CN104996718A - Cavia porcllus pneumonia preventing and curing feed preparation method - Google Patents
Cavia porcllus pneumonia preventing and curing feed preparation method Download PDFInfo
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- CN104996718A CN104996718A CN201510426326.5A CN201510426326A CN104996718A CN 104996718 A CN104996718 A CN 104996718A CN 201510426326 A CN201510426326 A CN 201510426326A CN 104996718 A CN104996718 A CN 104996718A
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Abstract
The present invention discloses a cavia porcllus pneumonia preventing and curing feed preparation method which comprises the following steps: adding towel gourd vine juice while stir-frying fructus arctii and roripa montana, cooling, frying again with almonds, boiling, concentrating and filtering to obtain a first filtrate; mixing and infiltrating capsella bursa-pastoris with white wine, water-proof steaming, drying and smashing, adding fried raw glycyrrhiza uralensis and heartleaf houttuynia herbs together to conduct decocting, concentrating and filtering to obtain a second filtrate; and using ailanthus altissima leaves and artemisia argyi leaves as main components, mixing and smashing, adding the first and second filtrates, decocting, concentrating, refrigerating, mixing with tapioca flour to conduct mixing and pelleting, and oven-drying and sterilizing to obtain the cavia porcllus pneumonia preventing and curing feed. The preparation method ensures individual drug property of the medicinal materials, and the feed reduces the pneumonia morbidity of cavia porcllus after the cavia porcllus is fed by the feed, decreases the bacterial gastrointestinal disease infection rate of cavia porcllus, enhances the immunity of cavia porcllus, and enables the melanin in cavia porcllus to increase and the cavia porcllus meat to have better health-care effects.
Description
Technical field
The present invention relates to feed producing method, more particularly, the present invention relates to a kind of preparation method preventing and treating the feed of black globefish pneumonia.
Background technology
Black globefish, originates in South America, is a kind of globefish that build is less, and another name guinea pig, wild mountain globefish, netherlands rat, cavy, because whole body black is gained the name.Black globefish is had a sweet temper, and likes gregarious, timid, be afraid of frightened, be afraid of interference, oxyacoia.Whole body black wool, Black Eyes, black face, black pin, without tail, ear and four limbs short and small, be not good at jump, generally do not sting people, also do not arrest.
Black globefish is mammality plant-eating animal, its bodily form little (0.5--0.65 kilogram), medicine, eat dual-purpose.Black globefish, based on herbvore, is typical grain-saving type hog, crosses the raising of 3-4 month, can go on the market to body weight 0.65 kilogram.Ancient Chinese just has the custom of edible black globefish leopard cat meat, and it can be used as high-grade edible wild herbs meat and fish dishes to be selected into Chinese famous dish spectrum.It is card that the delicious food of black globefish leopard cat has " the globefish leopard cat of ringdove in the sky, ground " by oneself.
At present, wild black globefish is progressively exhausted, and the black globefish of artificial feeding may meet with various disease at growing period, it is wherein the peak period of black globefish pneumonia infection at the beginning of last month of spring in winter, the symptom that metainfective black globefish occurs accelerated breathing, dry cough, chilly, temperature decline, subtracts food or go on a hunger strike, may cause death time serious, the demand therefore in order to make the quantity of black globefish meet people, need badly and find novel black globefish feed to prevent black globefish pneumonia, make the growth that black globefish energy is healthy.
Summary of the invention
An object of the present invention is to solve at least the problems referred to above and/or defect, and the advantage will illustrated at least is below provided.
A further object of the invention is to provide a kind of preparation method preventing and treating the feed of black globefish pneumonia, luffa vine juice infiltrates great burdock achene and decocts together with almond with rear in lepidium seed, raw Radix Glycyrrhizae after shepherd's purse and frying decocts together with fish raw meat, join with in fresh Chinese toon leaf and the tarragon feed that is key component respectively, the medicinal material property of medicine separately can better be ensured, reduce the incidence of disease of black globefish pneumonia, decrease the infection rate of the bacillary enterogastric diseases of black globefish, enhance the immunity of black globefish, melanin in black globefish body is increased, and black globefish meat has better health-care effect.
In order to realize, according to these objects of the present invention and other advantage, providing a kind of preparation method preventing and treating the feed of black globefish pneumonia, comprising:
Step one: after great burdock achene and lepidium seed are mixed by quality proportioning 1: 1, frying 10 ~ 15min at 50 ~ 55 DEG C, stir-fry limit, limit adds luffa vine juice, the mass ratio of described luffa vine juice and described great burdock achene is 1: 5, after frying completes, cooling obtains mixture, almond is added in described mixture, described almond and described great burdock achene mass ratio are 1: 2, frying 3 ~ 6min at 45 ~ 50 DEG C, pulverize after cooling, obtain the first mixture, in described first mixture, add distilled water decoct 1 ~ 2 time, filtration after each decoction completes, refilter after coarse filtration liquid is merged, obtain the first coarse filtration liquid, the first concentrate is obtained after described first coarse filtration liquid is concentrated, after refrigeration 12 ~ 18h, get the supernatant liquid filtering of described first concentrate, collect the first filtrate,
Step 2: cut the segment of growing into 2 ~ 3cm after being cleaned by shepherd's purse, described shepherd's purse and described great burdock achene mass ratio are 2: 1, shepherd's purse after segment and white spirit mixed are infiltrated 1h, the mass ratio of described white wine and described shepherd's purse is 1: 6 ~ 1: 8, after shepherd's purse water proof after infiltration is steamed 20 ~ 30min, dry 15 ~ 20min at 70 ~ 75 DEG C, for subsequent use after dried shepherd's purse is pulverized;
Be that 1: 1 mixing is rear by raw Radix Glycyrrhizae and cordate houttuynia according to mass ratio to pulverize, cool for subsequent use at 65 ~ 70 DEG C after frying 10 ~ 15min, shepherd's purse after pulverizing and raw Radix Glycyrrhizae after frying and cordate houttuynia mixture are mixed according to mass ratio 2: 1, after obtaining the second mixture, adding distil water decocts 1 ~ 3 time, filtration after each decoction completes, through centrifugation after filtrate is merged, the second coarse filtration liquid is obtained after filtration, the second concentrate is obtained after concentrated, refrigeration 10 ~ 15h, the supernatant liquid filtering getting the second concentrate obtains the second filtrate;
Step 3: pulverize after Chinese toon leaf is mixed with tarragon, wherein, the mass ratio of Chinese toon leaf, tarragon and described great burdock achene is 10: 3: 1, adds described first filtrate and described second filtrate, after obtaining the 3rd mixture after pulverizing, adding distil water decocts 3 times, filtration after each decoction completes, filters after the mixture filtrate of 3 gained being merged, obtains the 3rd filtrate, the pH regulating described 3rd filtrate with citric acid is 5.2 ~ 5.8, obtains the 3rd concentrate after concentrated;
Step 4: after the stored refrigerated 20 ~ 24h of described 3rd concentrate, mix rear granulation with tapioca starch according to quality proportioning 7: 1, sterilizing after drying, packing, preserves under room temperature.
Preferably, the leaf of Chinese toon described in step 3 is through pretreatment: after being cleaned by Chinese toon leaf, in yellow rice wine, infiltrate 2 ~ 3h, the mass ratio of yellow rice wine and Chinese toon leaf is 1: 3 ~ 1: 4, after Chinese toon leaf and yellow rice wine mixture water proof are steamed 15 ~ 20min, at 60 ~ 65 DEG C, dry 20 ~ 30min obtains; Described in step 3, tarragon is through pretreatment: after being cleaned by tarragon, is infiltrate after 10 ~ 15min in the alcohol of 95% in volume fraction, with distilled water flushing 1 ~ 2 time, and dry 10 ~ 20min at 55 ~ 60 DEG C.
Preferably, in first mixture described in step one, adding distil water decocts 2 times, the consumption of twice adding distil water is 6 times amount of described first mixture quality, in second mixture described in step 2, adding distil water decocts 3 times, the consumption of distilled water is followed successively by 8 times amount of described second mixture quality, 6 times amount and 6 times amount, in 3rd mixture described in step 3, adding distil water decocts 3 times, and the consumption of distilled water is followed successively by 8 times amount of described 3rd mixture quality, 6 times amount and 6 times amount.
Preferably, decoct 2 times after the first mixture adding distil water described in step one, first time decocts 60min at 45 DEG C, and second time decocts 40min at 40 DEG C; In second mixture described in step 2, adding distil water decocts 3 times, and first time decocts 60min at 72 DEG C, and second time decocts 50min at 70 DEG C, and third time decocts 30min at 68 DEG C; In 3rd mixture described in step 3, adding distil water decocts 3 times, and first time decocts 60min at 70 DEG C, and second time decocts 40min at 68 DEG C, and third time decocts 30min at 65 DEG C.
Preferably, in step one, the density of concentrated gained first concentrate is 1.06g/mL, and in step 2, the density of concentrated gained second concentrate is 1.03g/mL, and in step 3, the density of concentrated gained the 3rd concentrate is 1.08g/mL.
Preferably, step one all adopts reduced pressure concentration to concentrating in step 3, take recirculated water as heat medium, in step one, described first coarse filtration liquid is concentrated in vacuum decompressioning and concentrating tank, control temperature is 50 ~ 55 DEG C, vacuum is 0.05 ~ 0.06MPa, in step 2, described second coarse filtration liquid is concentrated in vacuum decompressioning and concentrating tank, control temperature is 65 ~ 70 DEG C, vacuum is 0.05 ~ 0.06MPa, in step 3, described 3rd filtrate is concentrated in vacuum decompressioning and concentrating tank, control temperature is 60 ~ 65 DEG C, vacuum is 0.05 ~ 0.06MPa.
Preferably, in step 2, centrifugation is operating as and controls centrifuge speed 6000 ~ 7000r/min, gets the supernatant after centrifugation after centrifugal 10 ~ 15min.
Preferably, in the filter operation in step 2 after centrifugation and step 3 mixture filtrate merge after filter operation all adopt aperture to be the filtering with microporous membrane of 0.45 ~ 0.8 μm, control operation pressure is 0.015MPa, and flow velocity is 5 ~ 8ml/min.
The present invention at least comprises following beneficial effect:
1, luffa vine juice is added during frying, the compositions such as the saponin contained in luffa vine juice have relieving cough and reducing sputum and antibacterial action, luffa vine juice is infiltrated in great burdock achene and lepidium seed, can better play a role with active ingredients such as the arctiin in great burdock achene and the benzyl mustard oils in lepidium seed, reach the effect of preventing and treating pneumonia, after adding almond, frying at the frying temperature lower than great burdock achene and lepidium seed, the active ingredient in almond can not be destroyed, the concocting method of this kind frying at twice can make the active ingredient for pneumonia in medicinal material more easily decoct out, improve medicinal material utilization rate.
2, shepherd's purse is after white wine infiltrates, carrotene wherein, vitamin C and other active principles is made more easily to decoct out, white wine infiltrates certain sterilizing effect, water proof steams rear white wine and is distilled out of, do not residue in shepherd's purse, raw Radix Glycyrrhizae, cordate houttuynia and shepherd's purse decoct together, can prevent and treat pneumonia, decrease the infection rate of the bacillary enterogastric diseases of black globefish, enhance the immunity of black globefish.
3, tarragon after infiltrating in alcohol, and the active ingredient making the volatile oil, flavones etc. wherein contained have bactericidal action more easily decocts out.
4, the great burdock achene after the infiltration of luffa vine juice decocts 2 times after frying together with lepidium seed and almond, and raw Radix Glycyrrhizae, cordate houttuynia and shepherd's purse decoct 3 times together, decoct operation of being more convenient in batches, and the medicinal material property of medicine separately can better be ensured, reduce the destruction to active ingredient in medicinal material, wherein, raw Radix Glycyrrhizae, cordate houttuynia and shepherd's purse need to decoct more times than great burdock achene, lepidium seed and almond, just can make the better stripping of the active ingredient in raw Radix Glycyrrhizae, cordate houttuynia and shepherd's purse.
5, select fresh Chinese toon leaf and tarragon to be feed key component, wide material sources are with low cost, and after the black globefish of feeding, black globefish has satiety, and after adding tarragon, nutritional labeling is abundanter, improves feed taste, enhances the immunity of black globefish, reduce the incidence of disease of pneumonia.
6, adopt that micro porous filtration, transition speed higher than conventional filtering method precision is fast, absorption is few, to come off without medium and easy to operate.
7, reduced pressure concentration mode is taked, control vacuum is 0.05 ~ 0.06MPa, more fully the active ingredient in medicinal material can be concentrated out than traditional normal pressure condensing mode, control temperature is 70 ~ 75 DEG C, temperature is no more than 100 DEG C, can not destroy the active ingredient in medicinal material, take recirculated water as heat medium, make temperature more easy to control, be heated evenly.
8, after adopting this kind of black globefish of black globefish feed feeding, the black globefish pneumonia incidence of disease obviously declines, black globefish hair color vivid and in body melanin increase, black globefish meat has better health-care effect.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, can implement according to this with reference to description word to make those skilled in the art.
Embodiment 1
Step one: after great burdock achene and lepidium seed being mixed by quality proportioning 1: 1,50 DEG C of frying 10min, stir-fry limit, limit adds luffa vine juice, and the mass ratio of described luffa vine juice and described great burdock achene is 1: 5, and after frying completes, cooling obtains mixture.
In described mixture, add almond, described almond and described great burdock achene mass ratio are 1: 2, at 45 DEG C of frying 3min, pulverize, obtain the first mixture after cooling.
In described first mixture, add distilled water decoct 1 time, at 45 DEG C, decoct 60min, the consumption of institute's adding distil water is 6 times amount of described first mixture quality, has decocted rear filtration, refilters, obtain the first coarse filtration liquid after being merged by coarse filtration liquid.
By the described first thick filtrate reduced in volume, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 50 DEG C, vacuum is 0.05MPa, obtains the first concentrate that density is 1.06g/mL, after concentrated after refrigeration 12h, get the supernatant liquid filtering of described first concentrate, collect the first filtrate.
Step 2: cut the segment of growing into 2cm after being cleaned by shepherd's purse, described shepherd's purse and described great burdock achene mass ratio are 2: 1, shepherd's purse after segment and white spirit mixed are infiltrated 1h, the mass ratio of described white wine and described shepherd's purse is 1: 6, after shepherd's purse water proof after infiltration is steamed 20min, dry 15min at 70 DEG C, for subsequent use after dried shepherd's purse is pulverized.
Be that 1: 1 mixing is rear by raw Radix Glycyrrhizae and cordate houttuynia according to mass ratio to pulverize, cool for subsequent use after 65 DEG C of frying 10min.
Shepherd's purse after pulverizing and raw Radix Glycyrrhizae after frying and cordate houttuynia mixture are mixed according to mass ratio 2: 1, after obtaining the second mixture, adding distil water decocts 1 time, 60min is decocted at 72 DEG C, the consumption of distilled water is 8 times amount of described second mixture quality, filtration after decoction completes, through centrifugation after filtrate is merged, centrifugation is operating as and controls centrifuge speed 6000r/min, the supernatant after centrifugation is got after centrifugal 10min, employing aperture is the filtering with microporous membrane of 0.45 μm, control operation pressure is 0.015MPa, flow velocity is 5ml/min, obtain the second coarse filtration liquid.
By the described second thick filtrate reduced in volume, be heat medium with recirculated water, concentrate in vacuum decompressioning and concentrating tank, control temperature is 65 DEG C, and vacuum is 0.05MPa, obtains the second concentrate that density is 1.03g/mL, after refrigeration 10h, the supernatant liquid filtering getting the second concentrate obtains the second filtrate.
Step 3: after being cleaned by fresh Chinese toon leaf, infiltrate 2h in yellow rice wine, the mass ratio of yellow rice wine and Chinese toon leaf is 1: 3, after Chinese toon leaf and yellow rice wine mixture water proof are steamed 15min, for subsequent use after dry 20min at 60 DEG C; After fresh tarragon is cleaned, be after infiltrating 10min in the alcohol of 95% in volume fraction, with distilled water flushing 1 time, for subsequent use after dry 10min at 55 DEG C.
Pulverize after Chinese toon leaf after process is mixed with tarragon, wherein, Chinese toon leaf, the mass ratio of tarragon and described great burdock achene is 10: 3: 1, described first filtrate and described second filtrate is added after pulverizing, after obtaining the 3rd mixture, adding distil water decocts 3 times, first time decocts 60min at 70 DEG C, second time decocts 40min at 68 DEG C, third time decocts 30min at 65 DEG C, the consumption of distilled water is followed successively by 8 times amount of described 3rd mixture quality, 6 times amount and 6 times amount, filtration after each decoction completes, the mixture filtrate of 3 gained is merged, employing aperture is the filtering with microporous membrane of 0.45 μm, control operation pressure is 0.015MPa, flow velocity is 5ml/min, obtain the 3rd filtrate.
Regulate the pH of described 3rd filtrate to be 5.2 rear reduced pressure concentrations with citric acid, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 60 DEG C, and vacuum is 0.05MPa, obtains the 3rd concentrate that density is 1.08g/mL.
Step 4: after the stored refrigerated 20h of described 3rd concentrate, mix rear granulation with tapioca starch according to quality proportioning 7: 1, sterilizing after drying, packing, preserves under room temperature.
Embodiment 2
Step one: after great burdock achene and lepidium seed being mixed by quality proportioning 1: 1,55 DEG C of frying 15min, stir-fry limit, limit adds luffa vine juice, and the mass ratio of described luffa vine juice and described great burdock achene is 1: 5, and after frying completes, cooling obtains mixture.
In described mixture, add almond, described almond and described great burdock achene mass ratio are 1: 2, at 50 DEG C of frying 6min, pulverize, obtain the first mixture after cooling.
In described first mixture, add distilled water decoct 2 times, first time decocts 60min at 45 DEG C, second time decocts 40min at 40 DEG C, the consumption of twice adding distil water is 6 times amount of described first mixture quality, filtration after each decoction completes, refilter after coarse filtration liquid is merged, obtain the first coarse filtration liquid.
By the described first thick filtrate reduced in volume, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 55 DEG C, vacuum is 0.06MPa, obtains the first concentrate that density is 1.06g/mL, after concentrated after refrigeration 18h, get the supernatant liquid filtering of described first concentrate, collect the first filtrate.
Step 2: cut the segment of growing into 3cm after being cleaned by shepherd's purse, described shepherd's purse and described great burdock achene mass ratio are 2: 1, shepherd's purse after segment and white spirit mixed are infiltrated 1h, the mass ratio of described white wine and described shepherd's purse is 1: 8, after shepherd's purse water proof after infiltration is steamed 30min, dry 20min at 75 DEG C, for subsequent use after dried shepherd's purse is pulverized.
Be that 1: 1 mixing is rear by raw Radix Glycyrrhizae and cordate houttuynia according to mass ratio to pulverize, cool for subsequent use at 70 DEG C after frying 15min.
Shepherd's purse after pulverizing and raw Radix Glycyrrhizae after frying and cordate houttuynia mixture are mixed according to mass ratio 2: 1, after obtaining the second mixture, adding distil water decocts 3 times, first time decocts 60min at 72 DEG C, second time decocts 50min at 70 DEG C, third time decocts 30min at 68 DEG C, the consumption of distilled water is followed successively by 8 times amount of described second mixture quality, 6 times amount and 6 times amount, filtration after each decoction completes, through centrifugation after filtrate is merged, centrifugation is operating as and controls centrifuge speed 7000r/min, the supernatant after centrifugation is got after centrifugal 15min, employing aperture is the filtering with microporous membrane of 0.8 μm, control operation pressure is 0.015MPa, flow velocity is 8ml/min, obtain the second coarse filtration liquid.
By the described second thick filtrate reduced in volume, be heat medium with recirculated water, concentrate in vacuum decompressioning and concentrating tank, control temperature is 70 DEG C, and vacuum is 0.06MPa, obtains the second concentrate that density is 1.03g/mL, after refrigeration 15h, the supernatant liquid filtering getting the second concentrate obtains the second filtrate.
Step 3: after being cleaned by fresh Chinese toon leaf, infiltrate 3h in yellow rice wine, the mass ratio of yellow rice wine and Chinese toon leaf is 1: 4, after Chinese toon leaf and yellow rice wine mixture water proof are steamed 20min, for subsequent use after dry 30min at 65 DEG C; After fresh tarragon is cleaned, be after infiltrating 15min in the alcohol of 95% in volume fraction, with distilled water flushing 2 times, for subsequent use after 60 DEG C of dry 20min.
Pulverize after Chinese toon leaf after process is mixed with tarragon, wherein, Chinese toon leaf, the mass ratio of tarragon and described great burdock achene is 10: 3: 1, described first filtrate and described second filtrate is added after pulverizing, after obtaining the 3rd mixture, adding distil water decocts 3 times, first time decocts 60min at 70 DEG C, second time decocts 40min at 68 DEG C, third time decocts 30min at 65 DEG C, the consumption of distilled water is followed successively by 8 times amount of described 3rd mixture quality, 6 times amount and 6 times amount, filtration after each decoction completes, the mixture filtrate of 3 gained is merged, employing aperture is the filtering with microporous membrane of 0.8 μm, control operation pressure is 0.015MPa, flow velocity is 8ml/min, obtain the 3rd filtrate.
Regulate the pH of described 3rd filtrate to be 5.8 rear reduced pressure concentrations with citric acid, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 65 DEG C, and vacuum is 0.06MPa, obtains the 3rd concentrate that density is 1.08g/mL.
Step 4: after the stored refrigerated 24h of described 3rd concentrate, mix rear granulation with tapioca starch according to quality proportioning 7: 1, sterilizing after drying, packing, preserves under room temperature.
Embodiment 3
Step one: after great burdock achene and lepidium seed being mixed by quality proportioning 1: 1, frying 12min at 52 DEG C, stir-fry limit, limit adds luffa vine juice, and the mass ratio of described luffa vine juice and described great burdock achene is 1: 5, and after frying completes, cooling obtains mixture.
In described mixture, add almond, described almond and described great burdock achene mass ratio are 1: 2, frying 4min at 48 DEG C, pulverize, obtain the first mixture after cooling.
In described first mixture, add distilled water decoct 2 times, first time decocts 60min at 45 DEG C, second time decocts 40min at 40 DEG C, the consumption of twice adding distil water is 6 times amount of described first mixture quality, filtration after each decoction completes, refilter after coarse filtration liquid is merged, obtain the first coarse filtration liquid.
By the described first thick filtrate reduced in volume, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 52 DEG C, vacuum is 0.05MPa, obtains the first concentrate that density is 1.06g/mL, after concentrated after refrigeration 15h, get the supernatant liquid filtering of described first concentrate, collect the first filtrate.
Step 2: cut the segment of growing into 2cm after being cleaned by shepherd's purse, described shepherd's purse and described great burdock achene mass ratio are 2: 1, shepherd's purse after segment and white spirit mixed are infiltrated 1h, the mass ratio of described white wine and described shepherd's purse is 1: 7, after shepherd's purse water proof after infiltration is steamed 25min, dry 18min at 72 DEG C, for subsequent use after dried shepherd's purse is pulverized.
Be that 1: 1 mixing is rear by raw Radix Glycyrrhizae and cordate houttuynia according to mass ratio to pulverize, cool for subsequent use after 68 DEG C of frying 12min.
Shepherd's purse after pulverizing and raw Radix Glycyrrhizae after frying and cordate houttuynia mixture are mixed according to mass ratio 2: 1, after obtaining the second mixture, adding distil water decocts 2 times, first time decocts 60min at 72 DEG C, second time decocts 50min at 70 DEG C, the consumption of distilled water is followed successively by 8 times amount and 6 times amount of described second mixture quality, filtration after each decoction completes, through centrifugation after filtrate is merged, centrifugation is operating as and controls centrifuge speed 6500r/min, the supernatant after centrifugation is got after centrifugal 12min, employing aperture is the filtering with microporous membrane of 0.6 μm, control operation pressure is 0.015MPa, flow velocity is 6ml/min, obtain the second coarse filtration liquid.
By the described second thick filtrate reduced in volume, be heat medium with recirculated water, concentrate in vacuum decompressioning and concentrating tank, control temperature is 68 DEG C, and vacuum is 0.05MPa, obtains the second concentrate that density is 1.03g/mL, after refrigeration 12h, the supernatant liquid filtering getting the second concentrate obtains the second filtrate.
Step 3: after being cleaned by fresh Chinese toon leaf, infiltrate 2h in yellow rice wine, the mass ratio of yellow rice wine and Chinese toon leaf is 1: 4, after Chinese toon leaf and yellow rice wine mixture water proof are steamed 18min, for subsequent use after dry 25min at 62 DEG C; After fresh tarragon is cleaned, be after infiltrating 12min in the alcohol of 95% in volume fraction, with distilled water flushing 2 times, for subsequent use after dry 15min at 58 DEG C.
Pulverize after Chinese toon leaf after process is mixed with tarragon, wherein, Chinese toon leaf, the mass ratio of tarragon and described great burdock achene is 10: 3: 1, described first filtrate and described second filtrate is added after pulverizing, after obtaining the 3rd mixture, adding distil water decocts 3 times, first time decocts 60min at 70 DEG C, second time decocts 40min at 68 DEG C, third time decocts 30min at 65 DEG C, the consumption of distilled water is followed successively by 8 times amount of described 3rd mixture quality, 6 times amount and 6 times amount, filtration after each decoction completes, the mixture filtrate of 3 gained is merged, employing aperture is the filtering with microporous membrane of 0.6 μm, control operation pressure is 0.015MPa, flow velocity is 6ml/min, obtain the 3rd filtrate.
Regulate the pH of described 3rd filtrate to be 5.5 rear reduced pressure concentrations with citric acid, take recirculated water as heat medium, concentrate in vacuum decompressioning and concentrating tank, control temperature is 62 DEG C, and vacuum is 0.05MPa, obtains the 3rd concentrate that density is 1.08g/mL.
Step 4: after the stored refrigerated 22h of described 3rd concentrate, mix rear granulation with tapioca starch according to quality proportioning 7: 1, sterilizing after drying, packing, preserves under room temperature.
Although embodiment of the present invention are open as above, but it is not restricted to listed in description and embodiment utilization, it can be applied to various applicable the field of the invention completely, for those skilled in the art, can easily realize other amendment, therefore do not deviating under the universal that claim and equivalency range limit, the present invention is not limited to specific details and illustrates here and the embodiment described.
Claims (8)
1. prevent and treat a preparation method for the feed of black globefish pneumonia, it is characterized in that, comprising:
Step one: after great burdock achene and lepidium seed are mixed by quality proportioning 1: 1, frying 10 ~ 15min at 50 ~ 55 DEG C, stir-fry limit, limit adds luffa vine juice, the mass ratio of described luffa vine juice and described great burdock achene is 1: 5, after frying completes, cooling obtains mixture, almond is added in described mixture, described almond and described great burdock achene mass ratio are 1: 2, frying 3 ~ 6min at 45 ~ 50 DEG C, pulverize after cooling, obtain the first mixture, in described first mixture, add distilled water decoct 1 ~ 2 time, filtration after each decoction completes, refilter after coarse filtration liquid is merged, obtain the first coarse filtration liquid, the first concentrate is obtained after described first coarse filtration liquid is concentrated, after refrigeration 12 ~ 18h, get the supernatant liquid filtering of described first concentrate, collect the first filtrate,
Step 2: cut the segment of growing into 2 ~ 3cm after being cleaned by shepherd's purse, described shepherd's purse and described great burdock achene mass ratio are 2: 1, shepherd's purse after segment and white spirit mixed are infiltrated 1h, the mass ratio of described white wine and described shepherd's purse is 1: 6 ~ 1: 8, after shepherd's purse water proof after infiltration is steamed 20 ~ 30min, dry 15 ~ 20min at 70 ~ 75 DEG C, for subsequent use after dried shepherd's purse is pulverized;
Be that 1: 1 mixing is rear by raw Radix Glycyrrhizae and cordate houttuynia according to mass ratio to pulverize, cool for subsequent use at 65 ~ 70 DEG C after frying 10 ~ 15min, shepherd's purse after pulverizing and raw Radix Glycyrrhizae after frying and cordate houttuynia mixture are mixed according to mass ratio 2: 1, after obtaining the second mixture, adding distil water decocts 1 ~ 3 time, filtration after each decoction completes, through centrifugation after filtrate is merged, the second coarse filtration liquid is obtained after filtration, the second concentrate is obtained after concentrated, refrigeration 10 ~ 15h, the supernatant liquid filtering getting the second concentrate obtains the second filtrate;
Step 3: pulverize after Chinese toon leaf is mixed with tarragon, wherein, the mass ratio of Chinese toon leaf, tarragon and described great burdock achene is 10: 3: 1, adds described first filtrate and described second filtrate, after obtaining the 3rd mixture after pulverizing, adding distil water decocts 3 times, filtration after each decoction completes, filters after the mixture filtrate of 3 gained being merged, obtains the 3rd filtrate, the pH regulating described 3rd filtrate with citric acid is 5.2 ~ 5.8, obtains the 3rd concentrate after concentrated;
Step 4: after the stored refrigerated 20 ~ 24h of described 3rd concentrate, mix rear granulation with tapioca starch according to quality proportioning 7: 1, sterilizing after drying, packing, preserves under room temperature.
2. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 1, it is characterized in that, the leaf of Chinese toon described in step 3 is through pretreatment: after being cleaned by Chinese toon leaf, 2 ~ 3h is infiltrated in yellow rice wine, the mass ratio of yellow rice wine and Chinese toon leaf is 1: 3 ~ 1: 4, after Chinese toon leaf and yellow rice wine mixture water proof are steamed 15 ~ 20min, at 60 ~ 65 DEG C, dry 20 ~ 30min obtains; Described in step 3, tarragon is through pretreatment: after being cleaned by tarragon, is infiltrate after 10 ~ 15min in the alcohol of 95% in volume fraction, with distilled water flushing 1 ~ 2 time, and dry 10 ~ 20min at 55 ~ 60 DEG C.
3. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 2, it is characterized in that, in first mixture described in step one, adding distil water decocts 2 times, the consumption of twice adding distil water is 6 times amount of described first mixture quality, in second mixture described in step 2, adding distil water decocts 3 times, the consumption of distilled water is followed successively by 8 times amount of described second mixture quality, 6 times amount and 6 times amount, in 3rd mixture described in step 3, adding distil water decocts 3 times, the consumption of distilled water is followed successively by 8 times amount of described 3rd mixture quality, 6 times amount and 6 times amount.
4. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 3, it is characterized in that, decoct 2 times after the first mixture adding distil water described in step one, first time decocts 60min at 45 DEG C, and second time decocts 40min at 40 DEG C; In second mixture described in step 2, adding distil water decocts 3 times, and first time decocts 60min at 72 DEG C, and second time decocts 50min at 70 DEG C, and third time decocts 30min at 68 DEG C; In 3rd mixture described in step 3, adding distil water decocts 3 times, and first time decocts 60min at 70 DEG C, and second time decocts 40min at 68 DEG C, and third time decocts 30min at 65 DEG C.
5. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 4, it is characterized in that, in step one, the density of concentrated gained first concentrate is 1.06g/mL, in step 2, the density of concentrated gained second concentrate is 1.03g/mL, and in step 3, the density of concentrated gained the 3rd concentrate is 1.08g/mL.
6. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 5, it is characterized in that, step one all adopts reduced pressure concentration to concentrating in step 3, take recirculated water as heat medium, in step one, described first coarse filtration liquid is concentrated in vacuum decompressioning and concentrating tank, control temperature is 50 ~ 55 DEG C, vacuum is 0.05 ~ 0.06MPa, in step 2, described second coarse filtration liquid is concentrated in vacuum decompressioning and concentrating tank, control temperature is 65 ~ 70 DEG C, vacuum is 0.05 ~ 0.06MPa, in step 3, described 3rd filtrate is concentrated in vacuum decompressioning and concentrating tank, control temperature is 60 ~ 65 DEG C, vacuum is 0.05 ~ 0.06MPa.
7. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 6, it is characterized in that, in step 2, centrifugation is operating as and controls centrifuge speed 6000 ~ 7000r/min, gets the supernatant after centrifugation after centrifugal 10 ~ 15min.
8. prevent and treat the preparation method of the feed of black globefish pneumonia as claimed in claim 7, it is characterized in that, in filter operation in step 2 after centrifugation and step 3 mixture filtrate merge after filter operation all adopt aperture to be the filtering with microporous membrane of 0.45 ~ 0.8 μm, control operation pressure is 0.015MPa, and flow velocity is 5 ~ 8ml/min.
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