymeric amide 1 part ~ 3 parts, pimaric acid 1 part ~ 3 parts, maleic anhydride 1 part ~ 3 parts, propyl group acid esters 2 parts ~ 3 parts.
2. putty powder according to claim 1, is characterized in that, described styrene analog thermoplastic elastomer is made up of styrene-ethylene, butadiene-styrene, isoprene styrene.
3. putty powder according to claim 2, is characterized in that, the weight percent of described styrene analog thermoplastic elastomer consists of: styrene-ethylene 10% ~ 30%, butadiene-styrene 20% ~ 40%, isoprene styrene 40% ~ 60%.
4. putty powder according to claim 1, is characterized in that, described particulate material comprises: sierozem power, light calcium carbonate, gypsum, diatomite, White Bentonite, titanium dioxide.
5. putty powder according to claim 4, it is characterized in that, the weight part of described particle consists of: sierozem power 8 parts ~ 10 parts, light calcium carbonate 8 parts ~ 10 parts, 2 parts ~ 10 parts, gypsum, 8 parts ~ 10 parts, diatomite, White Bentonite 8 parts ~ 10 parts, titanium dioxide 6 parts ~ 10 parts.
6. putty powder according to claim 1, is characterized in that, described admixture is: Tripotassium Citrate, lemon oil and macromole silicone oil.
7. putty powder according to claim 6, is characterized in that, the weight part of described admixture consists of: Tripotassium Citrate 4 parts ~ 10 parts, lemon oil 4 parts ~ 10 parts, macromole silicone oil 2 parts ~ 10 parts.
8. a making method for putty powder as claimed in claim 1, is characterized in that, the concrete steps of described making method are:
Step S01, particulate material is pulverized: particulate material supper micron mill being crushed to particle diameter is 50 μm ~ 100 μm;
Step S02, batch mixing: the particulate material after pulverizing is added admixture under rotating speed stirs, stirs 10 minutes ~ 15 minutes, to completely even;
Step S03, dispersion: add gel polymerization material on batch mixing completely basis, high speed dispersion 20 minutes ~ 30 minutes, the particle diameter to material is 40 μm ~ 50 μm.
9. making method according to claim 8, in step S02, is characterized in that, the rotating speed of described stirring is 1000r/min ~ 1200r/min.
10. making method according to claim 8, in step S03, is characterized in that, the condition of described high speed dispersion is: process under stirring pulverizing rotating speed is the condition of 3000r/min ~ 4000r/min.
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| CN201510502531.5A CN105295492A (en) | 2015-08-17 | 2015-08-17 | Putty powder and preparation method thereof |
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| CN201510502531.5A CN105295492A (en) | 2015-08-17 | 2015-08-17 | Putty powder and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082916A (en) * | 2016-06-22 | 2016-11-09 | 安徽天富泵阀有限公司 | A kind of leveling putty rubber powder for the self priming pump pump housing |
| US11771094B2 (en) | 2017-06-14 | 2023-10-03 | Premix Oy | Antimicrobial polymer composition |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1743388A (en) * | 2005-10-11 | 2006-03-08 | 济南大学 | Waterproof cracking-proof dry-powder putty for exposed wall |
| CN103086664A (en) * | 2013-01-08 | 2013-05-08 | 张立功 | Internal wall putty and production process thereof |
| CN103351130A (en) * | 2013-06-21 | 2013-10-16 | 天长市开林化工有限公司 | Preparation method and using method of anti-stripping exterior wall putty powder |
| CN104556898A (en) * | 2014-12-22 | 2015-04-29 | 安徽朗凯奇防水科技股份有限公司 | Environment-friendly high-adhesion-stress special putty for ceramic tile surfaces and preparation method thereof |
-
2015
- 2015-08-17 CN CN201510502531.5A patent/CN105295492A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1743388A (en) * | 2005-10-11 | 2006-03-08 | 济南大学 | Waterproof cracking-proof dry-powder putty for exposed wall |
| CN103086664A (en) * | 2013-01-08 | 2013-05-08 | 张立功 | Internal wall putty and production process thereof |
| CN103351130A (en) * | 2013-06-21 | 2013-10-16 | 天长市开林化工有限公司 | Preparation method and using method of anti-stripping exterior wall putty powder |
| CN104556898A (en) * | 2014-12-22 | 2015-04-29 | 安徽朗凯奇防水科技股份有限公司 | Environment-friendly high-adhesion-stress special putty for ceramic tile surfaces and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 徐峰等: "《建筑涂料》", 31 August 2007, 中国建筑工业出版社 * |
| 李里特: "《粮油贮藏加工工艺学》", 31 August 2002, 中国农业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082916A (en) * | 2016-06-22 | 2016-11-09 | 安徽天富泵阀有限公司 | A kind of leveling putty rubber powder for the self priming pump pump housing |
| US11771094B2 (en) | 2017-06-14 | 2023-10-03 | Premix Oy | Antimicrobial polymer composition |
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Application publication date: 20160203 |