CN105199937B - A kind of sophora bud vinegar, sophora bud health care oral liquid and preparation method thereof - Google Patents
A kind of sophora bud vinegar, sophora bud health care oral liquid and preparation method thereof Download PDFInfo
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- CN105199937B CN105199937B CN201510602530.8A CN201510602530A CN105199937B CN 105199937 B CN105199937 B CN 105199937B CN 201510602530 A CN201510602530 A CN 201510602530A CN 105199937 B CN105199937 B CN 105199937B
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Abstract
The invention discloses a kind of sophora bud vinegar, sophora bud health care oral liquid and preparation method thereof.Sophora bud vinegar is prepared by method comprising the following steps：1) sophora bud powder is mixed with water, hot water extraction, filters, obtain sophora bud residue and sophora bud water extract；2) sophora bud residue is mixed with edible alcohol, ultrasound extraction, filtering, obtains sophora bud alcoholic extract；3) sophora bud water extract and sophora bud alcoholic extract are mixed, obtains Huai Goat；4) in gained Huai Goat, it is inoculated with Pasteur's acetobacter, it is 3.6~4.0% to ferment to total acidity, to obtain the final product.Sophora bud vinegar provided by the invention, nutrition and functional component in the sophora bud are fully extracted by different solvents, sophora bud vinegar then is made using microbial fermentation；Fermentation process makes rutin sophorin preferably be converted into the stronger Quercetin of bioactivity；Content, solubility and the stability of the major function factor in sophora bud vinegar such as Quercetin greatly improve at the same time, sophora bud vinegar is had the function of good nutrition and health care.
Description
Technical field
The invention belongs to Huai Goat technical field, and in particular to a kind of sophora bud vinegar, sophora bud health care oral liquid and its system
Preparation Method.
Background technology
The sophora bud is the bud of legume Chinese scholartree, is a kind of plant resources of dietotherapeutic.Sophora bud rich in nutrition content, especially
It is that amino acid classes are complete, protein content is higher, also containing the trace element such as abundant calcium, iron, potassium, zinc, copper, magnesium and dimension
Raw element.The sophora bud is also traditional Chinese medicine material, its bitter, be slightly cold, and has cool blood, hemostasis, clearing liver, improving eyesight, blood pressure lowering, drop blood
Fat, increase coronary blood flow, improve microcirculation and other effects.
In recent years, research both at home and abroad finds that it contains the bioactive ingredients such as abundant flavones, phenolic acid, polysaccharide, saponin, especially
It is that rutin sophorin content is up to more than 30% in some kinds.Huai Goat rutin sophorin (the active ingredient such as rutin), Quercetins
It is referred to as " sophora bud essence ", has been applied in daily cosmetic industry as sun-rays proof beauty-care additive.CN103044505A discloses one
Extract the novel process for pretreating of rutin kind from the sophora bud, including boiling, dry, crush, hot water is scalded, washes mother liquor,
Effective extraction has been carried out to rutin.
CN102807596A discloses a kind of extracting method of rutin, including the sophora bud handles, uses methanol heating extraction, mistake
Filter, be concentrated under reduced pressure, crystallizing, reducing the sewage disposal difficulty of traditional heavy extraction process of alkali carries acid, Extraction of rutin rate and
Purity all improves.
In the prior art, Huai Goat has paid close attention to the functional components such as rutin sophorin, Quercetin more, in these functional components
In extraction and separation, on the one hand, a large amount of waste liquids can be brought, the processing to environment and waste liquid causes pressure；On the other hand, in the sophora bud
Remaining functional components do not obtain abundant profit in the nutritional ingredients such as abundant water soluble protein, amino acid and residue
With causing the wasting of resources.
The content of the invention
The object of the present invention is to provide a kind of sophora bud vinegar, so as to solve in the prior art, Huai Goat cannot be to the sophora bud
Nutritional ingredient comprehensively utilized, the reluctant problem of production waste liquid in extraction process.
Second object of the present invention is to provide a kind of sophora bud health care oral liquid using above-mentioned sophora bud vinegar.
Third object of the present invention is to provide the preparation method of above-mentioned sophora bud health care oral liquid.
In order to realize the above object the technical solution adopted in the present invention is：
A kind of sophora bud vinegar, is prepared by method comprising the following steps：
1) sophora bud powder is mixed with water, is extracted at 60~80 DEG C, filtered, obtain sophora bud residue and sophora bud water extract；
2) sophora bud residue obtained by step 1) is mixed with alcohol, the ultrasound extraction at 40~60 DEG C, filtering, obtains sophora bud wine
Essence extract；
3) sophora bud alcoholic extract obtained by sophora bud water extract obtained by step 1) and step 2) is mixed, obtaining alcoholic strength is
5.2%~6.2% Huai Goat；
4) in Huai Goat obtained by step 3), Pasteur's acetobacter is inoculated with, it is 3.6%~4.0% to ferment to total acidity,
To obtain the final product.
Sophora bud vinegar provided by the invention, step 1) obtain water miscible protein, amino acid, carbon with the hot water extraction sophora bud
The nutritional ingredients such as hydrate, vitamin and mineral, can make full use of the nutriment in the sophora bud, reduce waste, may be used also
Nutrition is provided for the fermentation process of step 4), while makes the content of the nutriments such as the amino acid of final products, mineral matter significantly
Improve；Due in the sophora bud flavone component such as rutin sophorin, Quercetin it is water-soluble relatively poor, step 2) is further extracted with alcohol
Residue, can fully extract sophora bud active ingredient, increase the dissolution of alcohol-soluble functional component；Step 3) is sophora bud water extract and Chinese scholartree
The mixed process of rice wine essence extract, by controlling alcoholic strength to adjust the ratio of water extract and alcohol extract, make nutrition into
Point eurythmy, stability increase, be ready for the fermentation process of step 4)；Step 4) utilizes Modern microbiological fermentation skill
Art is conducive to sophora bud main composition rutin sophorin and is converted into Quercetin；The fermentation of Pasteur's acetobacter produces acetic acid, reduces zymotic fluid
PH value, the sour water solution for being also beneficial to rutin sophorin is converted into Quercetin, its bioactivity and healthcare function relative to rutin sophorin more
It is good, there is the surcharge of higher；Simultaneously because dissolubility and stability of the Quercetin in acetum further enhance, most
Eventually greatly improve the content of Quercetin and stability in sophora bud vinegar, make the nutrition and health care function of sophora bud vinegar more prominent.
Sophora bud vinegar provided by the invention, realizes the comprehensive utilization to the various nutritional ingredients of the sophora bud, and whole process is without useless
Liquid produces, and the residue after final alcoholic extraction can also be used as feed conversion, alleviate environment and liquid waste processing pressure, realizes
Green production.
In step 1), the mass ratio of sophora bud powder and water is 8~10:1.In step 2), the alcohol is volumetric concentration 72%
Edible alcohol, the mass volume ratio of sophora bud residue and alcohol is 6~8:1.
In step 1), the sophora bud powder is after the sophora bud is cleaned, and dries to doing, crushed 20~60 mesh sieves and be made.Step
1) it is described to be filtered into heat filtering.
In step 3), the volume ratio of the sophora bud water extract and sophora bud alcoholic extract is 8~10:1.
The time of the step 1) extraction is 40~60min；The time of the step 2) extraction is 20~30min.
The ferment control total acidity of Pasteur's acetobacter.Preferably, the step 4) fermentation is temp.-differential aerobic fementation,
Fermentation time is 3 days；Wherein, the 1st day 31 DEG C of fermentation temperature, throughput 120L/h；2nd day 33 DEG C of fermentation temperature, throughput
150L/h；3rd day 30 DEG C of fermentation temperature, throughput 100L/h.
Preferably, Pasteur's acetobacter liquid of Huai Goat volume 20% is inoculated with, the viable count of bacterium solution is 1.5 × 108~
3.5×108cfu/mL。
A kind of sophora bud health care oral liquid using above-mentioned sophora bud vinegar, is made of the component of following mass parts：Sophora bud vinegar 25~
30 parts, 70~75 parts of water, 2~3 parts of fructose, 3~4 parts of honey, 0.08~0.12 part of ascorbic acid, sodium citrate 0.01~0.02
Part, 0.001~0.002 part of 0.001~0.002 part of calcium gluconate and potassium chloride.
Sophora bud health care oral liquid provided by the invention, using sophora bud vinegar as main nutrient composition, with fructose, honey, Vitamin C
Acid, sodium citrate, the mixture of calcium gluconate and potassium chloride are reasonably combined, make the oral liquid sweet and sour taste, it is full of nutrition, protect
Health-care function is obvious, safe, without side-effects, and especially suitable middle-aged and elderly people takes.Long-term use can play enhancing body hair
Thin vascular resistance, reduce the effects such as capillary fragility, coronary artery dilator, increase coronary blood flow, improvement microcirculation, also
Taken for hypertension, hyperlipidemia, coronary heart disease, chronic bronchitis patient, play auxiliary therapeutic action.
The preparation method of above-mentioned sophora bud health care oral liquid, including：Sophora bud vinegar is uniformly mixed with water, adds fructose, bee
Honey, ascorbic acid, sodium citrate, the mixture of calcium gluconate and potassium chloride, are uniformly mixed, through ultrafiltration, sterilization, to obtain the final product.
The preparation method of above-mentioned sophora bud health care oral liquid provided by the invention, with short production cycle, disposable used device is few,
It is strong to produce controllability, easy to operate and control, product quality is stablized, suitable for promoting and applying.
Embodiment
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
The sophora bud vinegar of the present embodiment, is prepared by method comprising the following steps：
1) the fresh sophora bud of the 7-8 months just spewing tongue is picked, is cleaned with clear water, dries to doing, crushed 40 mesh sieves；It will be made
Sophora bud powder add 8 times of quality water, in 80 DEG C soak 40min, filter while hot, obtain sophora bud water extract and sophora bud residue, it is cold
It is spare；
2) by sophora bud residue obtained by step 1), the matter of the edible alcohol of concentration 72%, sophora bud residue and edible alcohol is added
It is 1 to measure volume ratio：8, ultrasound extraction 30min, filtering at 40 DEG C, obtain sophora bud alcoholic extract, cooling is spare；
3) sophora bud alcoholic extract obtained by sophora bud water extract obtained by step 1) and step 2) is pressed 8：1 volume ratio mixing,
Obtain the Huai Goat that alcoholic strength is 6.2%；
4) in the Huai Goat obtained by step 3), it is inoculated with Pasteur's vinegar bar of 20% activation of the volume of Huai Goat
Bacterium solution, the viable count of bacterium solution is 1.5 × 108Cfu/mL, temp.-differential aerobic fementation 3 days；1st day 31 DEG C of fermentation temperature, throughput
120L/h；2nd day 33 DEG C of fermentation temperature, throughput 150L/h；3rd day 30 DEG C of fermentation temperature, throughput 100L/h；Treat total acidity
When reaching 4.0%, to obtain the final product.
The sophora bud health care oral liquid of the present embodiment, is made of the component of following mass parts：28 parts of sophora bud vinegar, 72 parts of water, fruit
0.001 part of 2 parts of sugar, 4 parts of honey, 0.08 part of ascorbic acid, 0.02 part of sodium citrate, 0.002 part of calcium gluconate and potassium chloride.
The preparation method of the sophora bud health care oral liquid of the present embodiment, including sophora bud vinegar is uniformly mixed with water, addition fructose,
Honey, ascorbic acid, sodium citrate, the mixture of calcium gluconate and potassium chloride, are uniformly mixed, through ultra filtering clarifying, Ran Hou
After 130 DEG C of high-temperature instantaneous sterilizations, up to sophora bud vinegar health care oral liquid；Again through sterile filling, sealing, inspection, labeling, vanning, i.e.,
It can be put in storage.
Embodiment 2
The sophora bud vinegar of the present embodiment, is prepared by method comprising the following steps：
1) the fresh sophora bud of the 7-8 months just spewing tongue is picked, is cleaned with clear water, dries to doing, crushed 20 mesh sieves；It will be made
Sophora bud powder add 9 times of quality water, in 70 DEG C soak 50min, filter while hot, obtain sophora bud water extract and sophora bud residue, it is cold
It is spare；
2) by sophora bud residue obtained by step 1), the matter of the edible alcohol of concentration 72%, sophora bud residue and edible alcohol is added
It is 1 to measure volume ratio：7, ultrasound extraction 25min, filtering at 50 DEG C, obtain sophora bud alcoholic extract, cooling is spare；
3) sophora bud alcoholic extract obtained by sophora bud water extract obtained by step 1) and step 2) is pressed 9：1 volume ratio mixing,
Obtain the Huai Goat that alcoholic strength is 5.7%；
4) in the Huai Goat obtained by step 3), it is inoculated with Pasteur's vinegar bar of 20% activation of the volume of Huai Goat
Bacterium solution, the viable count of bacterium solution is 3.5 × 108Cfu/mL, temp.-differential aerobic fementation 3 days；1st day 31 DEG C of fermentation temperature, throughput
120L/h；2nd day 33 DEG C of fermentation temperature, throughput 150L/h；3rd day 30 DEG C of fermentation temperature, throughput 100L/h；Treat total acidity
When reaching 3.8%, to obtain the final product.
The sophora bud health care oral liquid of the present embodiment, is made of the component of following mass parts：25 parts of sophora bud vinegar, 75 parts of water, fruit
2.5 parts of sugar, 3.5 parts of honey, 0.1 part of ascorbic acid, 0.01 part of sodium citrate, 0.001 part of calcium gluconate and potassium chloride 0.002
Part.
The preparation method of the sophora bud health care oral liquid of the present embodiment, it is same as Example 1.
Embodiment 3
The sophora bud vinegar of the present embodiment, is prepared by method comprising the following steps：
1) the fresh sophora bud of the 7-8 months just spewing tongue is picked, is cleaned with clear water, dries to doing, crushed 60 mesh sieves；It will be made
Sophora bud powder add 10 times of quality water, in 60 DEG C soak 60min, filter while hot, obtain sophora bud water extract and sophora bud residue, it is cold
It is spare；
2) by sophora bud residue obtained by step 1), the matter of the edible alcohol of concentration 72%, sophora bud residue and edible alcohol is added
It is 1 to measure volume ratio：6, ultrasound extraction 20min, filtering at 60 DEG C, obtain sophora bud alcoholic extract, cooling is spare；
3) sophora bud alcoholic extract obtained by sophora bud water extract obtained by step 1) and step 2) is pressed 10：1 volume ratio mixing,
Obtain the Huai Goat that alcoholic strength is 5.2%；
4) in the Huai Goat obtained by step 3), it is inoculated with Pasteur's vinegar bar of 20% activation of the volume of Huai Goat
Bacterium solution, the viable count of bacterium solution is 2.5 × 108Cfu/mL, temp.-differential aerobic fementation 3 days；1st day 31 DEG C of fermentation temperature, throughput
120L/h；2nd day 33 DEG C of fermentation temperature, throughput 150L/h；3rd day 30 DEG C of fermentation temperature, throughput 100L/h；Treat total acidity
When reaching 3.6%, to obtain the final product.
The sophora bud health care oral liquid of the present embodiment, is made of the component of following mass parts：30 parts of sophora bud vinegar, 70 parts of water, fruit
0.001 part of 3 parts of sugar, 3 parts of honey, 0.12 part of ascorbic acid, 0.01 part of sodium citrate, 0.002 part of calcium gluconate and potassium chloride.
The preparation method of the sophora bud health care oral liquid of the present embodiment, it is same as Example 1.
Test example
Huai Goat obtained by step 3) and step 4) gained Chinese scholartree in embodiment 1~3 are detected using high performance liquid chromatography
The content of Quercetin, rutin sophorin, testing result are as shown in table 1 in rice vinegar.
Functional component testing result in Huai Goat and sophora bud vinegar in 1 each embodiment of table
Huai Goat is to work(such as the Quercetin in the sophora bud, rutin sophorin elements obtained by the results showed that step 3) of table 1
Energy component has carried out comprehensive extraction, and the Huai Goat rutin sophorin content by hybrid modulation is up to 2.51g/L, and Quercetin is
0.13g/L, and after fermentation process by step 4) and sour water solution, it is stronger that rutin sophorin is largely converted into feature
Quercetin, the content of Quercetin can reach 1.22g/L in sophora bud vinegar, the nutrition and health care function of sophora bud vinegar is obtained into one
Step improves.
Claims (5)
1. a kind of sophora bud vinegar, it is characterised in that be prepared by method comprising the following steps：
1）Sophora bud powder is mixed with water, is extracted at 60~80 DEG C, filters, obtains sophora bud residue and sophora bud water extract；
2）By step 1）Gained sophora bud residue is mixed with alcohol, and the ultrasound extraction at 40~60 DEG C, filtering, obtains sophora bud alcohol and carry
Take thing；
3）By step 1）Gained sophora bud water extract and step 2）Gained sophora bud alcoholic extract mixes, obtain alcoholic strength for 5.2%~
6.2% Huai Goat；
4）In step 3）In gained Huai Goat, it is inoculated with Pasteur's acetobacter, it is 3.6%~4.0% to ferment to total acidity, to obtain the final product；
Step 1）In, the mass ratio of sophora bud powder and water is 8~10:1；Step 2）In, the alcohol is the food that volumetric concentration is 72%
With alcohol, the mass volume ratio of sophora bud residue and alcohol is 6~8:1；Step 3）In, the sophora bud water extract is carried with sophora bud alcohol
The volume ratio for taking thing is 8~10:1.
2. sophora bud vinegar as claimed in claim 1, it is characterised in that step 1）The time of the extraction is 40~60min；Step
2）The time of the extraction is 20~30min.
3. sophora bud vinegar as claimed in claim 1, it is characterised in that step 4）The fermentation is temp.-differential aerobic fementation, fermentation
Time is 3 days；Wherein, the 1st day 31 DEG C of fermentation temperature, throughput 120L/h；2nd day 33 DEG C of fermentation temperature, throughput 150L/h；
3rd day 30 DEG C of fermentation temperature, throughput 100L/h.
4. a kind of usage right requires the sophora bud health care oral liquid of 1 sophora bud vinegar, it is characterised in that by the group of following mass parts
It is grouped into：25~30 parts of sophora bud vinegar, 70~75 parts of water, 2~3 parts of fructose, 3~4 parts of honey, 0.08~0.12 part of ascorbic acid,
0.001~0.002 part of 0.01~0.02 part of sodium citrate, 0.001~0.002 part of calcium gluconate and potassium chloride.
A kind of 5. preparation method of sophora bud health care oral liquid as claimed in claim 4, it is characterised in that including：By sophora bud vinegar
It is uniformly mixed with water, adds fructose, honey, ascorbic acid, sodium citrate, calcium gluconate and potassium chloride, be uniformly mixed, through super
Filter, sterilization, to obtain the final product.
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695269A (en) * | 2016-03-25 | 2016-06-22 | 安徽瑞思威尔科技有限公司 | Sophora flower bud wine and preparation method |
| CN105918753A (en) * | 2016-05-05 | 2016-09-07 | 华若延 | Preparation method of solid granular drink |
| CN107874109A (en) * | 2016-09-29 | 2018-04-06 | 桂林洁宇环保科技有限责任公司 | A kind of preparation method of sophora bud health care oatmeal |
| CN106811391A (en) * | 2017-03-27 | 2017-06-09 | 广东石油化工学院 | A kind of preparation method of hawthorn hill gooseberry compound fruit vinegar |
| CN107334052A (en) * | 2017-05-31 | 2017-11-10 | 黄秋丽 | A kind of sophora flower steamed bun and preparation method thereof |
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