CN105168378B - A kind of modified attapulgite preparation and preparation method thereof for preventing and treating chicken coccidiasis - Google Patents
A kind of modified attapulgite preparation and preparation method thereof for preventing and treating chicken coccidiasis Download PDFInfo
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Abstract
The invention discloses a kind of modified attapulgite preparations and preparation method thereof for preventing and treating chicken coccidiasis, for chicken coccidiasis, by the mechanism of action of modified attapulgite and various bacteria agents and herb extracts, by Bifidobacterium, saccharomycete, lactic acid bacteria, oligosaccharide, semen plantaginis, kuh-seng, honeysuckle, there is Herba Andrographitis these types the bacteria agent and Chinese herbal medicine of different efficacies and characteristic to carry out reasonable screening compounding, it is added in modified attapulgite, and disclose a kind of effective preparation method, manufactured modified attapulgite preparation is not only good to the preventive and therapeutic effect effect of chicken coccidiasis, therapeutic effect reaches 95% or more, reduce its frequency of disease development, and it is nontoxic, ecological, environmental protective, effectively reduce antibiotic, reduce the residue of veterinary drug of animal foodstuff, furthermore the modified attapulgite preparation is prepared convenient, holding time is long, with very strong practical value.
Description
Technical field
The present invention relates to the cultural techniques of chicken, more particularly, to a kind of modified attapulgite preparation and its system for preventing and treating chicken coccidiasis
Preparation Method.
Background technique
World's attapulgite clay proved reserves are 1.5 hundred million tons or so, and China's reserves account for the 50% of the whole world, Jiangsu Province's reserves
The 79% of the whole nation is accounted for again.Geologic Survey Inst., Jiangsu Province's latest survey the result shows that, the domestic attapulgite clay grade in Xuyi County
Height, reserves are big, and there are about more than 6,700 ten thousand tons.Attapulgite clay is widely applied mainly as adsorbent, decolorising agent etc. at present, but attached
Value added not high, price only has thousand yuan or so/ton.This is the mineral products money that Jiangsu Province is valuable, takes advantage in the whole nation or even the whole world
Source should be subject to deep development and utilization, improve added value, contribute for the economic development in Jiangsu.
Currently, attapulgite clay for animals prevents and treats the preparation of intestines problem not yet.Modified recessed soil is verified than general
Logical recessed soil is in adsorption capacity, function and effect beyond very much.The application of modified attapulgite can be played at aspect once and energetically be acted on:
Food safety.The usage amount that antibiotic, anticoccidial drug can be effectively reduced reduces the residue of veterinary drug of animal foodstuff, and effective
The intestines problem for preventing and treating chicken.
The modified attapulgite preparation and its preparation that the globidiosis of a kind of pair of chicken is effectively prevented are worth research.
Summary of the invention
Goal of the invention: In order to solve the problems of in the prior art, the invention proposes one kind to effectively reduce antibiosis
Element, reduces the residue of veterinary drug of animal foodstuff, the modified attapulgite preparation of prevention and treatment chicken coccidiasis of the control efficiency up to 95% or more and its
Preparation method
Technical solution: to achieve these objectives, the present invention takes following technical scheme: a kind of modification preventing and treating chicken coccidiasis is recessed
Native preparation, including as follows by weight prepare raw material: 25-35 parts of modified attapulgites, 5-8 parts 100-300 times of Bifidobacterium it is dilute
Release liquid, 3-6 parts of saccharomycete wettable powders, 100-200 times of dilution of 3-6 parts of lactic acid bacterias, 4-6 portions of oligosaccharide, 3-6 parts of Chinese herbaceous peonies
Son, 5-10 parts of kuh-sengs, 3-5 portions of honeysuckles, 3-6 parts of Herba Andrographitis, 100-200 parts of deionized waters；Wherein modified attapulgite is by 10%
Copper-loaded recessed soil, 20% carry the recessed soil of chromium, 30% carry the recessed soil of zinc, 10% precipitated calcium carbonate, 10% powdered rice hulls, 10% dish
The seed dregs of rice, 5% surfactant and 5% surface modifier composition.
Further, the Bifidobacterium is bifidobacterium bifidum.
Further, the saccharomycete is torulopsis.
Further, the lactic acid bacteria is Plant Lactobacilli.
Further, the semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis are wettable powder.
Further, the surfactant is cationic surfactant.
Further, the surface modifier is Inorganic surface modifiers.
Further, the oligosaccharide is soyabean oligosaccharides.
The preparation method of the modified attapulgite preparation of above-mentioned prevention and treatment chicken coccidiasis, comprising the following steps:
(a) preparation of copper-loaded recessed soil: filter is filtered to take after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with copper salt solution, solid-to-liquid ratio 1:30, is shaken in 70-80 DEG C of constant temperature
It swings in device, abandons supernatant after centrifugation is stood after 300r/min oscillation 3-4h, dried in 105 DEG C of drying boxes to constant weight, grinding, mistake
150 meshes obtain copper-loaded recessed soil；
(b) it carries the preparation of the recessed soil of chromium: filtering to take filter after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with chromium salt solution, solid-to-liquid ratio 1:30, is shaken in 70-80 DEG C of constant temperature
It swings in device, abandons supernatant after centrifugation is stood after 300r/min oscillation 3-4h, dried in 105 DEG C of drying boxes to constant weight, grinding, mistake
150 meshes obtain carrying the recessed soil of chromium；
(c) it carries the preparation of the recessed soil of zinc: filtering to take filter after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with zinc solution, solid-to-liquid ratio 1:30, is shaken in 70-80 DEG C of constant temperature
It swings in device, abandons supernatant after centrifugation is stood after 300r/min oscillation 3-4h, dried in 105 DEG C of drying boxes to constant weight, grinding, mistake
150 meshes obtain carrying the recessed soil of zinc；
(d) it the preparation of modified attapulgite: takes the desired amount of above-mentioned copper-loaded recessed soil being prepared, copper-loaded recessed soil, carry the recessed soil of zinc
It is blended in the desired amount of precipitated calcium carbonate, powdered rice hulls, rapeseed dregs after stirring 20-30min in blender, surfactant is added
And surface modifier continues to stir evenly, and crosses 150 meshes after 80-100 DEG C of baking 2-3h in an oven；
(e) take the desired amount of modified attapulgite that the desired amount of 100-300 times of dilution of Bifidobacterium, saccharomycete wettable is added
Pulvis, 100-200 times of dilution of lactic acid bacteria, oligosaccharide and half amount water, cultivate for 24 hours at 35 DEG C -45 DEG C after mixing evenly
Obtain culture solution A；
(f) the desired amount of semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis and remaining water are uniformly mixed and are heated to 120 DEG C of dimensions
Cooled to room temperature obtains culture solution B after holding 40-50min；
(g) culture solution A and culture solution B are mixed evenly, anaerobism, which is placed at room temperature for 36h or more, can be obtained required modification
Recessed soil preparation.
The utility model has the advantages that a kind of modified attapulgite preparation and preparation method thereof for preventing and treating chicken coccidiasis provided by the invention, for
Chicken coccidiasis, by the mechanism of action of modified attapulgite and various bacteria agents and herb extracts, by Bifidobacterium, saccharomycete, cream
Sour bacterium, oligosaccharide, semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis these types have bacteria agent and the medium-height grass of different efficacies and characteristic
Medicine carries out reasonable screening compounding, is added in modified attapulgite, and disclose a kind of effective preparation method, manufactured modification is recessed
Native preparation is not only good to the preventive and therapeutic effect effect of chicken coccidiasis, and therapeutic effect reaches 95% or more, reduces its frequency of disease development, and nothing
Poison is harmless, and ecological, environmental protective effectively reduces antibiotic, reduces the residue of veterinary drug of animal foodstuff, and furthermore the modified attapulgite preparation is prepared
Convenient, the holding time is long, has very strong practical value.
Specific embodiment
Embodiment 1:
It is a kind of prevent and treat chicken coccidiasis modified attapulgite preparation, including as follows by weight prepare raw material: 25 parts of modifications
Recessed soil, 100-200 times of 100-300 times of dilution of 5 parts of Bifidobacteriums, 3 parts of saccharomycete wettable powders, 3 parts of lactic acid bacterias dilution,
4 portions of oligosaccharide, 3 portions of semen plantaginis, 5 parts of kuh-sengs, 3 portions of honeysuckles, 3 parts of Herba Andrographitis, 100 parts of deionized waters；Wherein modified attapulgite by
10% it is copper-loaded it is recessed soil, 20% carry chromium it is recessed soil, 30% the recessed soil of load zinc, 10% precipitated calcium carbonate, 10% powdered rice hulls,
10% rapeseed dregs, 5% surfactant and 5% surface modifier composition.
Wherein, Bifidobacterium is bifidobacterium bifidum；Saccharomycete is torulopsis；Lactic acid bacteria is Plant Lactobacilli；Vehicle
Preceding son, kuh-seng, honeysuckle, Herba Andrographitis are wettable powder；The surfactant is cationic surfactant；The table
Face modifying agent is Inorganic surface modifiers；The oligosaccharide is soyabean oligosaccharides.
The preparation method of the modified attapulgite preparation of above-mentioned prevention and treatment chicken coccidiasis, comprising the following steps:
(a) preparation of copper-loaded recessed soil: filter residue is filtered to take after common recessed soil is impregnated 1h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 2h in 300 DEG C of Muffle furnaces with copper salt solution, solid-to-liquid ratio 1:30, in 70 DEG C of constant temperature oscillators, 300r/
Abandon supernatant after standing centrifugation after min oscillation 3h, dried in 105 DEG C of drying boxes to constant weight, grinding, cross 150 meshes obtain it is copper-loaded
Recessed soil；
(b) it carries the preparation of the recessed soil of chromium: filtering to take filter residue after common recessed soil is impregnated 1h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 2h in 300 DEG C of Muffle furnaces with chromium salt solution, solid-to-liquid ratio 1:30, in 70 DEG C of constant temperature oscillators, 300r/
Supernatant is abandoned after standing centrifugation after min oscillation 3h, is dried in 105 DEG C of drying boxes to constant weight, grinding, 150 meshes is crossed and obtains carrying chromium
Recessed soil；
(c) it carries the preparation of the recessed soil of zinc: filtering to take filter residue after common recessed soil is impregnated 1h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 2h in 300 DEG C of Muffle furnaces with zinc solution, solid-to-liquid ratio 1:30, in 70 DEG C of constant temperature oscillators, 300r/
Supernatant is abandoned after standing centrifugation after min oscillation 3h, is dried in 105 DEG C of drying boxes to constant weight, grinding, 150 meshes is crossed and obtains carrying zinc
Recessed soil；
(d) it the preparation of modified attapulgite: takes the desired amount of above-mentioned copper-loaded recessed soil being prepared, copper-loaded recessed soil, carry the recessed soil of zinc
With the desired amount of precipitated calcium carbonate, powdered rice hulls, rapeseed dregs be blended in blender stir 20min after, be added surfactant and
Surface modifier continues to stir evenly, and crosses 150 meshes after 80 DEG C of baking 2h in an oven；
(e) take the desired amount of modified attapulgite that the desired amount of 100-300 times of dilution of Bifidobacterium, saccharomycete wettable is added
Pulvis, 100-200 times of dilution of lactic acid bacteria, oligosaccharide and half amount water, cultivate at 35 DEG C DEG C obtain for 24 hours after mixing evenly
Culture solution A；
(f) the desired amount of semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis and remaining water are uniformly mixed and are heated to 120 DEG C of dimensions
Cooled to room temperature obtains culture solution B after holding 40min；
(g) culture solution A and culture solution B are mixed evenly, anaerobism, which is placed at room temperature for 36h or more, can be obtained required modification
Recessed soil preparation.
Embodiment 2:
It is a kind of prevent and treat chicken coccidiasis modified attapulgite preparation, including as follows by weight prepare raw material: 35 parts of modifications
Recessed soil, 100-200 times of 100-300 times of dilution of 8 parts of Bifidobacteriums, 6 parts of saccharomycete wettable powders, 6 parts of lactic acid bacterias dilution,
6 portions of oligosaccharide, 6 portions of semen plantaginis, 10 parts of kuh-sengs, 5 portions of honeysuckles, 6 parts of Herba Andrographitis, 200 parts of deionized waters；Wherein modified attapulgite by
10% it is copper-loaded it is recessed soil, 20% carry chromium it is recessed soil, 30% the recessed soil of load zinc, 10% precipitated calcium carbonate, 10% powdered rice hulls,
10% rapeseed dregs, 5% surfactant and 5% surface modifier composition.
Wherein, Bifidobacterium is bifidobacterium bifidum；Saccharomycete is torulopsis；Lactic acid bacteria is Plant Lactobacilli；Vehicle
Preceding son, kuh-seng, honeysuckle, Herba Andrographitis are wettable powder；The surfactant is cationic surfactant；The table
Face modifying agent is Inorganic surface modifiers；The oligosaccharide is soyabean oligosaccharides.
The preparation method of the modified attapulgite preparation of above-mentioned prevention and treatment chicken coccidiasis, comprising the following steps:
(a) preparation of copper-loaded recessed soil: filter residue is filtered to take after common recessed soil is impregnated 2h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 4h in 400 DEG C of Muffle furnaces with copper salt solution, solid-to-liquid ratio 1:30, in 80 DEG C of constant temperature oscillators, 300r/
Abandon supernatant after standing centrifugation after min oscillation 4h, dried in 105 DEG C of drying boxes to constant weight, grinding, cross 150 meshes obtain it is copper-loaded
Recessed soil；
(b) it carries the preparation of the recessed soil of chromium: filtering to take filter residue after common recessed soil is impregnated 2h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 4h in 400 DEG C of Muffle furnaces with chromium salt solution, solid-to-liquid ratio 1:30, in 80 DEG C of constant temperature oscillators, 300r/
Supernatant is abandoned after standing centrifugation after min oscillation 4h, is dried in 105 DEG C of drying boxes to constant weight, grinding, 150 meshes is crossed and obtains carrying chromium
Recessed soil；
(c) it carries the preparation of the recessed soil of zinc: filtering to take filter residue after common recessed soil is impregnated 2h with 5% sodium hydroxide solution first
It is uniformly mixed after toasting 4h in 400 DEG C of Muffle furnaces with zinc solution, solid-to-liquid ratio 1:30, in 80 DEG C of constant temperature oscillators, 300r/
Supernatant is abandoned after standing centrifugation after min oscillation 4h, is dried in 105 DEG C of drying boxes to constant weight, grinding, 150 meshes is crossed and obtains carrying zinc
Recessed soil；
(d) it the preparation of modified attapulgite: takes the desired amount of above-mentioned copper-loaded recessed soil being prepared, copper-loaded recessed soil, carry the recessed soil of zinc
With the desired amount of precipitated calcium carbonate, powdered rice hulls, rapeseed dregs be blended in blender stir 30min after, be added surfactant and
Surface modifier continues to stir evenly, and crosses 150 meshes after 100 DEG C of baking 3h in an oven；
(e) take the desired amount of modified attapulgite that the desired amount of 100-300 times of dilution of Bifidobacterium, saccharomycete wettable is added
Pulvis, 100-200 times of dilution of lactic acid bacteria, oligosaccharide and half amount water, cultivate at 45 DEG C trained for 24 hours after mixing evenly
Nutrient solution A；
(f) the desired amount of semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis and remaining water are uniformly mixed and are heated to 120 DEG C of dimensions
Cooled to room temperature obtains culture solution B after holding 50min；
(g) culture solution A and culture solution B are mixed evenly, anaerobism, which is placed at room temperature for 36h or more, can be obtained required modification
Recessed soil preparation.
Embodiment 3:
It is a kind of prevent and treat chicken coccidiasis modified attapulgite preparation, including as follows by weight prepare raw material: 30 parts of modifications
Recessed soil, 100-200 times of 100-300 times of dilution of 6 parts of Bifidobacteriums, 5 parts of saccharomycete wettable powders, 4 parts of lactic acid bacterias dilution,
5 portions of oligosaccharide, 5 portions of semen plantaginis, 8 parts of kuh-sengs, 4 portions of honeysuckles, 5 parts of Herba Andrographitis, 150 parts of deionized waters；Wherein modified attapulgite by
10% it is copper-loaded it is recessed soil, 20% carry chromium it is recessed soil, 30% the recessed soil of load zinc, 10% precipitated calcium carbonate, 10% powdered rice hulls,
10% rapeseed dregs, 5% surfactant and 5% surface modifier composition.
Wherein, Bifidobacterium is bifidobacterium bifidum；Saccharomycete is torulopsis；Lactic acid bacteria is Plant Lactobacilli；Vehicle
Preceding son, kuh-seng, honeysuckle, Herba Andrographitis are wettable powder；The surfactant is cationic surfactant；The table
Face modifying agent is Inorganic surface modifiers；The oligosaccharide is soyabean oligosaccharides.
The preparation method of the modified attapulgite preparation of above-mentioned prevention and treatment chicken coccidiasis, comprising the following steps:
(a) preparation of copper-loaded recessed soil: filter is filtered to take after common recessed soil is impregnated 1.5h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 3h in 350 DEG C of Muffle furnaces with copper salt solution, solid-to-liquid ratio 1:30, in 75 DEG C of constant temperature oscillators,
Supernatant is abandoned after standing centrifugation after 300r/min oscillation 3.5h, is dried in 105 DEG C of drying boxes to constant weight, grinding, is crossed 150 meshes and obtain
To copper-loaded recessed soil；
(b) it carries the preparation of the recessed soil of chromium: filtering to take filter after common recessed soil is impregnated 1.5h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 3h in 350 DEG C of Muffle furnaces with chromium salt solution, solid-to-liquid ratio 1:30, in 75 DEG C of constant temperature oscillators,
Supernatant is abandoned after standing centrifugation after 300r/min oscillation 3.5h, is dried in 105 DEG C of drying boxes to constant weight, grinding, is crossed 150 meshes and obtain
To the load recessed soil of chromium；
(c) it carries the preparation of the recessed soil of zinc: filtering to take filter after common recessed soil is impregnated 1.5h with 5% sodium hydroxide solution first
Slag is uniformly mixed after toasting 3h in 350 DEG C of Muffle furnaces with zinc solution, solid-to-liquid ratio 1:30, in 75 DEG C of constant temperature oscillators,
Supernatant is abandoned after standing centrifugation after 300r/min oscillation 3.5h, is dried in 105 DEG C of drying boxes to constant weight, grinding, is crossed 150 meshes and obtain
To the load recessed soil of zinc；
(d) it the preparation of modified attapulgite: takes the desired amount of above-mentioned copper-loaded recessed soil being prepared, copper-loaded recessed soil, carry the recessed soil of zinc
With the desired amount of precipitated calcium carbonate, powdered rice hulls, rapeseed dregs be blended in blender stir 25min after, be added surfactant and
Surface modifier continues to stir evenly, and crosses 150 meshes after 90 DEG C of baking 2.5h in an oven；
(e) take the desired amount of modified attapulgite that the desired amount of 100-300 times of dilution of Bifidobacterium, saccharomycete wettable is added
Pulvis, 100-200 times of dilution of lactic acid bacteria, oligosaccharide and half amount water, cultivate at 40 DEG C trained for 24 hours after mixing evenly
Nutrient solution A；
(f) the desired amount of semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis and remaining water are uniformly mixed and are heated to 120 DEG C of dimensions
Cooled to room temperature obtains culture solution B after holding 45min；
(g) culture solution A and culture solution B are mixed evenly, anaerobism, which is placed at room temperature for 36h or more, can be obtained required modification
Recessed soil preparation.
2014, researcher chose 100 in area Jurong, Jiangsu Province Jurong Hao Yuan ecological agriculture Science and Technology Ltd.
Chicken is tested, and is divided into two groups, control group using traditional medicine composition of using, test group is using the system of the embodiment of the present invention 3
The modified attapulgite preparation of work, test group and control group, other cultivating conditions are identical, terminate from cultivation is started to cultivation, test group
The disease incidence of chicken coccidiasis is 3%, and control group disease incidence is 30%；Modified attapulgite preparation prepared by the present invention is not only to Eimeria species
The preventive and therapeutic effect effect of disease is good, and therapeutic effect reaches 95% or more, reduces its frequency of disease development, and nontoxic, and ecological, environmental protective has
Effect reduces antibiotic, reduces the residue of veterinary drug of animal foodstuff, and furthermore the modified attapulgite preparation is prepared convenient, and the holding time is long, tool
There is very strong practical value.
It should be pointed out that for those skilled in the art, without departing from the principle of the present invention,
It can also make several improvements, these improvement also should be regarded as protection scope of the present invention.
Claims (2)
1. it is a kind of prevent and treat chicken coccidiasis modified attapulgite preparation, it is characterised in that including as follows by weight prepare raw material:
25-35 parts of modified attapulgites, 100-300 times of dilution of 5-8 parts of Bifidobacteriums, 3-6 parts of saccharomycete wettable powders, 3-6 parts of lactic acid
100-200 times of dilution of bacterium, 4-6 portions of oligosaccharide, 3-6 portions of semen plantaginis, 5-10 parts of kuh-sengs, 3-5 portions of honeysuckles, 3-6 parts of Herba Andrographitis,
100-200 parts of deionized waters；Wherein copper-loaded recessed native, 20% load chromium recessed soil, 30% load zinc recessed soil, 10% of the modified attapulgite by 10%
Precipitated calcium carbonate, 10% powdered rice hulls, 10% rapeseed dregs, 5% surfactant and 5% surface modifier composition；Institute
Stating Bifidobacterium is bifidobacterium bifidum；The saccharomycete is torulopsis；The lactic acid bacteria is Plant Lactobacilli；The vehicle
Preceding son, kuh-seng, honeysuckle, Herba Andrographitis are wettable powder；The surfactant is cationic surfactant；The table
Face modifying agent is Inorganic surface modifiers；The oligosaccharide is soyabean oligosaccharides.
2. a kind of preparation method of the modified attapulgite preparation of prevention and treatment chicken coccidiasis described in claim 1, it is characterised in that including
Following steps:
(a) preparation of copper-loaded recessed soil: filter residue is filtered to take after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first and is existed
It is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with copper salt solution, solid-to-liquid ratio 1:30, in 70-80 DEG C of constant temperature oscillator
In, supernatant is abandoned after centrifugation is stood after 300r/min oscillation 3-4h, is dried in 105 DEG C of drying boxes to constant weight, grinding crosses 150
Mesh obtains copper-loaded recessed soil；
(b) it carries the preparation of the recessed soil of chromium: filtering to take filter residue after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first and exist
It is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with chromium salt solution, solid-to-liquid ratio 1:30, in 70-80 DEG C of constant temperature oscillator
In, supernatant is abandoned after centrifugation is stood after 300r/min oscillation 3-4h, is dried in 105 DEG C of drying boxes to constant weight, grinding crosses 150
Mesh obtains carrying the recessed soil of chromium；
(c) it carries the preparation of the recessed soil of zinc: filtering to take filter residue after common recessed soil is impregnated 1-2h with 5% sodium hydroxide solution first and exist
It is uniformly mixed after toasting 2-4h in 300-400 DEG C of Muffle furnace with zinc solution, solid-to-liquid ratio 1:30, in 70-80 DEG C of constant temperature oscillator
In, supernatant is abandoned after centrifugation is stood after 300r/min oscillation 3-4h, is dried in 105 DEG C of drying boxes to constant weight, grinding crosses 150
Mesh obtains carrying the recessed soil of zinc；
(d) it the preparation of modified attapulgite: takes the desired amount of above-mentioned copper-loaded recessed soil being prepared, copper-loaded recessed soil, carry the recessed soil of zinc and institute
Precipitated calcium carbonate, powdered rice hulls, the rapeseed dregs of requirement are blended in blender after stirring 20-30min, and surfactant and table is added
Face modifying agent continues to stir evenly, and crosses 150 meshes after 80-100 DEG C of baking 2-3h in an oven；
(e) take the desired amount of modified attapulgite that the desired amount of 100-300 times of dilution of Bifidobacterium, saccharomycete wettable powder is added
Agent, 100-200 times of dilution of lactic acid bacteria, oligosaccharide and half amount water, after mixing evenly cultivate at 35 DEG C -45 DEG C for 24 hours
To culture solution A；
(f) the desired amount of semen plantaginis, kuh-seng, honeysuckle, Herba Andrographitis and remaining water are uniformly mixed and are heated to 120 DEG C of maintenances
Cooled to room temperature obtains culture solution B after 40-50min；
(g) culture solution A and culture solution B are mixed evenly, anaerobism, which is placed at room temperature for 36h or more, can be obtained required modified attapulgite
Preparation.
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Inventor after: Chen Yongxia Inventor after: Jiang Jiasen Inventor after: Guo Ping Inventor before: Chen Rongxia Inventor before: Jiang Jiasen Inventor before: Guo Ping |