CN108894000A - A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application - Google Patents
A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application Download PDFInfo
- Publication number
- CN108894000A CN108894000A CN201810640253.3A CN201810640253A CN108894000A CN 108894000 A CN108894000 A CN 108894000A CN 201810640253 A CN201810640253 A CN 201810640253A CN 108894000 A CN108894000 A CN 108894000A
- Authority
- CN
- China
- Prior art keywords
- cream jasmin
- jasmin france
- synthetic leather
- spansule
- france
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0061—Organic fillers or organic fibrous fillers, e.g. ground leather waste, wood bark, cork powder, vegetable flour; Other organic compounding ingredients; Post-treatment with organic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
- D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N2211/00—Specially adapted uses
- D06N2211/12—Decorative or sun protection articles
- D06N2211/28—Artificial leather
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Textile Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Abstract
The present invention provides a kind of cream jasmin france spansule of use for synthetic leather, prepares raw materials used be calculated by mass percentage and is made of 0.50%-1.39% cream jasmin france, 3.29%-6.97% styrene, 0.33%-0.84% Tween-80,0.07%-0.14% ammonium persulfate and balance deionized water.The cream jasmin france spansule of the use for synthetic leather is to be coated to obtain to cream jasmin france using styrene as wall material by emulsion polymerization, and cream jasmin france utilization rate is 94.07%-98.69%, average grain diameter 200.8nm-315.7nm.The cream jasmin france spansule of the use for synthetic leather can be effectively improved the effumability of cream jasmin france, improve its stability, and cream jasmin france can be made persistently to discharge, it realizes the long-acting flavoring of synthetic leather, and can effectively cover the bad smell in synthetic leather and the synthetic leather after flavoring is made to have simple and elegant jasmine fragrant.
Description
Technical field
The present invention relates to a kind of sustained release essence capsule, in particular to a kind of use for synthetic leather cream jasmin france spansule and its system
Preparation Method belongs to chemical field.
Background technique
Usually using the non-woven fabrics of dipping as lamina reticularis, microvoid polyurethane layer is made synthetic leather as grain layer.Its front and back sides
It is all quite similar with natural leather and there is certain gas permeability, compared to for artificial leather closer to natural leather, therefore quilt
It is widely applied in daily life.But polyurethane has certain sharp aroma, is easy to influence the usage experience of consumer.For
This bad smell bring of improvement influences, and studying, there is the synthetic leather product of agreeable odor to have become the trend for market.
Flavors and fragrances makes an addition in food or daily necessities frequently as a kind of additive.But its is volatile, and direct flavoring fragrance is difficult to for a long time
Retain.Therefore carrying out flavoring by compound essence spansule can effectively improve residence time of the essence on synthetic leather, and
And the bad smell of product can be effectively improved.
At present synthetic leather processing process by by the polyurethane compositions in raw material be changed to the lesser aqueous polyurethane of smell with
The synthetic leather product with smaller bad smell is produced, though this method improves the thorn of organic solvent in original urethane raw
Nose smell, but bad smell possessed by polyurethane itself fails to be covered, therefore finally obtained synthetic leather product exists
Bad smell covers halfway technical problem.
Summary of the invention
An object of the present invention is to solve the problems, such as that above-mentioned synthetic leather product is provided with bad smell
A kind of cream jasmin france spansule of use for synthetic leather, the jasmine fragrance characteristic odor and synthetic leather of the use for synthetic leather spansule
In bad smell can be cooperateed with, mask the bad smell of former synthetic leather, and make the synthetic leather after flavoring with jasmine
Fragrant.
The second object of the present invention is to provide a kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather,
The preparation method is due to being embedded cream jasmin france by microcapsules technology, so that originally volatile cream jasmin france becomes steady
It is fixed, therefore have the characteristics that long-acting slow-release flavoring.
The third object of the present invention be to provide the cream jasmin france spansule of above-mentioned use for synthetic leather a kind of to synthetic leather into
The method of row flavoring processing.
Technical principle of the invention
Essence selected by the present invention is cream jasmin france.Jasmine belongs to the authentic fresh rhythm fragrance of a flower, clear fresh elegant, comfortable suitable
People.It is often applied in the flavoring of all kinds of daily necessities as one of floral notes most important in perfume industry.Cream jasmin france is special
It is obvious to levy fragrance, good cover can be played the role of to the bad smell in synthetic leather, and makes the product after flavoring with battle array
Battle array fragrance.
Further, the present invention prepares cream jasmin france spansule by emulsion polymerization, and carries out at flavoring to synthetic leather
Reason, realizes the further improvement to synthetic leather smell.
Technical solution of the present invention
A kind of use for synthetic leather cream jasmin france spansule, is calculated by mass percentage, and prepares raw materials used composition and contains
It measures as follows：
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
A kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather, includes the following steps：
(1), the preparation of cream jasmin france, steps are as follows：
By the raw materials used composition of cream jasmin france and content is prepared, by benzyl acetate, Ergol, Java Cananga Oil, first position penta
Base cinnamic aldehyde, leaf-alcohol, linalool, eugenol, benzylalcohol, phenethyl acetate, narceol and dipropylene glycol be uniformly mixed to get
Cream jasmin france；
(2), the preparation of the cream jasmin france spansule of use for synthetic leather, steps are as follows：
By preparation use for synthetic leather cream jasmin france spansule used in raw material, first by cream jasmin france, styrene, spit
Temperature -80 is add to deionized water, and under nitrogen protection, is stirred controlled at 25-35 DEG C, revolving speed for 500rpm/min
It is warming up to 75 DEG C after 20-40min, ammonium persulfate is then added, continues controlled at 75 DEG C, revolving speed to be 500rpm/min progress
React 3h, the cream jasmin france spansule being then dried again controlled at 20-25 DEG C to get use for synthetic leather.
The average grain diameter of the cream jasmin france spansule of above-mentioned resulting use for synthetic leather is 200.8nm-315.7nm, jasmine
Essence utilization rate is 94.07%-98.69%.
A kind of cream jasmin france spansule of above-mentioned use for synthetic leather is used to carry out flavoring processing to synthetic leather, due to synthesis
The source of bad smell is mainly the smell that polyurethane prepares residual monomer in leather, therefore the raw material in synthetic leather preparation process
Preparation stage, by the cream jasmin france spansule of use for synthetic leather：The mass ratio of polyurethane is 1-5 in feed liquid：100 ratio, will
The cream jasmin france spansule of use for synthetic leather is directly added into be prepared in slurry process in synthetic leather, successively by coating, being bonded, coagulate
The processes such as gelatinization, surface treatment finally obtain the synthetic leather handled through cream jasmin france spansule flavoring.
Technical effect of the invention
A kind of cream jasmin france spansule of use for synthetic leather of the invention uses fragrance coordination technique first, passes through difference
The synergistic effect of perfume material fragrance and synthetic leather own smell effectively masks the adverse chemical smell in synthetic leather, solves
Synthetic leather has the problem of bad smell in the prior art, is finally reached the smell of nature collaboration.
Further, the cream jasmin france spansule of a kind of use for synthetic leather of the invention, due to using emulsion polymerization with benzene
Ethylene is that wall material prepares cream jasmin france spansule to improve cream jasmin france stability, solves that cream jasmin france is volatile to ask
Topic；Cream jasmin france by slow releasing function can be more permanent reside on synthetic leather, fragrance remaining time was up to 3 months after measured.
Further, when a kind of cream jasmin france spansule of use for synthetic leather of the invention is used to carry out flavoring to synthetic leather,
Due to being directly added in the slurry preparation stage, and the cream jasmin france spansule usage amount of use for synthetic leather is less, therefore has and add
The features such as fragrant easy to operate, flavoring is at low cost.
Specific embodiment
The present invention is described in further detail below by embodiment, but does not limit the present invention.
The measuring method of cream jasmin france utilization rate in various embodiments of the present invention can refer to document (Pan Yongjun, Xue Hanbing,
Zhang Fei, Zheng is at the preparation and characterization [J] dyeing and finishing technique for assigning cream jasmin france microcapsules, 2009,31 (11):33-37).
Synthetic leather in various embodiments of the present invention is after the processing of cream jasmin france spansule, and fragrance remaining time is according to document
(application study [J] the fragrance flavor and cosmetic of Xiao Zuobing, Yang Bin, Ye Lin nano essence on cotton fabric, 2007 (06):10-
12) method in is measured.
Various raw materials used in each embodiment can be obtained by commercially available approach in the present invention.
Embodiment 1
A kind of cream jasmin france spansule of use for synthetic leather, is calculated by mass percentage, prepare it is raw materials used composition and
Content is as follows：
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
A kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather, includes the following steps：
(1), the preparation of cream jasmin france, steps are as follows：
By the raw materials used composition of cream jasmin france and content is prepared, by benzyl acetate, Ergol, Java Cananga Oil, first position penta
Base cinnamic aldehyde, leaf-alcohol, linalool, eugenol, benzylalcohol, phenethyl acetate, narceol and dipropylene glycol be uniformly mixed to get
Cream jasmin france；
(2), the preparation of the cream jasmin france spansule of use for synthetic leather, steps are as follows：
By preparation use for synthetic leather cream jasmin france spansule used in raw material, first by cream jasmin france, styrene, spit
Temperature -80 is add to deionized water, and under nitrogen protection, is stirred controlled at 25-35 DEG C, revolving speed for 500rpm/min
It is warming up to 75 DEG C after 40min, ammonium persulfate is then added, continues controlled at 75 DEG C, revolving speed to be that 500rpm/min is carried out instead
3h is answered, the cream jasmin france spansule being then dried again controlled at 20-25 DEG C to get use for synthetic leather.
The average grain diameter of the cream jasmin france spansule of above-mentioned resulting use for synthetic leather is 200.8nm, and cream jasmin france utilizes
Rate is 94.07%.
Embodiment 2
A kind of use for synthetic leather cream jasmin france spansule, is calculated by mass percentage, and prepares raw materials used composition and contains
It measures as follows：
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
A kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather finally obtains synthesis with embodiment 1
The cream jasmin france spansule of leather.
The average grain diameter of the cream jasmin france spansule of above-mentioned resulting use for synthetic leather is 208.9nm, and cream jasmin france utilizes
Rate is 94.91%.
Embodiment 3
A kind of use for synthetic leather cream jasmin france spansule, is calculated by mass percentage, and prepares raw materials used composition and contains
It measures as follows：
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
A kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather finally obtains synthesis with embodiment 1
The cream jasmin france spansule of leather.
The average grain diameter of the cream jasmin france spansule of above-mentioned resulting use for synthetic leather is 257.6nm, and cream jasmin france utilizes
Rate is 95.85%.
Embodiment 4
A kind of use for synthetic leather cream jasmin france spansule, is calculated by mass percentage, prepare raw materials used composition and
Content is as follows：
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
A kind of preparation method of the cream jasmin france spansule of above-mentioned use for synthetic leather finally obtains synthesis with embodiment 1
The cream jasmin france spansule of leather.
The average grain diameter of the cream jasmin france spansule of above-mentioned resulting use for synthetic leather is 315.7nm, and cream jasmin france utilizes
Rate is 98.69%.
Application Example
The cream jasmin france spansule of the resulting use for synthetic leather of above-described embodiment 1-4 is used to carry out at flavoring synthetic leather
Reason is prepared since the source of bad smell in synthetic leather is mainly the smell that polyurethane prepares residual monomer in synthetic leather
Stock preparation stage, by the cream jasmin france spansule of use for synthetic leather：The mass ratio of polyurethane is 1 in feed liquid：100 ratio
The cream jasmin france spansule of use for synthetic leather is directly added into and prepares in slurry process in synthetic leather by example, successively by coating, patch
The processes such as conjunction, gelation, surface treatment finally obtain the synthesis of the cream jasmin france spansule flavoring processing through use for synthetic leather
Leather.
It is above-mentioned it is resulting through use for synthetic leather cream jasmin france spansule flavoring processing synthetic leather with without use for synthetic leather
Cream jasmin france spansule flavoring handle resulting synthetic leather and compare, the bad smell of flavoring treated synthetic leather obtains bright
Aobvious to improve, specific assessment method is tested by sensory evaluation.
Above-mentioned sensory evaluation method is：To treated the synthetic leather of the cream jasmin france spansule flavoring through use for synthetic leather and
The synthetic leather of cream jasmin france spansule flavoring processing without use for synthetic leather carries out sensory test respectively, selects 7 volunteers
As sensory evaluation test man, two kinds of synthetic leather are evaluated to sensory evaluation test man respectively, it is desirable that sensory evaluation test
Member is felt as foundation with oneself, is scored two kinds of synthetic leather, it is specified that score is 1-5 grades, and 1 grade is most weak for bad smell, and 5
Grade is that bad smell is most strong, and the scoring of record sensory evaluation test man is as the voucher covered to bad smell.
Cream jasmin france spansule flavoring through use for synthetic leather treated synthetic leather as can be seen from the above table, due to adding
Enter the cream jasmin france spansule of use for synthetic leather, can effectively cover the bad smell of synthetic leather really, is indicated above this
The cream jasmin france spansule of use for synthetic leather provided by inventing has great importance for the improvement of synthetic leather smell.
In conclusion a kind of cream jasmin france spansule of use for synthetic leather of the invention, for the bad smell of synthetic leather
Certain cover effect can be reached, and there is longer fragrance remaining time, longest can achieve 3 months.
Above said content is only the basic explanation under present inventive concept, and is appointed made by technical solution according to the present invention
What equivalent transformation, is within the scope of protection of the invention.
Claims (8)
1. a kind of cream jasmin france spansule of use for synthetic leather, it is characterised in that the cream jasmin france of the use for synthetic leather is sustained glue
The average grain diameter of capsule is 200.8nm-315.7nm, and cream jasmin france utilization rate is 94.07%-98.69%, is calculated by mass percentage,
It prepares raw materials used composition and content is as follows：
Cream jasmin france 0.50%-1.39%
Styrene 3.29%-6.97%
Tween-80 0.33%-0.84%
Ammonium persulfate 0.07%-0.14%
Surplus is deionized water；
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
Benzyl acetate 20.0-32.0%
Ergol 12.0-20.0%
Java Cananga Oil 10.0-15.0%
Alpha-amyl cinnamic aldehyde 8.0-10.0%
Leaf-alcohol 3.0-5.0%
Linalool 5.0-8.0%
Eugenol 2.0-3.0%
Benzylalcohol 1.0-2.0%
Phenethyl acetate 1.0-2.0%
Narceol 1.0-2.0%
Dipropylene glycol 1.0-37.0%.
2. a kind of cream jasmin france spansule of use for synthetic leather as described in claim 1, it is characterised in that the synthetic leather
The average grain diameter of cream jasmin france spansule is 200.8nm, and cream jasmin france utilization rate is 94.07%, by mass percentage
It calculates, prepares raw materials used composition and content is as follows：
Cream jasmin france 0.50%
Styrene 3.30%
Tween-80 0.33%
Ammonium persulfate 0.07%
Surplus is deionized water；
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
Benzyl acetate 20.0%
Ergol 12.0%
Java Cananga Oil 10.0%
Alpha-amyl cinnamic aldehyde 8.0%
Leaf-alcohol 3.0%
Linalool 5.0%
Eugenol 2.0%
Benzylalcohol 1.0%
Phenethyl acetate 1.0%
Narceol 1.0%
Dipropylene glycol 37.0%.
3. a kind of cream jasmin france spansule of use for synthetic leather as described in claim 1, it is characterised in that the synthetic leather
The average grain diameter of cream jasmin france spansule is 208.90nm, and cream jasmin france utilization rate is 94.91%, by mass percentage
It calculates, prepares raw materials used composition and content is as follows：
Cream jasmin france 0.59%
Styrene 3.29%
Tween-80 0.51%
Ammonium persulfate 0.09%
Surplus is deionized water；
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
Benzyl acetate 25.0%
Ergol 15.0%
Java Cananga Oil 12.0%
Alpha-amyl cinnamic aldehyde 9.0%
Leaf-alcohol 4.0%
Linalool 6.0%
Eugenol 2.5%
Benzylalcohol 1.5%
Phenethyl acetate 1.5%
Narceol 1.5%
Dipropylene glycol 22.0%.
4. a kind of cream jasmin france spansule of use for synthetic leather as described in claim 1, it is characterised in that the synthetic leather
The average grain diameter of cream jasmin france spansule is 257.60nm, and cream jasmin france utilization rate is 95.85%, by mass percentage
It calculates, prepares raw materials used composition and content is as follows：
Cream jasmin france 0.68%
Styrene 3.46%
Tween-80 0.66%
Ammonium persulfate 0.08%
Surplus is deionized water；
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
Benzyl acetate 32.0%
Ergol 20.0%
Java Cananga Oil 15.0%
Alpha-amyl cinnamic aldehyde 10.0%
Leaf-alcohol 5.0%
Linalool 8.0%
Eugenol 3.0%
Benzylalcohol 2.0%
Phenethyl acetate 2.0%
Narceol 2.0%
Dipropylene glycol 1.0%.
5. a kind of cream jasmin france spansule of use for synthetic leather as described in claim 1, it is characterised in that the synthetic leather
The average grain diameter of cream jasmin france spansule is 315.70nm, and cream jasmin france utilization rate is 98.69%, by mass percentage
It calculates, prepares raw materials used composition and content is as follows：
Cream jasmin france 1.39%
Styrene 6.97%
Tween-80 0.84%
Ammonium persulfate 0.14%
Surplus is deionized water；
It in the cream jasmin france, is calculated by mass percentage, prepares raw materials used composition and content is as follows：
Benzyl acetate 30.0%
Ergol 18.0%
Java Cananga Oil 14.0%
Alpha-amyl cinnamic aldehyde 9.0%
Leaf-alcohol 4.0%
Linalool 7.0%
Eugenol 2.5%
Benzylalcohol 1.5%
Phenethyl acetate 1.5%
Narceol 1.5%
Dipropylene glycol 11.0%.
6. a kind of preparation side of the cream jasmin france spansule of use for synthetic leather as described in claim 1-5 any claim
Method, it is characterised in that specifically include following steps：
（1）, cream jasmin france preparation, steps are as follows：
By the composition of raw material used in cream jasmin france and content is prepared, by benzyl acetate, Ergol, Java Cananga Oil, first position amyl
Cinnamic aldehyde, leaf-alcohol, linalool, eugenol, benzylalcohol, phenethyl acetate, narceol and dipropylene glycol are uniformly mixed to get jasmine
Jasmine essence；
（2）, use for synthetic leather cream jasmin france spansule preparation, steps are as follows：
Cream jasmin france spansule by preparation use for synthetic leather is raw materials used, first adds cream jasmin france, styrene, Tween-80
Enter into deionized water, is that 500rpm/min is stirred 20-40min controlled at 25-35 DEG C, revolving speed under nitrogen protection
After be warming up to 75 DEG C, be then added ammonium persulfate, continue controlled at 75 DEG C, revolving speed to be that 500rpm/min carries out reaction 3h,
Then the cream jasmin france spansule being dried again controlled at 25-30 DEG C to get use for synthetic leather.
7. the cream jasmin france spansule of use for synthetic leather a method as claimed in any one of claims 1 to 5 is used to carry out at flavoring synthetic leather
Reason, steps are as follows：
It is prepared in slurry process in synthetic leather, by the cream jasmin france spansule of use for synthetic leather：The mass ratio of polyurethane in feed liquid
For 1-5：The cream jasmin france spansule of use for synthetic leather is added directly into urethane raw liquid, successively passes through by 100 ratio
Coating, fitting, gelation, surface treatment finally obtain the synthetic leather handled through cream jasmin france spansule flavoring.
8. the cream jasmin france spansule of use for synthetic leather as claimed in claim 7 is used to carry out flavoring processing to synthetic leather,
It is characterized in that preparing in slurry process in synthetic leather, by the cream jasmin france spansule of use for synthetic leather：The matter of polyurethane in feed liquid
Amount is than being 1：The cream jasmin france spansule of use for synthetic leather is added directly into urethane raw liquid by 100 ratio.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810640253.3A CN108894000A (en) | 2018-06-20 | 2018-06-20 | A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810640253.3A CN108894000A (en) | 2018-06-20 | 2018-06-20 | A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108894000A true CN108894000A (en) | 2018-11-27 |
Family
ID=64345312
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810640253.3A Pending CN108894000A (en) | 2018-06-20 | 2018-06-20 | A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108894000A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674667A (en) * | 2019-01-25 | 2019-04-26 | 广州积美国际贸易有限公司 | A kind of hair washing essence that fragrance retention is lasting |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101003950A (en) * | 2006-01-20 | 2007-07-25 | 长阳实业有限公司 | Synthetic leather, and fabricating method |
| CN101187083A (en) * | 2007-12-04 | 2008-05-28 | 华东理工大学 | Fragrant artificial lawn fiber and its preparation method |
| CN102634415A (en) * | 2012-04-26 | 2012-08-15 | 华南师范大学 | Nanometer essence capsule and preparation method thereof |
| CN107083457A (en) * | 2017-06-15 | 2017-08-22 | 上海应用技术大学 | A kind of leather cream jasmin france capsule |
| CN107916579A (en) * | 2017-12-07 | 2018-04-17 | 钟磊 | A kind of artificial leather and preparation method thereof |
-
2018
- 2018-06-20 CN CN201810640253.3A patent/CN108894000A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101003950A (en) * | 2006-01-20 | 2007-07-25 | 长阳实业有限公司 | Synthetic leather, and fabricating method |
| CN101187083A (en) * | 2007-12-04 | 2008-05-28 | 华东理工大学 | Fragrant artificial lawn fiber and its preparation method |
| CN102634415A (en) * | 2012-04-26 | 2012-08-15 | 华南师范大学 | Nanometer essence capsule and preparation method thereof |
| CN107083457A (en) * | 2017-06-15 | 2017-08-22 | 上海应用技术大学 | A kind of leather cream jasmin france capsule |
| CN107916579A (en) * | 2017-12-07 | 2018-04-17 | 钟磊 | A kind of artificial leather and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674667A (en) * | 2019-01-25 | 2019-04-26 | 广州积美国际贸易有限公司 | A kind of hair washing essence that fragrance retention is lasting |
| CN109674667B (en) * | 2019-01-25 | 2022-01-21 | 毓美生物科技(广州)有限公司 | Shampoo essence with lasting fragrance retention |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1705469A (en) | Polymeric assisted benefit agent delivrery systems | |
| JP2013529222A (en) | Perfume compositions and their use | |
| CN110229717A (en) | Daily use chemicals flavoring rose essence | |
| CN110106024A (en) | Daily use chemicals honey essence | |
| CN108894000A (en) | A kind of cream jasmin france slow-release microcapsule of use for synthetic leather and its preparation method and application | |
| KR20090025095A (en) | Fabric having aromatic microcapsule, mixure and method of manufacturing thereof | |
| CN103343455A (en) | Aromatic fabric production method | |
| CN104357603A (en) | Multi-effect leather finishing agent | |
| CN107419611A (en) | One kind carries fragrant cigarette paper and preparation method thereof | |
| CN102268493A (en) | Method for preparing rose-fragrance leather | |
| JPH03240665A (en) | Flavored tea bag hanging thread and tea bag material | |
| CN108203624A (en) | Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method | |
| CN102199875A (en) | Treatment process for environment depollution textiles | |
| CN104769089A (en) | Improvements in or relating to organic compounds | |
| KR100521157B1 (en) | Processing Method of Ginseng Rice | |
| CN108755159A (en) | A kind of lemon extract spansule of use for synthetic leather and preparation method thereof | |
| US8790706B2 (en) | Fluid powder dentifrice for the treatment of the gums, and a corresponding production method | |
| CN108560255A (en) | A kind of osmanthus flower fragrance spansule of use for synthetic leather and its preparation method and application | |
| CN108893999A (en) | A kind of muguet compound spansule of use for synthetic leather and its preparation method and application | |
| CN105624342B (en) | A kind of production method of the resistance to tortuous Effect Leather of low temperature | |
| CN106379645A (en) | Aluminum foil paper capable of accelerating cigarette alcoholization | |
| CN106109271A (en) | A kind of cosmetic essence | |
| CN102551191A (en) | Natamycin complex formulation for controlling mildew of redried tobacco strips and control method thereby | |
| CN105219529A (en) | A kind of fragrant leather lavender oil and its preparation method and application | |
| CN105113235A (en) | Slow-release aromatic for leather and preparation method of slow-release aromatic |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20181127 |