CN105147570A - Frosted whitening gel capable of removing blackheads and preparation method of frosted whitening gel - Google Patents
Frosted whitening gel capable of removing blackheads and preparation method of frosted whitening gel Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses frosted whitening gel capable of removing blackheads and a preparation method of the frosted whitening gel. The gel comprises the following substances: an ice crystal forming agent, sodium alginate, polyvinyl alcohol, hydroxypropyl methyl cellulose, glycerinum, propylene glycol, green bean powder, silica gel, a green bean powder extract solution, a witch hazel extract solution, a myosotis extract solution, a green tea extract solution, a mulberry leaf extract solution, a bletilla striata extract solution, an alkyl glycoside surfactant APG, sorbic acid, ethylparaben and distilled water. Compared with the prior art, the frosted whitening gel capable of removing blackheads disclosed by the invention contains a plurality of nutritional ingredients; by combination with a traditional Chinese medicine extract, the problem of the blackheads is solved by a relatively mild method; the problem of the blackheads is effectively relieved after the frosted whitening gel is used for a long period of time; and the skin is relatively fine and smooth.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to clean white gel of a kind of pore cleanser frosted and preparation method thereof.
Background technology
Blackhead, also known as blackhead, is hardened fat obturator, usually appears at the position such as forehead, nose, when oils and fats gland is subject to undue stimulation, when pore is full of unnecessary oils and fats and causes obstruction, at nose and peripheral part thereof, often has greasy sensation.These oils and fatss finally can harden, then become blackhead with Oxidations such as the dust in air, dirts.
Everybody has a love of beauty, but the application on human skin of usual long small pox and blackhead is all comparatively coarse, and pore is also very large, and have a lot of oils and fats grains to block the pore opened, repeatedly brought out into small pox, serious more has rough situation.
A lot of people pore cleanser all by every means, applies some make up and covers oneself rough skin, or goes extruding with hands, hardly realizes, so only skin can be allowed to be absorbed in vicious cycle.And existing clean cleansing milk pore cleanser effect is commercially obvious not, take effect slow, substantially of little use for serious large grain blackhead.
The influence factor increased due to blackhead has multiple, such as gene genetic, ultraviolet radiation, excessive clean skin, crowded small pox, dyssecretosis, medicine, cosmetics etc., and for these factors, provide a kind of effective, the product of non-stimulated pore cleanser is very important.
Summary of the invention
For solving the problems of the technologies described above, the invention provides the clean white gel of a kind of pore cleanser frosted, containing natural component extract, effective, have no side effect.
Present invention also offers the preparation method of the clean white gel of a kind of pore cleanser frosted, the gel prepared not only effectively alleviates blackhead problem, also allows skin more fine and smooth soft.
The clean white gel of a kind of pore cleanser frosted provided by the invention, containing following material:
Described Semen phaseoli radiati extracting solution is prepared by the following method:
Take Semen phaseoli radiati appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Semen phaseoli radiati weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
Described Radix Hamamelidis Mollis extracting solution is prepared by the following method:
Take Radix Hamamelidis Mollis appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Radix Hamamelidis Mollis weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
Described Myosotis sylvatica extracting solution is prepared by the following method.
Take Myosotis sylvatica appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 8-15 times of water gaging 1st time, extract 0.5-2h, add 8-15 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-12 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Myosotis sylvatica weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
Described Rhizoma Bletillae extraction solution is prepared by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 10-18 times of water gaging 1st time, extract 0.5-2h, add 10-18 times of water gaging the 2nd time, extract 0.5-1.5h, add 8-15 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
Described green tea extractive liquor is prepared by the following method:
Take green tea appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, at every turn by three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 3-6 times of g/ml of green tea weight, filtration is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, and centrifugal 10-20min, gets the supernatant and get final product.
Described Mori folium extract is prepared by the following method:
Take Folium Mori appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 10-15 times of water gaging 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-12 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Folium Mori weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
The clean white gel preparation method of a kind of pore cleanser provided by the invention, comprises the following steps:
A) take ice crystal forming agent 0.5-1.5g, join in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 1, stand-by;
B) take sodium alginate 1.5-3g, join in 50-100ml distilled water, 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 2, stand-by;
C) weighing polyvinyl alcohol 7.5-15g, joins in 50-100ml distilled water, and 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 3, stand-by;
D) take hydroxypropyl emthylcellulose 1-2g, join in 50-100ml distilled water, 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 4, stand-by;
E) take Semen phaseoli radiati in right amount in pulverizer, after pulverizing, powder is placed in mortar again, carries out sieve and gets, obtain fine and smooth Semen phaseoli radiati powder after grinding evenly with 80-120 object sieve;
F) take Semen phaseoli radiati extracting solution 1-5ml respectively, Radix Hamamelidis Mollis extracting solution 1-5ml, Myosotis sylvatica extracting solution 1-5ml, Rhizoma Bletillae extraction solution 1-5ml, green tea extractive liquor 0.5-2ml, Mori folium extract 0.5-2ml and Semen phaseoli radiati powder 0.5-1.5g, stir, obtain mixed liquor;
G) get previous swelling good gel 1, gel 2, gel 3, gel 4, mixing, add 2-5ml glycerol, 2-5ml propylene glycol, stirs;
H) add step f again) mixed liquor prepared, and add 1-3mg silica gel, stir, compound;
I) sorbic acid 0.01-1mg, ethyl hydroxybenzoate 0.01-1mg is taken, add 1-3ml distilled water, 60-90 DEG C of heating makes it dissolve, step h is added after to be dissolved) in gained compound, continue to add 0.5-1.5g alkyl glucoside surfactant APG, mix homogeneously, obtains the clean white gel of pore cleanser frosted.
Various compositions in the present invention are as follows:
Concha Ostreae alkali in Semen phaseoli radiati extract and different Concha Ostreae alkali have remarkable clean moistening effect, remove sebum function outstanding, effectively can remove the deep layer refuse of skin.Meanwhile, Semen phaseoli radiati has moisturizing ingredient and mineral, and supply skin adequate water, natural polysaccharides forms moisture film transparent, springy at skin surface.Compendium of Material Medica is recorded: " Semen phaseoli radiati abnormal smells from the patient is sweet cold, nontoxic ... to separate all medicinal herbs, the oxen and horses, all poison of metal and stone." mean, gold, stone, arsenicum, all poison of vegetation in Semen phaseoli radiati energy antidote.Therefore, can help to discharge the facial industrial pollution be subject to.
Radix Hamamelidis Mollis includes tannin matter can regulate sebum secretion, Hydrolyzed Protein and Milk Protein, the effect of have calmness, pacifying, and is improved effect, effectively can helps the regeneration capacity at skin night to be full of cracks, sunburn, acne.Because releiving, restrain, antibacterial, defying age, because there being the significant curative effect of convergence control oil, sterilization, for children in adolescence or the more serious skin of fuel-displaced situation, be only selection.
Myosotis sylvatica is rich in vitamin C, can slow down the generation of wrinkle and black speck, skin whitening, and can body metabolism be promoted, delaying cell aging, improve immunity, avoid the generation of wrinkle and black speck, particularly have certain eliminating effect to freckle, acne, skin-protecting face nursing, to enhance metabolism.
The Pseudobulbus Bletillae (Rhizoma Bletillae) is astringing to arrest bleeding Chinese medicine simply, rich in starch, glucose, Pseudobulbus Bletillae polysaccharose (Bletilla glucomannan), volatile oil, phlegmatic temperament etc., and external is embrocated, and can eliminate the vestige that acne on the face stays, and beauty treatment speckle removing, makes skin smooth seamless.The Pseudobulbus Bletillae (Rhizoma Bletillae), as the Special Traditional Chinese Medicine extract of this product, not only has effect to the improvement of skin blackhead, or natural thickening agent.
Green tea extractive liquor is the active component extracted from green tea, mainly comprises tea polyphenols etc.Tea polyphenols is water-soluble substances, washes one's face can know the greasy of face with it, and convergence pore, has sterilization, sterilizing, resisting age of skin, reduces the radiation of daylight middle-ultraviolet lamp to effects such as the damages of skin.Tea polyphenols can shielding of ultraviolet and remove the free radical of ultraviolet induction, thus the normal function of protection melanocyte, the formation of check melanin.Lipid oxidation is produced simultaneously and suppress, alleviate pigmentation.
Folium Mori have effect of heat-clearing and toxic substances removing, and it improves significantly to facial colour spot acne tool.Folium Mori are rich in the trace element of flavonoid glycoside, phenols, aminoacid, organic acid, carotene, vitamin and multiple needed by human, and this is to improving and the metabolism of regulation of skin tissue, particularly suppress Pigmented generation and develop all have positive role.
Glycerol is the most universal the most common moisturizing ingredient in cosmetics, sebum can be avoided to a certain extent to clean the problem of rear moisture-retaining capacity decline, extract humidity from air simultaneously, horny layer can be made to maintain hydration status, moisturizing effect is very good, by rear skin beauty water profit, softness, touch up very comfortable.Glycerol character gentleness can bring the effect of soft moisturizing, and safety is good, not easily causes allergy.
The surfactant that alkyl glucoside surfactant is organic monomer-glucose of utilizing nature the most extensively to exist is development of raw materials, belongs to non-ionic surface active agent, is referred to as new generation of green surfactant, can totally biodegradable.
Ice crystal forming agent gel contained by this product, sodium alginate gel, polyvinyl alcohol gel, hydroxypropyl emthylcellulose gel are all good residuites, are good thickening agent and wetting agent.Meanwhile, polyvinyl alcohol has film property, when cleaning skin, is easier to take away the blackhead at skin surface.
Gel designed by the present invention is a kind of multi-functional gel, and it is except basic cleaning function, and massaged face by fine particle in addition, film property takes away face's blackhead and dirt, has astriction simultaneously, energy pore refining, makes skin clean white salubrious.Gel-type vehicle contained in product has good moisture-keeping function; Radix Hamamelidis Mollis extracting solution can regulate sebum secretion, and having the tender effect in vain of moisturizing, be improved effect to acne, is good antioxidant; Myosotis sylvatica extracting solution can be used for treating freckle as well as acne, looks improving and the skin nourishing; Rhizoma Bletillae extraction solution has thickening property, film property, has fading effect to acne speckle print; Green tea and Folium Mori extract can remove free radical, good in oxidation resistance; Silica gel and Semen phaseoli radiati fine particle can exfoliations, and skin is infiltrated in Semen phaseoli radiati nutrition simultaneously.Above composition all has good effect for the blackhead of skin, and each composition complements each other.
The clean white gel of pore cleanser frosted provided by the invention contains multiple nutritional components, in conjunction with Chinese medicine extract, relative to pore cleanser product existing on market, solves blackhead problem with the method for milder.Life-time service, not only effectively alleviates blackhead problem, also allows skin more fine and smooth soft.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described further.
Embodiment 1
The clean white gel of a kind of pore cleanser frosted, containing following material:
The clean white gel preparation method of a kind of pore cleanser, comprises the following steps:
The preparation of 1.1 Semen phaseoli radiati extracting solution
Take Semen phaseoli radiati appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Semen phaseoli radiati weight, filtration is placed on centrifugal 20min in 4 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 1.2 Radix Hamamelidis Mollis extracting solution
Take Radix Hamamelidis Mollis appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Radix Hamamelidis Mollis weight, filtration is placed on centrifugal 15min in 5 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 1.3 Myosotis sylvatica extracting solution
Take Myosotis sylvatica appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Myosotis sylvatica weight, filtration is placed on centrifugal 15min in 4 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 1.4 Rhizoma Bletillae extraction solution
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filtration is placed on centrifugal 15min in 4 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 1.5 green tea extractive liquors
Take green tea appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of green tea weight, filtration is placed on centrifugal 15min in 5 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 1.6 Mori folium extract
Take Folium Mori appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Folium Mori weight, filtration is placed on centrifugal 15min in 5 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of the clean white gel of 1.7 pore cleanser frosteds
A) take ice crystal forming agent 0.5g, join in the beaker that 50ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 1, stand-by;
B) take sodium alginate 2g, join in the beaker that 70ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 2, stand-by;
C) weighing polyvinyl alcohol 8g, joins in the beaker that 70ml distilled water is housed, and 80 DEG C of heating in water bath, heat while stirring, and leaves standstill and makes it fully swelling, obtain gel 3, stand-by;
D) take hydroxypropyl emthylcellulose 2g, join in the beaker that 100ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 4, stand-by;
E) take Semen phaseoli radiati in right amount in pulverizer, after pulverizing, powder is placed in mortar again, carries out sieve and gets, obtain fine and smooth Semen phaseoli radiati powder after grinding evenly with 120 object sieves;
F) take Semen phaseoli radiati extracting solution 3ml respectively, Radix Hamamelidis Mollis extracting solution 3ml, Myosotis sylvatica extracting solution 3ml, Rhizoma Bletillae extraction solution 3ml, green tea extractive liquor 2ml, Mori folium extract 1ml and Semen phaseoli radiati powder 1g are placed in beaker 1, and stir;
G) get previous swelling good gel 1, gel 2, gel 3, gel 4 join in beaker 2, and add 3ml glycerol, 3ml propylene glycol, stirs with blender;
H) pour extracting solution in beaker 1 into beaker 2 again, and add 2mg silica gel, stir;
I) take sorbic acid 1mg, ethyl hydroxybenzoate 1mg, add the heating of 2ml distilled water and make it dissolve, pick and place after to be dissolved in beaker 2, add 1g alkyl glucoside surfactant APG, after mix homogeneously, namely obtain the clean white gel of pore cleanser frosted.
Embodiment 2
The clean white gel of a kind of pore cleanser frosted, containing following material:
The clean white gel preparation method of a kind of pore cleanser, comprises the following steps:
The preparation of 2.1 Semen phaseoli radiati extracting solution
Take Semen phaseoli radiati appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Semen phaseoli radiati weight, filtration is placed on centrifugal 10min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 2.2 Radix Hamamelidis Mollis extracting solution
Take Radix Hamamelidis Mollis appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Radix Hamamelidis Mollis weight, filtration is placed on centrifugal 15min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 2.3 Myosotis sylvatica extracting solution
Take Myosotis sylvatica appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Myosotis sylvatica weight, filtration is placed on centrifugal 15min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 2.4 Rhizoma Bletillae extraction solution
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filtration is placed on centrifugal 15min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 2.5 green tea extractive liquors
Take green tea appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of green tea weight, filtration is placed on centrifugal 15min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 2.6 Mori folium extract
Take Folium Mori appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Folium Mori weight, filtration is placed on centrifugal 15min in 10 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of the clean white gel of 2.7 pore cleanser frosteds
A) take ice crystal forming agent 1.5g, join in the beaker that 100ml distilled water is housed, 85 DEG C of heating in water bath, heat hot limit, limit is stirred, and leaves standstill and makes it fully swelling, obtain gel 1, stand-by;
B) take sodium alginate 3g, join in the beaker that 100ml distilled water is housed, 85 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 2, stand-by;
C) weighing polyvinyl alcohol 15g, joins in the beaker that 100ml distilled water is housed, and 85 DEG C of heating in water bath, heat while stirring, and leaves standstill and makes it fully swelling, obtain gel 3, stand-by;
D) take hydroxypropyl emthylcellulose 2g, join in the beaker that 100ml distilled water is housed, 85 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 4, stand-by;
E) take Semen phaseoli radiati in right amount in pulverizer, after pulverizing, powder is placed in mortar again, carries out sieve and gets, obtain fine and smooth Semen phaseoli radiati powder after grinding evenly with 100 object sieves;
F) take Semen phaseoli radiati extracting solution 5ml respectively, Radix Hamamelidis Mollis extracting solution 5ml, Myosotis sylvatica extracting solution 5ml, Rhizoma Bletillae extraction solution 5ml, green tea extractive liquor 2ml, Mori folium extract 2ml and Semen phaseoli radiati powder 1.5g are placed in beaker 1, and stir;
G) get previous swelling good gel 1, gel 2, gel 3, gel 4 join in beaker 2, and add 5ml glycerol, 5ml propylene glycol, stirs with blender;
H) pour extracting solution in beaker 1 into beaker 2 again, and add 3mg silica gel, stir;
I) take sorbic acid 1mg, ethyl hydroxybenzoate 1mg, add the heating of 3ml distilled water and make it dissolve, pick and place after to be dissolved in beaker 2, add 1.5g alkyl glucoside surfactant APG, after mix homogeneously, namely obtain the clean white gel of pore cleanser frosted.
Embodiment 3
The clean white gel of a kind of pore cleanser frosted, containing following material:
The clean white gel preparation method of a kind of pore cleanser, comprises the following steps:
The preparation of 3.1 Semen phaseoli radiatis
Take Semen phaseoli radiati appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 7 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Semen phaseoli radiati weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 3.2 Radix Hamamelidis Mollis extracting solution
Take Radix Hamamelidis Mollis appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 8 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Radix Hamamelidis Mollis weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 3.3 Myosotis sylvatica extracting solution
Take Myosotis sylvatica appropriate, soak 0.5h, heating decocts extraction 3 times, add 13 times of water gagings 1st time, extract 1h, add 13 times of water gagings the 2nd time, extract 1h, add 10 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Myosotis sylvatica weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 3.4 Rhizoma Bletillae extraction solution
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.5h, heating decocts extraction 3 times, add 15 times of water gagings 1st time, extract 1h, add 15 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 3.5 green tea extractive liquors
Take green tea appropriate, soak 0.5h, heating decocts extraction 3 times, add 12 times of water gagings 1st time, extract 1h, add 6 times of water gagings the 2nd time, extract 1h, add 7 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of green tea weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of 3.6 Mori folium extract
Take Folium Mori appropriate, soak 0.5h, heating decocts extraction 3 times, add 13 times of water gagings 1st time, extract 1h, add 9 times of water gagings the 2nd time, extract 1h, add 108 times of water gagings the 3rd time, extract 1h, each filtration, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Folium Mori weight, filtration is placed on centrifugal 15min in 2 DEG C of high speed centrifuges, gets the supernatant and get final product.
The preparation of the clean white gel of 3.7 pore cleanser frosteds
A) take ice crystal forming agent 0.5g, join in the beaker that 50ml distilled water is housed, 80 DEG C of heating in water bath, heat hot limit, limit is stirred, and leaves standstill and makes it fully swelling, obtain gel 1, stand-by;
B) take sodium alginate 1.5g, join in the beaker that 50ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 2, stand-by;
C) weighing polyvinyl alcohol 7.5g, joins in the beaker that 50ml distilled water is housed, and 80 DEG C of heating in water bath, heat while stirring, and leaves standstill and makes it fully swelling, obtain gel 3, stand-by;
D) take hydroxypropyl emthylcellulose 1g, join in the beaker that 50ml distilled water is housed, 80 DEG C of heating in water bath, heat while stirring, and leave standstill and make it fully swelling, obtain gel 4, stand-by;
E) take Semen phaseoli radiati in right amount in pulverizer, after pulverizing, powder is placed in mortar again, carries out sieve and gets, obtain fine and smooth Semen phaseoli radiati powder after grinding evenly with 100 object sieves;
F) take Semen phaseoli radiati extracting solution 1ml respectively, Radix Hamamelidis Mollis extracting solution 1ml, Myosotis sylvatica extracting solution 1ml, Rhizoma Bletillae extraction solution 1ml, green tea extractive liquor 1ml, Mori folium extract 1ml and Semen phaseoli radiati powder 0.5g are placed in beaker 1, and stir;
G) get previous swelling good gel 1, gel 2, gel 3, gel 4 join in beaker 2, and add 2ml glycerol, 2ml propylene glycol, stirs with blender;
H) pour extracting solution in beaker 1 into beaker 2 again, and add 1mg silica gel, stir;
I) take sorbic acid 0.09mg, ethyl hydroxybenzoate 0.09mg, add the 80 DEG C of heating of 2ml distilled water and make it dissolve, pick and place after to be dissolved in beaker 2, add 1.0g alkyl glucoside surfactant APG, after mix homogeneously, namely obtain the clean white gel of pore cleanser frosted.
Embodiment 4
The physical and chemical index of embodiment 1,2,3 is as follows:
4.1 character
The transparent light green of this product, viscosity is thicker, even particle distribution, the gel that stretchability is good.
4.2pH value checks
Get this product, measure with pH meter, recording pH value is between 6.8-7.0.
4.3 caloric test
Gel is packaged in Clear glass bottles and jars, within one month, observes without lamination in the refrigerator cold-storage of 4 DEG C.In the calorstat of 55 DEG C, put 24h, gel is without layering, the phenomenon such as spoiled.
4.4 centrifugal test
Gel is packaged in the centrifugal 20min of 3000r/min in tool plug test tube, without lamination.
4.5 room temperatures place experiment
Embodiment gel is placed in Clear glass bottles and jars, and room temperature leaves standstill investigation 6 months, without lamination, with after feel unchanged, abnormal smells from the patient is unchanged.
4.6 irritation tests, anaphylaxis are tested
White mice back cuts off hair, smears the gel prepared by embodiment respectively in cutting plucked position, and is not coated with position and compares, and result does not have zest and anaphylaxis.
Gel prepared by Example is applied in volunteer (16-50 year, 80 people) gesture and facial expression in right amount, observes, all do not occur rubescent, dermexanthesis, foaming phenomena after spending 30 minutes.
Embodiment 5
This gel resultant effect is investigated
Trial effect is below utilized to carry out the effect of the gel that Evaluation operation example 1,2,3 produces.Adopt public-opinion poll point system, choose 100 20-40 year age bracket women as object on probation, be divided into arbitrarily two groups, respectively with gel cleaning face prepared by embodiment 1,2,3.Every day uses twice sooner or later, and service time is two months.Every result of use total score is 5 points: 5 be divided into best result, represents very well, very satisfaction; 4 are divided into better; 3 are divided into and can accept; Less than 3 points is bad, can not accept.It is below every average.The results are shown in Table 1:
Table 1 resultant effect is investigated
In sum, the gel exquisiteness obtained by the present invention is soft and smooth, has good pore cleanser effect, moisture retention, whitening, and during use, sensation is fine and smooth soft and smooth, and good by rear skin elasticity, water is tender glossy.
Claims (8)
1. the clean white gel of pore cleanser frosted, is characterized in that, the clean white gel of described pore cleanser frosted contains following material:
2. the clean white gel of pore cleanser frosted according to claim 1, it is characterized in that, described Semen phaseoli radiati extracting solution is prepared by the following method:
Take Semen phaseoli radiati appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Semen phaseoli radiati weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
3. the clean white gel of pore cleanser frosted according to claim 1 and 2, it is characterized in that, described Radix Hamamelidis Mollis extracting solution is prepared by the following method:
Take Radix Hamamelidis Mollis appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Radix Hamamelidis Mollis weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
4. the clean white gel of pore cleanser frosted according to claim 1 and 2, it is characterized in that, described Myosotis sylvatica extracting solution is prepared by the following method.
Take Myosotis sylvatica appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 8-15 times of water gaging 1st time, extract 0.5-2h, add 8-15 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-12 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Myosotis sylvatica weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
5. the clean white gel of pore cleanser frosted according to claim 1 and 2, is characterized in that,
Described Rhizoma Bletillae extraction solution is prepared by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 10-18 times of water gaging 1st time, extract 0.5-2h, add 10-18 times of water gaging the 2nd time, extract 0.5-1.5h, add 8-15 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
6. the clean white gel of pore cleanser frosted according to claim 1 and 2, it is characterized in that, described green tea extractive liquor is prepared by the following method:
Take green tea appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 6-12 times of water gaging 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, at every turn by three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate is to 3-6 times of g/ml of green tea weight, filtration is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, and centrifugal 10-20min, gets the supernatant and get final product.
7. the clean white gel of pore cleanser frosted according to claim 1 and 2, it is characterized in that, described Mori folium extract is prepared by the following method:
Take Folium Mori appropriate, soak 0.15-0.8h, heating decocts extraction 3 times, add 10-15 times of water gaging 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-12 times of water gaging the 3rd time, extract 0.5-1.5h, each use three layers of filtered through gauze, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Folium Mori weight, filters and is placed in 2-10 DEG C of low-temperature and high-speed centrifuge, centrifugal 10-20min, gets the supernatant and get final product.
8. the clean white gel preparation method of the pore cleanser described in any one of claim 1-7, it is characterized in that, described preparation method comprises the following steps:
A) take ice crystal forming agent 0.5-1.5g, join in 50-100ml distilled water, 60-80 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 1, stand-by;
B) take sodium alginate 1.5-3g, join in 50-100ml distilled water, 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 2, stand-by;
C) weighing polyvinyl alcohol 7.5-15g, joins in 50-100ml distilled water, and 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 3, stand-by;
D) take hydroxypropyl emthylcellulose 1-2g, join in 50-100ml distilled water, 60-90 DEG C of heating in water bath, heats while stirring, and leaves standstill and makes it fully swelling, obtain gel 4, stand-by;
E) take Semen phaseoli radiati in right amount in pulverizer, after pulverizing, powder is placed in mortar again, carries out sieve and gets, obtain fine and smooth Semen phaseoli radiati powder after grinding evenly with 80-120 object sieve;
F) take Semen phaseoli radiati extracting solution 1-5ml respectively, Radix Hamamelidis Mollis extracting solution 1-5ml, Myosotis sylvatica extracting solution 1-5ml, Rhizoma Bletillae extraction solution 1-5ml, green tea extractive liquor 0.5-2ml, Mori folium extract 0.5-2ml and Semen phaseoli radiati powder 0.5-1.5g, stir, obtain mixed liquor;
G) get previous swelling good gel 1, gel 2, gel 3, gel 4, mixing, add 2-5ml glycerol, 2-5ml propylene glycol, stirs;
H) add step f again) mixed liquor prepared, and add 1-3mg silica gel, stir, compound;
I) sorbic acid 0.01-1mg, ethyl hydroxybenzoate 0.01-1mg is taken, add 1-3ml distilled water, 60-90 DEG C of heating makes it dissolve, step h is added after to be dissolved) in gained compound, continue to add 0.5-1.5g alkyl glucoside surfactant APG, mix homogeneously, obtains the clean white gel of pore cleanser frosted.
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Effective date of registration: 20190415 Address after: 510000 Xinghe Road, Xicheng Industrial Zone, Renhe Town, Baiyun District, Guangzhou, Guangdong, China Patentee after: Guangzhou Tianyi Cosmetics Co., Ltd. Address before: 241002 No. 22 Wenchang West Road, Yijiang Higher Education Park, Wuhu, Anhui Patentee before: Wannan Medical College |