CN106833976A - A kind of method that silk fibroin protein solution prepares fibroin essential oil handmade soap - Google Patents
A kind of method that silk fibroin protein solution prepares fibroin essential oil handmade soap Download PDFInfo
- Publication number
- CN106833976A CN106833976A CN201611155599.1A CN201611155599A CN106833976A CN 106833976 A CN106833976 A CN 106833976A CN 201611155599 A CN201611155599 A CN 201611155599A CN 106833976 A CN106833976 A CN 106833976A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- soap
- silk fibroin
- fibroin
- handmade soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/40—Proteins
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
Abstract
The invention discloses a kind of method that fibroin essential oil handmade soap is prepared with silk fibroin protein solution, configuration concentration is 0.5% 3.5% silk fibroin protein solution, by silk fibroin protein solution with liquefaction soap base according to 1mL silk fibroin protein solutions:1.0g soap bases -1mL silk fibroin solutions:The ratio mixing of 3.0g soap bases, add pigment, essential oil and olive oil, pH is adjusted to neutral and alkali using vitamin E, the steps such as a period of time are stood after gentle agitation, the present invention has power consumption low in whole processing procedure, biological safety is high, it is cheap, simple to operate, the advantage such as environmentally safe, by fibroin handmade soap obtained in the invention, there are greater advantages on moist moistening effect after use.
Description
Technical field
The invention belongs to the processing method of fibroin albumen, specifically, it is related to one kind silk fibroin protein solution to prepare fibroin
The method of essential oil handmade soap.
Background technology
Shi Chansi big countries of China, carry out silk this year except applying in addition to traditional field of textiles, more because of its good mechanics
Performance, superior biocompatibility, degradability and various and relatively simple processing and fabricating mode also have regulatable structure
The advantages of, impressive progress is also achieved in the application and development of biomedicine field, also just because fibroin albumen is in bio-medical material
Application, be that its application on skin care item provides the foundation.
Silk fiber is made a kind of white or flaxen powdery macromolecule protein through hydrolysis, purification, crushing, drying, interior
Containing ten several amino acid, with good hygroscopicity and moisture retention, good permeability, adhesive force is strong, can be with the change of temperature and humidity
Change and absorb or release moisture, the balance of Hydrophile-Lipophile can be kept, reflected light can be reduced, absorb ultraviolet, to protection skin, prevent
Only dry skin, tanned, sunburn have special efficacy.The skin of people can be made to keep growing commonly using the cosmetics of addition fibroin powder
Profit, tender white, high resilience, increase natural colour, anti-aging.
Handmade soap, is exactly that oneself DIY makes perfumed soap.Only need to grease, NaOH, 3 kinds of materials of water.Manual perfumed soap both can use
Wash one's face, remove ornaments and formal dress, can be used as taking a shower again and use.The foam of Manual perfumed soap is fine and smooth abundant, can thoroughly remove the greasy dirt of pore depths.Make
Skin moistens gloss, high resilience.Preparation method is also classified into two kinds, hot preparation method and cold preparation method, and heat system forms typically all common
Essential oil handmade soap；And with cold preparation method it is cold system, referred to as cold congealed fat handmade soap processed；They expect the preparation method cycle from former material
It is completely different, it may also be said to be as far apart as heaven and earth.Essential oil soap makes fast mostly into translucent, and colourful floats very much
It is bright；Cold congealed fat soap fabrication cycle processed is long, not gaudy.
The handmade soap being made of silk fibroin protein solution using this method has good hygroscopicity and moisture retention, can play class
The effect of NMF (Natural moistariz-ing factor, NMF) in keratoderma is similar to, skin is prevented
Corrugation.And have splendid nutrition, moisten, moisturizing, sun-screening function, and the physiological function and activity of skin can be strengthened, make skin
It is soft, soft, glossy, high resilience.
The content of the invention
The present invention is just being directed to the vacancy field that the characteristic and existing handmade soap of fibroin albumen make, and have developed one kind
Process is simple, treatment is conveniently and the main component with nourishing, moisturizing, anti-sunlight function is the handmade soap preparation of fibroin albumen
Method.
To achieve these goals, concrete technical scheme of the invention is as follows：
The invention discloses a kind of method that essential oil handmade soap is prepared with fibroin albumen, specific preparation process is as follows：
1) configuration concentration is the silk fibroin protein solution of 0.5%-3.5%；2) by silk fibroin protein solution with liquefaction soap base according to
1mL silk fibroin protein solutions:1.0g soap bases -1mL silk fibroin solutions:The ratio mixing of 3.0g soap bases, adds pigment, essential oil and olive
Oil, neutral and alkali is adjusted to using vitamin E by pH, and a period of time is stood after gentle agitation；When ratio is too low, the taste of product is reduced
Lubricant nature energy, glossiness and blebbing amount；When ratio is too high, soap base is excessively dilute to cause handmade soap hardness not enough, adds essential oil.
3) solution that will be mixed stands solidification a period of time in being injected into mould, takes out the handmade soap that must be cured.
Used as further improving, silk fibroin protein solution of the present invention is silk fibroin protein solution prepared by fresh extractor
Or by the obtained silk fibroin protein solution of silk fibroin powder dissolving.When for fresh extractor, then fibroin albumen and deionized water
Ratio is 1:50-1:100, and purification of dialysing；When bath raio is too small, the fibroin concentration extracted is too low, cause water, heat and when
Between waste, influence using effect, economic benefit decline；When bath raio is too high, fibroin extracts and not exclusively causes to waste, and improves into
, if silk fibroin powder dissolves, be then dissolved in silk fibroin powder in deionized water by this.
Used as further improving, fibroin albumen of the present invention is silk fibroin protein or tussore silk fibroin.
Used as further improving, liquid soap base of the present invention is Transparent soap base or milky soap base, using microwave
The mode of heating or external heat is formed.
Used as further improving, the pigment used by the present invention is natural pigment, essential oil dripping quantity be 0.5-1.5 drops/
100mL.Natural pigment is natural pigment harmless to the body, and color is various, and changeable dripping quantity or combination as needed is added dropwise,
So as to regulate and control the color of handmade soap, when essential oil concentration being added dropwise being too high, with certain corrosivity and raising cost；When dropwise addition essential oil
When concentration is too low, essential oil effect is not notable, and influences the taste of handmade soap.
Used as further improving, the olive oil quantity that the present invention is added dropwise is 0.15mL/100mL -0.5mL/100mL；
Excessive concentration causes the hardness of handmade soap to decline, and the too low lubricant effect for causing handmade soap of concentration is inadequate.
Used as further improving, what the essential oil that the present invention is added dropwise included meeting national standard is applied to each of cosmetics
Class essential oil such as tea tree ethereal oil, Lavender, Rosa Damascana, refined jasmine oil etc..Without under the conditions of hypersensitive, suitable concn
All kinds of essential oils have relieving mood, anti-oxidant, antibacterial bacteriostatic, mosquito dispersing and other effects.
Used as further improving, it is 7-9 that the present invention is added dropwise vitamin E modulation pH, the pH for being adjusted；When pH is acidity
When, handmade soap has certain corrosivity, and using effect is poor；When pH alkalescence is too strong, moisturizing effect is reduced.
Used as further improving, agitating mode of the present invention is at the uniform velocity soft thoroughly stirring 0.25h-2h；When stirring
When mixing not thorough, solution mixing is uneven to cause layering, when stirring overweight, a large amount of aeration craft is produced in whipping process
The quality of soap, when the time is too short, handmade soap solidification is incomplete, and take out causes alteration of form by force, when overlong time then increases
Between cost, reduce production efficiency.
Compared with prior art, the present invention has following prominent characteristics：
(1) present invention is low with power consumption in whole processing procedure, and biological safety is high, cheap, side simple to operate
Just, the advantage such as environmentally safe；
(2) by fibroin handmade soap obtained in the invention have nourishings, moisturizing, the biological characteristics of whitening and uniformly it is sparkling and crystal-clear
Bright physical property；
(3) by fibroin handmade soap obtained in the invention, exclusive use can just reach target property；
(4) by fibroin essential oil handmade soap obtained in the invention, the change of the species according to addition essential oil disappears with sterilization
The additional benefits such as scorching, convergence pore, relieving mood, natural mosquito expelling.Suitable for the skin of different qualities, such as oiliness and acne
Skin, Dry etc., can clear the head, and rejuvenate, anti-depression；
(5) by fibroin handmade soap obtained in the invention, there are greater advantages on moist moistening effect after use；
(6) by fibroin handmade soap obtained in the invention, can be produced according to user preferences of different colors, different shapes
Various styles；
(7) whole to prepare reaction condition gentle, it is to avoid uses organic solvent pollution on the environment, operating procedure letter
It is single.
Specific embodiment
It is of the invention main by following scheme implementation：
(1) silk fibroin solution is added in the Transparent soap base of a certain amount of thawing that with the addition of base oil and essential oil etc., is made into
Finite concentration, being stirred continuously is well mixed it, pours into mould after the demoulding after its cooled and solidified.
(2) silk fibroin solution is added in the translucent soap base of a certain amount of thawing that with the addition of base oil and essential oil etc., is matched somebody with somebody
Into finite concentration, being stirred continuously is well mixed it, pours into mould after the demoulding after its cooled and solidified.
Technical scheme is described in further detail below by specific embodiment, following examples are right
It is of the invention explanation and the invention is not limited in following examples.
Embodiment 1
(1) respectively by fibroin albumen and water according to 1:50、1:75、1:100 bath raio extracts silk fibroin protein solution, carries out
Analysis purification
(2) by 400g Transparent soap base micro-wave oven heating and meltings.
(3) 200mL silk fibroin protein solutions and 2ml olive oil, Rosa Damascana 0.5ml are added.
(4) test pH is 7.2, without vitamin C.
(5) scrape off soap lye blibbing and pour into ready silica gel mould.
(6) 0.5h, the complete cooled and solidified of soap lye, the demoulding are placed.
(7) handmade soap is wrapped in the dry place storage in cool place 3-5 days with preservative film, you can use.
Embodiment 2
(1) weigh 5.25g fibroin powders to be dissolved in 150g deionized waters, stirring is to being completely dissolved.
(2) weigh 100g translucent soaps to be based in beaker, heating by electric cooker melts.
(3) 100ml silk fibroin solutions are added, olive oil 1.5ml, tea tree ethereal oil 0.25ml, natural purple pigment is added
0.3ml。
(4) test pH is 7.8, adds 1/4 vitamin C for crushing and being dissolved in 2ml water.
(5) scrape off soap lye blibbing and pour into ready silica gel mould.
(6) 0.25h, the complete cooled and solidified of soap lye, the demoulding are placed.
(7) handmade soap is wrapped in the dry place storage in cool place 3-5 days with preservative film, you can use.
Embodiment 3
(1) by fibroin albumen and water according to 1:75 bath raioes extract silk fibroin protein solution, carry out dialysis purification
(2) weigh 450g translucent soaps to be based in beaker, heating by electric cooker melts.
(3) 150ml silk fibroin solutions are added, after being well mixed, 100mL mixed liquors is taken respectively and is fitted into 5 beakers, added respectively
Enter olive oil 0.15mL, 0.25mL, 0.3mL, 0.4mL, 0.5mL, tea tree ethereal oil 0.8ml, natural purple pigment 1ml.
(4) test pH is 7.2, without vitamin C.
(5) scrape off soap lye blibbing and pour into ready silica gel mould.
(6) 4h, the complete cooled and solidified of soap lye, the demoulding are placed.
(7) handmade soap is wrapped in the dry place storage in cool place 3-5 days with preservative film, you can use.
Finally, in addition it is also necessary to it is noted that listed above is only several specific embodiments of the invention.Obviously, the present invention
Above example is not limited to, there can also be many deformations.One of ordinary skill in the art can be straight from present disclosure
The all deformations derived or associate are connect, protection scope of the present invention is considered as.
Claims (10)
1. a kind of method that silk fibroin protein solution prepares essential oil handmade soap, it is characterised in that specific preparation process is as follows：
1) configuration concentration is the silk fibroin protein solution of 0.5%-3.5%；
2) by silk fibroin protein solution and liquefaction soap base according to 1mL silk fibroin protein solutions:1.0g soap bases -1mL silk fibroin solutions:3.0g
The ratio mixing of soap base, adds pigment, essential oil and olive oil, and pH is adjusted into neutral and alkali using vitamin E, is stood after gentle agitation
For a period of time；
3) solution that will be mixed stands solidification a period of time in being injected into mould, takes out the handmade soap that must be cured.
2. the method that fibroin albumen according to claim 1 prepares essential oil handmade soap, it is characterised in that described fibroin
Protein solution is that silk fibroin protein solution prepared by fresh extractor or silk fibroin powder dissolving are obtained, when for fresh extractor, then
The ratio of fibroin albumen and deionized water is 1:50-1:100, and purification of dialysing；If silk fibroin powder dissolves, then by fibroin
Albumen powder is dissolved in deionized water.
3. the method that fibroin albumen according to claim 1 and 2 prepares essential oil handmade soap, it is characterised in that described
Fibroin albumen is silk fibroin protein or tussore silk fibroin.
4. fibroin albumen according to claim 3 prepares the method liquid soap base of essential oil handmade soap, it is characterised in that institute
The liquid soap base stated be Transparent soap base or milky soap base using heating using microwave or external heat it is square into.
5. the method that fibroin albumen according to claim 3 prepares essential oil handmade soap, it is characterised in that pigment used
It is natural pigment, described essential oil dripping quantity is 0.5-1.5 drops/100mL.
6. the method that fibroin albumen according to claim 3 prepares essential oil handmade soap, it is characterised in that the essence being added dropwise
Oil includes meeting all kinds of essential oils for being applied to cosmetics of national standard.
7. the method that fibroin albumen according to claim 6 prepares essential oil handmade soap, it is characterised in that described is all kinds of
Essential oil is tea tree ethereal oil or Lavender or Rosa Damascana or refined jasmine oil.
8. the method that fibroin albumen according to claim 3 prepares essential oil handmade soap, it is characterised in that the olive being added dropwise
Olive oil quantity is 0.10mL/100mL -0.5mL/100mL.
9. the method that essential oil handmade soap is prepared with fibroin albumen according to claim 1 or 2 or 4 or 5 or 6 or 7 or 8, its
It is characterised by, the described pH for being adjusted is 7-9.
10. the method that fibroin albumen according to claim 9 prepares essential oil handmade soap, it is characterised in that described stirs
It is at the uniform velocity soft thoroughly stirring 0.25h-2h to mix mode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611155599.1A CN106833976A (en) | 2016-12-14 | 2016-12-14 | A kind of method that silk fibroin protein solution prepares fibroin essential oil handmade soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611155599.1A CN106833976A (en) | 2016-12-14 | 2016-12-14 | A kind of method that silk fibroin protein solution prepares fibroin essential oil handmade soap |
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| Publication Number | Publication Date |
|---|---|
| CN106833976A true CN106833976A (en) | 2017-06-13 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611155599.1A Pending CN106833976A (en) | 2016-12-14 | 2016-12-14 | A kind of method that silk fibroin protein solution prepares fibroin essential oil handmade soap |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107312654A (en) * | 2017-07-13 | 2017-11-03 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the skin repair soap containing fibroin albumen |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1080320A (en) * | 1992-06-16 | 1994-01-05 | 张许昌 | Natural silksaine proteins and vitamin soothing soap |
| JP3738247B2 (en) * | 2002-11-18 | 2006-01-25 | 株式会社オードレマン | Detergent composition containing amorphous silk fibroin |
| JP2007031635A (en) * | 2005-07-29 | 2007-02-08 | Organic Germanium Kk | Soap composition |
| CN105441227A (en) * | 2015-11-30 | 2016-03-30 | 梁宏杰 | Handmade forget-me-not soap and production method thereof |
-
2016
- 2016-12-14 CN CN201611155599.1A patent/CN106833976A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1080320A (en) * | 1992-06-16 | 1994-01-05 | 张许昌 | Natural silksaine proteins and vitamin soothing soap |
| JP3738247B2 (en) * | 2002-11-18 | 2006-01-25 | 株式会社オードレマン | Detergent composition containing amorphous silk fibroin |
| JP2007031635A (en) * | 2005-07-29 | 2007-02-08 | Organic Germanium Kk | Soap composition |
| CN105441227A (en) * | 2015-11-30 | 2016-03-30 | 梁宏杰 | Handmade forget-me-not soap and production method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 张一心 主编: "《纺织材料》", 31 December 2005, 中国纺织出版社 * |
| 杨月欣 主编: "《健康伴侣维生素E》", 31 August 2003, 北京大学医学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107312654A (en) * | 2017-07-13 | 2017-11-03 | 芜湖慧宇商贸有限公司 | A kind of preparation method of the skin repair soap containing fibroin albumen |
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Application publication date: 20170613 |
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