CN104911743B - 一种保暖智能型调温聚酰胺纤维及其制备方法 - Google Patents
一种保暖智能型调温聚酰胺纤维及其制备方法 Download PDFInfo
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- CN104911743B CN104911743B CN201510298740.2A CN201510298740A CN104911743B CN 104911743 B CN104911743 B CN 104911743B CN 201510298740 A CN201510298740 A CN 201510298740A CN 104911743 B CN104911743 B CN 104911743B
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- 239000004952 Polyamide Substances 0.000 claims abstract description 21
- 229920002647 polyamide Polymers 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 229920000642 polymer Polymers 0.000 claims abstract description 15
- 239000004156 Azodicarbonamide Substances 0.000 claims abstract description 14
- XOZUGNYVDXMRKW-AATRIKPKSA-N azodicarbonamide Chemical compound NC(=O)\N=N\C(N)=O XOZUGNYVDXMRKW-AATRIKPKSA-N 0.000 claims abstract description 14
- 235000019399 azodicarbonamide Nutrition 0.000 claims abstract description 14
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 12
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- 239000002202 Polyethylene glycol Substances 0.000 claims description 6
- 229920001223 polyethylene glycol Polymers 0.000 claims description 6
- 229920002292 Nylon 6 Polymers 0.000 claims description 5
- -1 polyethylene terephthalate Polymers 0.000 claims description 5
- OKIRBHVFJGXOIS-UHFFFAOYSA-N 1,2-di(propan-2-yl)benzene Chemical compound CC(C)C1=CC=CC=C1C(C)C OKIRBHVFJGXOIS-UHFFFAOYSA-N 0.000 claims description 4
- 229920002302 Nylon 6,6 Polymers 0.000 claims description 4
- VUQPJRPDRDVQMN-UHFFFAOYSA-N 1-chlorooctadecane Chemical compound CCCCCCCCCCCCCCCCCCCl VUQPJRPDRDVQMN-UHFFFAOYSA-N 0.000 claims description 3
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- LSXWFXONGKSEMY-UHFFFAOYSA-N di-tert-butyl peroxide Chemical compound CC(C)(C)OOC(C)(C)C LSXWFXONGKSEMY-UHFFFAOYSA-N 0.000 claims description 3
- NQGIJDNPUZEBRU-UHFFFAOYSA-N dodecanoyl chloride Chemical compound CCCCCCCCCCCC(Cl)=O NQGIJDNPUZEBRU-UHFFFAOYSA-N 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
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- 229920006152 PA1010 Polymers 0.000 claims description 2
- 125000002252 acyl group Chemical group 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims description 2
- 229940070765 laurate Drugs 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims description 2
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- 239000012188 paraffin wax Substances 0.000 claims description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 2
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims 2
- 229920000299 Nylon 12 Polymers 0.000 claims 1
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- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical group C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 4
- 239000010985 leather Substances 0.000 description 4
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- 239000004677 Nylon Substances 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
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- 238000002166 wet spinning Methods 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- RWXMAAYKJDQVTF-UHFFFAOYSA-N 2-(2-hydroxyethoxy)ethyl prop-2-enoate Chemical compound OCCOCCOC(=O)C=C RWXMAAYKJDQVTF-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
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- 230000001105 regulatory effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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CN107587207A (zh) * | 2016-07-06 | 2018-01-16 | 中国石化仪征化纤有限责任公司 | 一种发热相变皮芯纤维及其制备方法 |
CN108084969A (zh) * | 2017-11-29 | 2018-05-29 | 贵州迈博润科技有限公司 | 可编织熔纺聚合物中空纤维/石蜡相变储能材料及其制备方法 |
CN108588871B (zh) * | 2018-04-26 | 2020-12-18 | 东华大学 | 一种近红外光诱导牵伸制备异形高强度聚酰胺6纤维的制备方法 |
CN109778344B (zh) * | 2019-01-02 | 2021-08-10 | 华南理工大学 | 一种非连续相变调温纤维及其制备方法 |
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WO2003062513A2 (en) * | 2000-10-19 | 2003-07-31 | Outlast Technologies, Inc. | Temperature adaptable textile fibers and method of preparing same |
CN101845683B (zh) * | 2010-05-07 | 2012-07-04 | 盈保纤维科技(仁化)有限公司 | 一种储热调温纤维 |
CN101906670B (zh) * | 2010-08-26 | 2011-12-14 | 东华大学 | 熔纺型固-液复合相变纤维的纺丝设备及其制备方法 |
CN102505179B (zh) * | 2011-10-13 | 2014-07-02 | 大连工业大学 | 一种蓄热调温纤维的制备方法 |
CN103627162A (zh) * | 2013-01-29 | 2014-03-12 | 南京理工大学 | 聚氨酯蓄热保温泡沫及其制备方法 |
CN103102552A (zh) * | 2013-03-12 | 2013-05-15 | 泰山体育产业集团有限公司 | 一种相变保温聚烯烃泡沫材料及其制备方法 |
CN103881231B (zh) * | 2014-03-25 | 2015-12-09 | 大连工业大学 | 一种基于乙烯-醋酸乙烯酯共聚物的蓄热储能间隔条及其制备方法 |
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Address after: 201620 Shanghai, North Renmin Road, Songjiang District, No. 2999 Applicant after: DONGHUA University Applicant after: CHANGLE HENGSHEN SYNTHETIC FIBER Co.,Ltd. Address before: 201620 Shanghai, North Renmin Road, Songjiang District, No. 2999 Applicant before: Donghua University |
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Inventor after: Zhu Meifang Inventor after: Chen Wei Inventor after: Xiang Hengxue Inventor after: Xia Wei Inventor after: Chen Wenping Inventor after: Chen Lijun Inventor after: Zhao Jie Inventor before: Zhu Meifang Inventor before: Xiang Hengxue Inventor before: Xia Wei Inventor before: Chen Wenping |
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Address after: 201620 No. 2999 North Renmin Road, Shanghai, Songjiang District Patentee after: DONGHUA University Country or region after: China Patentee after: Fujian Hengshen Synthetic Fiber Technology Co.,Ltd. Address before: 201620 No. 2999 North Renmin Road, Shanghai, Songjiang District Patentee before: DONGHUA University Country or region before: China Patentee before: CHANGLE HENGSHEN SYNTHETIC FIBER Co.,Ltd. |