CN104939023B - A kind of preparation method of rich magnesium salts - Google Patents
A kind of preparation method of rich magnesium salts Download PDFInfo
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- CN104939023B CN104939023B CN201510404818.4A CN201510404818A CN104939023B CN 104939023 B CN104939023 B CN 104939023B CN 201510404818 A CN201510404818 A CN 201510404818A CN 104939023 B CN104939023 B CN 104939023B
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- rich magnesium
- sodium chloride
- magnesium salts
- magnesium
- extract
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- 159000000003 magnesium salts Chemical class 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 62
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 60
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 52
- 239000011777 magnesium Substances 0.000 claims abstract description 52
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 52
- 239000011780 sodium chloride Substances 0.000 claims abstract description 31
- 241000206607 Porphyra umbilicalis Species 0.000 claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 17
- 241001474374 Blennius Species 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 16
- 235000013305 food Nutrition 0.000 claims abstract description 14
- 238000010992 reflux Methods 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 6
- 238000010438 heat treatment Methods 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 12
- 239000000047 product Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 6
- 238000001514 detection method Methods 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000000052 vinegar Substances 0.000 claims description 5
- 235000021419 vinegar Nutrition 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 10
- 230000008569 process Effects 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 abstract description 4
- 235000012631 food intake Nutrition 0.000 abstract description 3
- 239000012535 impurity Substances 0.000 abstract description 3
- 235000013311 vegetables Nutrition 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 2
- 230000009471 action Effects 0.000 description 5
- 230000033001 locomotion Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 238000005842 biochemical reaction Methods 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 230000003834 intracellular effect Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 206010020772 Hypertension Diseases 0.000 description 1
- 206010061216 Infarction Diseases 0.000 description 1
- 208000008167 Magnesium Deficiency Diseases 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- 208000010428 Muscle Weakness Diseases 0.000 description 1
- 206010028372 Muscular weakness Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 208000003217 Tetany Diseases 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 230000002996 emotional effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000005714 functional activity Effects 0.000 description 1
- 230000004217 heart function Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000007574 infarction Effects 0.000 description 1
- 235000004764 magnesium deficiency Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000004118 muscle contraction Effects 0.000 description 1
- 230000002232 neuromuscular Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001243 protein synthesis Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 230000014616 translation Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to field of health care food, a kind of preparation method of rich magnesium salts is specifically disclosed.Alimentary acetic acid will be added after seaweed refluxing extraction and obtains rich magnesium extract, then by rich magnesium extract and sodium chloride hybrid process into rich magnesium salts, finally sealed is packed.The present invention utilizes seaweed magnesium content highest characteristic, laver powder is extracted and removed after invalid impurity, add alimentary acetic acid, the magnesium elements in seaweed are remained by chemically and physically method and mixed with sodium chloride, ensure the basis of magnesium element content in magnesium salts, raw material and processing auxiliary material (alimentary acetic acid) are food grade or edible vegetables simultaneously, it is ensured that food consumption safety.
Description
Technical field
The present invention relates to field of health care food, a kind of preparation method of rich magnesium salts is specifically disclosed.
Background technology
Magnesium is trace element necessary to mammal and the mankind, and it is intracellular important cation, participates in protein
Synthesis and muscle contraction.Magnesium, which lacks, is clinically mainly shown as uneasy, emotional mood, tetany, reflection
It is hyperfunction etc..
Magnesium plays highly important role in human motion functional activity.Why people lives, entirely by human body one
Serial complicated biochemical reaction maintains vital movement, and being catalyzed these biochemical reactions then needs thousands of kinds to promote enzyme (biology
Catalyst).External scientist's research finds that magnesium can activate 325 enzyme systems, is to work as it the activator that magnesium calls vital movement
Have nothing to be ashamed of.In recent years, external scientist's research is pointed out, " magnesium " food is wanted after people in middle age.To eat the food enriched containing magnesium more.
Angiocardiopathy, such as coronary heart disease, hypertension, high fat of blood, miocardial infarction, diabetes are more occurs after people in middle age, this with
Internal content of magnesium reduction is relevant.
Magnesium is the intracellular cation that potassium is only second in human body, and it participates in a series of metabolic processes, including bone in vivo
And the formation of cell, there is substantial connection with neuromuscular and cardiac function.The general daily demand to magnesium of adult, Nan Xingwei
350 milligrams, women is 300 milligrams, if magnesium deficiency, can cause muscle weakness, endurance reduction.Due to motion, when particularly long
Between magnesium in a large amount of consumers of high-intensity exercise, so as to reduce the movable function of muscle, or even also occur that tic, spasm etc..
The content of the invention
In order to solve technical problem present in prior art, it is an object of the invention to provide a kind of preparation of rich magnesium salts
Method, using seaweed magnesium content highest characteristic, laver powder is extracted and removed after invalid impurity, added alimentary acetic acid, pass through
Chemically and physically the magnesium elements in seaweed are remained and mixed with sodium chloride by method, it is ensured that magnesium element content in magnesium salts
Basis, while raw material and processing auxiliary material (alimentary acetic acid) are food grade or edible vegetables, it is ensured that food consumption safety.
The technical solution adopted in the present invention is as follows：
A kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 20~30 times of weight than water, be heated to reflux carrying
Take 2~3 times, the time extracted every time is 30~60min, merging filtrate concentration adds alimentary acetic acid mixing into concentrate and stirred
Mix, fully filtered after reaction, rich magnesium extract is dried in vacuo to obtain after concentration；
According to surveying and determination：Contain 460 milligrams of magnesium in seaweed magnesium content highest, every 100 grams of seaweeds, occupy the hat of various foods, be called
" treasure-houses of magnesium elements ", laver powder is extracted magnesium elements therein by will add acidic materials after processing, is filtered out miscellaneous
Containing abundant magnesium elements in extract after matter, while using seaweed as raw materials for production, will not have been produced in process
Evil material, is the optimal selection of the flavoring of magnesium elements.
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, simultaneously
The pure water that addition accounts for sodium chloride gross mass 4~10% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride
Stop stirring, obtain mixed material；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet after sealing
Row heats, and heat treatment temperature is 90~150 DEG C, and the time is 30~180min, and the mixture after heating is added
Dewater treatment is carried out in rotary vacuum dryer, dewater treatment temperature is 35~65 DEG C, and the time is 30~180min, dewater treatment
After obtain rich magnesium salts product；
(4), pack：
Product after step (3) dewater treatment is packed.
Further, the sodium chloride described in the step (2) is the food grade sodium chloride for meeting national Specification, quality
Percentage composition >=91%, granularity is 0.1~3.5mm.
Further, the step (1) monitors ph value of mixture during alimentary acetic acid is added by pH value detection means,
When mixed liquor is in faintly acid, stop adding alimentary acetic acid action.
Further, the weight ratio of sodium chloride and rich magnesium extract is 50~20 in the step (2)：0.1~5.
The preparation method of richness magnesium salts of the invention, its advantage is shown：
Using seaweed magnesium content highest characteristic, laver powder is extracted and removed after invalid impurity, add alimentary acetic acid, led to
Cross chemically and physically method and remain the magnesium elements in seaweed and mixed with sodium chloride, it is ensured that magnesium element content in magnesium salts
Basis, while raw material and processing auxiliary material (alimentary acetic acid) be food grade or edible vegetables, it is ensured that food consumption safety.
Embodiment
The present invention is further illustrated with reference to embodiments.
Embodiment 1
A kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 30 times of weight than water, heating and refluxing extraction 3
Secondary, the time extracted every time is 60min, and merging filtrate concentration adds alimentary acetic acid mixing into concentrate, adding food
With ph value of mixture is monitored by pH value detection means in process of acetic acid, when mixed liquor is in faintly acid, stop adding vinegar
Filtered after acid action, fully reaction, rich magnesium extract is dried in vacuo to obtain after concentration；
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, simultaneously
The pure water that addition accounts for sodium chloride gross mass 9% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride and stopped
Stirring, obtains mixed material, described sodium chloride and the weight ratio of rich magnesium extract are 40：3；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet after sealing
Row heats, and heat treatment temperature is 110 DEG C, and the time is 170min, and the mixture after heating is added into revolution vacuum
Carry out dewater treatment in drying machine, dewater treatment temperature is 55 DEG C, the time is to obtain rich magnesium salts production after 140min, dewater treatment
Product；
(4), pack
Product after step (3) dewater treatment is packed.
Embodiment 2
A kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 25 times of weight than water, heating and refluxing extraction 2
Secondary, the time extracted every time is 60min, and merging filtrate concentration adds alimentary acetic acid mixing into concentrate, adding food
With ph value of mixture is monitored by pH value detection means in process of acetic acid, when mixed liquor is in faintly acid, stop adding vinegar
Filtered after acid action, fully reaction, rich magnesium extract is dried in vacuo to obtain after concentration；
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, simultaneously
The pure water that addition accounts for sodium chloride gross mass 9% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride and stopped
Stirring, obtains mixed material, described sodium chloride and the weight ratio of rich magnesium extract are 50：2；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet after sealing
Row heats, and heat treatment temperature is 120 DEG C, and the time is 140min, and the mixture after heating is added into revolution vacuum
Carry out dewater treatment in drying machine, dewater treatment temperature is 50 DEG C, the time is to obtain rich magnesium salts production after 130min, dewater treatment
Product；
(4), pack
Product after step (3) dewater treatment is packed.
Embodiment 3
A kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 20 times of weight than water, heating and refluxing extraction 3
Secondary, the time extracted every time is 30min, and merging filtrate concentration adds alimentary acetic acid mixing into concentrate, adding food
With ph value of mixture is monitored by pH value detection means in process of acetic acid, when mixed liquor is in faintly acid, stop adding vinegar
Filtered after acid action, fully reaction, rich magnesium extract is dried in vacuo to obtain after concentration；
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, simultaneously
The pure water that addition accounts for sodium chloride gross mass 4% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride and stopped
Stirring, obtains mixed material, described sodium chloride and the weight ratio of rich magnesium extract are 30：0.5；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet after sealing
Row heats, and heat treatment temperature is 150 DEG C, and the time is 180min, and the mixture after heating is added into revolution vacuum
Carry out dewater treatment in drying machine, dewater treatment temperature is 65 DEG C, the time is to obtain rich magnesium salts production after 180min, dewater treatment
Product；
(4), pack
Product after step (3) dewater treatment is packed.
Embodiment 4
A kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 30 times of weight than water, heating and refluxing extraction 3
Secondary, the time extracted every time is 60min, and merging filtrate concentration adds alimentary acetic acid mixing into concentrate, adding food
With ph value of mixture is monitored by pH value detection means in process of acetic acid, when mixed liquor is in faintly acid, stop adding vinegar
Filtered after acid action, fully reaction, rich magnesium extract is dried in vacuo to obtain after concentration；
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, simultaneously
The pure water that addition accounts for sodium chloride gross mass 10% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride and stopped
Stirring, obtains mixed material, described sodium chloride and the weight ratio of rich magnesium extract are 50：2；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet after sealing
Row heats, and heat treatment temperature is 110 DEG C, and the time is 90min, and the mixture after heating is added into revolution vacuum does
Carry out dewater treatment in dry machine, dewater treatment temperature is 60 DEG C, the time is to obtain rich magnesium salts product after 90min, dewater treatment；
(4), pack
Product after step (3) dewater treatment is packed.
Above content is only to present inventive concept example and explanation, affiliated those skilled in the art couple
Described specific embodiment is made various modifications or supplement or substituted using similar mode, without departing from invention
Conceive or surmount scope defined in the claims, protection scope of the present invention all should be belonged to.
Claims (4)
1. a kind of preparation method of rich magnesium salts, it is characterised in that comprise the following steps：
(1), the preparation of seaweed extract
Dry laver is broken into laver powder, every time into laver powder add 20~30 times of weight than water, heating and refluxing extraction 2~
3 times, the time extracted every time is 30~60min, and merging filtrate concentration adds alimentary acetic acid mixing into concentrate, filled
Divide after reaction and filter, rich magnesium extract is dried in vacuo to obtain after concentration；
(2), batch mixing
The sodium chloride weighed up is placed in open mixer, rich magnesium extract is added under conditions of being stirred continuously, is added simultaneously
The pure water for accounting for sodium chloride gross mass 4~10% is thoroughly mixed, until rich magnesium extract is completely dispersed in sodium chloride and stopped
Stirring, obtains mixed material；
(3) prepared by rich magnesium salts
The mixed material obtained in step (2) is fitted into sealed pressure vessel and sealed, is put into high-temperature cabinet and is added after sealing
Heat treatment, heat treatment temperature is 90~150 DEG C, and the time is 30~180min, and the mixture after heating is added and turned round
Carry out dewater treatment in vacuum drier, dewater treatment temperature is 35~65 DEG C, the time is after 30~180min, dewater treatment
To rich magnesium salts product；
(4), pack
Product after step (3) dewater treatment is packed.
2. the preparation method of rich magnesium salts according to claim 1, it is characterised in that the chlorination described in the step (2)
Sodium is the food grade sodium chloride for meeting national Specification, and weight/mass percentage composition >=91%, granularity is 0.1~3.5mm.
3. the preparation method of rich magnesium salts according to claim 1, it is characterised in that the step (1) is adding vinegar
Ph value of mixture is monitored by pH value detection means during acid, when mixed liquor is in faintly acid, stops addition alimentary acetic acid and moves
Make.
4. the preparation method of rich magnesium salts according to claim 1, it is characterised in that sodium chloride and richness in the step (2)
The weight ratio of magnesium extract is 50~20：0.1~5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510404818.4A CN104939023B (en) | 2015-07-10 | 2015-07-10 | A kind of preparation method of rich magnesium salts |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510404818.4A CN104939023B (en) | 2015-07-10 | 2015-07-10 | A kind of preparation method of rich magnesium salts |
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| CN104939023A CN104939023A (en) | 2015-09-30 |
| CN104939023B true CN104939023B (en) | 2017-09-29 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105149221B (en) * | 2015-10-28 | 2017-05-03 | 天津海吉纳盐品有限公司 | Detection processing production line for natural mineral salt and detection processing method |
| CN107319483A (en) * | 2017-06-27 | 2017-11-07 | 中原工学院 | A kind of green All Pure Nature richness dimension pregnant precious salt of comprehensive nutrient type and preparation method thereof |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60156357A (en) * | 1984-01-27 | 1985-08-16 | Nikken Sutamii Kk | Natural mineral salt and production thereof |
| JPH0616688B2 (en) * | 1990-08-27 | 1994-03-09 | 森下仁丹株式会社 | Salt substitute |
| KR100448673B1 (en) * | 2000-02-22 | 2004-09-16 | 홍영표 | Plant salt of preparation method and Plant salt |
| JP4131689B2 (en) * | 2002-10-01 | 2008-08-13 | 天野実業株式会社 | Method for producing algal salt |
| KR20040047487A (en) * | 2002-11-28 | 2004-06-05 | 김선재 | Preparation of Mineral and Salt from Sea-weed |
| CN1276727C (en) * | 2003-05-12 | 2006-09-27 | 赵晓迪 | Bio-nutritious iodine salt of natural algae |
| US7208189B2 (en) * | 2004-04-06 | 2007-04-24 | Council Of Scientific And Industrial Research | Low sodium salt of botanic origin |
| JP2007049967A (en) * | 2005-08-19 | 2007-03-01 | Adachi Trader:Kk | Sea alga extract-containing alga salt and method for producing the same |
| CN101774545B (en) * | 2008-12-30 | 2012-03-07 | 刘树军 | Algae iodate and method for extracting algae iodate from algae |
| CN101897427A (en) * | 2009-05-31 | 2010-12-01 | 中盐国本盐业有限公司 | Seaweed iodated salt and processing method thereof |
| CN103271326A (en) * | 2013-05-15 | 2013-09-04 | 宋杰 | Method for preparing seaweed nutritious salt |
| CN104495754B (en) * | 2014-11-28 | 2016-06-29 | 益盐堂（应城）健康盐制盐有限公司 | A kind of extracting method of Iodine |
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