CN105078847B - A kind of plant hair conditioner and preparation method thereof - Google Patents
A kind of plant hair conditioner and preparation method thereof Download PDFInfo
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- CN105078847B CN105078847B CN201510606451.4A CN201510606451A CN105078847B CN 105078847 B CN105078847 B CN 105078847B CN 201510606451 A CN201510606451 A CN 201510606451A CN 105078847 B CN105078847 B CN 105078847B
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Abstract
The invention discloses a kind of plant hair conditioner and preparation method thereof, the plant hair conditioner, by percentage to the quality, including following components：Grape seed extract 1~5%, butter berry extract 1~5%, shea butter 1~3%, 16~18 alcohol 1~5%, propane diols 1~5%, amino acid humectant 0.2~1%, surplus are rice washing water.The preparation method includes：Using 16~18 alcohol and shea butter as oil phase, propane diols and rice washing water are as aqueous phase, oil phase and aqueous phase are heated with stirring to 80~85 DEG C respectively, after raw material is all uniformly dissolved, while stirring oil phase, while aqueous phase is gently added in oil phase, continue to stir, stir while cooling, when temperature is down to 45~50 DEG C, add grape seed extract, butter berry extract and amino acid humectant, continue to stir, it is to be mixed uniformly after, cooling, take out, stand 20~30h, you can obtain the plant hair conditioner.The present invention have anti-oxidant, uvioresistant, for nutrition needed for hair supplement, make hair submissiveer and other effects.
Description
Technical field
The invention belongs to Cosmetic Manufacture technical field, and in particular to a kind of plant hair conditioner and preparation method thereof.
Background technology
It is personal daily nursing behavior that hair, which washes shield, caused by the daily metabolism of human body and living environment, meeting on hair and scalp
There are the pollutants such as certain grease, sweat mixed with dirt, sand and dust, with the continuous deterioration of people's living environment, on PM2.5 in air is continuous
Rise, the life to people causes very big puzzlement, and because the PM2.5 particle diameters in atmosphere pollution are small, specific surface area is big, activity
By force, easily incidentally poisonous and harmful substances (for example, heavy metal, microorganism etc.), residence time in an atmosphere are grown, these tiny
In the deep enough hair hair scale piece gap for depositing to people of grain energy, the hair follicle root of scalp more can be deeply deposited to, so as to influence people
Hair and scalp health.
Hair conditioner present in prior art is mostly that chemical substance compounds to obtain, such as the foam performance surfactant component moon
Laureth sulfuric ester ammonium, Texapon Special, dodecanamide propyl sweet tea Lay alkali, the cation opsonizing agent of cellulose origin synthesis
And silicone oil, these materials can wash away grease, the dust of hair surface to a certain extent, hair nursed, still,
Chemical composition remains in can also produce harm to human body on scalp or hair, at silicate-containing oil conditioner product residual hair and hair follicle,
Hair follicle breathing is made to be obstructed, nutrition vim and vigour are insufficient, or even trigger hair loss problem.
The content of the invention
In order to solve the above problems, the invention provides a kind of plant hair conditioner, for nutrition needed for hair supplement so that head
Hair is submissiveer, and does not stimulate naturally, will not block hair follicle.
A kind of plant hair conditioner, by percentage to the quality, including following components：
Grape seed extract 1~5%, butter berry extract 1~5%, shea butter 1~3%, 16~18 alcohol 1~5%,
Propane diols 1~5%, amino acid humectant 0.2~1%, surplus are rice washing water.
Preferably, by percentage to the quality, the plant hair conditioner includes following components：
Grape seed extract 2~5%, butter berry extract 2~5%, shea butter 1.5~3%, 16~18 alcohol 2~
5%th, propane diols 2~5%, amino acid humectant 0.5~1%, surplus are rice washing water.
As it is further preferred that by percentage to the quality, the plant hair conditioner includes following components：
Grape seed extract 4%, butter berry extract 5%, shea butter 3%, 16~18 alcohol 5%, propane diols 3%, ammonia
Base acid NMF 1%, surplus are rice washing water.
Preferably, the preparation method of the grape seed extract includes：
(1) grape pip is crushed to obtain grape pip powder, by grape pip powder and deionized water by volume 1:30
~40 are mixed, and after being well mixed, are removed filter residue, are obtained Grape seed solution；
(2) it is 1 with its volume ratio in the Grape seed solution, middle addition:2~3 absolute ethyl alcohol carries out ultrasonic extraction 10
~15h, revolving, obtains grape pip crude extract；
(3) grape pip crude extract is separated with polymeric membrane, obtains grape pip refining liquid；
(4) finally grape pip refining liquid is spray-dried, crushes and produce grape seed extract.
Preferably, the preparation method of the butter berry extract includes：
(1) by butter fruit and deionized water by volume 1:20~30 are squeezed, and remove filter residue, it is molten to obtain butter fruit
Liquid；
(2) it is 1 to be added in the butter fruit solution with its volume ratio:2~3 absolute ethyl alcohol progress ultrasonic extraction 10~
15h, revolving, obtains butter fruit crude extract；
(3) butter fruit crude extract is separated with polymeric membrane, obtains butter fruit refining liquid；
(4) finally butter fruit refining liquid is spray-dried, crushes and produce butter berry extract.
Preferably, EAT when butter fruit extract solution or grape pip extract solution are spray-dried for 140~
160 DEG C, leaving air temp is 70~90 DEG C.
Preferably, the preparation method of the rice washing water is：Add deionized water in rice to be eluriated, filtering is big
Rice, obtains the rice washing water；Wherein the volume ratio of rice and deionized water is 1:10~20.
Present invention also offers the preparation method of above-mentioned plant hair conditioner, including：Using 16~18 alcohol and shea butter as
Oil phase and aqueous phase are heated with stirring to 80~85 DEG C respectively, treat that raw material all dissolves by oil phase, propane diols and rice washing water as aqueous phase
After uniformly, oil phase is stirred on one side, while aqueous phase is gently added in oil phase, continues to stir, stir while cool, treat temperature
When degree is down to 45~50 DEG C, adds grape seed extract, butter berry extract and amino acid humectant, continue to stir, treat
After stirring, cool down, take out, stand 20~30h, you can obtain the plant hair conditioner.
Preferably, mixing speed is 80~120r/min.
Compared with prior art, beneficial effects of the present invention are embodied in：
(1) low in raw material price of plant hair conditioner of the invention, preparation method is simple and convenient, and its each index meets hair care
Plain (QB/T 1975-2013) and《Cosmetics health specification》The requirement of version specification in 2007.And the present invention has antioxygen
Change, uvioresistant, for nutrition needed for hair supplement, make hair submissiveer, more beautiful and other effects, plant hair conditioner of the invention is green
Colour circle is protected, reduces environmental pollution, and does not grow dandruff, do not block hair follicle；
(2) plant hair conditioner hair conditioner of the invention its viscosity, smears degree, Yi Chong compared with the product of existing market
It is smooth degree when feel when washing, washing by water, wet hair feel, wet hair feel, dry hair, wet hair comb rationality, the cardability of dry hair, fluffy
The performance such as degree, hair soft degree, glossiness and elasticity is superior to existing market product.
Brief description of the drawings
Fig. 1 be plant hair conditioner and the existing hair conditioner product of the present invention viscosity respectively when in use, smear and
Comparing result in terms of washability.
Fig. 2 is pair of the smooth degree of hair after plant hair conditioner and the existing hair conditioner product for using the present invention
Compare result.
Fig. 3 be using after the plant hair conditioner of the present invention and existing hair conditioner product, the wet hair comb rationality of hair with
And the comparing result of hair drying comb rationality.
Fig. 4 is that hair is soft after wet hair and dry hair using after the plant hair conditioner of the present invention and existing hair conditioner product
The comparing result of softness.
Fig. 5 be using the present invention plant hair conditioner and existing hair conditioner product after, do hair after hair fluffy degree,
The comparing result that hair gloss and hair elasticity are felt.
Fig. 6 is contrast knot of the evaluator to overall assessment after the plant hair conditioner of the present invention and existing hair conditioner product
Fruit.
Fig. 7 is contrast knot of the subject to favorable rating after the plant hair conditioner of the present invention and existing hair conditioner product
Fruit.
Embodiment
The preparation method of the plant hair conditioner of the present invention, comprises the following steps：
(1) grape pip and butter fruit solution are prepared
Grape pip is collected, grape pip is smashed, obtains grape pip powder, grape pip powder and deionized water are pressed into body
Product ratio 1:30~40 are mixed, and after being well mixed, are removed filter residue, are obtained Grape seed solution；
Using commercially available butter fruit as raw material, by butter fruit and deionized water by volume 1:20~30 are squeezed, and are removed
Filter residue, obtain butter fruit solution；
(2) grape pip crude extract and butter fruit crude extract are prepared
It is respectively 1 will be added in the solution in step (1) with its volume ratio:2~3 absolute ethyl alcohol carries out ultrasonic extraction
10~15h, revolving, obtains grape pip crude extract and butter fruit crude extract；
(3) grape pip refining liquid and butter fruit refining liquid are prepared
Butter fruit crude extract is separated with polymeric membrane, obtains butter fruit refining liquid；Wherein polymeric membrane is retention
Component is the polymeric membrane of 5000~10000 dalton, and filter pressure is 0.2MPa~0.5Mpa, and filtration temperature is normal temperature；
(4) grape seed extract, butter berry extract are prepared
Grape pip refining liquid and butter fruit refining liquid in step (3) are spray-dried (wherein respectively：Be spray-dried into
Air temperature is 140~160 DEG C, and leaving air temp is 70~90 DEG C), the solids of gained after drying is crushed, respectively obtains grape
Seed extract powder and butter fruit extract powder, refrigeration are standby.
(5) preparation of rice washing water
Using commercially available rice as raw material, add deionized water and eluriated, the volume ratio of wherein rice and deionized water is
1:10~20, rice is filtered, obtains rice washing water.
(6) using 16~18 alcohol and shea butter as oil phase, propane diols and rice washing water as aqueous phase, respectively by oil phase and water
80~85 DEG C are mutually heated with stirring to, after raw material is all uniformly dissolved, while stirring oil phase, while aqueous phase is gently added into oil
Xiang Zhong, continue to stir, stir while cool, when temperature is down to 45~50 DEG C, add grape seed extract, butter fruit
Extract and amino acid humectant, continue to stir, it is to be mixed uniformly after, cool down, take out, stand 20~30h, you can obtain institute
State plant hair conditioner.
Above-mentioned experimental method, it is conventional method unless otherwise specified；The reagent and material, unless otherwise specified,
Commercially obtain.According to the method described above the step of, has carried out the preparation of multiple plant hair conditioner, is only that have adjusted this hair
The raw material type and content of bright plant hair conditioner, obtain a series of embodiments, are specifically shown in Table 1.
The plant hair conditioner of the invention that the different material species and content of table 1 are prepared
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Grape seed extract/% | 1.0 | 3.0 | 5.0 | 4.0 | 2.0 | 5.0 |
| Butter berry extract/% | 2.0 | 1.0 | 3.0 | 5.0 | 4.0 | 3.5 |
| Shea butter/% | 3.0 | 1.0 | 3.0 | 3.0 | 3.0 | 2.0. |
| 16~18 alcohol/% | 1.0 | 3.0 | 2.0 | 5.0 | 2.0 | 3.0 |
| Propane diols/% | 5.0 | 5.0 | 1.0 | 3.0 | 2.5 | 5.0 |
| Amino acid humectant/% | 1.0 | 0.2 | 0.5 | 1.0 | 0.6 | 0.8 |
| Rice washing water/% | 87.0 | 86.8 | 85.5 | 79.0 | 85.9 | 80.7 |
| Overall merit | ☆☆☆ | ☆☆☆ | ☆☆☆☆ | ☆☆☆☆☆ | ☆☆☆☆ | ☆☆☆☆ |
Note：Tested using crowd's half a head, carry out overall merit, ☆ is more, shows that overall merit is higher.
The plant hair conditioner being prepared is formulated according to table 1 to draw after testing：Noxious material arsenic, lead, mercury do not detect；Excrement
Coliform, pseudomonas aeruginosa and staphylococcus aureus do not detect；Total plate count ＜ 10CFU/ml；Yeast and mold
Total ＜ 10CFU/ml.24h is kept in (40 ± 1) DEG C, without lamination after recovering to room temperature；Kept in (- 8 ± 2) DEG C
24h, without lamination after recovering to room temperature；Total solid >=4.0/%, each index meet hair conditioner (QB/T 1975-
2013) and《Cosmetics health specification》The requirement of version specification in 2007.
The effect evaluation method for the plant hair conditioner that embodiment 1~6 is prepared is tested using crowd's half a head, appraisal procedure
It is as follows：
Subject dries up for hair, the crowd of the dry hair quality of hair, by having experience evaluator come the effect of test product.
Evaluator first helps subject to clean hair twice with 10~20g of shampoo of clean type, is rinsed with water, pinches decaptitating
Most of moisture on hair, hair therefrom between be divided into left and right two parts, two half a heads are respectively using a test hair conditioner sample
20g, left and right two parts hair is gently rubbed with right-hand man respectively, is applied to completely on all hairs to hair conditioner, and assess hair conditioner
Denseness and spreadability, about rub 3 minutes, then wash by water, the compliance of hair, hair conditioner washability, punching are felt in bath
There are smoothness, the flexibility that the right and left hair is felt by evaluator after washing, and both sides are combed simultaneously with two identical combs
Hair, assess easy cardability.Hair is blown to 8 one-tenth with hair dryer to do, assesses compliance, glossiness and the comb of both sides hair again
The performance of reason；
Evaluation, the overall merit highest of the as shown by data example 4 of table 1, preferred embodiment 4 are made according to above-mentioned evaluation method.
Example 4 is prepared into plant hair conditioner according to above-mentioned preparation technology, prepared hair conditioner (is labeled as：Y) it is in great demand with the market
Hair conditioner brand A (is labeled as：YA) compareed, subject is entered according to hair products crowd test (half a head test) method is washed
Row test, gives a mark, 5 points are best result, and 1 point minimum point, integrated data is averaged, finally to each stage performance of hair washing
By tidal data recovering statistical analysis.
(1) comfort level that hair conditioner uses has three viscosity, property easy to apply and easy washability indexs, wherein sticky journey
It is 1~5 point to spend fraction, better closer to 3 points, too thick higher than 3 points, too dilute less than 3 points, as a result sees Fig. 1.
As can be seen from Figure 1, the viscosity of plant hair conditioner of the invention is slightly better than existing market product, smears degree with showing
Have that market product is similar, easily rinse performance and show more excellent than existing market product.
(2) comparison of smooth degree, is divided into the sensation during bath when hair conditioner uses, and wet hair is felt after flushing and hair is done
Submissive sense afterwards, is as a result shown in Fig. 2.
As can be seen from Figure 2, the feel of hair conditioner of the invention in bath is good compared with existing market product, and hand during wet hair
Sense is slightly better than existing market product, but is more or less the same, and without significant difference, smooth degree is omited than existing market product when doing hair
It is good.
(3) easy cardability after hair conditioner is used, is divided into wet hair comb rationality and hair drying comb rationality, as a result sees Fig. 3.Can from Fig. 3
Go out, the easy cardability of wet hair and dry hair is all better than existing market product.
(4) the rear hair pliability of hair conditioner, pliability and the pliability after dry hair, are as a result shown in Fig. 4 when being divided into wet hair.From
Fig. 4 can be seen that on the hair soft degree in wet hair and dry hair that test sample is more superior than existing market product.
(5) performance test after the dry hair of hair conditioner is divided into the comparison that fluffy degree, hair gloss and hair elasticity are felt,
Fluffy degree is better closer to 1, as a result sees Fig. 5.
Hair shows as after dry hair：Hair after the washing of given the test agent is more docile, fluffy without existing market product,
Glossiness and elasticity are better than existing market product.
(6) aggregate performance degree and preference contrast, and are scored by aggregate performance of the evaluator to two hair conditioner, and by
Examination person is then selected the fancy grade of two hair conditioner, as a result sees Fig. 6 and Fig. 7.
Aggregate performance of the appraiser to two hair conditioner as can be seen from Figure 6 is assessed, and given the test agent is better than existing market production
Product, and it is also that given the test agent produces far beyond existing market that subject, which can be seen, in the fancy grade of two hair care degree to compare from Fig. 7
Product.
In addition, also sending barber shop and social crowd to be applicable hair conditioner prepared by laboratory, applicable crowd is cured hundred people, satisfied
Degree has good repair to damaged hair up to more than 95%.
Finally it should be noted that above example is only to illustrative and not limiting technical scheme, although reference
The present invention is described in detail above-described embodiment, it will be appreciated by those skilled in the art that can still be carried out to the present invention
Modification or equivalent substitution, any modification or partial replacement without departing from the spirit and scope of the present invention, it all should cover
In scope of the presently claimed invention.
Claims (8)
- A kind of 1. plant hair conditioner, it is characterised in that by percentage to the quality, including following components：Grape seed extract 1~5%, butter berry extract 1~5%, shea butter 1~3%, 16~18 alcohol 1~5%, the third two Alcohol 1~5%, amino acid humectant 0.2~1%, surplus are rice washing water；Wherein, the preparation method of the grape seed extract includes：(1) grape pip is crushed to obtain grape pip powder, by grape pip powder and deionized water by volume 1:30~40 Mixed, after being well mixed, remove filter residue, obtain Grape seed solution；(2) it is 1 to be added in above-mentioned Grape seed solution with its volume ratio:2~3 absolute ethyl alcohol carries out 10~15h of ultrasonic extraction, Revolving, obtains grape pip crude extract；(3) grape pip crude extract is separated with polymeric membrane, obtains grape pip refining liquid；(4) finally grape pip refining liquid is spray-dried, crushes and produce grape seed extract；Wherein, the preparation method of the butter berry extract includes：(1) by butter fruit and deionized water by volume 1:20~30 are squeezed, and are removed filter residue, are obtained butter fruit solution；(2) it is 1 to be added in above-mentioned butter fruit solution with its volume ratio:2~3 absolute ethyl alcohol carries out 10~15h of ultrasonic extraction, Revolving, obtains butter fruit crude extract；(3) butter fruit crude extract is separated with polymeric membrane, obtains butter fruit refining liquid；(4) finally butter fruit refining liquid is spray-dried, crushes and produce butter berry extract.
- 2. plant hair conditioner as claimed in claim 1, it is characterised in that by percentage to the quality, the plant hair conditioner bag Include following components：Grape seed extract 2~5%, butter berry extract 2~5%, shea butter 1.5~3%, 16~18 alcohol 2~5%, third Glycol 2~5%, amino acid humectant 0.4~1%, surplus are rice washing water.
- 3. plant hair conditioner as claimed in claim 2, it is characterised in that by percentage to the quality, the plant hair conditioner bag Include following components：Grape seed extract 4%, butter berry extract 5%, shea butter 3%, 16~18 alcohol 5%, propane diols 3%, amino acid NMF 1%, surplus are rice washing water.
- 4. plant hair conditioner as claimed in claim 1, it is characterised in that the polymeric membrane be retention component be 5000~ The polymeric membrane of 10000 dalton, filter pressure are 0.2~0.5Mpa, and temperature is normal temperature.
- 5. plant hair conditioner as claimed in claim 1, it is characterised in that carry out butter fruit refining liquid or grape pip refining liquid Spray drying, the EAT of spray drying is 140~160 DEG C, and leaving air temp is 70~90 DEG C.
- 6. plant hair conditioner as claimed in claim 1, it is characterised in that the preparation method of the rice washing water is：In rice Add deionized water to be eluriated, filter rice, obtain the rice washing water；Wherein the volume ratio of rice and deionized water is 1:10 ~20.
- 7. the preparation method of the plant hair conditioner as described in claim 1~6 is any, it is characterised in that including：By 16~18 alcohol Oil phase and aqueous phase are heated with stirring to 80~85 DEG C respectively as aqueous phase as oil phase, propane diols and rice washing water with shea butter, After raw material is all uniformly dissolved, while stirring oil phase, while aqueous phase is gently added in oil phase, continues to stir, while stirring Mix while cool, when temperature is down to 45~50 DEG C, add grape seed extract, butter berry extract and amino acid moisturizing Agent, continue to stir, it is to be mixed uniformly after, cool down, take out, stand 20~30h, you can obtain the plant hair conditioner.
- 8. the preparation method of plant hair conditioner as claimed in claim 7, it is characterised in that mixing speed is 80~120r/ min。
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| CN108836895A (en) * | 2018-06-27 | 2018-11-20 | 跨越生物科技（滁州）有限公司 | One kind can the submissive antibacterial nutritious hair conditioner of hair |
| CN109908057A (en) * | 2019-04-01 | 2019-06-21 | 贵州阿斯科科技开发有限公司 | A kind of Chinese herbal medicine skin care item and preparation method thereof |
| CN113181101B (en) * | 2021-05-26 | 2023-04-28 | 建昌帮药业有限公司 | Hair conditioner |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104224634A (en) * | 2014-09-30 | 2014-12-24 | 澳宝化妆品（惠州）有限公司 | Hair conditioning combination and application thereof in hair conditioning products |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104224634A (en) * | 2014-09-30 | 2014-12-24 | 澳宝化妆品（惠州）有限公司 | Hair conditioning combination and application thereof in hair conditioning products |
Non-Patent Citations (4)
| Title |
|---|
| 化妆品配方;佚名;《日用化学品科学》;20090731;第32卷(第7期);第52-54页 * |
| 化妆品配方;佚名;《日用化学品科学》;20140630;第37卷(第6期);第52-56页 * |
| 护发品市场的增长及趋势;潘华;《日用化学品科学》;20070630;第30卷(第6期);第33-37页 * |
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Effective date of registration: 20211008 Address after: 550000 shawen Industrial Park, Guiyang National High tech Industrial Development Zone, Guiyang City, Guizhou Province Patentee after: Guizhou engineering composite material Center Co.,Ltd. Patentee after: GUIZHOU ASIKE TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 550000 a2-6, new material industrial park, Baiyun North Road, Guiyang City, Guizhou Province Patentee before: GUIZHOU ENGINEERING COMPOSITE MATERIAL CENTER Patentee before: GUIZHOU ASIKE TECHNOLOGY DEVELOPMENT Co.,Ltd. |
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