CN105199937A - Sophora flower bud vinegar, sophora flower bud health-care oral liquid and preparation method of sophora flower bud health-care oral liquid - Google Patents
Sophora flower bud vinegar, sophora flower bud health-care oral liquid and preparation method of sophora flower bud health-care oral liquid Download PDFInfo
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Abstract
The invention discloses sophora flower bud vinegar, sophora flower bud health-care oral liquid and a preparation method of the sophora flower bud health-care oral liquid. The sophora flower bud vinegar is prepared through a method including the following steps that 1, sophora flower bud flour is mixed with water, hot water extraction and filtration are conducted, and sophora flower bud residues and sophora flower bud aqueous extract are obtained; 2, the sophora flower bud residues are mixed with edible alcohol, ultrasonic extraction and filtration are conducted, and sophora flower bud alcohol extract is obtained; 3, the sophora flower bud aqueous extract and the sophora flower bud alcohol extract are mixed, so that sophora flower bud extract is obtained; 4, acetobacter pasteurianus is inoculated into the obtained sophora flower bud extract, fermentation is carried out till the total acidity is 3.6%-4.0%, and accordingly the sophora flower bud vinegar is obtained. According to the sophora flower bud vinegar, nutritional and functional ingredients in sophora flower buds are fully extracted through different solvents, and then microbial fermentation is adopted, so that the sophora flower buds are made into the sophora flower bud vinegar; rutin is used in the fermentation process, and can be better converted into quercetin with higher biological activity; meanwhile, the content, solubility and stability of main functional factors such as the quercetin in the sophora flower bud vinegar are greatly improved, and therefore the sophora flower bud vinegar has good nutritional and health-care functions.
Description
Technical field
The invention belongs to Huai Goat technical field, be specifically related to a kind of sophora bud vinegar, sophora bud health care oral liquid and preparation method thereof.
Background technology
The sophora bud is the bud of leguminous plants Chinese scholartree, is a kind of plant resources of dietotherapeutic.Sophora bud rich in nutrition content, especially amino acid classes are complete, protein content is higher, also containing trace element such as abundant calcium, iron, potassium, zinc, copper, magnesium etc. and VITAMIN.The sophora bud is also traditional Chinese medicine material, its bitter, is slightly cold, and has cool blood, hemostasis, clearing liver, improving eyesight, hypotensive, reducing blood-fat, increase coronary artery blood flow, improves the effects such as microcirculation.
In recent years, research both at home and abroad finds that it contains bioactive ingredients such as enriching flavones, phenolic acid, polysaccharide, saponin, especially violaguercitrin content in some kind up to more than 30%.(effective constituent such as rutin), Quercetin is called as Huai Goat violaguercitrin " sophora bud essence ", has been applied in daily cosmetic industry as sun-rays proof beauty-care additive.CN103044505A discloses a kind of novel process for pretreating extracting rutin from the sophora bud, comprises boiling, dries, pulverizes, hot water is scalded, wash the steps such as mother liquor, carried out effective extraction to rutin.
CN102807596A discloses the extracting method of a kind of rutin, comprise sophora bud process, use the steps such as methyl alcohol heating extraction, filtration, concentrating under reduced pressure, crystallization, decrease the sewage disposal difficulty that traditional alkali puies forward the heavy extraction process of acid, Extraction of rutin rate and purity all improve.
In prior art, Huai Goat has paid close attention to the functional component such as violaguercitrin, Quercetin more, in the Extraction and separation of these functional components, on the one hand, can bring a large amount of waste liquid, to the process build-up of pressure of environment and waste liquid; On the other hand, in the nutritive ingredient such as water soluble protein, amino acid abundant in the sophora bud and residue, remaining functional ingredient is not fully used, and causes the wasting of resources.
Summary of the invention
The object of this invention is to provide a kind of sophora bud vinegar, thus solve in prior art, Huai Goat can not fully utilize the nutritive ingredient of the sophora bud, the reluctant problem of production waste liquid in leaching process.
Second object of the present invention is to provide a kind of sophora bud health care oral liquid using above-mentioned sophora bud vinegar.
3rd object of the present invention is to provide the preparation method of above-mentioned sophora bud health care oral liquid.
In order to realize above object, the technical solution adopted in the present invention is:
A kind of sophora bud vinegar, is prepared by the method comprised the following steps:
1) sophora bud powder is mixed with water, lixiviate at 60 ~ 80 DEG C, filter, obtain sophora bud residue and sophora bud aqueous extract;
2) by step 1) gained sophora bud residue mixes with alcohol, ultrasonic lixiviate at 40 ~ 60 DEG C, and filter, obtain sophora bud ethanol extract;
3) by step 1) gained sophora bud aqueous extract and step 2) mixing of gained sophora bud ethanol extract, obtain the Huai Goat that alcoholic strength is 5.2% ~ 6.2%;
4) in step 3) in gained Huai Goat, inoculation Acetobacter pasteurianus, fermenting to total acidity is 3.6% ~ 4.0%, to obtain final product.
Sophora bud vinegar provided by the invention, step 1) with hot water extraction's sophora bud, obtain the nutritive ingredients such as water miscible protein, amino acid, carbohydrate, VITAMIN and mineral substance, the nutritive substance in the sophora bud can be made full use of, cut the waste, also can be step 4) fermenting process nutrition is provided, make the content of the nutritive substances such as the amino acid of the finished product, mineral substance greatly improve simultaneously; Water-soluble relatively poor due to the flavone component such as violaguercitrin, Quercetin in the sophora bud, step 2) with the further leaching residue of alcohol, can fully extract sophora bud activeconstituents, increase the stripping of alcohol dissolubility functional component; Step 3) be the mixing process of sophora bud aqueous extract and sophora bud ethanol extract, can regulate the ratio of aqueous extract and alcohol extract by controlling alcoholic strength, the eurythmy of nutritive ingredient, stability are increased, and are step 4) fermenting process ready; Step 4) utilize Modern microbiological fermentation technique to be conducive to sophora bud main composition violaguercitrin to be converted into Quercetin; Acetobacter pasteurianus fermentation produces acetic acid, and reduce the pH value of fermented liquid, the acid hydrolysis being also conducive to violaguercitrin is converted into Quercetin, its biological activity and nourishing function better relative to violaguercitrin, there is higher value added; Simultaneously because the solvability of Quercetin in acetum and stability strengthen further, finally make the content of Quercetin in sophora bud vinegar and stability greatly improve, make the nutrition and health care function of sophora bud vinegar more outstanding.
Sophora bud vinegar provided by the invention, achieves the comprehensive utilization to the various nutritive ingredient of the sophora bud, and whole process produces without waste liquid, and the residue after final alcoholic extraction also as feed utilisation, can alleviate environment and liquid waste disposal pressure, achieve green production.
Step 1) in, the mass ratio of sophora bud powder and water is 8 ~ 10:1.Step 2) in, described alcohol is the edible ethanol of volumetric concentration 72%, and the mass volume ratio of sophora bud residue and alcohol is 6 ~ 8:1.
Step 1) in, described sophora bud powder is after being cleaned by the sophora bud, and airing, to dry, pulverized 20 ~ 60 mesh sieves and obtained.Step 1) described in be filtered into heat filtering.
Step 3) in, the volume ratio of described sophora bud aqueous extract and sophora bud ethanol extract is 8 ~ 10:1.
Step 1) time of described lixiviate is 40 ~ 60min; Step 2) time of described lixiviate is 20 ~ 30min.
The ferment control total acidity of Acetobacter pasteurianus.Preferably, step 4) described fermentation is temp .-differential aerobic fermentation, fermentation time is 3 days; Wherein, the 1st day leavening temperature 31 DEG C, air flow 120L/h; 2nd day leavening temperature 33 DEG C, air flow 150L/h; 3rd day leavening temperature 30 DEG C, air flow 100L/h.
Preferably, the Acetobacter pasteurianus liquid of inoculation Huai Goat volume 20%, the viable count of bacterium liquid is 1.5 × 10
8~ 3.5 × 10
8cfu/mL.
A kind of sophora bud health care oral liquid using above-mentioned sophora bud vinegar, be made up of the component of following mass parts: sophora bud vinegar 25 ~ 30 parts, 70 ~ 75 parts, water, 2 ~ 3 parts, fructose, honey 3 ~ 4 parts, 0.08 ~ 0.12 part, xitix, Trisodium Citrate 0.01 ~ 0.02 part, calglucon 0.001 ~ 0.002 part and 0.001 ~ 0.002 part, Repone K.
Sophora bud health care oral liquid provided by the invention, with sophora bud vinegar for main nutrient composition, reasonably combined with the mixture of fructose, honey, xitix, Trisodium Citrate, calglucon and Repone K, make this oral liquid sweet and sour taste, nutritious, nourishing function is obvious, security is high, have no side effect, and is especially applicable to the elderly and takes.Long-term taking can play enhancing body capillary resistance, reduces capillary fragility, coronary artery dilator, increase coronary flow, improve the effects such as microcirculation, hypertension, hyperlipidemia, coronary heart disease, chronic bronchitis patient also can be supplied to take, play auxiliary therapeutic action.
The preparation method of above-mentioned sophora bud health care oral liquid, comprising: mixed with water by sophora bud vinegar, adds the mixture of fructose, honey, xitix, Trisodium Citrate, calglucon and Repone K, mixes, and through ultrafiltration, sterilization, to obtain final product.
The preparation method of above-mentioned sophora bud health care oral liquid provided by the invention, with short production cycle, disposable used device is few, and production controllability is strong, and easy to operate and control, constant product quality, is suitable for applying.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
The sophora bud vinegar of the present embodiment, is prepared from by the method comprised the following steps:
1) pluck the fresh sophora bud of the 7-8 month firm spewing tongue, clean with clear water, airing, to dry, pulverized 40 mesh sieves; Obtained sophora bud powder is added the water of 8 times of quality, soak 40min in 80 DEG C, filtered while hot, obtains sophora bud aqueous extract and sophora bud residue, cools for subsequent use;
2) by step 1) gained sophora bud residue, add the edible ethanol of concentration 72%, the mass volume ratio of sophora bud residue and edible ethanol is 1:8, ultrasonic lixiviate 30min at 40 DEG C, filters, obtains sophora bud ethanol extract, cool for subsequent use;
3) by step 1) gained sophora bud aqueous extract and step 2) gained sophora bud ethanol extract presses the volume ratio mixing of 8:1, obtains the Huai Goat that alcoholic strength is 6.2%;
4) in step 3) in the Huai Goat of gained, the Acetobacter pasteurianus liquid of 20% activation of the volume of inoculation Huai Goat, the viable count of bacterium liquid is 1.5 × 10
8cfu/mL, temp .-differential aerobic fermentation 3 days; 1st day leavening temperature 31 DEG C, air flow 120L/h; 2nd day leavening temperature 33 DEG C, air flow 150L/h; 3rd day leavening temperature 30 DEG C, air flow 100L/h; When total acidity reaches 4.0%, to obtain final product.
The sophora bud health care oral liquid of the present embodiment, is made up of the component of following mass parts: sophora bud vinegar 28 parts, 72 parts, water, 2 parts, fructose, honey 4 parts, 0.08 part, xitix, Trisodium Citrate 0.02 part, calglucon 0.002 part and 0.001 part, Repone K.
The preparation method of the sophora bud health care oral liquid of the present embodiment, comprise and sophora bud vinegar is mixed with water, add the mixture of fructose, honey, xitix, Trisodium Citrate, calglucon and Repone K, mix, through ultra filtering clarifying, then, after 130 DEG C of high-temperature instantaneous sterilizations, sophora bud vinegar health care oral liquid is obtained; Again through sterile filling, sealing, inspection, labeling, vanning, can put in storage.
Embodiment 2
The sophora bud vinegar of the present embodiment, is prepared from by the method comprised the following steps:
1) pluck the fresh sophora bud of the 7-8 month firm spewing tongue, clean with clear water, airing, to dry, pulverized 20 mesh sieves; Obtained sophora bud powder is added the water of 9 times of quality, soak 50min in 70 DEG C, filtered while hot, obtains sophora bud aqueous extract and sophora bud residue, cools for subsequent use;
2) by step 1) gained sophora bud residue, add the edible ethanol of concentration 72%, the mass volume ratio of sophora bud residue and edible ethanol is 1:7, ultrasonic lixiviate 25min at 50 DEG C, filters, obtains sophora bud ethanol extract, cool for subsequent use;
3) by step 1) gained sophora bud aqueous extract and step 2) gained sophora bud ethanol extract presses the volume ratio mixing of 9:1, obtains the Huai Goat that alcoholic strength is 5.7%;
4) in step 3) in the Huai Goat of gained, the Acetobacter pasteurianus liquid of 20% activation of the volume of inoculation Huai Goat, the viable count of bacterium liquid is 3.5 × 10
8cfu/mL, temp .-differential aerobic fermentation 3 days; 1st day leavening temperature 31 DEG C, air flow 120L/h; 2nd day leavening temperature 33 DEG C, air flow 150L/h; 3rd day leavening temperature 30 DEG C, air flow 100L/h; When total acidity reaches 3.8%, to obtain final product.
The sophora bud health care oral liquid of the present embodiment, is made up of the component of following mass parts: sophora bud vinegar 25 parts, 75 parts, water, 2.5 parts, fructose, honey 3.5 parts, 0.1 part, xitix, Trisodium Citrate 0.01 part, calglucon 0.001 part and 0.002 part, Repone K.
The preparation method of the sophora bud health care oral liquid of the present embodiment is identical with embodiment 1.
Embodiment 3
The sophora bud vinegar of the present embodiment, is prepared from by the method comprised the following steps:
1) pluck the fresh sophora bud of the 7-8 month firm spewing tongue, clean with clear water, airing, to dry, pulverized 60 mesh sieves; Obtained sophora bud powder is added the water of 10 times of quality, soak 60min in 60 DEG C, filtered while hot, obtains sophora bud aqueous extract and sophora bud residue, cools for subsequent use;
2) by step 1) gained sophora bud residue, add the edible ethanol of concentration 72%, the mass volume ratio of sophora bud residue and edible ethanol is 1:6, ultrasonic lixiviate 20min at 60 DEG C, filters, obtains sophora bud ethanol extract, cool for subsequent use;
3) by step 1) gained sophora bud aqueous extract and step 2) gained sophora bud ethanol extract presses the volume ratio mixing of 10:1, obtains the Huai Goat that alcoholic strength is 5.2%;
4) in step 3) in the Huai Goat of gained, the Acetobacter pasteurianus liquid of 20% activation of the volume of inoculation Huai Goat, the viable count of bacterium liquid is 2.5 × 10
8cfu/mL, temp .-differential aerobic fermentation 3 days; 1st day leavening temperature 31 DEG C, air flow 120L/h; 2nd day leavening temperature 33 DEG C, air flow 150L/h; 3rd day leavening temperature 30 DEG C, air flow 100L/h; When total acidity reaches 3.6%, to obtain final product.
The sophora bud health care oral liquid of the present embodiment, is made up of the component of following mass parts: sophora bud vinegar 30 parts, 70 parts, water, 3 parts, fructose, honey 3 parts, 0.12 part, xitix, Trisodium Citrate 0.01 part, calglucon 0.002 part and 0.001 part, Repone K.
The preparation method of the sophora bud health care oral liquid of the present embodiment is identical with embodiment 1.
Test example
High performance liquid chromatography is adopted to detect step 3 in embodiment 1 ~ 3) gained Huai Goat and step 4) content of Quercetin, violaguercitrin in gained sophora bud vinegar, detected result is as shown in table 1.
Functional component detected result in Huai Goat and sophora bud vinegar in each embodiment of table 1
From the test-results of table 1, step 3) gained Huai Goat to the Quercetin in the sophora bud, violaguercitrin element etc. functional component carried out comprehensive extraction, Huai Goat violaguercitrin content through hybrid modulation is up to 2.51g/L, Quercetin is 0.13g/L, and through step 4) fermentation process and acid hydrolysis after, violaguercitrin is converted into functional stronger Quercetin in a large number, in sophora bud vinegar, the content of Quercetin can reach 1.22g/L, and the nutrition and health care function of sophora bud vinegar is further enhanced.
Claims (8)
1. a sophora bud vinegar, is characterized in that, is prepared by the method comprised the following steps:
1) sophora bud powder is mixed with water, lixiviate at 60 ~ 80 DEG C, filter, obtain sophora bud residue and sophora bud aqueous extract;
2) by step 1) gained sophora bud residue mixes with alcohol, ultrasonic lixiviate at 40 ~ 60 DEG C, and filter, obtain sophora bud ethanol extract;
3) by step 1) gained sophora bud aqueous extract and step 2) mixing of gained sophora bud ethanol extract, obtain the Huai Goat that alcoholic strength is 5.2% ~ 6.2%;
4) in step 3) in gained Huai Goat, inoculation Acetobacter pasteurianus, fermenting to total acidity is 3.6% ~ 4.0%, to obtain final product.
2. sophora bud vinegar as claimed in claim 1, is characterized in that, step 1) in, the mass ratio of sophora bud powder and water is 8 ~ 10:1.
3. sophora bud vinegar as claimed in claim 2, is characterized in that, step 2) in, described alcohol to be volumetric concentration be 72% edible ethanol, the mass volume ratio of sophora bud residue and alcohol is 6 ~ 8:1.
4. sophora bud vinegar as claimed in claim 3, is characterized in that, step 3) in, the volume ratio of described sophora bud aqueous extract and sophora bud ethanol extract is 8 ~ 10:1.
5. sophora bud vinegar as claimed in claim 1, is characterized in that, step 1) time of described lixiviate is 40 ~ 60min; Step 2) time of described lixiviate is 20 ~ 30min.
6. sophora bud vinegar as claimed in claim 1, is characterized in that, step 4) described fermentation is temp .-differential aerobic fermentation, fermentation time is 3 days; Wherein, the 1st day leavening temperature 31 DEG C, air flow 120L/h; 2nd day leavening temperature 33 DEG C, air flow 150L/h; 3rd day leavening temperature 30 DEG C, air flow 100L/h.
7. one kind uses the sophora bud health care oral liquid of sophora bud vinegar described in claim 1, it is characterized in that, be made up of the component of following mass parts: sophora bud vinegar 25 ~ 30 parts, 70 ~ 75 parts, water, 2 ~ 3 parts, fructose, honey 3 ~ 4 parts, 0.08 ~ 0.12 part, xitix, Trisodium Citrate 0.01 ~ 0.02 part, calglucon 0.001 ~ 0.002 part and 0.001 ~ 0.002 part, Repone K.
8. a preparation method for sophora bud health care oral liquid as claimed in claim 7, is characterized in that, comprising: mixed with water by sophora bud vinegar, add fructose, honey, xitix, Trisodium Citrate, calglucon and Repone K, mix, through ultrafiltration, sterilization, to obtain final product.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105695269A (en) * | 2016-03-25 | 2016-06-22 | 安徽瑞思威尔科技有限公司 | Sophora flower bud wine and preparation method |
| CN105918753A (en) * | 2016-05-05 | 2016-09-07 | 华若延 | Preparation method of solid granular drink |
| CN106811391A (en) * | 2017-03-27 | 2017-06-09 | 广东石油化工学院 | A kind of preparation method of hawthorn hill gooseberry compound fruit vinegar |
| CN107334052A (en) * | 2017-05-31 | 2017-11-10 | 黄秋丽 | A kind of sophora flower steamed bun and preparation method thereof |
| CN107874109A (en) * | 2016-09-29 | 2018-04-06 | 桂林洁宇环保科技有限责任公司 | A kind of preparation method of sophora bud health care oatmeal |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105695269A (en) * | 2016-03-25 | 2016-06-22 | 安徽瑞思威尔科技有限公司 | Sophora flower bud wine and preparation method |
| CN105918753A (en) * | 2016-05-05 | 2016-09-07 | 华若延 | Preparation method of solid granular drink |
| CN107874109A (en) * | 2016-09-29 | 2018-04-06 | 桂林洁宇环保科技有限责任公司 | A kind of preparation method of sophora bud health care oatmeal |
| CN106811391A (en) * | 2017-03-27 | 2017-06-09 | 广东石油化工学院 | A kind of preparation method of hawthorn hill gooseberry compound fruit vinegar |
| CN107334052A (en) * | 2017-05-31 | 2017-11-10 | 黄秋丽 | A kind of sophora flower steamed bun and preparation method thereof |
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| CN105199937B (en) | 2018-04-24 |
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