CN105079492A - Dendrobium officinale and solomon's seal capsule and preparation method thereof - Google Patents
Dendrobium officinale and solomon's seal capsule and preparation method thereof Download PDFInfo
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- CN105079492A CN105079492A CN201510325865.XA CN201510325865A CN105079492A CN 105079492 A CN105079492 A CN 105079492A CN 201510325865 A CN201510325865 A CN 201510325865A CN 105079492 A CN105079492 A CN 105079492A
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- herba dendrobii
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Abstract
The invention discloses a dendrobium officinale and solomon's seal capsule which is prepared from the following components in parts by weight: 40-50 parts of dendrobium officinale, and 10-20 parts of solomon's seal. The dendrobium officinale and solomon's seal capsule is prepared by taking dendrobium officinale as the main material and solomon's seal as the auxiliary material; through the synergistic interaction of the raw materials, the dendrobium officinale and solomon's seal capsule has the health efficacies of boosting immunity and relieving physical fatigue, in addition, the dendrobium officinale and solomon's seal capsule is convenient to take, good in absorption by the human body, and high in utilization ratio, can meet health requirements of people of all levels, and has huge market potential. The invention further discloses a preparation method of the dendrobium officinale and solomon's seal capsule, which comprises the following steps: carrying out ultrasonic enzymolysis on dendrobium officinale, carrying out alcohol extraction, concentrating, and drying to obtain dendrobium officinale extract powder; smashing solomon's seal, carrying out water extraction, concentrating, and drying to obtain solomon's seal extract powder; and mixing the dendrobium officinale extract powder and the solomon's seal extract powder, and preparing the capsule. The preparation method is simple in processing steps, low in requirements for equipment, stable in process, strong in operability, and high in production efficiency, thus being suitable for industrial production.
Description
Technical field
The present invention relates to health product preparing technical field, especially relate to a kind of Herba Dendrobii Rhizoma Polygonati capsule and preparation method thereof.
Background technology
Herba Dendrobii (Dendrobiumofficinale), belongs to the orchid family, Dendrobium, Herba Dendrobii kind, the perennial herbaceous plant that grows nonparasitically upon another plant.Herba Dendrobii is mainly containing dendrobium polysaccharide, alkaloid, aminoacid, the plurality of active ingredients such as trace element and phenolic compound, there is nourishing YIN and moistening the lung, nourishing the stomach to promote the production of body fluid, brain nourishing and eyesight improving, protect the liver mind calming, resolving heat and reducing pathogenic fire, the asthenia of tonifying five ZANG-organs, to make light of one's life by commiting suicide the magical effect of prolonging life, to chronic fatigue syndrome, pneumonopathy, coronary heart disease, nephropathy, chronic hepatopathy, hypertension, hyperlipidemia, hyperglycemia, diabetes, chronic gastropathy, dry syndrome, the diseases such as cancer have definite curative effect and conditioning rehabilitative action, and can body immunity be strengthened, antioxidation, defying age, excessive to tobacco and wine, overwork, night life is excessive, use eye brain overwork, hoarseness, dry mouth and tougue, the rehabilitations such as the deficiency of YIN that decline of old gonosome low force have special efficacy.
Rhizoma Polygonati has boosting qi and nourishing yin, spleen invigorating, lung moistening, and effect of kidney tonifying, is usually used in deficiency of spleen-QI and stomach-QI, fatigue and asthenia, deficiency of stomach-Yin, xerostomia lack of appetite, deficiency of the lung cough caused by dryness, chronic cough hemoptysis, asthenia of essence and blood, soreness of the waist and knees, and early whitening of beard and hair, interior-heat is quenched one's thirst.
But current Herba Dendrobii, Rhizoma Polygonati all also exist inconvenient eating, effective ingredient is low by the absorption rate of human body, the problems such as effect is not remarkable, if the medicinal efficacy of Herba Dendrobii, Rhizoma Polygonati therefore can be made full use of, developing a kind of is major ingredient with Herba Dendrobii, Rhizoma Polygonati is adjuvant, and the more significant health promoting product of taking convenience, result of use, exists huge market value undoubtedly.
Summary of the invention
The object of the invention is to provide a kind of compatibility reasonable, taking convenience, absorption of human body is good, and utilization rate is high, has enhancing immunity, the Herba Dendrobii Rhizoma Polygonati capsule of the effects such as alleviating physical fatigue.
Present invention also offers a kind of Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof, processing step is simple, low for equipment requirements, process stabilizing, and workable, production efficiency is high, is applicable to suitability for industrialized production.
To achieve these goals, the present invention is by the following technical solutions:
A kind of Herba Dendrobii Rhizoma Polygonati capsule, is made up of the raw material of following weight portion: 40 ~ 50 parts of Herba Dendrobii, 10 ~ 20 parts of Rhizoma Polygonatis.Herba Dendrobii Rhizoma Polygonati capsule of the present invention makes full use of the medicinal efficacy of Herba Dendrobii, Rhizoma Polygonati, take Herba Dendrobii as major ingredient, Rhizoma Polygonati is that adjuvant is made, by the Synergistic of each raw material, there is the health-care effect such as enhancing immunity, alleviating physical fatigue, taking convenience, absorption of human body is good, utilization rate is high, can meet the health care demand of each aspect personage, have huge market potential.
A kind of Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof, comprises the following steps:
(1) prepare burden
Herba Dendrobii, Rhizoma Polygonati is taken by above-mentioned weight, stand-by.
(2) Herba Dendrobii extract powder is prepared
(1) Herba Dendrobii weighed up is cleaned, dries, pulverized, cross 60 ~ 80 mesh sieves and obtain dendrobium officinale powder.
(2) add water be incorporated as the compound enzyme of Herba Dendrobii quality 0.3 ~ 0.5% in dendrobium officinale powder after, the addition of water is as the criterion with just submergence dendrobium officinale powder, regulates pH to be 5 ~ 6, be warming up to 50 ~ 60 DEG C after stirring, 90 ~ 95 DEG C of enzyme denaturing are warming up to, cooling after ultrasonic enzymolysis 1 ~ 2h.Effective ingredient in Herba Dendrobii is wrapped in cell wall usually, and cell wall increase effective ingredient from cell to Extraction medium diffusion resistance to mass tranfer, the extraction ratio of effective ingredient can be affected, therefore the present invention assists alcohol extracting method to improve the extraction ratio of effective ingredient and the extracting efficiency of alcohol extracting method in Herba Dendrobii by conbined enzymolysis, can be made the ingredient degradation such as cellulose, pectin in cell wall and Cytoplasm by enzymolysis, in reduction Herba Dendrobii, effective ingredient is from the resistance to mass tranfer of the diffusion that is situated between to extraction in cell.
(3) regulate pH be 8 ~ 9, then be incorporated as dendrobium officinale powder quality 8 ~ 12 times 75 ~ 80% alcoholic solution, be warming up to 75 ~ 80 DEG C of reflux, extract, 2 times, each 0.5 ~ 1 hour, merge alcohol extract, filter, reclaim ethanol, obtain extracting solution.Invention adopts alcohol extraction to ensure that the effective ingredient in Herba Dendrobii can fully leach, and ethanol can reclaim, and is conducive to reducing costs.
(4) be 1.08 ~ 1.12 (20 DEG C) by extracting solution vacuum concentration to relative density, obtain Herba Dendrobii extractum.
(5) by Herba Dendrobii extractum spraying dry, Herba Dendrobii extract powder is obtained.
(3) Rhizoma Polygonati extract powder is prepared
A () is incorporated as the water of Rhizoma Polygonati quality 10 ~ 12 times after being pulverized by Rhizoma Polygonati, be heated to 100 DEG C of lixiviates 2 times, each lixiviate 1 ~ 2h, filters and collect filtrate, obtaining lixiviating solution.
B lixiviating solution vacuum concentration to relative density is 1.08 ~ 1.12 (20 DEG C) by (), obtain Rhizoma Polygonati extractum.
C (), by Rhizoma Polygonati extractum spraying dry, obtains Rhizoma Polygonati extract powder.
(4) capsule is prepared
Pulverize after being mixed homogeneously with Rhizoma Polygonati extract powder by obtained Herba Dendrobii extract powder, cross 30 ~ 40 mesh sieves, particulate processed, granulate, finally carries out capsule fill and namely obtains Herba Dendrobii Rhizoma Polygonati capsule.
As preferably, in step (2), described compound enzyme is made up of cellulase, pectase and papain, and wherein the mass percentage of each enzyme is: 20 ~ 25% pectases, 5 ~ 10% papains, and surplus is cellulase.Main component dendrobium polysaccharide in Herba Dendrobii is often together with protein bound, exist with the form of proteoglycan, and the cell wall of Herba Dendrobii cell increase effective ingredient from cell to Extraction medium diffusion resistance to mass tranfer, above-mentioned two kinds of factors make the extraction time of Herba Dendrobii longer, the extraction ratio of extracting efficiency and effective ingredient is low, based on this, the present invention is by strict screening, select by cellulase, the compound enzyme of pectase and papain composition carries out enzymolysis to Herba Dendrobii, wherein papain can the effective protein that combines of enzymolysis and polysaccharide, polysaccharide is discharged and improves the yield of polysaccharide, reduce the content of protein in polysaccharide simultaneously, cellulase can abundant swelling cell wall, impels intracellular polysaccharide in abundant stripping, pectic substance between pectase energy degradation of cell, cell separation out, thus is conducive to cellulase and acts on Herba Dendrobii cell, improves extraction ratio, by the synergism of 3 kinds of enzymes, can by the constituent of cell wall hydrolysis or degraded, destroy the structure of cell wall, the effective ingredient of Herba Dendrobii is fully come out, dissolve, be suspended in solvent, thus reach the object improving extraction efficiency (alcohol extraction time shorten is 0.5 ~ 1h) and extraction ratio.
As preferably, in step (2), supersonic frequency is 40 ~ 50kHz.Hyperacoustic frequency is key point of the present invention, underfrequency, although comparatively strong for active forces such as the cavitation of single and shearings, within a certain period of time due to underfrequency, corresponding useful effect number of times is less, not obvious for the effect improving hydrolysis result; Otherwise amplitude is less, at every turn more weak to the active force of material, also not obvious for the effect improving hydrolysis result, therefore adopt the supersonic frequency of 40 ~ 50kHz to carry out ultrasonic enzymolysis in the present invention, its action effect is best.
As preferably, step (4) is with step (b), and the technological parameter of vacuum concentration is: thickening temperature 60 ~ 70 DEG C, and vacuum is-0.08 ~-0.09MPa.
As preferably, step (5) is with step (c), and spray-dired technological parameter is: inlet temperature: 170 ~ 180 DEG C; Outlet temperature: 60 ~ 70 DEG C; Feed liquor speed: 40 ~ 45ml/min.
Therefore, the present invention has following beneficial effect:
(1) Herba Dendrobii Rhizoma Polygonati capsule of the present invention makes full use of the medicinal efficacy of Herba Dendrobii, Rhizoma Polygonati, take Herba Dendrobii as major ingredient, Rhizoma Polygonati is that adjuvant is made, by the Synergistic of each raw material, there is the health-care effect such as enhancing immunity, alleviating physical fatigue, taking convenience, absorption of human body is good, utilization rate is high, can meet the health care demand of each aspect personage, have huge market potential;
(2) compound enzyme be made up of cellulase, pectase and papain is selected to carry out ultrasonic enzymolysis to Herba Dendrobii in advance at alcohol, alcohol extracting method is assisted by ULTRASONIC COMPLEX enzymatic isolation method, thus improve the object of extraction efficiency and extraction ratio to reach effective ingredient in Herba Dendrobii, processing step is simple, low for equipment requirements, process stabilizing, workable, production efficiency is high, is applicable to suitability for industrialized production.
Detailed description of the invention
Below by detailed description of the invention, the present invention will be further described.
Embodiment 1
(1) prepare burden
By 400Kg Herba Dendrobii, the proportioning of 100Kg Rhizoma Polygonati takes Herba Dendrobii, Rhizoma Polygonati, stand-by.
(2) Herba Dendrobii extract powder is prepared
(1) Herba Dendrobii weighed up is cleaned, dries, pulverized, cross 60 mesh sieves and obtain dendrobium officinale powder.
(2) add water be incorporated as the compound enzyme of Herba Dendrobii quality 0.3% in dendrobium officinale powder after, the addition of water is as the criterion with just submergence dendrobium officinale powder, regulate pH to be 5 after stirring, be warming up to 50 DEG C, after ultrasonic enzymolysis 1h, be warming up to 90 DEG C of enzyme denaturing, cooling, wherein compound enzyme is made up of cellulase, pectase and papain, and wherein the mass percentage of each enzyme is: 20% pectase, 5% papain, surplus is cellulase, and supersonic frequency is 40kHz.
(3) regulate pH be 8, then be incorporated as dendrobium officinale powder quality 8 times 75% alcoholic solution, be warming up to 75 DEG C of reflux, extract, 2 times, each 0.5 hour, merge alcohol extract, filter, reclaim ethanol, obtain extracting solution.
(4) be 1.08 (20 DEG C) by extracting solution vacuum concentration to relative density, obtain Herba Dendrobii extractum, the technological parameter of vacuum concentration is: thickening temperature 60 DEG C, and vacuum is-0.08MPa.
(5) by Herba Dendrobii extractum spraying dry, obtain Herba Dendrobii extract powder, spray-dired technological parameter is: inlet temperature: 170 DEG C; Outlet temperature: 60 DEG C; Feed liquor speed: 40ml/min.
(3) Rhizoma Polygonati extract powder is prepared
A () is incorporated as the water of Rhizoma Polygonati quality 10 times after being pulverized by Rhizoma Polygonati, be heated to 100 DEG C of lixiviates 2 times, each lixiviate 1h, filters and collect filtrate, obtaining lixiviating solution.
B lixiviating solution vacuum concentration to relative density is 1.08 (20 DEG C) by (), obtain Rhizoma Polygonati extractum, the technological parameter of vacuum concentration is: thickening temperature 60 DEG C, and vacuum is-0.08MPa.
C (), by Rhizoma Polygonati extractum spraying dry, obtains Rhizoma Polygonati extract powder, spray-dired technological parameter is: inlet temperature: 170 DEG C; Outlet temperature: 60 DEG C; Feed liquor speed: 40ml/min.
(4) capsule is prepared
Pulverize after being mixed homogeneously with Rhizoma Polygonati extract powder by obtained Herba Dendrobii extract powder, cross 30 mesh sieves, particulate processed, granulate, finally carries out capsule fill and namely obtains Herba Dendrobii Rhizoma Polygonati capsule.
Embodiment 2
(1) prepare burden
By 500Kg Herba Dendrobii, the proportioning of 200Kg Rhizoma Polygonati takes Herba Dendrobii, Rhizoma Polygonati, stand-by.
(2) Herba Dendrobii extract powder is prepared
(1) Herba Dendrobii weighed up is cleaned, dries, pulverized, cross 80 mesh sieves and obtain dendrobium officinale powder.
(2) add water be incorporated as the compound enzyme of Herba Dendrobii quality 0.5% in dendrobium officinale powder after, the addition of water is as the criterion with just submergence dendrobium officinale powder, regulate pH to be 6 after stirring, be warming up to 60 DEG C, after ultrasonic enzymolysis 2h, be warming up to 95 DEG C of enzyme denaturing, cooling, wherein compound enzyme is made up of cellulase, pectase and papain, and wherein the mass percentage of each enzyme is: 25% pectase, 10% papain, surplus is cellulase, and supersonic frequency is 50kHz.
(3) regulate pH be 9, then be incorporated as dendrobium officinale powder quality 12 times 80% alcoholic solution, be warming up to 80 DEG C of reflux, extract, 2 times, each 1 hour, merge alcohol extract, filter, reclaim ethanol, obtain extracting solution.
(4) be 1.12 (20 DEG C) by extracting solution vacuum concentration to relative density, obtain Herba Dendrobii extractum, the technological parameter of vacuum concentration is: thickening temperature 70 DEG C, and vacuum is-0.09MPa.
(5) by Herba Dendrobii extractum spraying dry, obtain Herba Dendrobii extract powder, spray-dired technological parameter is: inlet temperature: 180 DEG C; Outlet temperature: 70 DEG C; Feed liquor speed: 45ml/min.
(3) Rhizoma Polygonati extract powder is prepared
A () is incorporated as the water of Rhizoma Polygonati quality 12 times after being pulverized by Rhizoma Polygonati, be heated to 100 DEG C of lixiviates 2 times, each lixiviate 2h, filters and collect filtrate, obtaining lixiviating solution.
B lixiviating solution vacuum concentration to relative density is 1.12 (20 DEG C) by (), obtain Rhizoma Polygonati extractum, the technological parameter of vacuum concentration is: thickening temperature 70 DEG C, and vacuum is-0.09MPa.
C (), by Rhizoma Polygonati extractum spraying dry, obtains Rhizoma Polygonati extract powder, spray-dired technological parameter is: inlet temperature: 180 DEG C; Outlet temperature: 70 DEG C; Feed liquor speed: 45ml/min.
(4) capsule is prepared
Pulverize after being mixed homogeneously with Rhizoma Polygonati extract powder by obtained Herba Dendrobii extract powder, cross 40 mesh sieves, particulate processed, granulate, finally carries out capsule fill and namely obtains Herba Dendrobii Rhizoma Polygonati capsule.
Embodiment 3
(1) prepare burden
By 480Kg Herba Dendrobii, the proportioning of 120Kg Rhizoma Polygonati takes Herba Dendrobii, Rhizoma Polygonati, stand-by.
(2) Herba Dendrobii extract powder is prepared
(1) Herba Dendrobii weighed up is cleaned, dries, pulverized, cross 70 mesh sieves and obtain dendrobium officinale powder.
(2) add water be incorporated as the compound enzyme of Herba Dendrobii quality 0.4% in dendrobium officinale powder after, the addition of water is as the criterion with just submergence dendrobium officinale powder, regulate pH to be 5.5 after stirring, be warming up to 55 DEG C, after ultrasonic enzymolysis 1.5h, be warming up to 92 DEG C of enzyme denaturing, cooling, wherein compound enzyme is made up of cellulase, pectase and papain, and wherein the mass percentage of each enzyme is: 22% pectase, 8% papain, surplus is cellulase, and supersonic frequency is 45kHz.
(3) regulate pH be 8.5, then be incorporated as dendrobium officinale powder quality 10 times 78% alcoholic solution, be warming up to 78 DEG C of reflux, extract, 2 times, each 0.6 hour, merge alcohol extract, filter, reclaim ethanol, obtain extracting solution.
(4) be 1.1 (20 DEG C) by extracting solution vacuum concentration to relative density, obtain Herba Dendrobii extractum, the technological parameter of vacuum concentration is: thickening temperature 65 DEG C, and vacuum is-0.085MPa.
(5) by Herba Dendrobii extractum spraying dry, obtain Herba Dendrobii extract powder, spray-dired technological parameter is: inlet temperature: 175 DEG C; Outlet temperature: 65 DEG C; Feed liquor speed: 42ml/min.
(3) Rhizoma Polygonati extract powder is prepared
A () is incorporated as the water of Rhizoma Polygonati quality 11 times after being pulverized by Rhizoma Polygonati, be heated to 100 DEG C of lixiviates 2 times, each lixiviate 1.5h, filters and collect filtrate, obtaining lixiviating solution.
B lixiviating solution vacuum concentration to relative density is 1.1 (20 DEG C) by (), obtain Rhizoma Polygonati extractum, the technological parameter of vacuum concentration is: thickening temperature 65 DEG C, and vacuum is-0.085MPa.
C (), by Rhizoma Polygonati extractum spraying dry, obtains Rhizoma Polygonati extract powder, spray-dired technological parameter is: inlet temperature: 175 DEG C; Outlet temperature: 65 DEG C; Feed liquor speed: 42ml/min.
(4) capsule is prepared
Pulverize after being mixed homogeneously with Rhizoma Polygonati extract powder by obtained Herba Dendrobii extract powder, cross 35 mesh sieves, particulate processed, granulate, finally carries out capsule fill and namely obtains Herba Dendrobii Rhizoma Polygonati capsule.
The quality index of the Herba Dendrobii Rhizoma Polygonati capsule that the present invention obtains is:
One. organoleptic indicator
| Project | Index |
| Color and luster | Pale brown or yellow |
| Tissue morphology | Fine particulate |
| Taste, abnormal smells from the patient | There is the distinctive fragranced of Herba Dendrobii |
| Impurity | Free from admixture |
Two. physical and chemical index
| Project | Index |
| Moisture/(%) | ≤6.0 |
| Ash/(%) | ≤6.0 |
| Disintegration/(min) | ≤30 |
| Arsenic (in As), (mg/kg) | ≤1.0 |
| Plumbous (in Pa), (mg/kg) | ≤1.5 |
| Tribute (in Hg), (mg/kg) | ≤0.3 |
| Gamma Hexaochlorocyclohexane/(mg/kg) | ≤0.2 |
| (clofenotane/(mg/kg) | ≤0.2 |
Three. microbiological indicator
Four. effective component index
| Project | Index |
| Crude polysaccharides (in glucosan)/(g/100g) | ≥7.74 |
Above-described embodiment is one of the present invention preferably scheme, not does any pro forma restriction to the present invention, also has other variant and remodeling under the prerequisite not exceeding the technical scheme described in claim.
Claims (6)
1. a Herba Dendrobii Rhizoma Polygonati capsule, is characterized in that, is made up of the raw material of following weight portion: 40 ~ 50 parts of Herba Dendrobii, 10 ~ 20 parts of Rhizoma Polygonatis.
2. a Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof as claimed in claim 1, is characterized in that, comprise the following steps:
(1) prepare burden
Herba Dendrobii, Rhizoma Polygonati is taken by above-mentioned weight, stand-by;
(2) Herba Dendrobii extract powder is prepared
(1) Herba Dendrobii weighed up is cleaned, dries, pulverized, cross 60 ~ 80 mesh sieves and obtain dendrobium officinale powder;
(2) add water be incorporated as the compound enzyme of Herba Dendrobii quality 0.3 ~ 0.5% in dendrobium officinale powder after, the addition of water is as the criterion with just submergence dendrobium officinale powder, regulates pH to be 5 ~ 6, be warming up to 50 ~ 60 DEG C after stirring, 90 ~ 95 DEG C of enzyme denaturing are warming up to, cooling after ultrasonic enzymolysis 1 ~ 2h;
(3) regulate pH be 8 ~ 9, then be incorporated as dendrobium officinale powder quality 8 ~ 12 times 75 ~ 80% alcoholic solution, be warming up to 75 ~ 80 DEG C of reflux, extract, 2 times, each 0.5 ~ 1 hour, merge alcohol extract, filter, reclaim ethanol, obtain extracting solution;
(4) be 1.08 ~ 1.12 (20 DEG C) by extracting solution vacuum concentration to relative density, obtain Herba Dendrobii extractum;
(5) by Herba Dendrobii extractum spraying dry, Herba Dendrobii extract powder is obtained;
(3) Rhizoma Polygonati extract powder is prepared
A () is incorporated as the water of Rhizoma Polygonati quality 10 ~ 12 times after being pulverized by Rhizoma Polygonati, be heated to 100 DEG C of lixiviates 2 times, each lixiviate 1 ~ 2h, filters and collect filtrate, obtaining lixiviating solution;
B lixiviating solution vacuum concentration to relative density is 1.08 ~ 1.12 (20 DEG C) by (), obtain Rhizoma Polygonati extractum;
C (), by Rhizoma Polygonati extractum spraying dry, obtains Rhizoma Polygonati extract powder;
(4) capsule is prepared
Pulverize after being mixed homogeneously with Rhizoma Polygonati extract powder by obtained Herba Dendrobii extract powder, cross 30 ~ 40 mesh sieves, particulate processed, granulate, finally carries out capsule fill and namely obtains Herba Dendrobii Rhizoma Polygonati capsule.
3. Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof according to claim 2, it is characterized in that, in step (2), described compound enzyme is made up of cellulase, pectase and papain, wherein the mass percentage of each enzyme is: 20 ~ 25% pectases, 5 ~ 10% papains, surplus is cellulase.
4. Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof according to claim 2, is characterized in that, in step (2), supersonic frequency is 40 ~ 50kHz.
5. Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof according to claim 2, is characterized in that, step (4) is with step (b), and the technological parameter of vacuum concentration is: thickening temperature 60 ~ 70 DEG C, and vacuum is-0.08 ~-0.09MPa.
6. Herba Dendrobii Rhizoma Polygonati capsule preparation method thereof according to claim 2, is characterized in that, step (5) is with step (c), and spray-dired technological parameter is: inlet temperature: 170 ~ 180 DEG C; Outlet temperature: 60 ~ 70 DEG C; Feed liquor speed: 40 ~ 45ml/min.
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| CN106360213A (en) * | 2016-08-26 | 2017-02-01 | 福州仁量生物制品有限公司 | Rhizoma polygonati plant beverage and preparation method thereof |
| CN107029120A (en) * | 2017-05-08 | 2017-08-11 | 文山农业科技成果转化服务中心 | A kind of preparation method of the stem of noble dendrobium and sealwort paste nourishing agent |
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| CN111249398A (en) * | 2020-03-11 | 2020-06-09 | 中科花鹿农业发展有限公司 | Dendrobium officinale and deer blood composition, preparation method and application thereof, and nourishing paste |
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