CN105293562B - 制备Tb掺杂Ag2S稀磁半导体微米颗粒的方法 - Google Patents
制备Tb掺杂Ag2S稀磁半导体微米颗粒的方法 Download PDFInfo
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- CN105293562B CN105293562B CN201510806984.7A CN201510806984A CN105293562B CN 105293562 B CN105293562 B CN 105293562B CN 201510806984 A CN201510806984 A CN 201510806984A CN 105293562 B CN105293562 B CN 105293562B
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- Prior art keywords
- doping
- thiocarbamide
- silver nitrate
- magnetic semiconductor
- nitrate
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- 239000004065 semiconductor Substances 0.000 title claims abstract description 27
- 239000002245 particle Substances 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 15
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 44
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000006184 cosolvent Substances 0.000 claims abstract description 19
- 230000004044 response Effects 0.000 claims abstract description 17
- 229910001961 silver nitrate Inorganic materials 0.000 claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- YJVUGDIORBKPLC-UHFFFAOYSA-N terbium(3+);trinitrate Chemical compound [Tb+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O YJVUGDIORBKPLC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 11
- 238000003801 milling Methods 0.000 claims abstract description 11
- 235000019743 Choline chloride Nutrition 0.000 claims abstract description 8
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004202 carbamide Substances 0.000 claims abstract description 7
- 239000012153 distilled water Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001763 2-hydroxyethyl(trimethyl)azanium Substances 0.000 claims abstract description 5
- SGMZJAMFUVOLNK-UHFFFAOYSA-M choline chloride Chemical compound [Cl-].C[N+](C)(C)CCO SGMZJAMFUVOLNK-UHFFFAOYSA-M 0.000 claims abstract description 5
- 229960003178 choline chloride Drugs 0.000 claims abstract description 5
- 229910002651 NO3 Inorganic materials 0.000 claims description 7
- 238000002604 ultrasonography Methods 0.000 claims description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 5
- 101710134784 Agnoprotein Proteins 0.000 claims description 2
- 229910052771 Terbium Inorganic materials 0.000 claims 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims 1
- GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 claims 1
- 229910052946 acanthite Inorganic materials 0.000 abstract description 8
- FSJWWSXPIWGYKC-UHFFFAOYSA-M silver;silver;sulfanide Chemical compound [SH-].[Ag].[Ag+] FSJWWSXPIWGYKC-UHFFFAOYSA-M 0.000 abstract description 8
- 239000004094 surface-active agent Substances 0.000 abstract description 6
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 238000005303 weighing Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 5
- 238000007605 air drying Methods 0.000 description 4
- 238000005485 electric heating Methods 0.000 description 4
- 230000005415 magnetization Effects 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000005622 photoelectricity Effects 0.000 description 2
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000010365 information processing Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000015654 memory Effects 0.000 description 1
- XRRQZKOZJFDXON-UHFFFAOYSA-N nitric acid;silver Chemical compound [Ag].O[N+]([O-])=O XRRQZKOZJFDXON-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Investigating Or Analyzing Materials By The Use Of Fluid Adsorption Or Reactions (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
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Application Number | Priority Date | Filing Date | Title |
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CN201510806984.7A CN105293562B (zh) | 2015-11-22 | 2015-11-22 | 制备Tb掺杂Ag2S稀磁半导体微米颗粒的方法 |
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CN201510806984.7A CN105293562B (zh) | 2015-11-22 | 2015-11-22 | 制备Tb掺杂Ag2S稀磁半导体微米颗粒的方法 |
Publications (2)
Publication Number | Publication Date |
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CN105293562A CN105293562A (zh) | 2016-02-03 |
CN105293562B true CN105293562B (zh) | 2017-06-20 |
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CN201510806984.7A Expired - Fee Related CN105293562B (zh) | 2015-11-22 | 2015-11-22 | 制备Tb掺杂Ag2S稀磁半导体微米颗粒的方法 |
Country Status (1)
Country | Link |
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CN (1) | CN105293562B (zh) |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101654277B (zh) * | 2009-09-16 | 2011-07-20 | 天津大学 | 梭形或棒状硫化银纳米颗粒制备方法 |
CN103265063B (zh) * | 2013-05-31 | 2014-07-09 | 吉林大学 | 制备Y掺杂Ag2S稀磁半导体纳米颗粒的方法 |
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- 2015-11-22 CN CN201510806984.7A patent/CN105293562B/zh not_active Expired - Fee Related
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Effective date of registration: 20161205 Address after: 510665 Guangdong city of Guangzhou province Tianhe District Software Park Building No. 59 Middle East block, Grand Building Room 501 Applicant after: Guangdong million cattle Intellectual Property Operation Co., Ltd. Address before: 330001 Jiangxi province Qingyunpu District of Nanchang City Nan Road No. 138 Applicant before: Wu Bin |
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Effective date of registration: 20170508 Address after: Baoan District Shenzhen City manhole street 518100 of Guangdong province Jidali Industrial District 6 building two floor East Applicant after: Shenzhen Creation Technology Co., Ltd. Address before: 510665 Guangdong city of Guangzhou province Tianhe District Software Park Building No. 59 Middle East block, Grand Building Room 501 Applicant before: Guangdong million cattle Intellectual Property Operation Co., Ltd. |
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