CN105232355A - No-clean hand lotion and preparation method thereof - Google Patents

No-clean hand lotion and preparation method thereof Download PDF

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Publication number
CN105232355A
CN105232355A CN201510678686.4A CN201510678686A CN105232355A CN 105232355 A CN105232355 A CN 105232355A CN 201510678686 A CN201510678686 A CN 201510678686A CN 105232355 A CN105232355 A CN 105232355A
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China
Prior art keywords
parts
hands
dew
washed
reactant liquor
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Pending
Application number
CN201510678686.4A
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Chinese (zh)
Inventor
夏穆兰
彭锡彩
宋铜山
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Hubei Mulan Tongda Technology Co Ltd
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Hubei Mulan Tongda Technology Co Ltd
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Priority to CN201510678686.4A priority Critical patent/CN105232355A/en
Publication of CN105232355A publication Critical patent/CN105232355A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a no-clean hand lotion and a preparation method, and relates to the field of a detergent. In parts by mass, every 100 parts of the no-clean hand lotion consists of the following ingredients: 0.1-0.4 parts of carbomer, 40-70 parts of alcohol, 0.01-0.3 parts of triclosan, 1.5-5 parts of Tween, 0.1-0.4 parts of triethanolamine and the balance of pure water or mineral water. The triclosan is effective in inhibiting such harmful bacteria including escherichia coli, staphylococcus aureus and candida albicans, and meanwhile, the triclosan is capable of protecting beneficial bacteria. The no-clean hand lotion disclosed by the invention, after being sprayed and smeared, is in the form of a gel and is free from generation of a great amount of foam; when the no-clean hand lotion is used, the gel can be directly smeared on hand skin so as to rapidly kill bacteria on the hand skin with the triclosan and the alcohol therein, and the gel can be cleaned from the hand when being wiped with tissue paper; and compared with the prior art which requires a great amount of water to flush, the no-clean hand lotion is capable of saving water resource, and the no-clean hand lotion is available all times and is free from environmental limitation.

Description

A kind of leave is washed one's hands and is revealed and preparation method thereof
Technical field
The present invention relates to detergent applications, be specifically related to a kind of leave wash one's hands dew and preparation method thereof.
Background technology
Because hand needs to contact a lot of article every day, these article are not only with dust, antibacterial, oils and fats, also may with corrosive elements, need to clear up, because traditional soap alkalescence is heavier, xerosis cutis can be caused after using coarse, therefore, the relatively mild handwashing liquid of most people's choice for use is as detergent, handwashing liquid has the feature of foaming abundancy, exquisiteness, gentleness, low stimulation, and usually adopt disposable mode of getting liquid, the secondary pollution of user skin can not be caused, be widely used.
But current handwashing liquid in use, can produce a large amount of foams, and containing a small amount of alkaline components in foam, if rinse not thorough, hand skin has a certain amount of residual, impacts, need a large amount of water, compare waste during flushing hand skin; Meanwhile, when environment for use is poor, when not having enough water, handwashing liquid can not be used to clean, and environment for use is restricted.
Summary of the invention
For the defect existed in prior art, a kind of leave is the object of the present invention is to provide to wash one's hands dew and preparation method thereof, can not only saving water resource, and not by the restriction of environment for use.
For reaching above object, the technical scheme that the present invention takes is:
A kind of leave is washed one's hands dew, and it is characterized in that: by mass parts, every 100 parts of leaves are following composition in washing one's hands and revealing:
Surplus is pure water or mineral water.
On the basis of technique scheme, by mass parts, described every 100 parts of leaves are washed one's hands in dew, and the content of described triclosan is 0.01 ~ 0.04 part.
On the basis of technique scheme, by mass parts, described every 100 parts of leaves are washed one's hands in dew, and alcohol content is 50 ~ 65 parts.
On the basis of technique scheme, by mass parts, described every 100 parts of leaves are washed one's hands in dew, and alcohol content is 60 parts.
On the basis of technique scheme, the mass ratio of described carbomer and triethanolamine is 1:1.
On the basis of technique scheme, by mass parts, described every 100 parts of leaves are washed one's hands in dew, and the mass parts of described carbomer and triethanolamine is 0.2 ~ 0.3 part.
On the basis of technique scheme, by mass parts, described every 100 parts of leaves are washed one's hands in dew, and the mass parts of described carbomer and triethanolamine is 0.22 part.
Leave according to any one of claim 1 to 7 wash one's hands dew a preparation method, comprise the following steps:
Pure water or mineral water are added in reactor, in reactor, add 0.1 ~ 0.4 part of carbomer by the speed of 0.01 ~ 0.05 part/min and stir, after being warming up to 40 ~ 45 DEG C after insulated and stirred 1 ~ 1.5h, being warming up to 60 ~ 65 DEG C, insulated and stirred 10 ~ 20min, obtains the first reactant liquor;
0.01 ~ 0.3 part of triclosan and 1 ~ 3 part of tween to be mixed in hermetic container and after stirring, add 40 ~ 70 parts of ethanol mix homogeneously, obtain the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, be under the condition of-0.06 ~-0.08Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, add 0.1 ~ 0.4 part of triethanolamine, 0.5 ~ 2 part of tween is added after stirring, be under the condition of-0.06 ~-0.08Mpa in vacuum, stir after 20 ~ 40min, filter and obtain leave and to wash one's hands dew.
Compared with prior art, the invention has the advantages that:
(1) leave in the present invention is washed one's hands dew, and comprise 0.01 ~ 0.3 part of triclosan, 40 ~ 70 parts of ethanol, triclosan effectively can suppress noxious bacteria: escherichia coli, staphylococcus aureus, Candida albicans, can protect beneficial bacteria simultaneously.
Leave of the present invention is gel after washing one's hands and revealing spraying, a large amount of foams can not be produced, directly gel is spread upon on hand skin during use, wash one's hands triclosan in dew and ethanol just can kill rapidly on hand skin and obtains antibacterial, can hand be cleaned by napkin wiping, and use compared with large water gaging rinses in prior art, can saving water resource, and can use at any time, not by environmental limit.
(2) leave in the present invention is washed one's hands dew, and when the content of triclosan is 0.01 ~ 0.04 part, when alcohol content is 50 ~ 65 parts, effectively can suppress noxious bacteria, and after using, ethanol volatilizees rapidly, take away triclosan residue, avoid triclosan to accumulate and injure skin.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
The embodiment of the present invention provide a kind of leave wash one's hands dew and preparation method thereof, by mass parts, every 100 parts of leaves wash one's hands dew in, be following composition:
Surplus is pure water or mineral water.
In the embodiment of the present invention, by mass parts, every 100 parts of leaves are washed one's hands in dew, and the optimum content of triclosan is 0.01 part ~ 0.04 part.
In the present embodiment, the mass ratio of carbomer and triethanolamine is 1:1, and by mass parts, every 100 parts of leaves are washed one's hands in dew, and the mass parts of carbomer and triethanolamine can be 0.2 ~ 0.3 part; In the present embodiment, the mass parts optimum of carbomer and triethanolamine is 0.22 part.
In the present embodiment, by mass parts, every 100 parts of leaves are washed one's hands in dew, and alcohol content is 50 ~ 65 parts, and optimum is 60 parts.
In the present invention under the content of triclosan is the condition of 0.01 ~ 0.3 part, when alcohol content is 40 ~ 70 parts, triclosan effectively can suppress noxious bacteria: escherichia coli, staphylococcus aureus, Candida albicans, can protect beneficial bacteria simultaneously.And when the content of triclosan is 0.01 ~ 0.04 part, when alcohol content is 50 ~ 65 parts, effectively can suppress noxious bacteria, and after using, ethanol volatilizees rapidly, takes away triclosan residue, avoids triclosan to accumulate and injures skin.
Leave of the present invention is gel after washing one's hands and revealing spraying, a large amount of foams can not be produced, directly gel is spread upon on hand skin during use, wash one's hands triclosan in dew and ethanol just can kill rapidly on hand skin and obtains antibacterial, can hand be cleaned by napkin wiping, and use compared with large water gaging rinses in prior art, can saving water resource, and can use at any time, not by environmental limit.
The preparation method that the present invention also provides a kind of leave to wash one's hands dew, comprises the following steps:
Pure water or mineral water are added in reactor, in reactor, add 0.1 ~ 0.4 part of carbomer by the speed of 0.01 ~ 0.05 part/min and stir, after being warming up to 40 ~ 45 DEG C after insulated and stirred 1 ~ 1.5h, being warming up to 60 ~ 65 DEG C, insulated and stirred 10 ~ 20min, obtains the first reactant liquor;
0.05 ~ 0.3 part of triclosan and 1 ~ 3 part of tween to be mixed in hermetic container and after stirring, add 40 ~ 70 parts of ethanol mix homogeneously, obtain the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, be under the condition of-0.06 ~-0.08Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, add 0.1 ~ 0.4 part of triethanolamine, 0.5 ~ 2 part of tween is added after stirring, be under the condition of-0.06 ~-0.08Mpa in vacuum, stir after 20 ~ 40min, filter and obtain leave and to wash one's hands dew.
Below, by 5 embodiments, the present invention is described in detail
Embodiment 1
Pure water or mineral water are added in reactor, in reactor, adds 0.1 part of carbomer by the speed of 0.01 part/min and stir, after being warming up to 45 DEG C after insulated and stirred 1, being warming up to 60 DEG C, insulated and stirred 10min, obtaining the first reactant liquor;
0.05 part of triclosan and 1 part of tween to be mixed in hermetic container and after stirring, add 40 parts of ethanol mix homogeneously, obtaining the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, is under the condition of-0.06Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, adding 0.1 part of triethanolamine, add 2 parts of tweens after stirring, is under the condition of-0.08Mpa in vacuum, stir after 20min, filter and obtain leave and to wash one's hands dew.
Embodiment 2
Pure water or mineral water are added in reactor, in reactor, adds 0.4 part of carbomer by the speed of 0.05 part/min and stir, after being warming up to 45 DEG C after insulated and stirred 1.5h, being warming up to 60 DEG C, insulated and stirred 15min, obtaining the first reactant liquor;
0.3 part of triclosan and 3 parts of tweens to be mixed in hermetic container and after stirring, add 70 parts of ethanol mix homogeneously, obtaining the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, is under the condition of-0.07Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, adding 0.4 part of triethanolamine, add 0.5 part of tween after stirring, is under the condition of-0.08Mpa in vacuum, stir after 30min, filter and obtain leave and to wash one's hands dew.
Embodiment 3
Pure water or mineral water are added in reactor, in reactor, adds 0.3 part of carbomer by the speed of 0.3 part/min and stir, after being warming up to 43 DEG C after insulated and stirred 1.2h, being warming up to 63 DEG C, insulated and stirred 18min, obtaining the first reactant liquor;
0.2 part of triclosan and 2 parts of tweens to be mixed in hermetic container and after stirring, add 50 parts of ethanol mix homogeneously, obtaining the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, is under the condition of-0.06Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, adding 0.3 part of triethanolamine, add 1 part of tween after stirring, is under the condition of-0.08Mpa in vacuum, stir after 30min, filter and obtain leave and to wash one's hands dew.
Embodiment 4
Pure water or mineral water are added in reactor, in reactor, adds 0.22 part of carbomer by the speed of 0.01 ~ 0.05 part/min and stir, after being warming up to 40 DEG C after insulated and stirred 1.5h, being warming up to 60 DEG C, insulated and stirred 16min, obtaining the first reactant liquor;
0.04 part of triclosan and 2 parts of tweens to be mixed in hermetic container and after stirring, add 60 parts of ethanol mix homogeneously, obtaining the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, is under the condition of-0.08Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, adding 0.22 part of triethanolamine, add 1.5 parts of tweens after stirring, is under the condition of-0.07Mpa in vacuum, stir after 30min, filter and obtain leave and to wash one's hands dew.
Embodiment 5
Pure water or mineral water are added in reactor, in reactor, adds 0.3 part of carbomer by the speed of 0.03 part/min and stir, after being warming up to 45 DEG C after insulated and stirred 1.3h, being warming up to 63 DEG C, insulated and stirred 15min, obtaining the first reactant liquor;
0.02 part of triclosan and 1 ~ 3 part of tween to be mixed in hermetic container and after stirring, add 65 parts of ethanol mix homogeneously, obtaining the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, is under the condition of-0.08Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, adding 0.3 part of triethanolamine, add 0.5 part of tween after stirring, is under the condition of-0.06Mpa in vacuum, stir after 40min, filter and obtain leave and to wash one's hands dew.
The present invention is not limited to above-mentioned embodiment, and for those skilled in the art, under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications are also considered as within protection scope of the present invention.The content be not described in detail in this description belongs to the known prior art of professional and technical personnel in the field.

Claims (8)

1. a leave is washed one's hands dew, it is characterized in that: by mass parts, and every 100 parts of leaves are washed one's hands in dew, are following composition:
2. a kind of leave as claimed in claim 1 is washed one's hands dew, it is characterized in that: by mass parts, and described every 100 parts of leaves are washed one's hands in dew, and the content of described triclosan is 0.01 ~ 0.04 part.
3. a kind of leave as claimed in claim 1 is washed one's hands dew, it is characterized in that: by mass parts, and described every 100 parts of leaves are washed one's hands in dew, and alcohol content is 50 ~ 65 parts.
4. a kind of leave as claimed in claim 3 is washed one's hands dew, it is characterized in that: by mass parts, and described every 100 parts of leaves are washed one's hands in dew, and alcohol content is 60 parts.
5. a kind of leave as claimed in claim 1 is washed one's hands dew, it is characterized in that: the mass ratio of described carbomer and triethanolamine is 1:1.
6. a kind of leave as claimed in claim 5 is washed one's hands dew, it is characterized in that: by mass parts, and described every 100 parts of leaves are washed one's hands in dew, and the mass parts of described carbomer and triethanolamine is 0.2 ~ 0.3 part.
7. a kind of leave as claimed in claim 6 is washed one's hands dew, it is characterized in that: by mass parts, and described every 100 parts of leaves are washed one's hands in dew, and the mass parts of described carbomer and triethanolamine is 0.22 part.
8. the leave according to any one of claim 1 to 7 wash one's hands dew a preparation method, it is characterized in that: comprise the following steps:
Pure water or mineral water are added in reactor, in reactor, add 0.1 ~ 0.4 part of carbomer by the speed of 0.01 ~ 0.05 part/min and stir, after being warming up to 40 ~ 45 DEG C after insulated and stirred 1 ~ 1.5h, being warming up to 60 ~ 65 DEG C, insulated and stirred 10 ~ 20min, obtains the first reactant liquor;
0.01 ~ 0.3 part of triclosan and 1 ~ 3 part of tween to be mixed in hermetic container and after stirring, add 40 ~ 70 parts of ethanol mix homogeneously, obtain the second reactant liquor, mix in the second reactant liquor suction reactor with the first reactant liquor, be under the condition of-0.06 ~-0.08Mpa in vacuum, be stirred to the first reactant liquor to mix homogeneously with the second reactant liquor, add 0.1 ~ 0.4 part of triethanolamine, 0.5 ~ 2 part of tween is added after stirring, be under the condition of-0.06 ~-0.08Mpa in vacuum, stir after 20 ~ 40min, filter and obtain leave and to wash one's hands dew.
CN201510678686.4A 2015-10-19 2015-10-19 No-clean hand lotion and preparation method thereof Pending CN105232355A (en)

Priority Applications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528561A (en) * 2018-12-06 2019-03-29 浙江大学自贡创新中心 A kind of disposable hand cleanser of mineral salt
CN111944617A (en) * 2020-08-19 2020-11-17 河南昇阳生物科技有限公司 Composite water-free hand sanitizer containing amino acid

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1480221A (en) * 2003-07-09 2004-03-10 中国医学科学院生物医学工程研究所 Washing free gel for disinfection
US20080139656A1 (en) * 2004-12-09 2008-06-12 The Dial Corporation Compositions Having a High Antiviral and Antibacterial Efficacy
CN104873432A (en) * 2015-05-28 2015-09-02 南阳市汇博生物技术有限公司 Hand-care disposable disinfection gel and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1480221A (en) * 2003-07-09 2004-03-10 中国医学科学院生物医学工程研究所 Washing free gel for disinfection
US20080139656A1 (en) * 2004-12-09 2008-06-12 The Dial Corporation Compositions Having a High Antiviral and Antibacterial Efficacy
CN104873432A (en) * 2015-05-28 2015-09-02 南阳市汇博生物技术有限公司 Hand-care disposable disinfection gel and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528561A (en) * 2018-12-06 2019-03-29 浙江大学自贡创新中心 A kind of disposable hand cleanser of mineral salt
CN111944617A (en) * 2020-08-19 2020-11-17 河南昇阳生物科技有限公司 Composite water-free hand sanitizer containing amino acid

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Application publication date: 20160113