CN104973910A - Production method for flower traditional Chinese medicine - Google Patents

Production method for flower traditional Chinese medicine Download PDF

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CN104973910A
CN104973910A CN201510383096.9A CN201510383096A CN104973910A CN 104973910 A CN104973910 A CN 104973910A CN 201510383096 A CN201510383096 A CN 201510383096A CN 104973910 A CN104973910 A CN 104973910A
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grams
chinese medicine
nutrient substance
production method
trace element
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高旌
刘畅
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HEFEI KAIGE INFORMATION TECHNOLOGY Co Ltd
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HEFEI KAIGE INFORMATION TECHNOLOGY Co Ltd
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Abstract

The invention discloses a production method for a flower traditional Chinese medicine, which belongs to the field production of traditional Chinese medicine. The flower traditional Chinese medicine refers to honeysuckle flower. Nutrients a, b and c are used during the growth of the flower traditional Chinese medicine. The nutrient a is prepared by equally weighing potassium salts of 4 kinds of 5'-mixed nucleotide, summing to 4 g, then weighing 3 g of manganese sulfate, 2 g of borax and 4 g of ferrous sulphate and then successively carrying out mixing, crushing and sieving with a 100-mesh screen; the nutrient b is prepared by equally weighing sodium salts of 4 kinds of 5'-mixed nucleotide, summing to 4 g, then weighing 3 g of manganese sulfate, 2 g of borax and 4 g of ferrous sulphate and then successively carrying out mixing, crushing and sieving with a 100-mesh screen; and the nutrient c is prepared by weighing 8 g of a nucleotide potassium salt, 7 g of maize starch and 5 g of medium trace element, crushing and sieving nucleotide potassium salt and medium trace element, adding maize starch and carrying out uniform mixing. The nutrients are dissolved with water and then sprayed. The nutrients a, b and c are separately blended with 30 kg of water and then respectively sprayed in a seedling stage, a germination stage and an early bud stage once. The production method is convenient to operate and saves cost; and after application of the nutrients, the content of galuteolin in chrysanthemum and honeysuckle flower is greater than 0.054%, while the content of chlorogenic acid is greater than 1.5%.

Description

The production method of flower class Chinese medicine
The application is application number 201310579846.0, the applying date: on November 19th, 2013, and denomination of invention is the divisional application of " production method of flower class Chinese medicine ".
Technical field
The present invention relates to the production method of fruit and seed class Chinese medicine, particularly the production method of fruit and seed class medicinal plant and medicine materical crude slice and extract.
Background technology
, there is composition activeconstituents more, do not save in the production method of existing colored class Chinese medicine, not rationally, not easily standing storage and preparation method are simple not for activeconstituents proportioning, and purposes is problem not widely.Authorization Notice No. CN 102079666 B, the patent No. is 201010514231.6, name is called: a kind of nutrient substance promoting the growth of flower class Chinese medicinal materials, it is by nucleosides hydrochlorate, glucose, amino acid and medium trace element composition, its weight percent is: nucleosides hydrochlorate 10-30%, glucose 20-70%, amino acid/11 0-20%, medium trace element 10-30%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5'-CMP dipotassium, uridine 5'-monophosphate dipotassium four kind 5 ' the sylvite of-mixed nucleotides, described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate.Just there are the problems referred to above.
Summary of the invention
Object of the present invention overcomes above-mentioned deficiency exactly, one is provided to decrease activeconstituents in composition, reasonable ratio, its effect still can meet or exceed the patent No. and be: a kind of production method promoting the colored class Chinese medicine of the patent of invention of the nutrient substance of flower class Chinese medicinal materials growth of " 201010514231.6 ".
The present invention is achieved in that
The production method of flower class Chinese medicine, described colored class Chinese medicinal materials refers to Japanese Honeysuckle; In its process of growth, use nutrient substance: described nutrient substance is: a. etc. measure the sylvite totally 4 grams of four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, pulverizing, cross 100 mesh sieves, the nutrient substance obtained;
Etc. b. measure the sodium salt totally 4 grams of four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, to pulverize, cross 100 mesh sieves, the nutrient substance obtained;
C. take 8 grams of Nucleotide sylvite, W-Gum 7 grams, medium trace element 5 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, add W-Gum, mix, the nutrient substance obtained;
Described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium or sodium, 5'-bird adenylic acid (AMP) dipotassium or sodium, 5'-CMP dipotassium or sodium, 5 '-uridylic acid dipotassium or sodium, the potassium of four kinds of 5'-mixed nucleotides or sodium salt;
Described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate;
The application process of described nutrient substance is: spray with after water dissolution;
Described nutrient substance use opportunity and concentration is: at Japanese Honeysuckle seedling stage, germination period, bud initial stage respectively by a, b, c nutrient substance, be watered 30 kilograms, respectively spray once.
The production method of flower class Chinese medicine, uses rear described Japanese Honeysuckle galuteolin content and is greater than 0.054%; Chlorogenic acid content is greater than 1.5%.
The production method of flower class Chinese medicine, using rear Japanese Honeysuckle can increase production 22%; The gold and silver flower of results is large and evenly, uniformity coefficient can reach 70-90%.
The production method of flower class Chinese medicine, can make high-quality medicine materical crude slice by the Japanese Honeysuckle of results or extracting effective components yield can up to 10% than the gold and silver of produced in conventional processes.
Promote the nutrient substance of flower class Chinese medicinal materials growth, it is by nucleosides hydrochlorate, medium trace element forms, do not comprise glucose or/and amino acid, weight percent is: nucleosides hydrochlorate 30-70%, medium trace element 30-70%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium or sodium, 5'-bird adenylic acid (AMP) dipotassium or sodium, 5'-CMP dipotassium or sodium, the potassium of 5 '-uridylic acid dipotassium or sodium four kind 5 '-mixed nucleotides or sodium salt, described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate.
Promote the nutrient substance of flower class Chinese medicinal materials growth, screening formulation weight percent is: nucleosides hydrochlorate 40-60%, medium trace element 30-70%.
Promote the nutrient substance of flower class Chinese medicinal materials growth, the weight ratio of medium trace element is: Mn:B:Fe=3:2:4.
Promote the nutrient substance of flower class Chinese medicinal materials growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate.
Promote the nutrient substance of flower class Chinese medicinal materials growth, the weight percent of nucleosides hydrochlorate, medium trace element and weighting agent is: nucleosides hydrochlorate 10-30 %, medium trace element 10-30%, weighting agent 40-80%.
Promote the nutrient substance of flower class Chinese medicinal materials growth, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, Magnesium Stearate, magnesium sulfate or zinc sulfate, the weight percent of nucleosides hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate 15-20%, medium trace element 15-20%, weighting agent 40-70%.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, it is by nucleosides hydrochlorate, medium trace element forms, do not comprise glucose or/and amino acid, weight percent is: nucleosides hydrochlorate 30-70%, medium trace element 30-70%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium or sodium, 5'-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the potassium of 5 '-uridylic acid dipotassium or sodium four kind 5 '-mixed nucleotides or sodium salt, described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate, by nucleosides hydrochlorate, medium trace element mixes, pulverize, cross 50-200 mesh sieve.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, screening formulation weight percent is: nucleosides hydrochlorate 40-60%, medium trace element 30-70%.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, the weight ratio of medium trace element is: Mn:B:Fe=3:2:4.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, the weight percent of nucleosides hydrochlorate, medium trace element and weighting agent is: nucleosides hydrochlorate 10-30 %, medium trace element 10-30%, weighting agent 40-80%.
Promote the preparation method of the nutrient substance of flower class Chinese medicinal materials growth, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, Magnesium Stearate, magnesium sulfate or zinc sulfate, the weight percent of nucleosides hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate 15-20%, medium trace element 15-20%, weighting agent 40-70%.
The production method of flower class Chinese medicine, nutrient substance is used: described nutrient substance is primarily of nucleosides hydrochlorate in its process of growth, medium trace element forms, do not comprise glucose or/and amino acid, weight percent is: nucleosides hydrochlorate 30-70%, medium trace element 30-70%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5'-CMP dipotassium or sodium, the potassium of uridine 5'-monophosphate dipotassium or sodium four kinds of 5'-mixed nucleotides or sodium salt, described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate, the application process of described nutrient substance is: spray with after water dissolution.
The production method of flower class Chinese medicine is 100-400ppm by the concentration sprayed after water dissolution.
The production method of flower class Chinese medicine, the weight ratio of medium trace element is: Mn:B:Fe=3:2:4.
The production method of flower class Chinese medicine, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient compositions is: nucleosides hydrochlorate 10-30 %, medium trace element 10-30%, weighting agent 40-80%.
The production method of flower class Chinese medicine, the opportunity of using of described nutrient substance is: seedling stage of flower class Chinese medicinal materials or germination period, bud stage or/and initial bloom stage, full-bloom stage respectively once.
The production method of flower class Chinese medicine, the opportunity of using of described nutrient substance is: flower class Chinese medicinal materials bud stage or/and initial bloom stage, full-bloom stage respectively once.
The production method of flower class Chinese medicine, the consumption of described nutrient substance is every mu of 2-8 gram, is every mu of 20-40 liter by water-soluble water consumption.
The production method of flower class Chinese medicine, its feature is being: the consumption of described nutrient substance is at every turn every mu of 15-30 gram, is at every turn every mu of 20-40 liter by water-soluble water consumption.
State the production method of colored class Chinese medicine, its feature is being: the colored class Chinese medicinal materials flower of results greatly and evenly, uniformity coefficient can reach 70-90%, high by 19% than produced in conventional processes of its output, the Chinese medicinal materials of results, than the high 7-11% of produced in conventional processes, can be made high-quality medicine materical crude slice or the extracting effective components yield Chinese medicinal materials height 7-10% than produced in conventional processes by its Contents of Main Components.
Weighting agent of the present invention: starch refers to: green starch, yam starch, wheat starch, sweet potato starch, W-Gum, water caltrop starch, Lotus Root Starch, Chinese Water Chestnut Starch etc., preferred W-Gum.Dextrin refers to: white dextrin, yellow starch gum and Britain glue, cyclodextrin.Mierocrystalline cellulose refers to: methylcellulose gum, Vltra tears, Natvosol, carboxymethyl cellulose etc.
In the preparation of nutrient substance provided by the present invention, take nucleic acid as raw material: one is for raw material with commercially available nucleic acid, two is adopt the nucleic acid of dry method or wet production to be raw material from the mycelium after fermentation plant fermentation: 1., the hydrolysis of nucleic acid is the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid of 1:20-30 according to nucleic acid, buck weight ratio, alkali lye is 5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtain nucleosides hydrochlorate and deoxynucleoside acid salt solution, filter, filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry: concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization: dissolve the nucleosides hydrochlorate after doing and deoxynucleoside hydrochlorate with clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate (from the mycelium after fermentation plant fermentation adopt the nucleic acid of dry method or wet production be raw material also containing water soluble mixt and impurity);
4., medium trace element is got;
, by nucleosides hydrochlorate medium trace element mix, pulverize, sieve.
In nucleic acid hydrolysis process described in this preparation method, alkali lye used is sodium hydroxide or potassium hydroxide solution.
With commercially available nucleic acid for raw material, impure few after hydrolysis.
Three is commercially available: nucleosides hydrochlorate mainly refers to: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium, 5 '-cytidylic acid disodium or potassium, the sodium salt of 5 '-uridine monophosphate disodium or potassium four kinds of 5 '-mixed nucleotides or sylvite; Deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
The source of nucleosides hydrochlorate and deoxynucleoside hydrochlorate is take nucleic acid as raw material, adopt the nucleic acid of dry method or wet production to be raw material from the mycelium after fermentation plant fermentation, this kind of nucleic acid is a small amount of thymus nucleic acid (DNA) of main mixing with Yeast Nucleic Acid (RNA), makes with alkali lye hydrolysis.
Beneficial effect of the present invention:
Because the present invention does not decrease composition activeconstituents, so more economize in raw materials and cost containing glucose, amino acid.
Coordinate nucleosides hydrochlorate because the present invention contains medium trace element, reasonable ratio, promotes the growth of Rhizomatic traditional Chinese medicine more targeted specifically.
Although the present invention decreases activeconstituents, its effect does not still subtract and even produces better effect.
The present invention is not particularly containing glucose, glucose easily absorbs moisture deliquescence, nutrient substance containing glucose places the deliquescence that namely absorbs water more than a year under general condition of storage, there is product caking, make nucleosides hydrochlorate, cause quality product to reduce even to lose efficacy, so, the invention solves the problem of the not easily standing storage of nutrient substance.
Because the present invention also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc., the relevant regulations being generally not less than 20 grams as the foliage fertilizer minimum package of merchandise sales are adapted to the adding of weighting agent; Filler starch, dextrin, Mierocrystalline cellulose etc. also possess certain viscosity, make nutrient substance be attached to blade face after spraying and the plant surface time longer, make its action effect better; Weighting agent polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc. have dispersiveness and oilness, can extend the quality guaranteed period of nutrient substance.
Purposes of the present invention is: as fertilizer particularly as foliage fertilizer or nutrient substance or the application of plant-growth regulator in the growth promoting flower class Chinese medicine; Or the production being applied to colored class Chinese medicine can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The present invention is applied to the production of colored class Chinese medicine, with strong points, can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
So product of the present invention: saving, environmental protection (nontoxic, harmless, noresidue, without any adverse side effect), comprehensive to the purposes of flower class Chinese medicine, increase production, increase income, synergy, strengthen resistance, improve quality effective.
The present invention and No. 201010514231.6 patents, traditional product and method contrast tables 1
The present invention and No. 201010514231.6 patents, traditional product and method contrast tables 2
The present invention implements to spray agency part effect in table 3 to concrete crop
Note: content's index detection method is carried out with reference to national standard or industry standard, content is pressed dry product and is calculated
Embodiment:
Embodiment 1: wait the sylvite totally 4 grams measuring four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, pulverizing, cross 100 mesh sieves.
Embodiment 2: wait the sodium salt totally 4 grams measuring four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, pulverizing, cross 100 mesh sieves.
Embodiment 3: take 8 grams of Nucleotide sylvite, W-Gum 7 grams, medium trace element 5 grams, pulverizes nucleosides hydrochlorate, medium trace element, sieves, add W-Gum, mix, obtain nutrient substance.
Embodiment 4: chrysanthemum: first time is seedling stage (germination period), in April, with 20 grams of nutrient substances, is watered 20 liters, evenly sprays on one mu of chrysanthemum; Second time is initial bloom stage embodiment 1 nutrient substance, is watered 20 liters, evenly sprays on one mu of chrysanthemum; Full-bloom stage embodiment 2 nutrient substance, is watered 20 liters, evenly sprays on one mu of chrysanthemum for the third time, can increase production 19%, the chrysanthemum flower of results is large and evenly, uniformity coefficient can reach 70-90%, high by 19% than produced in conventional processes of its output, its Contents of Main Components is than the high 7-11% of produced in conventional processes.
Embodiment 5: Japanese Honeysuckle, seedling stage (germination period), bud initial stage by embodiment 1,2,3, are watered 30 kilograms respectively, and each spray once, can increase production 22%.
Embodiment 6: the colored class Chinese medicinal materials of results can be made high-quality medicine materical crude slice or the extracting effective components yield colored class Chinese medicinal materials height 7-10% than produced in conventional processes.

Claims (4)

1. spend the production method of class Chinese medicine, it is characterized in that: described colored class Chinese medicinal materials refers to Japanese Honeysuckle; In its process of growth, use nutrient substance: described nutrient substance is: a. etc. measure the sylvite totally 4 grams of four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, pulverizing, cross 100 mesh sieves, the nutrient substance obtained;
Etc. b. measure the sodium salt totally 4 grams of four kinds of 5 '-mixed nucleotides, manganous sulfate 3 grams, borax 2 grams, 4 grams, ferrous sulfate, mixing, to pulverize, cross 100 mesh sieves, the nutrient substance obtained;
C. take 8 grams of Nucleotide sylvite, W-Gum 7 grams, medium trace element 5 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, add W-Gum, mix, the nutrient substance obtained;
Described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5'-AMP dipotassium or sodium, 5'-bird adenylic acid (AMP) dipotassium or sodium, 5'-CMP dipotassium or sodium, 5 '-uridylic acid dipotassium or sodium, the potassium of four kinds of 5'-mixed nucleotides or sodium salt;
Described medium trace element refers to: Mn, B and Fe, specifically: manganous sulfate, borax and ferrous sulfate;
The application process of described nutrient substance is: spray with after water dissolution;
Described nutrient substance use opportunity and concentration is: at Japanese Honeysuckle seedling stage, germination period, bud initial stage respectively by a, b, c nutrient substance, be watered 30 kilograms, respectively spray once.
2. spend the production method of class Chinese medicine according to claim 1, it is characterized in that: use rear described Japanese Honeysuckle galuteolin content and be greater than 0.054%; Chlorogenic acid content is greater than 1.5%.
3. spend the production method of class Chinese medicine according to claim 1, it is characterized in that: using rear Japanese Honeysuckle can increase production 22%; The gold and silver flower of results is large and evenly, uniformity coefficient can reach 70-90%.
4. spend the production method of class Chinese medicine according to claim 1, it is characterized in that: the Japanese Honeysuckle of results can be made high-quality medicine materical crude slice or extracting effective components yield can up to 10% than the gold and silver of produced in conventional processes.
CN201510383096.9A 2013-11-19 2013-11-19 Production method for flower traditional Chinese medicine Withdrawn CN104973910A (en)

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CN201310579846.0A CN103613424B (en) 2013-11-19 2013-11-19 The production method of flos traditional Chinese medicine

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CN201510383096.9A Withdrawn CN104973910A (en) 2013-11-19 2013-11-19 Production method for flower traditional Chinese medicine
CN201510399796.7A Withdrawn CN104997830A (en) 2013-11-19 2013-11-19 Production method of flower type traditional Chinese medicinal decoction pieces
CN201510399793.3A Withdrawn CN105036848A (en) 2013-11-19 2013-11-19 Honeysuckle flower extract production method
CN201510403215.2A Withdrawn CN105030870A (en) 2013-11-19 2013-11-19 Preparation method of chrysanthemum flower decoction pieces
CN201310579846.0A Active CN103613424B (en) 2013-11-19 2013-11-19 The production method of flos traditional Chinese medicine

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CN201510399793.3A Withdrawn CN105036848A (en) 2013-11-19 2013-11-19 Honeysuckle flower extract production method
CN201510403215.2A Withdrawn CN105030870A (en) 2013-11-19 2013-11-19 Preparation method of chrysanthemum flower decoction pieces
CN201310579846.0A Active CN103613424B (en) 2013-11-19 2013-11-19 The production method of flos traditional Chinese medicine

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107823238A (en) * 2017-11-20 2018-03-23 安徽佳凯药业股份有限公司 A kind of production method of flos traditional Chinese medicine medicine materical crude slice

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Publication number Priority date Publication date Assignee Title
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CN102079666B (en) * 2010-10-21 2013-06-12 高旌 Nutrient for promoting growth of flower Chinese medicinal material
CN103288508B (en) * 2010-10-21 2014-10-29 安徽中天方生物科技有限公司 Preparation method of nutrient for promoting growth of flower Chinese medicinal materials
CN103113166B (en) * 2010-10-21 2014-07-23 合肥市济泉医药科技有限公司 Production method with good quality and high yield for medicinal plants trichosanthes kirilowii maxim and radices trichosanthis
CN103141201B (en) * 2010-10-21 2014-07-23 合肥市济泉医药科技有限公司 Good-quality and high-yield production method of fruit and seed medicinal plants

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Publication number Priority date Publication date Assignee Title
CN103314690A (en) * 2010-10-21 2013-09-25 高旌 High-quality high-yield flower-type traditional Chinese medicinal material production method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107823238A (en) * 2017-11-20 2018-03-23 安徽佳凯药业股份有限公司 A kind of production method of flos traditional Chinese medicine medicine materical crude slice

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CN103613424B (en) 2016-08-17
CN104997830A (en) 2015-10-28

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