CN105078847A - Plant hair conditioner and preparation method thereof - Google Patents
Plant hair conditioner and preparation method thereof Download PDFInfo
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- CN105078847A CN105078847A CN201510606451.4A CN201510606451A CN105078847A CN 105078847 A CN105078847 A CN 105078847A CN 201510606451 A CN201510606451 A CN 201510606451A CN 105078847 A CN105078847 A CN 105078847A
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Abstract
The invention discloses a plant hair conditioner and a preparation method thereof. The plant hair conditioner comprises, by mass, 1-5% of grape seed extract, 1-5% of avocado extract, 1-3% of shea butter, 1-5% of 16-18 alcohol, 1-5% of propylene glycol, 0.2-1% of amino acid moisturizing agent and the balance of rice washing water. The preparation method includes the steps that the 16-18 alcohol and the shea butter serve as an oil phase, the propylene glycol and the rice washing water serve as a water phase, the oil phase and the water phase are stirred and heated to 80-85 DEG C, after the raw materials are completely and evenly dissolved, the water phase is slowly added into the oil phase while the oil phase is stirred, stirring is continued, cooling is performed while stirring is performed, when the temperature is decreased to 45-50 DEG C, the grape seed extract, the avocado extract and the amino acid moisturizing agent are added, stirring is continued, and after stirring is performed evenly, the mixture is cooled and taken out for standing for 20-30 h so as to obtain the plant hair conditioner. The plant hair conditioner has the functions of resisting oxidation and ultraviolet rays, supplementing needed nutrition for hair, making the hair softer and the like.
Description
Technical field
The invention belongs to Cosmetic Manufacture technical field, be specifically related to kind of plant hair conditioner and preparation method thereof.
Background technology
Hair is washed and protected is personal daily nursing behavior, caused by the daily metabolism of human body and living environment, hair and scalp have certain oils and fats, antiperspirant dirt, the pollutant such as sand and dust, along with the continuous deterioration of people's living environment, PM2.5 in air constantly rises, very large puzzlement is caused to the life of people, because the PM2.5 particle diameter in atmospheric pollution is little, specific surface area is large, active strong, easily subsidiary poisonous, harmful substance (such as, heavy metal, microorganism etc.), the time of staying is in an atmosphere long, these fine particles can deep enoughly deposit in the hair hair scale sheet gap of people, more deeply can deposit to the hair follicle root of scalp, thus affect people's hair and scalp health.
Mostly the hair conditioner existed in prior art is that chemical substance is composite and obtains, as foam performance surfactant component laureth sulfuric ester ammonium, ammonium lauryl sulfate, the sweet Lay alkali of dodecanamide propyl, the cation opsonizing agent of cellulose origin synthesis and silicone oil, these materials can wash away the oils and fats of hair surface to a certain extent, dust, hair is nursed, but, chemical composition remains on scalp or hair also can produce harm to human body, silicate-containing oil conditioner product remain hair and hair follicle place, make hair follicle breathe be obstructed, nutrition vim and vigour are under-supply, even cause alopecia problem.
Summary of the invention
In order to solve the problem, the invention provides a kind of plant hair conditioner, for hair supplements desired nutritional, make hair submissiveer, and naturally not stimulate, can not hair follicle be blocked.
One kind of plant hair conditioner, by percentage to the quality, comprises following component:
Semen Vitis viniferae extract 1 ~ 5%, shea extract 1 ~ 5%, shea butter 1 ~ 3%, 16 ~ 18 alcohol 1 ~ 5%, propylene glycol 1 ~ 5%, amino acid humectant 0.2 ~ 1%, surplus are washing water of rice.
As preferably, by percentage to the quality, described plant hair conditioner comprises following component:
Semen Vitis viniferae extract 2 ~ 5%, shea extract 2 ~ 5%, shea butter 1.5 ~ 3%, 16 ~ 18 alcohol 2 ~ 5%, propylene glycol 2 ~ 5%, amino acid humectant 0.5 ~ 1%, surplus are washing water of rice.
As more preferably, by percentage to the quality, described plant hair conditioner comprises following component:
Semen Vitis viniferae extract 4%, shea extract 5%, shea butter 3%, 16 ~ 18 alcohol 5%, propylene glycol 3%, amino acid humectant 1%, surplus are washing water of rice.
As preferably, the preparation method of described Semen Vitis viniferae extract comprises:
(1) Semen Vitis viniferae is carried out pulverizing and obtain Semen Vitis viniferae powder, Semen Vitis viniferae powder is mixed 1:30 ~ 40 by volume with deionized water, after mix homogeneously, remove filtering residue, obtain Grape seed solution;
(2) at described Grape seed solution, in add with its volume ratio be that the dehydrated alcohol of 1:2 ~ 3 carries out supersound extraction 10 ~ 15h, revolve steaming, obtain Semen Vitis viniferae crude extract;
(3) Semen Vitis viniferae crude extract polymeric membrane is separated, obtains Semen Vitis viniferae refining liquid;
(4) finally Semen Vitis viniferae refining liquid is carried out spraying dry, pulverizes and obtains Semen Vitis viniferae extract.
As preferably, the preparation method of described shea extract comprises:
(1) shea and deionized water are squeezed 1:20 ~ 30 by volume, remove filtering residue, obtain shea solution;
(2) adding in described shea solution with its volume ratio is that the dehydrated alcohol of 1:2 ~ 3 carries out supersound extraction 10 ~ 15h, revolves steaming, obtains shea crude extract;
(3) shea crude extract polymeric membrane is separated, obtains shea refining liquid;
(4) finally shea refining liquid carried out spraying dry, pulverize and obtain shea extract.
As preferably, inlet temperature when shea extracting solution or Semen Vitis viniferae extracting solution being carried out spraying dry is 140 ~ 160 DEG C, and leaving air temp is 70 ~ 90 DEG C.
As preferably, the preparation method of described washing water of rice is: in rice, add deionized water eluriate, and filters rice, obtains described washing water of rice; Wherein the volume ratio of rice and deionized water is 1:10 ~ 20.
Present invention also offers the preparation method of above-mentioned plant hair conditioner, comprise: using 16 ~ 18 alcohol and shea butter as oil phase, propylene glycol and washing water of rice are as aqueous phase, respectively oil phase and aqueous phase are heated with stirring to 80 ~ 85 DEG C, after raw material is all uniformly dissolved, while stir oil phase, while aqueous phase is gently added in oil phase, continue to stir, stir while lower the temperature, when temperature is down to 45 ~ 50 DEG C, add Semen Vitis viniferae extract, shea extract and amino acid humectant, continue to stir, to be mixed evenly after, cooling, take out, leave standstill 20 ~ 30h, described plant hair conditioner can be obtained.
As preferably, mixing speed is 80 ~ 120r/min.
Compared with prior art, beneficial effect of the present invention is embodied in:
(1) low in raw material price of plant hair conditioner of the present invention, preparation method is simple and convenient, and its each index meets the requirement of hair conditioner (QB/T1975-2013) and " cosmetics health specification " version specification in 2007.And the present invention has antioxidation, uvioresistant, to supplement desired nutritional for hair, the effect such as make hair submissiveer, more beautiful, plant hair conditioner of the present invention environmental protection, reduce environmental pollution, and do not grow dandruff, do not block hair follicle;
(2) plant hair conditioner hair conditioner of the present invention is compared with the product of existing market, its viscosity, smear degree, easily rinse, bath time feel, wet send out a feel, wet send out a feel, dry when sending out the performance such as smooth degree, wet Comb rationality, dry cardability, loft, hair soft degree, glossiness and the elasticity sent out all be superior to existing market product.
Accompanying drawing explanation
Fig. 1 is the comparing result of plant hair conditioner of the present invention and existing hair conditioner product difference viscosity, smear and washability aspect in use.
Fig. 2 for after using plant hair conditioner of the present invention and existing hair conditioner product, the comparing result of the smooth degree of hair.
Fig. 3 for after using plant hair conditioner of the present invention and existing hair conditioner product, the wet Comb rationality of hair and the comparing result of hair drying comb rationality.
Fig. 4, for after use plant hair conditioner of the present invention and existing hair conditioner product, wets and sends out and the dry comparing result sending out rear hair pliability.
Fig. 5, for after use plant hair conditioner of the present invention and existing hair conditioner product, does the comparing result of a loft for hair after sending out, hair gloss degree and hair elasticity sensation.
Fig. 6 is the comparing result of evaluator to overall assessment after plant hair conditioner of the present invention and existing hair conditioner product.
Fig. 7 is the comparing result of experimenter to favorable rating after plant hair conditioner of the present invention and existing hair conditioner product.
Detailed description of the invention
The preparation method of plant hair conditioner of the present invention, comprises the following steps:
(1) Semen Vitis viniferae and shea solution is prepared
Collect Semen Vitis viniferae, Semen Vitis viniferae is shattered, obtains Semen Vitis viniferae powder, Semen Vitis viniferae powder is mixed 1:30 ~ 40 by volume with deionized water, after mix homogeneously, remove filtering residue, obtain Grape seed solution;
With commercially available shea for raw material, shea and deionized water are squeezed 1:20 ~ 30 by volume, remove filtering residue, obtain shea solution;
(2) Semen Vitis viniferae crude extract and shea crude extract is prepared
Respectively being that the dehydrated alcohol of 1:2 ~ 3 carries out supersound extraction 10 ~ 15h by adding in the solution in step (1) with its volume ratio, revolving steaming, obtaining Semen Vitis viniferae crude extract and shea crude extract;
(3) Semen Vitis viniferae refining liquid and shea refining liquid is prepared
Shea crude extract polymeric membrane is separated, obtains shea refining liquid; Wherein polymeric membrane is 5000 ~ 10000 daltonian polymeric membranes for retaining component, and filter pressure is 0.2MPa ~ 0.5Mpa, and filtration temperature is room temperature;
(4) Semen Vitis viniferae extract, shea extract is prepared
Semen Vitis viniferae refining liquid in step (3) and shea refining liquid are carried out spraying dry (wherein: spraying dry inlet temperature is 140 ~ 160 DEG C respectively, leaving air temp is 70 ~ 90 DEG C), the solids of gained after drying is pulverized, obtain Semen Vitis viniferae extract powder and shea extract powder respectively, cold preservation is for subsequent use.
(5) preparation of washing water of rice
With commercially available rice for raw material, add deionized water and eluriate, wherein the volume ratio of rice and deionized water is 1:10 ~ 20, filters rice, obtains washing water of rice.
(6) using 16 ~ 18 alcohol and shea butter as oil phase, propylene glycol and washing water of rice are as aqueous phase, respectively oil phase and aqueous phase are heated with stirring to 80 ~ 85 DEG C, after raw material is all uniformly dissolved, while stir oil phase, while aqueous phase is gently added in oil phase, continue to stir, stir and lower the temperature, when temperature is down to 45 ~ 50 DEG C, add Semen Vitis viniferae extract, shea extract and amino acid humectant, continue to stir, to be mixed evenly after, cooling, take out, leave standstill 20 ~ 30h, described plant hair conditioner can be obtained.
Above-mentioned experimental technique, if no special instructions, is conventional method; Described reagent and material, if no special instructions, all can obtain from commercial channels.Step has according to the method described above carried out the repeatedly preparation of plant hair conditioner, is only the raw material type and the content that have adjusted plant hair conditioner of the present invention, obtains a series of embodiment, specifically in table 1.
The plant hair conditioner of the present invention that table 1 different material kind and content prepare
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| Semen Vitis viniferae extract/% | 1.0 | 3.0 | 5.0 | 4.0 | 2.0 | 5.0 |
| Shea extract/% | 2.0 | 1.0 | 3.0 | 5.0 | 4.0 | 3.5 |
| Shea butter/% | 3.0 | 1.0 | 3.0 | 3.0 | 3.0 | 2.0. |
| 16 ~ 18 alcohol/% | 1.0 | 3.0 | 2.0 | 5.0 | 2.0 | 3.0 |
| Propylene glycol/% | 5.0 | 5.0 | 1.0 | 3.0 | 2.5 | 5.0 |
| Amino acid humectant/% | 1.0 | 0.2 | 0.5 | 1.0 | 0.6 | 0.8 |
| Washing water of rice/% | 87.0 | 86.8 | 85.5 | 79.0 | 85.9 | 80.7 |
| Overall merit | ☆☆☆ | ☆☆☆ | ☆☆☆☆ | ☆☆☆☆☆ | ☆☆☆☆ | ☆☆☆☆ |
Note: adopt the test of crowd's half a head, carry out overall merit, ☆ is more, shows that overall merit is higher.
The plant hair conditioner prepared according to table 1 formula draws after testing: noxious substance arsenic, lead, hydrargyrum all do not detect; Excrement colibacillus group, Pseudomonas aeruginosa and staphylococcus aureus all do not detect; Total plate count < 10CFU/ml; Yeast and mold sum < 10CFU/ml.Keep 24h in (40 ± 1) DEG C, return to after room temperature all without lamination; Keep 24h in (-8 ± 2) DEG C, return to after room temperature all without lamination; Total solid >=4.0/%, each index all meets the requirement of hair conditioner (QB/T1975-2013) and " cosmetics health specification " version specification in 2007.
The effect evaluation method of the plant hair conditioner that embodiment 1 ~ 6 prepares adopts the test of crowd's half a head, and appraisal procedure is as follows:
Experimenter for hair dry up, the crowd of the dry hair quality of hair, by the effect having experience evaluator to carry out test products.
Evaluator first helps experimenter to clean hair twice with the shampoo 10 ~ 20g of clean type, rinse with water, pinch the most of moisture on sending out of decaptitating, hair therefrom between be divided into left and right two parts, two half a heads respectively use a test hair conditioner sample 20g, left and right two parts hair is gently rubbed respectively with right-hand man, be applied on all hairs completely to hair conditioner, and assess denseness and the spreadability of hair conditioner, approximately rub 3 minutes, then wash by water, the compliance of sensation hair when washing by water, hair conditioner washability, the smoothness being felt the right and left hair by evaluator is had after flushing, flexibility, and with two identical combs combing both sides hair simultaneously, assess easy cardability.With hair dryer hair blown to 8 one-tenth and do, again assess the performance of the compliance of both sides hairs, glossiness and combing;
Make evaluation according to above-mentioned evaluation methodology, the data of table 1 show that the overall merit of example 4 is the highest, preferred embodiment 4.Example 4 is prepared plant hair conditioner according to above-mentioned preparation technology, prepared hair conditioner (being labeled as: Y) is contrasted with the hair conditioner brand A that is in great demand in market (being labeled as: YA), according to washing hair products crowd test (half a head test) method, experimenter is tested, each stage performance of hair washing is given a mark, 5 are divided into best result, 1 point minimum point, synthetic data is averaged, finally by tidal data recovering statistical analysis.
(1) comfort level that hair conditioner uses has viscosity, property easy to apply and easy washability three indexs, and wherein sliminess mark is 1 ~ 5 point, more better close to 3 points, too thick higher than 3 points, too rare lower than 3 points, the results are shown in Figure 1.
As can be seen from Figure 1, the viscosity of plant hair conditioner of the present invention is slightly better than existing market product, smears degree and existing market product similar, easily rinses Performance Ratio existing market product expression and obtains more excellent.
(2) when hair conditioner uses, the comparison of smooth degree, is divided into sensation during bath, after rinsing wet send out sensation and hair do after submissive sense, the results are shown in Figure 2.
As can be seen from Figure 2, comparatively existing market product is good for the feel of hair conditioner of the present invention when washing by water, and feel when wet is slightly better than existing market product, but is more or less the same, and does not have significant difference, and when dry, smooth degree is slightly better than existing market product.
(3) the rear easy cardability of hair conditioner, is divided into wet Comb rationality and hair drying comb rationality, the results are shown in Figure 3.As can be seen from Figure 3, wet send out and the dry easy cardability sent out all good than existing market product.
(4) the rear hair pliability of hair conditioner, when being divided into wet sending out pliability and dry send out after pliability, the results are shown in Figure 4.Send out and do wet on hair soft degree when sending out as can be seen from Figure 4, test sample is all superior than existing market product.
(5) hair conditioner does the comparison that the performance test after sending out is divided into loft, hair gloss degree and hair elasticity to feel, loft is more better close to 1, the results are shown in Figure 5.
The showing as of hair after dry sending out: the hair after the washing of given the test agent is more docile, and do not have existing market product fluffy, glossiness and elasticity are all good than existing market product.
(6) aggregate performance degree and preference contrast, marked to the aggregate performance of two hair conditioner by evaluator, experimenter then selects the fancy grade of two hair conditioner, the results are shown in Figure 6 and Fig. 7.
Appraiser assesses the aggregate performance of two hair conditioner as can be seen from Figure 6, and given the test agent is better than existing market product, and can see that experimenter is more also that given the test agent far exceeds existing market product at the fancy grade of two hair care degree from Fig. 7.
In addition, also sent by hair conditioner prepared by laboratory barber shop and social crowd to be suitable for, applicable crowd is healed hundred people, and satisfaction reaches more than 95%, has good repair to damaged hair.
Finally it should be noted that, above embodiment is the unrestricted technical scheme of the present invention in order to explanation only, although with reference to above-described embodiment to invention has been detailed description, those skilled in the art are to be understood that, still can modify to the present invention or equivalent replacement, and not departing from any modification or partial replacement of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.
Claims (10)
1. a kind of plant hair conditioner, is characterized in that, by percentage to the quality, comprises following component:
Semen Vitis viniferae extract 1 ~ 5%, shea extract 1 ~ 5%, shea butter 1 ~ 3%, 16 ~ 18 alcohol 1 ~ 5%, propylene glycol 1 ~ 5%, amino acid humectant 0.2 ~ 1%, surplus are washing water of rice.
2. plant hair conditioner as claimed in claim 1, it is characterized in that, by percentage to the quality, described plant hair conditioner comprises following component:
Semen Vitis viniferae extract 2 ~ 5%, shea extract 2 ~ 5%, shea butter 1.5 ~ 3%, 16 ~ 18 alcohol 2 ~ 5%, propylene glycol 2 ~ 5%, amino acid humectant 0.4 ~ 1%, surplus are washing water of rice.
3. plant hair conditioner as claimed in claim 2, it is characterized in that, by percentage to the quality, described plant hair conditioner comprises following component:
Semen Vitis viniferae extract 4%, shea extract 5%, shea butter 3%, 16 ~ 18 alcohol 5%, propylene glycol 3%, amino acid humectant 1%, surplus are washing water of rice.
4. plant hair conditioner as claimed in claim 1, it is characterized in that, the preparation method of described Semen Vitis viniferae extract comprises:
(1) Semen Vitis viniferae is carried out pulverizing and obtain Semen Vitis viniferae powder, Semen Vitis viniferae powder is mixed 1:30 ~ 40 by volume with deionized water, after mix homogeneously, remove filtering residue, obtain Grape seed solution;
(2) at above-mentioned Grape seed solution, in add with its volume ratio be that the dehydrated alcohol of 1:2 ~ 3 carries out supersound extraction 10 ~ 15h, revolve steaming, obtain Semen Vitis viniferae crude extract;
(3) Semen Vitis viniferae crude extract polymeric membrane is separated, obtains Semen Vitis viniferae refining liquid;
(4) finally Semen Vitis viniferae refining liquid is carried out spraying dry, pulverizes and obtains Semen Vitis viniferae extract.
5. plant hair conditioner as claimed in claim 1, it is characterized in that, the preparation method of described shea extract comprises:
(1) shea and deionized water are squeezed 1:20 ~ 30 by volume, remove filtering residue, obtain shea solution;
(2) adding in above-mentioned shea solution with its volume ratio is that the dehydrated alcohol of 1:2 ~ 3 carries out supersound extraction 10 ~ 15h, revolves steaming, obtains shea crude extract;
(3) shea crude extract polymeric membrane is separated, obtains shea refining liquid;
(4) finally shea refining liquid carried out spraying dry, pulverize and obtain shea extract.
6. the plant hair conditioner as described in as arbitrary in claim 4 or 5, it is characterized in that, described polymeric membrane is 5000 ~ 10000 daltonian polymeric membranes for retaining component, and filter pressure is 0.2 ~ 0.5Mpa, and temperature is room temperature.
7. the plant hair conditioner as described in as arbitrary in claim 4 or 5, it is characterized in that, shea refining liquid or Semen Vitis viniferae refining liquid are carried out spraying dry, and spray-dired inlet temperature is 140 ~ 160 DEG C, and leaving air temp is 70 ~ 90 DEG C.
8. plant hair conditioner as claimed in claim 1, it is characterized in that, the preparation method of described washing water of rice is: in rice, add deionized water eluriate, and filters rice, obtains described washing water of rice; Wherein the volume ratio of rice and deionized water is 1:10 ~ 20.
9. the preparation method of the plant hair conditioner as described in as arbitrary in claim 1 ~ 8, it is characterized in that, comprise: using 16 ~ 18 alcohol and shea butter as oil phase, propylene glycol and washing water of rice are as aqueous phase, respectively oil phase and aqueous phase are heated with stirring to 80 ~ 85 DEG C, after raw material is all uniformly dissolved, while stir oil phase, while aqueous phase is gently added in oil phase, continue to stir, stir while lower the temperature, when temperature is down to 45 ~ 50 DEG C, add Semen Vitis viniferae extract, shea extract and amino acid humectant, continue to stir, to be mixed evenly after, cooling, take out, leave standstill 20 ~ 30h, described plant hair conditioner can be obtained.
10. the preparation method of plant hair conditioner as claimed in claim 9, it is characterized in that, mixing speed is 80 ~ 120r/min.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108836895A (en) * | 2018-06-27 | 2018-11-20 | 跨越生物科技（滁州）有限公司 | One kind can the submissive antibacterial nutritious hair conditioner of hair |
| CN109908057A (en) * | 2019-04-01 | 2019-06-21 | 贵州阿斯科科技开发有限公司 | A kind of Chinese herbal medicine skin care item and preparation method thereof |
| CN113181101A (en) * | 2021-05-26 | 2021-07-30 | 建昌帮药业有限公司 | Hair conditioner |
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| CN104224634A (en) * | 2014-09-30 | 2014-12-24 | 澳宝化妆品（惠州）有限公司 | Hair conditioning combination and application thereof in hair conditioning products |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104224634A (en) * | 2014-09-30 | 2014-12-24 | 澳宝化妆品（惠州）有限公司 | Hair conditioning combination and application thereof in hair conditioning products |
Non-Patent Citations (3)
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| 佚名: "化妆品配方", 《日用化学品科学》 * |
| 李笑廷等: "美容美发市场新品", 《日用化学品科学》 * |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108836895A (en) * | 2018-06-27 | 2018-11-20 | 跨越生物科技（滁州）有限公司 | One kind can the submissive antibacterial nutritious hair conditioner of hair |
| CN109908057A (en) * | 2019-04-01 | 2019-06-21 | 贵州阿斯科科技开发有限公司 | A kind of Chinese herbal medicine skin care item and preparation method thereof |
| CN113181101A (en) * | 2021-05-26 | 2021-07-30 | 建昌帮药业有限公司 | Hair conditioner |
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