CN105106156A - Method for preparing armillaria luteo-virens chewable tablets capable of improving sleep - Google Patents
Method for preparing armillaria luteo-virens chewable tablets capable of improving sleep Download PDFInfo
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- CN105106156A CN105106156A CN201510608537.0A CN201510608537A CN105106156A CN 105106156 A CN105106156 A CN 105106156A CN 201510608537 A CN201510608537 A CN 201510608537A CN 105106156 A CN105106156 A CN 105106156A
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Abstract
The invention relates to a method for preparing armillaria luteo-virens chewable tablets capable of improving sleep. The method includes the following steps: (1) removing the root and base of the armillaria luteo-virens fruiting body, washing and removing impurities, drying, smashing, and sieving to obtain armillaria luteo-virens powder; (2) curing the armillaria luteo-virens powder, and drying and cooling to obtain cured armillaria luteo-virens powder; (3) mixing the cured armillaria luteo-virens powder with a filling agent and a corrigent uniformly, carrying out superfine grinding to obtain superfine powder; (4) spraying edible alcohol on the ultrafine powder, and stirring uniformly to prepare a soft material with moderate hardness; pressing and sieving the soft material to obtain the granular product; (5) drying the granular product and then adding a lubricant; after mixing uniformly, pressing to obtain circular tablets with the thickness of 0.7 cm and the radius of 1.5 cm; (6) drying the circular tablets, sterilizing and packaging, so as to obtain the chewable tablet finished product. According to the invention, the technology is simple and facilitates scale production.
Description
Technical field
The present invention relates to field of health care food, particularly relate to a kind of preparation method of Armillaria luteo-virens chewable tablet of improving water flood.
Background technology
Armillaria luteo-virens (
armillarialuteo-virens) be a kind of rare wild edible and medical fungi, be grown on the Alpine Grasslands of height above sea level more than 3000 meters, be mainly distributed in Qinghai, Tibet, Sichuan, Gansu.Research shows, Armillaria luteo-virens is not only containing rich in protein, aminoacid, saccharide, alkaloid, and containing can enhancing human body immunity, antioxidation, antitumor, help the composition of the physiologically actives such as sleep, be integrate edible, medicine and health care function mushroom fungus treasure.
Chewable tablet is the tablet under a class can chew posterior phraynx in oral cavity, and tablet is convenient to swallow after chewing, and also increases surface area, can promote medicine dissolving in vivo, absorption.For the medicine of difficult disintegrate, make chewable tablet and can accelerate its disintegrate, improve drug effect.Chewable tablet taking convenience, even if also can medication on time under the condition of hydropenia, be specially adapted to the patient that children's, old man, dysphagia or gastrointestinal function are poor, can reduces medicine and bear gastrointestinal.
Although chewable tablet sold in the market is of a great variety, mostly composition is single, only for particular condition, lacks not only nutritious but also have the chewable tablet of certain health care functions.Armillaria luteo-virens, except directly being eaten as food materials, has no and develops Related product.The present invention is directed to the blank of Armillaria luteo-virens health promoting product exploitation, a kind of instant, the chewable tablet with improving water flood effect that nutritious, mouthfeel is good are provided.
Summary of the invention
Technical problem to be solved by this invention is to provide the preparation method of the Armillaria luteo-virens chewable tablet of the improving water flood of simple, the easy large-scale production of a kind of technique.
For solving the problem, the preparation method of the Armillaria luteo-virens chewable tablet of a kind of improving water flood of the present invention, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, drying 12 ~ 24hr, pulverizing, excessively 60 ~ 120 mesh sieves, obtain Armillaria luteo-virens powder;
(2) by after the ripening of described Armillaria luteo-virens powder, dry to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening;
(3), after being mixed homogeneously by the weight ratio of 10 ~ 50%:40 ~ 80%:10% with filler and correctives by the Armillaria luteo-virens powder of described ripening, through micronizing, obtain superfine powder;
(4) in described superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 10 ~ 30 mesh sieve, obtains granular product;
(5) drying described granular product to its moisture is 1 ~ 10%, then adds the lubricant of its quality 1 ~ 5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously;
(6) described round sheet thing is dried to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
Described step (1), step (2), step (5), step (6) in bake out temperature be 30 ~ 60 DEG C.
Described step (2) in Armillaria luteo-virens powder cooking conditions refer to temperature be 115 ~ 121 DEG C, pressure be the condition of 0.07 ~ 0.1MPa under decatize 15 ~ 30min, or be 5 ~ 15 kilowatts of lower microwave ripening 1 ~ 15min at power.
Described step (3) in filler refer in lactose, mannitol, xylitol, maltose alcohol, Sorbitol, starch one or more combination.
Described step (3) in correctives refer in aspartame, protein sugar, citric acid, stevioside, Mint Essence, flavoring orange essence, apple essence one or more combination.
Described step (4) in edible ethanol fountain height refer in every 10g superfine powder and add edible ethanol 1 ~ 10mL that volumetric concentration is 30 ~ 90%.
Described step (5) in lubricant refer in magnesium stearate, xanthan gum, Pulvis Talci one or more.
The present invention compared with prior art has the following advantages:
1, present invention process is simple, repeatability is better, and the Armillaria luteo-virens chewable tablet steady quality obtained, can preserve for a long time, directly eat, be easy to carry.
2, raw material of the present invention is after soft material processed, pelletize, easy tabletting, and chewable tablet hardness is moderate, remains the mouthfeel of Armillaria luteo-virens uniqueness.
3, ingredient requirement of the present invention is not high, and market is bought or field acquisition, is easy to batch and gets the raw materials ready.
4, the chewable tablet that obtains of the present invention, fully retains nutrition and the functional component of Armillaria luteo-virens, long-term taking can improving water flood, improve immunity.
(1) be raw material by Armillaria luteo-virens sporophore, through pulverizing at ultralow temperature.In superfine powder, add the ultra-pure water of its quality 5 ~ 10 times, heating extraction 3 times, each 3hr, merge extractive liquid, concentrate and obtain concentrated solution.The aqueous dispersion of its quality 1 ~ 5 times of this concentrated solution, adding 95% ethanol to concentration is 80%, fully after mixing, puts precipitates overnight in 4 DEG C of refrigerators, collects supernatant, concentrated, dry, obtains Armillaria luteo-virens extract target components.Adding 15% methanol/water, to be dissolved to concentration be 200mg/mL, and microporous filter membrane filters, and is separated by high performance liquid chromatography, chromatographic column is DAC150(150 × 250mm, C1810 μm), type of elution is 15% methanol/water isocratic elution 70min, determined wavelength is 260nm, and separate colors spectrogram is shown in Fig. 1.
(2) Armillaria luteo-virens extract target components is on the impact of mice sleep:
Setup Experiments blank group, Chinese medicine (sedative jujube kernel capsule) positive controls, Western medicine (estazolam tablets) positive controls, Armillaria luteo-virens extract target components high dose group (32mg/kg) and low dose group (8mg/kg).Chinese medicine positive controls and Western medicine positive controls dosage convert through remarkable Mus dosage and draw, after fully being ground by medicine respectively, concentration is become to be the solution for standby of high dose group 1.28mg/mL, low dose group 0.32mg/mL, Chinese medicine positive controls 1.28mg/mL, Western medicine positive controls 0.003mg/mL with normal saline.The every average daily gavage of each experimental group once, fills with 0.5mL at every turn, blank group at identical administration time gavage 0.5mL normal saline, successive administration 15d.Mouse Weight, dietary amount, spontaneous activity in mice, above threshold dose of sodium pentobarbitone are caused to the test result such as mouse sleep time, hypnosis of pentobarbital sodium of subthreshold dose time and carry out statistical analysis.
(3) conclusion: Armillaria luteo-virens extract target components can reduce the autonomic activities of normal mouse body, shortens the time before falling asleep, extends the length of one's sleep, within the scope of experimental concentration, present obvious dose-dependent effect.Illustrate that Armillaria luteo-virens extract target components significantly can improve mice sleep, have obvious anti-insomnia effect.Specifically see accompanying drawing 2.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described in further detail.
Fig. 1 is Armillaria luteo-virens extract target components two dimensional separation chromatogram of the present invention.
Fig. 2 is Armillaria luteo-virens extract target components improving water flood result of the test of the present invention.
Detailed description of the invention
embodiment 1a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 30 DEG C of oven dry 24hr, pulverizing, cross 60 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 30 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 115 DEG C, pressure be the condition of 0.07MPa under decatize 30min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 50%:40%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, mannitol mix in the ratio (g/g) of 3:1.
Correctives refers to that stevioside, Mint Essence mix in the ratio (g/g) of 9:1.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 10 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 10mL that volumetric concentration is 30%.
(5) being dried by granular product to its moisture at 30 DEG C of temperature is 5%, then adds the lubricant of its quality 1%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 30 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 2a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 60 DEG C of oven dry 12hr, pulverizing, cross 120 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 60 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 121 DEG C, pressure be the condition of 0.1MPa under decatize 15min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 30%:60%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that xylitol, maltose alcohol mix in the ratio (g/g) of 7:5.
Correctives refers to that aspartame, citric acid, flavoring orange essence mix in the ratio (g/g) of 1:4:5.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 30 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 5mL that volumetric concentration is 90%.
(5) being dried by granular product to its moisture at 60 DEG C of temperature is 3%, then adds the lubricant of its quality 2%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to that magnesium stearate, Pulvis Talci mix in the ratio (g/g) of 1:1.
(6) round sheet thing is dried at 60 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 3a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 45 DEG C of oven dry 18hr, pulverizing, cross 100 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 45 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 15 kilowatts of lower microwave ripening 5min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 20%:70%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, Sorbitol mix in the ratio (g/g) of 13:1.
Correctives refers to that protein sugar, citric acid, apple essence mix in the ratio (g/g) of 1:6:3.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 20 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 1mL that volumetric concentration is 70%.
(5) being dried by granular product to its moisture at 45 DEG C of temperature is 4%, then adds the lubricant of its quality 2%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to xanthan gum.
(6) round sheet thing is dried at 45 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 4a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 50 DEG C of oven dry 15hr, pulverizing, cross 80 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 50 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 5 kilowatts of lower microwave ripening 15min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 10%:80%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that mannitol, maltose alcohol mix in the ratio (g/g) of 1:1.
Correctives refers to that aspartame, flavoring orange essence mix in the ratio (g/g) of 3:2.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 16 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 7mL that volumetric concentration is 50%.
(5) being dried by granular product to its moisture at 50 DEG C of temperature is 2%, then adds the lubricant of its quality 1.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 50 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 5a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 35 DEG C of oven dry 22hr, pulverizing, cross 80 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 35 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 120 DEG C, pressure be the condition of 0.08MPa under decatize 20min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 25%:65%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to lactose.
Correctives refers to aspartame.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 12 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 8mL that volumetric concentration is 45%.
(5) being dried by granular product to its moisture at 35 DEG C of temperature is 10%, then adds the lubricant of its quality 5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to Pulvis Talci.
(6) round sheet thing is dried at 35 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 6a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 40 DEG C of oven dry 16hr, pulverizing, cross 60 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 40 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 10 kilowatts of lower microwave ripening 1min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 35%:55%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to mannitol.
Correctives refers to protein sugar.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 25 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 6mL that volumetric concentration is 60%.
(5) being dried by granular product to its moisture at 40 DEG C of temperature is 1%, then adds the lubricant of its quality 4%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to that magnesium stearate, xanthan gum mix in the ratio (g/g) of 1:1.
(6) round sheet thing is dried at 40 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 7a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 55 DEG C of oven dry 20hr, pulverizing, cross 100 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 55 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 117 DEG C, pressure be the condition of 0.09MPa under decatize 25min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 25%:65%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to xylitol.
Correctives refers to citric acid.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 18 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 3mL that volumetric concentration is 85%.
(5) being dried by granular product to its moisture at 55 DEG C of temperature is 8%, then adds the lubricant of its quality 3%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to that xanthan gum, Pulvis Talci mix in the ratio (g/g) of 2:1.
(6) round sheet thing is dried at 55 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 8a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 45 DEG C of oven dry 14hr, pulverizing, cross 70 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 45 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 10 kilowatts of lower microwave ripening 10min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 15%:75%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to maltose alcohol.
Correctives refers to stevioside.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 14 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 9mL that volumetric concentration is 40%.
(5) being dried by granular product to its moisture at 45 DEG C of temperature is 6%, then adds the lubricant of its quality 2.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to that magnesium stearate, xanthan gum, Pulvis Talci mix in the ratio (g/g) of 1:1:1.
(6) round sheet thing is dried at 45 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 9a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 60 DEG C of oven dry 16hr, pulverizing, cross 100 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 60 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 119 DEG C, pressure be the condition of 0.08MPa under decatize 15min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 40%:50%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to Sorbitol.
Correctives refers to Mint Essence.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 16 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 2mL that volumetric concentration is 35%.
(5) being dried by granular product to its moisture at 60 DEG C of temperature is 9%, then adds the lubricant of its quality 3.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 60 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 10a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 50 DEG C of oven dry 12hr, pulverizing, cross 70 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 50 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 15 kilowatts of lower microwave ripening 15min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 20%:70%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to starch.
Correctives refers to flavoring orange essence.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 25 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 4mL that volumetric concentration is 65%.
(5) being dried by granular product to its moisture at 50 DEG C of temperature is 7%, then adds the lubricant of its quality 4.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to xanthan gum.
(6) round sheet thing is dried at 50 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 11a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 30 DEG C of oven dry 20hr, pulverizing, cross 120 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 30 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 118 DEG C, pressure be the condition of 0.1MPa under decatize 25min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 30%:60%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, mannitol, xylitol mix in the ratio (g/g) of 5:2:3.
Correctives refers to apple essence.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 30 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 5mL that volumetric concentration is 55%.
(5) being dried by granular product to its moisture at 30 DEG C of temperature is 5%, then adds the lubricant of its quality 1%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 30 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 12a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 35 DEG C of oven dry 24hr, pulverizing, cross 60 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 35 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 5 kilowatts of lower microwave ripening 5min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 45%:45%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, mannitol, xylitol, maltose alcohol mix in the ratio (g/g) of 7:1:1:1.
Correctives refers to that aspartame, protein sugar, citric acid, stevioside mix in the ratio of 6:1:1:2.
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 20 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 1mL that volumetric concentration is 75%.
(5) being dried by granular product to its moisture at 35 DEG C of temperature is 8%, then adds the lubricant of its quality 2.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 35 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 13a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 40 DEG C of oven dry 14hr, pulverizing, cross 80 mesh sieves.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 40 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 116 DEG C, pressure be the condition of 0.09MPa under decatize 30min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 15%:75%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, mannitol, xylitol, maltose alcohol, Sorbitol mix in 6:1:1:1:1 ratio (g/g).
Correctives refers to that aspartame, protein sugar, citric acid, stevioside, Mint Essence mix in 5:1:1:1:1 ratio (g/g).
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 10 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 10mL that volumetric concentration is 80%.
(5) being dried by granular product to its moisture at 40 DEG C of temperature is 3%, then adds the lubricant of its quality 1.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to Pulvis Talci.
(6) round sheet thing is dried at 40 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 14a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 55 DEG C of oven dry 18hr, pulverizing, cross 100 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 55 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refers to that at power be 10 kilowatts of lower microwave ripening 10min.
(3), after being mixed homogeneously by the weight ratio of 35%:55%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to that lactose, mannitol, xylitol, maltose alcohol, Sorbitol, starch mix in 4:1:1:1:1:2 ratio (g/g).
Correctives refers to that aspartame, protein sugar, citric acid, stevioside, Mint Essence, flavoring orange essence mix in 9:1:1:6:1:2 ratio (g/g).
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 18 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 5mL that volumetric concentration is 60%.
(5) being dried by granular product to its moisture at 55 DEG C of temperature is 1%, then adds the lubricant of its quality 3%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to xanthan gum.
(6) round sheet thing is dried at 55 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
embodiment 15a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, through 45 DEG C of oven dry 22hr, pulverizing, cross 70 mesh sieves, obtain Armillaria luteo-virens powder.
(2) by after the ripening of Armillaria luteo-virens powder, dry at 45 DEG C of temperature to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening.
Wherein: Armillaria luteo-virens powder cooking conditions refer to temperature be 118 DEG C, pressure be the condition of 0.07MPa under decatize 20min.
(3), after being mixed homogeneously by the weight ratio (g/g) of 40%:50%:10% with filler and correctives by the Armillaria luteo-virens powder of ripening, through micronizing, obtain superfine powder.
Wherein: filler refers to lactose.
Correctives refers to that aspartame, protein sugar, citric acid, stevioside, Mint Essence, flavoring orange essence, apple essence mix in 7:1:1:8:1:1:1 ratio (g/g).
(4) in superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 12 mesh sieve, obtains granular product.
Wherein: edible ethanol fountain height refers in every 10g superfine powder and adds the edible ethanol 7mL that volumetric concentration is 30%.
(5) being dried by granular product to its moisture at 45 DEG C of temperature is 10%, then adds the lubricant of its quality 3.5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously.
Wherein: lubricant refers to magnesium stearate.
(6) round sheet thing is dried at 45 DEG C of temperature to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
Claims (7)
1. a preparation method for the Armillaria luteo-virens chewable tablet of improving water flood, comprises the following steps:
(1), after Armillaria luteo-virens sporophore being removed the root base of a fruit, cleaning remove impurity, drying 12 ~ 24hr, pulverizing, excessively 60 ~ 120 mesh sieves, obtain Armillaria luteo-virens powder;
(2) by after the ripening of described Armillaria luteo-virens powder, dry to water content lower than 15%, cool under room temperature, obtain the Armillaria luteo-virens powder of ripening;
(3), after being mixed homogeneously by the weight ratio of 10 ~ 50%:40 ~ 80%:10% with filler and correctives by the Armillaria luteo-virens powder of described ripening, through micronizing, obtain superfine powder;
(4) in described superfine powder, spray edible ethanol, stir and make the soft material of soft or hard appropriateness, soft material repressed mistake 10 ~ 30 mesh sieve, obtains granular product;
(5) drying described granular product to its moisture is 1 ~ 10%, then adds the lubricant of its quality 1 ~ 5%, is pressed into the round sheet thing that thickness is 0.7cm, radius is 1.5cm after mix homogeneously;
(6) described round sheet thing is dried to moisture lower than 5% time take out, after ultraviolet sterilization 30min, adopt food stage packaging material PE to pack, obtain chewable tablet finished product.
2. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, is characterized in that: described step (1), step (2), step (5), step (6) in bake out temperature be 30 ~ 60 DEG C.
3. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, it is characterized in that: described step (2) in Armillaria luteo-virens powder cooking conditions refer to temperature be 115 ~ 121 DEG C, pressure be the condition of 0.07 ~ 0.1MPa under decatize 15 ~ 30min, or be 5 ~ 15 kilowatts of lower microwave ripening 1 ~ 15min at power.
4. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, is characterized in that: described step (3) in filler refer to one or more combinations in lactose, mannitol, xylitol, maltose alcohol, Sorbitol, starch.
5. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, is characterized in that: described step (3) in correctives refer to one or more combinations in aspartame, protein sugar, citric acid, stevioside, Mint Essence, flavoring orange essence, apple essence.
6. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, is characterized in that: described step (4) in edible ethanol fountain height refer in every 10g superfine powder and add edible ethanol 1 ~ 10mL that volumetric concentration is 30 ~ 90%.
7. the Armillaria luteo-virens chewable tablet of a kind of improving water flood as claimed in claim 1 and preparation method, is characterized in that: described step (5) in lubricant refer in magnesium stearate, xanthan gum, Pulvis Talci one or more.
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