CN105113235A - Slow-release aromatic for leather and preparation method of slow-release aromatic - Google Patents
Slow-release aromatic for leather and preparation method of slow-release aromatic Download PDFInfo
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- CN105113235A CN105113235A CN201510558481.2A CN201510558481A CN105113235A CN 105113235 A CN105113235 A CN 105113235A CN 201510558481 A CN201510558481 A CN 201510558481A CN 105113235 A CN105113235 A CN 105113235A
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Abstract
The invention discloses slow-release aromatic for leather. The slow-release aromatic comprises the following raw materials in percentage by weight: 0.3-1.2% of essence, 5-15% of hydroxypropyl-beta-cyclodextrin, 0.3-0.5% of arabic gum, 0.3-0.6% of Span80, 0.3-0.8% of Twain40, 5-10% of acrylic resin and the balance of deionized water. The invention further provides a preparation method of the slow-release aromatic. The preparation method comprises the following steps: adding essence, Span80 and Twain40 into a reaction container, further adding deionized water, and uniformly mixing so as to obtain essence emulsion; adding hydroxypropyl-beta-cyclodextrin into the essence emulsion, stirring to uniformly disperse the essence, adding arabic gum and acrylic resin, and continuously stirring, thereby obtaining the slow-release aromatic for leather. The slow-release aromatic disclosed by the invention can be used in leather wet processing and coating procedures, so that the perfumed leather is natural, harmonious and long-lasting in fragrance.
Description
Technical field
The invention belongs to chemical field, relate to a kind of aromatic, specifically a kind of leather slow release aromatic and preparation method thereof.
Background technology
Leather be with a class with natural raw hide for raw material, through the not perishable Animal Skin of sex change of the physics such as depilation and tanning, chemical process gained, belong to natural macromolecular material, there is higher snugness of fit and aesthetic property, along with the raising of people's daily life quality, leather and fur products has become contemporary society's identity and status symbol, occupies an important position in national economy.On the one hand, raw hide, in the process through processing, with the addition of retanning agent and various functionalization component existence bad smell more or less, can cover these smells, the leather that production quality is higher by perfuming process; On the other hand, luxurious leather and fur products, in today of economic development, as showing luxurious identity status symbol, being given leather a kind of simple and elegant and comfortable smell by preparing aroma type leather, will be improved the desire to purchase of consumer, strengthening the favor in market.But essence mainly directly to add in covering with paint workshop section or wet processing workshop section and carries out perfuming by existing fragrant leather, after perfuming, the fragrance fragrance remaining time of leather is shorter.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of leather slow release aromatic and preparation method thereof, described this leather slow release aromatic and preparation method thereof solves the technical problem that leather of the prior art has peculiar smell.
The invention provides a kind of leather slow release aromatic, count by weight percentage, composition and the content of its raw material are as follows:
Essence 0.3%-1.2%,
Hydroxypropylβ-cyclodextrin 5%-15%,
Arabic gum 0.3%-0.5%,
Sorbester p17 0.3%-0.6%,
Polysorbate40 0.3%-0.8%,
Acrylic resin 5%-10%,
Deionized water surplus.
Further, described essence is tuberose essence, osmanthus flower fragrance, cream jasmin france or flavoring rose essence.
Present invention also offers the preparation method of above-mentioned a kind of leather slow release aromatic, comprise the steps:
1) essence, hydroxypropylβ-cyclodextrin, Arabic gum, sorbester p17, polysorbate40, acrylic resin, deionized water is taken according to weight ratio;
2) essence, sorbester p17, polysorbate40 are added in a reaction vessel, then add deionized water, low whipping speed is stir 1-3h under 500-700r/min, mixes and obtains essence emulsion;
3) hydroxypropylβ-cyclodextrin is joined in described essence emulsion, low whipping speed is continue under 500-700r/min to stir 0.5-2h, essence is uniformly dispersed, adds Arabic gum and acrylic resin subsequently, continue to stir 1-2h, namely obtain leather slow release aromatic.
The present invention makes essence emulsification by the method for emulsification, and solubilising enters in the micella of emulsion.The hydroxypropylβ-cyclodextrin added in addition has special cavity structure, inner hydrophobic, external hydrophilic, utilizes this class formation to be also conducive in the coated air inlet cavity of essence.Arabic gum contributes to the stable of essence emulsion and hydroxypropylβ-cyclodextrin, and acrylic resin one class polyvinyl, can form the structure of interpenetrating networks after the drying, contribute to the slow releasing of essence.
Leather slow release aromatic of the present invention can be applicable to leather finish and wet processing workshop section, and compatibility is good, easy to use, and the fragrant leather fragrance obtained is comfortable, coordination, and effectively can hide leather self peculiar smell, fragrance remaining time can reach 30-60 days.
The present invention compares with prior art, and its technological progress is significant.Aromatic of the present invention can be applicable to leather wet processing and covers with paint, lacquer, colour wash, etc. workshop section, and after making perfuming, the fragrance of leather is coordinated naturally, and lasting is lasting.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but do not limit the present invention.
embodiment 1
A kind of leather slow release aromatic, count by weight percentage, composition and the content of its raw material are as follows:
Tuberose essence 0.3%
Hydroxypropylβ-cyclodextrin 5%
Arabic gum 0.3%
Sorbester p17 0.3%
Polysorbate40 0.3%
Acrylic resin 5%
Deionized water 88.8%
The preparation method of above-mentioned a kind of leather slow release aromatic comprises the steps:
(1), by tuberose essence, sorbester p17, polysorbate40 add in beaker, then add deionized water, low whipping speed is stir 1h under 500r/min, mixes and obtains essence emulsion;
(2), hydroxypropylβ-cyclodextrin is joined in the essence emulsion that operation (1) obtains, low whipping speed is continue under 500r/min to stir 1h, essence is uniformly dispersed, adds Arabic gum and acrylic resin subsequently, continue to stir 2h, namely obtain leather slow release aromatic.
The present invention has prepared a kind of leather slow release aromatic, is directly applied to leather greasing technique, and the tuberose fragrance of the fragrant leather obtained is remarkable and smell is comfortable pleasant, effectively covers and improves the original smell of leather; Fragrance remaining time is long, has good slow release effect, places and still has significant tuberose fragrance after 30 days.
embodiment 2
A kind of leather slow release aromatic, count by weight percentage, composition and the content of its raw material are as follows:
Osmanthus flower fragrance 0.9%
Hydroxypropylβ-cyclodextrin 15%
Arabic gum 0.5%
Sorbester p17 0.6%
Polysorbate40 0.8%
Acrylic resin 10%
Deionized water 72.2%
The preparation method of above-mentioned a kind of leather slow release aromatic comprises the steps:
(1), by osmanthus flower fragrance, sorbester p17, polysorbate40 add in beaker, then add deionized water, low whipping speed is stir 2h under 700r/min, mixes and obtains osmanthus flower fragrance emulsion;
(2), hydroxypropylβ-cyclodextrin is joined in the osmanthus flower fragrance emulsion that operation (1) obtains, low whipping speed is continue under 700r/min to stir 1h, osmanthus flower fragrance is uniformly dispersed, add Arabic gum and acrylic resin subsequently, continue to stir 1h, namely obtain leather slow release aromatic.
The present invention has prepared a kind of leather slow release aromatic, is directly applied to leather finish technique, and the sweet osmanthus fragrance of the fragrant leather obtained is remarkable and smell is comfortable pleasant, effectively covers and improves the original smell of leather; Fragrance remaining time is long, has good slow release effect, places and still has significant sweet osmanthus fragrance after 60 days.
embodiment 3
A kind of leather slow release aromatic, count by weight percentage, composition and the content of its raw material are as follows:
Cream jasmin france 1.2%
Hydroxypropylβ-cyclodextrin 10%
Arabic gum 0.4%
Sorbester p17 0.5%
Polysorbate40 0.7%
Acrylic resin 9%
Deionized water 78.2%
The preparation method of above-mentioned a kind of leather slow release aromatic comprises the steps:
(1), by cream jasmin france, sorbester p17, polysorbate40 add in beaker, then add deionized water, low whipping speed is stir 2h under 600r/min, mixes and obtains essence emulsion;
(2), hydroxypropylβ-cyclodextrin is joined in the cream jasmin france emulsion that operation (1) obtains, low whipping speed is continue under 600r/min to stir 1h, essence is uniformly dispersed, adds Arabic gum and acrylic resin subsequently, continue to stir 1h, namely obtain leather slow release aromatic.
The present invention has prepared a kind of leather slow release aromatic, is directly applied to leather greasing technique, and the jasmine fragrance of the fragrant leather obtained is remarkable and smell is comfortable pleasant, effectively covers and improves the original smell of leather; Fragrance remaining time is long, has good slow release effect, places and still has significant jasmine fragrance after 30 days.
embodiment 4
A kind of leather slow release aromatic, count by weight percentage, composition and the content of its raw material are as follows:
Flavoring rose essence 0.8%
Hydroxypropylβ-cyclodextrin 12%
Arabic gum 0.4%
Sorbester p17 0.5%
Polysorbate40 0.5%
Acrylic resin 10%
Deionized water 75.8%
The preparation method of above-mentioned a kind of leather slow release aromatic comprises the steps:
(1), by flavoring rose essence, sorbester p17, polysorbate40 add in beaker, then add deionized water, low whipping speed is stir 2h under 550r/min, mixes and obtains essence emulsion;
(2), hydroxypropylβ-cyclodextrin is joined in the essence emulsion that operation (1) obtains, low whipping speed is continue under 550r/min to stir 1h, essence is uniformly dispersed, adds Arabic gum and acrylic resin subsequently, continue to stir 2h, namely obtain leather slow release aromatic.
The present invention has prepared a kind of leather slow release aromatic, is directly applied to leather finish technique, and the rose fragrance of the fragrant leather obtained is remarkable and smell is comfortable pleasant, effectively covers and improves the original smell of leather; Fragrance remaining time is long, has good slow release effect, places and still has significant jasmine fragrance after 45 days.
Claims (3)
1. a leather slow release aromatic, is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Essence 0.3%-1.2%,
Hydroxypropylβ-cyclodextrin 5%-15%,
Arabic gum 0.3%-0.5%,
Sorbester p17 0.3%-0.6%,
Polysorbate40 0.3%-0.8%,
Acrylic resin 5%-10%,
Deionized water surplus.
2. a kind of leather slow release aromatic as claimed in claim 1, is characterized in that: described essence is tuberose essence, osmanthus flower fragrance, cream jasmin france or flavoring rose essence.
3. the preparation method of a kind of leather slow release aromatic according to claim 1, is characterized in that comprising the steps:
1) essence, hydroxypropylβ-cyclodextrin, Arabic gum, sorbester p17, polysorbate40, acrylic resin, deionized water is taken according to weight ratio;
2) essence, sorbester p17, polysorbate40 are added in a reaction vessel, then add deionized water, low whipping speed is stir 1-3h under 500-700r/min, mixes and obtains essence emulsion;
3) hydroxypropylβ-cyclodextrin is joined in described essence emulsion, low whipping speed is continue under 500-700r/min to stir 0.5-2h, essence is uniformly dispersed, adds Arabic gum and acrylic resin subsequently, continue to stir 1-2h, namely obtain leather slow release aromatic.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510558481.2A CN105113235A (en) | 2015-09-06 | 2015-09-06 | Slow-release aromatic for leather and preparation method of slow-release aromatic |
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| CN201510558481.2A CN105113235A (en) | 2015-09-06 | 2015-09-06 | Slow-release aromatic for leather and preparation method of slow-release aromatic |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105567426A (en) * | 2016-02-29 | 2016-05-11 | 上海应用技术学院 | Sweet osmanthus sustained-release essence and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095395A (en) * | 1993-05-20 | 1994-11-23 | 奇英精细化工(北京)有限公司 | Liquid protection agent for leather products and preparation method |
| CN1141981A (en) * | 1995-10-28 | 1997-02-05 | 刘福元 | Coating agent to make fabric stiff |
| CN1813103A (en) * | 2003-06-26 | 2006-08-02 | 西巴特殊化学品控股有限公司 | Aqueous liquid compositions of cyclodextrine or cyclodextrine derivatives and a process using the said composition |
| CN101187083A (en) * | 2007-12-04 | 2008-05-28 | 华东理工大学 | Fragrant artificial lawn fiber and its preparation method |
| CN102744924A (en) * | 2012-07-27 | 2012-10-24 | 山东泰山金润塑胶制品有限公司 | Odor release type cushion for recreation and manufacturing method of odor release type cushion for recreation |
| CN103114459A (en) * | 2013-03-11 | 2013-05-22 | 广西鑫深科技有限公司 | Fragrant artificial leather and preparation method thereof |
| CN103666287A (en) * | 2013-11-29 | 2014-03-26 | 江苏中新资源集团有限公司 | Leather brightener and preparation method thereof |
| CN104233833A (en) * | 2014-09-09 | 2014-12-24 | 江阴龙盛塑胶有限公司 | Double-faced flocked artificial leather |
| CN104312726A (en) * | 2014-10-27 | 2015-01-28 | 浙江理工大学 | Preparation method of essence microcapsules for leather bacteriostasis |
-
2015
- 2015-09-06 CN CN201510558481.2A patent/CN105113235A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095395A (en) * | 1993-05-20 | 1994-11-23 | 奇英精细化工(北京)有限公司 | Liquid protection agent for leather products and preparation method |
| CN1141981A (en) * | 1995-10-28 | 1997-02-05 | 刘福元 | Coating agent to make fabric stiff |
| CN1813103A (en) * | 2003-06-26 | 2006-08-02 | 西巴特殊化学品控股有限公司 | Aqueous liquid compositions of cyclodextrine or cyclodextrine derivatives and a process using the said composition |
| CN101187083A (en) * | 2007-12-04 | 2008-05-28 | 华东理工大学 | Fragrant artificial lawn fiber and its preparation method |
| CN102744924A (en) * | 2012-07-27 | 2012-10-24 | 山东泰山金润塑胶制品有限公司 | Odor release type cushion for recreation and manufacturing method of odor release type cushion for recreation |
| CN103114459A (en) * | 2013-03-11 | 2013-05-22 | 广西鑫深科技有限公司 | Fragrant artificial leather and preparation method thereof |
| CN103666287A (en) * | 2013-11-29 | 2014-03-26 | 江苏中新资源集团有限公司 | Leather brightener and preparation method thereof |
| CN104233833A (en) * | 2014-09-09 | 2014-12-24 | 江阴龙盛塑胶有限公司 | Double-faced flocked artificial leather |
| CN104312726A (en) * | 2014-10-27 | 2015-01-28 | 浙江理工大学 | Preparation method of essence microcapsules for leather bacteriostasis |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105567426A (en) * | 2016-02-29 | 2016-05-11 | 上海应用技术学院 | Sweet osmanthus sustained-release essence and preparation method thereof |
| CN105567426B (en) * | 2016-02-29 | 2019-06-28 | 上海应用技术学院 | A kind of sweet osmanthus sustained release essence and preparation method thereof |
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Application publication date: 20151202 |
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