CN105168066A - Process for preparing antiallergic essence by means of Chinese herbal medicine - Google Patents
Process for preparing antiallergic essence by means of Chinese herbal medicine Download PDFInfo
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- CN105168066A CN105168066A CN201510660609.6A CN201510660609A CN105168066A CN 105168066 A CN105168066 A CN 105168066A CN 201510660609 A CN201510660609 A CN 201510660609A CN 105168066 A CN105168066 A CN 105168066A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The invention relates to a process for preparing antiallergic essence by means of Chinese herbal medicine. The process comprises the steps of 1, mixing oat, liquorice, radix scutellariae, German camomile, olive leaves, arnica, tilia cordata, althaea officinalis and peony in certain proportion, and placing the mixture in a distillation still; 2, adding deionized water to the distillation still; 3, conducting primary extraction; 4, collecting liquid obtained through primary extraction; 5, conducting secondary extraction; 6, collecting liquid obtained through secondary extraction; 7, conducting combined filtration on the liquid obtained at the first time and the liquid obtained at the second time; 8, conducting primary concentration on the extracting solution obtained after filtration; 9, conducting ethanol precipitation, wherein ethanol is added to the concentrated solution, and supernatant liquid is taken out after even stirring and standing; 10, conducting biological concentration, wherein secondary concentration is conducted on the supernatant liquid to obtain the antiallergic essence. The process for preparing the antiallergic essence by means of Chinese herbal medicine is simple in production and low in cost.
Description
Technical field
The present invention relates to a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence.
Background technology
In recent years, due to reasons such as environmental pollution and drinking water source problems, autopath increases day by day, and allergy has had a strong impact on daily life.Therefore, various antiallergic agent class increase not poor.And take pure natural plant as the favor that the antiallergic essence of raw material also receives people.
Anaphylaxis refers to the reaction of the tissue injury that immunifacient body occurs when again accepting same antigen and stimulating or dysfunction.The feature of reaction be outbreak rapidly, strong reaction, disappear very fast; Generally can not disorganize cell, also can not cause and organize major injury, have obvious genetic predisposition and individual variation.The mechanism that anaphylaxis occurs is a complexity and abstract process, generally the mechanism that anaphylaxis occurs is divided into sensitisation phase, excitation phase and effective stage.
Antiallergic essence has good anticomplementary action, reaches anti-inflammatory efficacy, and can hyaluronidase inhibitor, plays antiinflammatory and analgesic effect.And antiallergic essence has outstanding antihistaminic release action, plays antiallergic effect.Test display: the Radix Paeoniae that antiallergic whitening compound extracted solution contains has good therapeutic effect to contact dermatitis, plays antipruritic, detumescence, anti-inflammatory efficacy.In addition antiallergic whitening compound extracted solution also has very strong white-skinned face function, and life-time service contains Radix Paeoniae, the cosmetics of Cortex Moutan can make skin beautiful white without speckle.Clinical trial shows, and after nursing for 1 week with the cream frost containing 3% antiallergic whitening and speckle dispelling compound extracted solution, skin allergy improves 38.6%, and after 2-3 weeks of nursing, skin allergy improves 83.6%.
Summary of the invention
The object of the invention is the shortcoming existed based on current technology, special for people's trial production go out a kind of can whitening, while can resist again the anti-allergic essence of people's allergy.
Herba bromi japonici: there is the effect reducing cholesterol, steadily blood glucose; Radix Glycyrrhizae: there is good cough-relieving, eliminate the phlegm, antiasthmatic effect; Radix Scutellariae: heat clearing and damp drying, removing heat from blood is antiabortive, detoxicating functions; Flos Matricariae chamomillae: wind dispelling induces sweat, cures cold, rheumatalgia, is exclusively used in spasmolytic, antiinflammatory, choleretic effect are strong; Folium olive: antibacterial, antioxidation; Arnica montana: alleviate muscular soreness or arthritis; Althaea officinalis L.: induce sweat cold expelling, diuresis, cough-relieving, the merit of eliminating inflammation and expelling toxin controls furuncle carbuncle, cough, tracheitis and anemofrigid cold etc.; Paeonia suffruticosa: clearing away heat and cooling blood, blood circulation promoting and blood stasis dispelling
Preparation process of the present invention is:
(1) with parts by weight, carried out according to a certain percentage being mixed to get Traditional Chinese drug mixture by following raw material, and put into distillating still; Above-described raw material and component ratio as follows: Herba bromi japonici: 3 ~ 6%, Radix Glycyrrhizae: 8 ~ 11%, Radix Scutellariae: 10 ~ 13%, Flos Matricariae chamomillae: 16 ~ 19%, Folium olive: 3 ~ 6%, arnica montana: 3 ~ 6%, Tilia cordata: 13 ~ 16%, Althaea officinalis L.: 18 ~ 21%, Paeonia suffruticosa: 8 ~ 11%;
(2) in distillating still, deionized water is added; By weight, water: Traditional Chinese drug mixture is 5.0 ~ 6.0:1;
(3) first time extracts: the temperature rise period, add thermal still, and by regulating the programming rate in the pressure and temperature control distillating still in distillating still, programming rate is 1.6 DEG C-2.6 DEG C/min to 65-85 DEG C, in this process, the pressure in distillating still is 0.25 ~ 0.35Mpa; Holding stage, regulate the pressure and temperature control in distillating still to make its temperature remain on 65-85 DEG C, the Stress control in distillating still is at 0.08 ~ 0.1MPa, and the time is 2h-3h;
(4) liquid of first time extraction is collected;
(5) deionized water adding raw material weight 2.0 ~ 3.0 times in the solid residue obtained after first time extraction process carries out second time and extracts;
(6) liquid that second time is extracted is collected;
(7) filter: the liquid being extracted acquisition first time extracts with second time the liquid obtained and merges, and with the filtration of 300-500 mesh filter screen, obtains the filtrate of removal solid residue;
(8) first time is concentrated: be 75 ~ 100 DEG C by the extracting solution that obtains after filtering in temperature, and vacuum is carry out first time concentration under the condition of 0.075 ~ 0.095Mpa, obtains concentrated solution;
(9) alcohol settling: the ethanol adding 2.2 ~ 2.7 times of concentrated solution weight in concentrated solution, at room temperature leaves standstill 24 hours after stirring, and takes out the supernatant;
(10) bioanalysis concentrates: the supernatant is carried out second time concentration under temperature 45 ~ 58 DEG C of conditions, obtains antiallergic essence.
As improvement, in described methanol precipitation step, the concentration of ethanol is 92% ~ 95%.
As improvement, in the described supernatant, the concentration of alcoholic solution is 50 ~ 65%.
As improvement, the density of described concentrated solution is 1.0280 ~ 1.0420kg/m
3.
As another improvement, the density of described antiallergic essence is 1.19200 ~ 1.2080kg/m
3.
As another improvement, described optimum feed stock and component ratio are: Herba bromi japonici: 5%, Radix Glycyrrhizae: 10%, Radix Scutellariae; 12%, Flos Matricariae chamomillae: 18%, Folium olive: 5%, arnica montana: 5%, Tilia cordata: 15%, Althaea officinalis L.: 20%, Paeonia suffruticosa: 10%.
As another improvement, described distillating still is ultrasonic extraction tank.
As another improvement, after described alcohol settling, mixing time is 30 ~ 50 minutes, mixing speed: 120 ~ 150 revs/min.
As further improving, what described bioanalysis concentrated employing is HACC clear liquor.
As further improving, the moisture content of described raw material is not higher than 6%.
Beneficial effect of the present invention: the invention provides a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence, the raw material that the essence adopting said method to make uses is fully natural green plant, overcome the easy allergy that essence before exists, the shortcoming of skin effect difference, also there is the advantages such as production process is simple, with low cost in this essence simultaneously, and then be popular in users.
Detailed description of the invention
Embodiment 1
(1) with parts by weight, carried out according to a certain percentage being mixed to get Traditional Chinese drug mixture by following raw material, and put into distillating still; Above-described raw material and component ratio as follows: Herba bromi japonici: 3%, Radix Glycyrrhizae: 8%, Radix Scutellariae: 11%, Flos Matricariae chamomillae: 19%, Folium olive: 5%, arnica montana: 6%, Tilia cordata: 16%, Althaea officinalis L.: 21%, Paeonia suffruticosa: 11%;
(2) in distillating still, deionized water is added; By weight, water: Traditional Chinese drug mixture is 5.0:1;
(3) first time extracts: the temperature rise period, add thermal still, and by regulating the programming rate in the pressure and temperature control distillating still in distillating still, programming rate is 1.6 DEG C/min to 65 DEG C, and in this process, the pressure in distillating still is 0.25Mpa; Holding stage, regulate the pressure and temperature control in distillating still to make its temperature remain on 65 DEG C, the Stress control in distillating still is at 0.08MPa, and the time is 2h;
(4) liquid of first time extraction is collected;
(5) deionized water adding raw material weight 2.0 times in the solid residue obtained after first time extraction process carries out second time and extracts;
(6) liquid that second time is extracted is collected;
(7) filter: the liquid being extracted acquisition first time extracts with second time the liquid obtained and merges, and with 300 mesh filter screens filtrations, obtain the filtrate of removal solid residue;
(8) first time is concentrated: be 75 DEG C by the extracting solution that obtains after filtering in temperature, and vacuum is carry out first time concentration under the condition of 0.075Mpa, and obtaining density is 1.0280kg/m
3concentrated solution; The concentration of ethanol is 92%;
(9) alcohol settling: the ethanol adding 2.2 times of concentrated solution weight in concentrated solution, at room temperature leaves standstill 24 hours after stirring, and takes out the supernatant; In the supernatant, the concentration of alcoholic solution is 50%;
(10) bioanalysis concentrates: the supernatant is carried out second time concentration under temperature 45 C condition, and obtaining density is 1.19200kg/m
3antiallergic essence.
Embodiment 2
(1) with parts by weight, carried out according to a certain percentage being mixed to get Traditional Chinese drug mixture by following raw material, and put into distillating still; Above-described raw material and component ratio as follows: Herba bromi japonici: 6%, Radix Glycyrrhizae: 11%, Radix Scutellariae: 13%, Flos Matricariae chamomillae: 19%, Folium olive: 4%, arnica montana: 4%, Tilia cordata: 15%, Althaea officinalis L.: 19%, Paeonia suffruticosa: 9%;
(2) in distillating still, deionized water is added; By weight, water: Traditional Chinese drug mixture is 5.5:1;
(3) first time extracts: the temperature rise period, add thermal still, and by regulating the programming rate in the pressure and temperature control distillating still in distillating still, programming rate is 2.2 DEG C/min to 78 DEG C, and in this process, the pressure in distillating still is 0.30Mpa; Holding stage, regulate the pressure and temperature control in distillating still to make its temperature remain on 75 DEG C, the Stress control in distillating still is at 0.09MPa, and the time is 2.5h;
(4) liquid of first time extraction is collected;
(5) deionized water adding raw material weight 2.5 times in the solid residue obtained after first time extraction process carries out second time and extracts;
(6) liquid that second time is extracted is collected;
(7) filter: the liquid being extracted acquisition first time extracts with second time the liquid obtained and merges, and with 400 mesh filter screens filtrations, obtain the filtrate of removal solid residue;
(8) first time is concentrated: be 90 DEG C by the extracting solution that obtains after filtering in temperature, and vacuum is carry out first time concentration under the condition of 0.085Mpa, and obtaining density is 1.0350kg/m
3concentrated solution; Concentration of alcohol is 93%;
(9) alcohol settling: the ethanol adding 2.5 times of concentrated solution weight in concentrated solution, at room temperature leaves standstill 24 hours after stirring, and takes out the supernatant; In the supernatant, concentration of alcohol is 58%;
(10) bioanalysis concentrates: the supernatant is carried out second time concentration under temperature 53 DEG C of conditions, and obtaining density is 1.1980kg/m
3antiallergic essence.
Embodiment 3
(1) with parts by weight, carried out according to a certain percentage being mixed to get Traditional Chinese drug mixture by following raw material, and put into distillating still; Above-described raw material and component ratio as follows: Herba bromi japonici: 6%, Radix Glycyrrhizae: 11%, Radix Scutellariae: 13%, Flos Matricariae chamomillae: 19%, Folium olive: 3%, arnica montana: 3%, Tilia cordata: 15%, Althaea officinalis L.: 20%, Paeonia suffruticosa: 10%;
(2) in distillating still, deionized water is added; By weight, water: Traditional Chinese drug mixture is 6.0:1;
(3) first time extracts: the temperature rise period, add thermal still, and by regulating the programming rate in the pressure and temperature control distillating still in distillating still, programming rate is 2.6 DEG C/min to 85 DEG C, and in this process, the pressure in distillating still is 0.35Mpa; Holding stage, regulate the pressure and temperature control in distillating still to make its temperature remain on 85 DEG C, the Stress control in distillating still is at 0.1MPa, and the time is 3h;
(4) liquid of first time extraction is collected;
(5) add raw material weight .0 deionized water doubly in the solid residue obtained after first time extraction process and carry out second time extraction;
(6) liquid that second time is extracted is collected;
(7) filter: the liquid being extracted acquisition first time extracts with second time the liquid obtained and merges, and with 500 mesh filter screens filtrations, obtain the filtrate of removal solid residue;
(8) first time is concentrated: by the extracting solution that obtains after filtering temperature 100 DEG C, vacuum is carry out first time concentration under the condition of 0.095Mpa, and obtaining density is 1.0420kg/m
3concentrated solution; The concentration of ethanol is 95%;
(9) alcohol settling: the ethanol adding 2.7 times of concentrated solution weight in concentrated solution, at room temperature leaves standstill 24 hours after stirring, and takes out the supernatant; In the supernatant, the concentration of alcoholic solution is 65%;
(10) bioanalysis concentrates: the supernatant is carried out second time concentration under temperature 58 DEG C of conditions, and obtaining density is 1.2080kg/m
3antiallergic essence.
Claims (10)
1. utilize Chinese herbal medicine to prepare a technique for antiallergic essence, it is characterized in that, specifically comprise the steps:
(1) with parts by weight, carried out according to a certain percentage being mixed to get Traditional Chinese drug mixture by following raw material, and put into distillating still; Above-described raw material and component ratio as follows: Herba bromi japonici: 3 ~ 6%, Radix Glycyrrhizae: 8 ~ 11%, Radix Scutellariae: 10 ~ 13%, Flos Matricariae chamomillae: 16 ~ 19%, Folium olive: 3 ~ 6%, arnica montana: 3 ~ 6%, Tilia cordata: 13 ~ 16%, Althaea officinalis L.: 18 ~ 21%, Paeonia suffruticosa: 8 ~ 11%.
(2) in distillating still, deionized water is added; By weight, water: Traditional Chinese drug mixture is 5.0 ~ 6.0:1;
(3) first time extracts: the temperature rise period, add thermal still, and by regulating the programming rate in the pressure and temperature control distillating still in distillating still, programming rate is 1.6 DEG C-2.6 DEG C/min to 65-85 DEG C, in this process, the pressure in distillating still is 0.25 ~ 0.35Mpa; Holding stage, regulate the pressure and temperature control in distillating still to make its temperature remain on 65-85 DEG C, the Stress control in distillating still is at 0.08 ~ 0.1MPa, and the time is 2h-3h;
(4) liquid of first time extraction is collected;
(5) deionized water adding raw material weight 2.0 ~ 3.0 times in the solid residue obtained after first time extraction process carries out second time and extracts;
(6) liquid that second time is extracted is collected;
(7) filter: the liquid being extracted acquisition first time extracts with second time the liquid obtained and merges, and with the filtration of 300-500 mesh filter screen, obtains the filtrate of removal solid residue;
(8) first time is concentrated: be 75 ~ 100 DEG C by the extracting solution that obtains after filtering in temperature, and vacuum is carry out first time concentration under the condition of 0.075 ~ 0.095Mpa, obtains concentrated solution;
(9) alcohol settling: the ethanol adding 2.2 ~ 2.7 times of concentrated solution weight in concentrated solution, at room temperature leaves standstill 24 hours after stirring, and takes out the supernatant;
(10) bioanalysis concentrates: the supernatant is carried out second time concentration under temperature 45 ~ 58 DEG C of conditions, obtains antiallergic essence.
2. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, it is characterized in that, in described methanol precipitation step, the concentration of ethanol is 92% ~ 95%.
3. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: in the described supernatant, the concentration of alcoholic solution is 50 ~ 65%.
4. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: the density of described concentrated solution is 1.0280 ~ 1.0420kg/m
3.
5. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: the density of described antiallergic essence is 1.19200 ~ 1.2080kg/m
3.
6. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: described optimum feed stock and component ratio are: Herba bromi japonici: 5%, Radix Glycyrrhizae: 10%, Radix Scutellariae; 12%, Flos Matricariae chamomillae: 18%, Folium olive: 5%, arnica montana: 5%, Tilia cordata: 15%, Althaea officinalis L.: 20%, Paeonia suffruticosa: 10%.
7. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: described distillating still is ultrasonic extraction tank.
8. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: after described alcohol settling, mixing time is 30 ~ 50 minutes, mixing speed: 120 ~ 150 revs/min.
9. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: what described bioanalysis concentrated employing is HACC clear liquor.
10. a kind of technique utilizing Chinese herbal medicine to prepare antiallergic essence as claimed in claim 1, is characterized in that: the moisture content of described raw material is not higher than 6%.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106307436A (en) * | 2016-08-17 | 2017-01-11 | 中国农业科学院农产品加工研究所 | Processing and preserving method of convenient marinated meat dishes |
| CN107469064A (en) * | 2016-06-08 | 2017-12-15 | 广州艾玫格生物科技有限公司 | Biological antiallergic compound |
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| JP2001139489A (en) * | 1999-11-17 | 2001-05-22 | Ichimaru Pharcos Co Ltd | Cosmetic composition |
| JP2004168705A (en) * | 2002-11-20 | 2004-06-17 | Pola Chem Ind Inc | Preparation for external use for ameliorating skin condition |
| JP2008031111A (en) * | 2006-07-31 | 2008-02-14 | Noevir Co Ltd | Arginase activity enhancer |
| CN102525853A (en) * | 2011-12-23 | 2012-07-04 | 广州市娇兰化妆品有限公司 | Compound natural plant extract with spot-removing function and preparation method and application thereof |
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Patent Citations (4)
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| JP2001139489A (en) * | 1999-11-17 | 2001-05-22 | Ichimaru Pharcos Co Ltd | Cosmetic composition |
| JP2004168705A (en) * | 2002-11-20 | 2004-06-17 | Pola Chem Ind Inc | Preparation for external use for ameliorating skin condition |
| JP2008031111A (en) * | 2006-07-31 | 2008-02-14 | Noevir Co Ltd | Arginase activity enhancer |
| CN102525853A (en) * | 2011-12-23 | 2012-07-04 | 广州市娇兰化妆品有限公司 | Compound natural plant extract with spot-removing function and preparation method and application thereof |
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| 国家食品药品监督管理局执业药师资格认证中心: "《99%的女人都在犯的护肤错误》", 31 January 2014, 中国医药科技出版社 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107469064A (en) * | 2016-06-08 | 2017-12-15 | 广州艾玫格生物科技有限公司 | Biological antiallergic compound |
| CN106307436A (en) * | 2016-08-17 | 2017-01-11 | 中国农业科学院农产品加工研究所 | Processing and preserving method of convenient marinated meat dishes |
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