CN105200777A - Crease-resistant non-ironing finishing technology of pure cotton fabric - Google Patents
Crease-resistant non-ironing finishing technology of pure cotton fabric Download PDFInfo
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- CN105200777A CN105200777A CN201510610972.7A CN201510610972A CN105200777A CN 105200777 A CN105200777 A CN 105200777A CN 201510610972 A CN201510610972 A CN 201510610972A CN 105200777 A CN105200777 A CN 105200777A
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Abstract
The invention discloses a crease-resistant non-ironing finishing technology of pure cotton fabric. The crease-resistant non-ironing finishing technology includes the following steps that crease-resistant finishing liquid is prepared, wherein the crease-resistant finishing liquid is prepared from 25-45 g of fibroin finishing liquid, 10-30 g of sulfonic acid type water-soluble polyurethane, 0.5-5 g of hydroxyethyl acrylate and the balance deionized water per liter of crease-resistant finishing liquid; dipping and rolling the pure cotton fabric in the crease-resistant finishing liquid twice; the dipped and rolled fabric is taken out for dehydration, and the take-up of the fabric is controlled to be 65%-70%; the dehydrated fabric is dried; the dehydrated fabric is washed three times and naturally aired. By means of the crease-resistant non-ironing finishing technology of pure cotton fabric, a good non-ironing finishing effect can be achieved, and the advantages of being good in hand feeling and comfortable to wear of the pure cotton fabric are kept; besides, the crease-resistant non-ironing finishing technology is safe, environmentally friendly and free of releasing formaldehyde.
Description
Technical field
The present invention relates to textile technology field, be specifically related to a kind of anti-crease and Iron-free technique of purified cotton cloth.
Background technology
Pure-cotton fabric take cotton as raw material, through the fabric that textile technology is produced, has the features such as moisture absorption, moisturizing, heat-resisting, alkaline-resisting, health.Pure-cotton fabric is comfortable and easy to wear, skin-friendly good, is subject to the extensive favor of people, especially in infant clothing, is regarded as safest fabric.But pure cotton fabric elasticity is poor, in dress and washing process, easily wrinkling and distortion, needs often to press or carry out wash and wear process.At present, the more wash and wear processing method of industrial application adopts resin finishing agent to arrange cloth, but production cost is higher, and easily discharge formaldehyde in dress and use procedure.Formaldehyde is a kind of poisonous chemicals, a kind of skin irritant and allergic agent, can severe irritation eyes, skin and mucous membrane, especially a kind of carcinogenic material.Therefore, a kind of crease-shedding finishing agent that is safe, nontoxic, environmental protection being applicable to pure cotton fabric is developed extremely urgent.
Summary of the invention
The invention provides a kind of anti-crease and Iron-free technique of purified cotton cloth, good Influencing Non-Ironing Finish can be obtained, and the advantage keeping the feel of pure cotton fabric good, comfortable and easy to wear; In addition, this anti-crease and Iron-free technique also safety and environmental protection, not Diazolidinyl Urea.
Technical scheme of the present invention is as follows:
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 25 ~ 45g, sulphur carboxylic acid type soluble polyurethane 10 ~ 30g, hydroxy-ethyl acrylate 0.5 ~ 5g in every 1L anti-crease finishing liquid, all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Cloth after dehydration is dried;
(4) cloth after dehydration is washed 3 times, naturally dry.
As the preferred technical solution of the present invention, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in every 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, all the other are deionized water.
The preparation method of the anti-crease finishing liquid related in technical scheme of the present invention and above-mentioned optimal technical scheme comprises the steps:
(1) silk is padded in the sodium carbonate liquor of 2g/L, carry out degumming process, then cold water washing post-drying;
(2) calcium chloride solution, deionized water and absolute ethyl alcohol are become mixed solution with the proportions of 1:7:2, process the Silk Soaking after coming unstuck in mixed solution by through step 1, at 70 DEG C, place 3h;
(3) substance transfer step 2 obtained, in NF membrane, through deionized water dialysis, removes Ca
2+, Cl
-ion, then through charcoal absorption, filtration, obtain fibroin liquid;
(4) fibroin liquid step 3 obtained mixes with sulphur carboxylic acid type soluble polyurethane, hydroxy-ethyl acrylate and deionized water, and ultrasonic agitation 90min obtains the anti-crease finishing liquid being applicable to pure cotton fabric.
The present invention has following technique effect:
The core process of anti-crease and Iron-free technique of the present invention is fibroin---the polyurethane compound anti-crease finishing liquid adopting safety and environmental protection.Wherein, fibroin liquid is widely used in the crease-resistant process of real silk fabric in recent years, and achieves good result.But in fibroin molecular structure lack can with the group of cotton fiber generation covalent cross-linking, if be therefore applied to separately poor effect in the crease-resistant process of pure cotton fabric; In order to address this problem, introduce sulphur carboxylic acid type soluble polyurethane in anti-crease finishing liquid of the present invention, there is deblocking reaction in this material, obtain the performed polymer that end group is-NCO under high temperature action, and cotton fiber is formed the film with cross-linked structure; On the other hand ,-NCO has very high reactivity, can react with the hydroxyl on cotton fiber, the amino groups on Fibroin Finishing Agent, improves the adhesion of finishing agent and cotton fiber.Hydroxy-ethyl acrylate is also added as crosslinking agent in anti-crease finishing liquid of the present invention, can at line style intermolecular bridging action, thus make the mutual bonding cross-linking of relevant group in cotton fiber, Fibroin Finishing Agent and polyurethane reticulate the material of structure, further enhance the crosslinked action between dressing liquid and cotton fiber.
Anti-crease and Iron-free technique in the present invention not only can improve pure cotton fabric dry/the crease-resistant recovery angle of hygrometric state, the soft feel of pure cotton fabric can also be kept; Anti-crease and Iron-free technique of the present invention effectively can also keep ultimate strength and the Tear strength retention rate of purified cotton cloth, ensures its useful life longevity.Adopt anti-crease finishing PROCESS FOR TREATMENT cotton of the present invention also to contribute to the rapid shaping of purified cotton cloth, high temperature pressing link (the non-ironing treatment process in published patent document CN102587136A and CN103103763A all needs this link) can be exempted.Anti-crease finishing technique of the present invention also has safety non-toxic environmental protection, the advantage of formaldehydeless release.
Detailed description of the invention
Below in conjunction with specific embodiments technical scheme of the present invention is clearly and completely described.
embodiment 1
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 25g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid comprises the steps:
(1) silk is padded in the sodium carbonate liquor of 2g/L, carry out degumming process, then cold water washing post-drying;
(2) calcium chloride solution, deionized water and absolute ethyl alcohol are become mixed solution with the proportions of 1:7:2, process the Silk Soaking after coming unstuck in mixed solution by through step 1, at 70 DEG C, place 3h;
(3) substance transfer step 2 obtained, in NF membrane, through deionized water dialysis, removes Ca
2+, Cl
-ion, then through charcoal absorption, filtration, obtain fibroin liquid;
(4) fibroin liquid step 3 obtained mixes with sulphur carboxylic acid type soluble polyurethane, hydroxy-ethyl acrylate and deionized water, and ultrasonic agitation 90min obtains the anti-crease finishing liquid being applicable to pure cotton fabric.
embodiment 2
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 30g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 3
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 4
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 40g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 5
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 45g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 6
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 10g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 7
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 15g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 8
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 25g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 9
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 30g, hydroxy-ethyl acrylate 2.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 10
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 0.5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 11
An anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) prepare anti-crease finishing liquid, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g in 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 20g, hydroxy-ethyl acrylate 5g, and all the other are deionized water;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Dry the cloth after dehydration, bake out temperature is 80 DEG C, and the time is 5min;
(4) cloth after dehydration is washed 3 times, naturally dry.
Wherein, the preparation method of anti-crease finishing liquid is with embodiment 1.
embodiment 12
To the purified cotton cloth through noniron finish in embodiment 1-11 do/measurement of hygrometric state creasy recovery angle to be to weigh its ironing-free performance and wrinkle resistance.It should be noted that easy-care properties and wrinkle resistance are slightly different.The diastrophic ability that fabric opposing kneading action power causes is called wrinkle resistance; And easy-care properties requires that fabric not only has wrinkle resistance in wearing process exactly, and do not need flatiron after washing, fabric still keeps formation state or goffering, dimensionally stable.Namely finish fabric all has excellent wrinkle resistance under dry and wet state.Dry/hygrometric state creasy recovery angle is commonly used to weigh wrinkle resistance; Flatness (DP level) after fabric washing is then used for weighing easy-care properties, but hygrometric state creasy recovery angle has necessarily contact with washing flatness, and in general, wet crease recovery angle is large, and non-ironing progression is also high.Therefore, hygrometric state creasy recovery angle also can be used for weighing the ironing-free performance of fabric.With reference to GB GB/T3819-1997 when dry/hygrometric state creasy recovery angle measures, horizontal folding fabric method AATCC crease recovery of fabrics tester is adopted to test.Dry state creasy recovery angle carries out under the condition of relative humidity (65 ± 1) %, and hygrometric state creasy recovery angle carries out under the condition of relative humidity (90 ± 1) %.
To the test carrying out breaking strength retention in embodiment 1-11 through the purified cotton cloth of noniron finish, test, with reference to GB GB/T3923.1-2013, is surveyed pure cotton fabric 5 through 5 latitudes, is averaged respectively; Fabric tear strength test is carried out to the pure cotton fabric before and after process, with reference to GB GB/T3917.1-2009, surveys pure cotton fabric 5 through 5 latitudes, average respectively.Above index is used for weighing the durability of purified cotton cloth.
In order to fully assess anti-crease and Iron-free technique of the present invention, also be provided with the purified cotton cloth without non-ironing process and the purified cotton cloth through the non-ironing process of resin finishing agent as a comparison case, do the performance test of/hygrometric state creasy recovery angle, breaking strength retention and Tear strength retention rate accordingly.
Above-mentioned test result is as shown in the table.
The performance test results of table 1 pure cotton fabric after anti-crease finishing
As can be seen from table, anti-crease finishing liquid of the present invention has good anti-wrinkle effect---and compare undressed pure cotton fabric, its dry/hygrometric state creasy recovery angle of pure cotton fabric through anti-crease finishing liquid process of the present invention all has obvious rising.Through the pure cotton fabric of anti-crease finishing liquid process of the present invention, there is the crease resistant finishing similar with resin finishing agent, but breaking strength retention and Tear strength retention rate are all obviously better than the pure cotton fabric after resin finishing agent arrangement, and maintain the soft feel of pure cotton fabric itself.
Above embodiment is only the present invention's part embodiment, instead of whole embodiments.The explanation of above embodiment just understands method of the present invention and core concept thereof for helping; For one of ordinary skill in the art, according to thought of the present invention not making other embodiments all obtained under creative work prerequisite, all belong to the scope of protection of the invention.
Claims (3)
1. an anti-crease and Iron-free technique for purified cotton cloth, comprises the steps:
(1) anti-crease finishing liquid is prepared;
(2) purified cotton cloth two leachings two in anti-crease finishing liquid are rolled;
(3) take out the cloth after padding to dewater, control cloth pick-up at 65%-70%; Cloth after dehydration is dried;
(4) cloth after dehydration is washed 3 times, naturally dry;
It is characterized in that, described anti-crease finishing liquid is following composition: comprise fibroin liquid 25 ~ 45g in every 1L anti-crease finishing liquid, sulphur carboxylic acid type soluble polyurethane 10 ~ 30g, hydroxy-ethyl acrylate 0.5 ~ 5g, all the other are deionized water.
2. the anti-crease and Iron-free technique of purified cotton cloth according to claim 1, it is characterized in that, described anti-crease finishing liquid is following composition: comprise fibroin liquid 35g, sulphur carboxylic acid type soluble polyurethane 20g in every 1L anti-crease finishing liquid, hydroxy-ethyl acrylate 2.5g, all the other are deionized water.
3. the anti-crease and Iron-free technique of purified cotton cloth according to claim 1, is characterized in that, the preparation method of described anti-crease finishing liquid comprises the steps:
(1) silk is padded in the sodium carbonate liquor of 2g/L, carry out degumming process, then cold water washing post-drying;
(2) calcium chloride solution, deionized water and absolute ethyl alcohol are become mixed solution with the proportions of 1:7:2, process the Silk Soaking after coming unstuck in mixed solution by through step 1, at 70 DEG C, place 3h;
(3) substance transfer step 2 obtained, in NF membrane, through deionized water dialysis, removes Ca
2+, Cl
-ion, then through charcoal absorption, filtration, obtain fibroin liquid;
(4) fibroin liquid step 3 obtained mixes with sulphur carboxylic acid type soluble polyurethane, hydroxy-ethyl acrylate and deionized water, and ultrasonic agitation 90min obtains the anti-crease finishing liquid being applicable to pure cotton fabric.
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CN105544209A (en) * | 2016-01-21 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Textile after-finishing process taking silk fibroin as medium |
CN105714556A (en) * | 2016-03-14 | 2016-06-29 | 湖州新创丝织品有限公司 | Treatment method for improving anti-winkle performance of cotton fabrics |
CN107034669A (en) * | 2017-04-24 | 2017-08-11 | 五邑大学 | A kind of method that anti-crease finishing is carried out to bafta |
CN107447507A (en) * | 2017-09-29 | 2017-12-08 | 界首市恒吉服饰有限责任公司 | A kind of method for lifting bafta anti-crease property energy |
CN107558166A (en) * | 2016-07-01 | 2018-01-09 | 姜维 | Water-soluble crease-resistant no-iron finishing agent |
CN108532087A (en) * | 2018-03-14 | 2018-09-14 | 广东溢达纺织有限公司 | Tatting wash-and-wear fabrics and preparation method thereof |
CN110158318A (en) * | 2019-05-31 | 2019-08-23 | 云南浩祥服饰有限公司 | A kind of dress ornament antibacterial crease-resistant type finishing agent and its method for sorting |
CN111793981A (en) * | 2020-07-10 | 2020-10-20 | 温州厚德服饰有限公司 | Moisture permeable cotton-padded clothes |
CN113186721A (en) * | 2021-05-10 | 2021-07-30 | 温州东廷服饰有限公司 | Finishing process of non-ironing trousers |
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Cited By (11)
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CN105544209A (en) * | 2016-01-21 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Textile after-finishing process taking silk fibroin as medium |
CN105714556A (en) * | 2016-03-14 | 2016-06-29 | 湖州新创丝织品有限公司 | Treatment method for improving anti-winkle performance of cotton fabrics |
CN107558166A (en) * | 2016-07-01 | 2018-01-09 | 姜维 | Water-soluble crease-resistant no-iron finishing agent |
CN107034669A (en) * | 2017-04-24 | 2017-08-11 | 五邑大学 | A kind of method that anti-crease finishing is carried out to bafta |
CN107034669B (en) * | 2017-04-24 | 2021-10-08 | 五邑大学 | Method for crease-resistant finishing of cotton fabric |
CN107447507A (en) * | 2017-09-29 | 2017-12-08 | 界首市恒吉服饰有限责任公司 | A kind of method for lifting bafta anti-crease property energy |
CN108532087A (en) * | 2018-03-14 | 2018-09-14 | 广东溢达纺织有限公司 | Tatting wash-and-wear fabrics and preparation method thereof |
CN110158318A (en) * | 2019-05-31 | 2019-08-23 | 云南浩祥服饰有限公司 | A kind of dress ornament antibacterial crease-resistant type finishing agent and its method for sorting |
CN111793981A (en) * | 2020-07-10 | 2020-10-20 | 温州厚德服饰有限公司 | Moisture permeable cotton-padded clothes |
CN113186721A (en) * | 2021-05-10 | 2021-07-30 | 温州东廷服饰有限公司 | Finishing process of non-ironing trousers |
CN113186721B (en) * | 2021-05-10 | 2023-08-01 | 浙江东廷服饰有限公司 | Finishing process of non-ironing trousers |
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