CN104906460A - Compound herba fibraureae recisae lotion and preparation method thereof - Google Patents
Compound herba fibraureae recisae lotion and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of traditional Chinese medicinal material processing, in particular to a compound herba fibraureae recisae lotion and a preparation method thereof. The compound herba fibraureae recisae lotion is prepared from 20-30 g of hedyotis hedyotidea, 20-30 g of eriocarpous glochidion leaves, 5-15 g of cape jasmine, 20-30 g of radix scutellariae, 10-20 g of rhizoma smilacis glabrae, 5-10 g of bletilla striata, 10-20 g of fructus cnidii, 45-55 g of herba fibraureae recisae, 2-4 ml of eucalyptus oil, 0.1-0.3 g of borneol, 1-3 g of sodium benzoate, 0.15-0.35 g of ethylparaben, 2-4 g of tween~80, 0.15-35 g of chlorhexidine acetate and the balance water, so that 1000 ml of the compound herba fibraureae recisae lotion is obtained. The compound herba fibraureae recisae lotion is simple in set prescription, easy and convenient to prepare, low in price, capable of being widely used for heat clearing, detoxifying, parasite killing, itching relieving and auxiliary treatment for symptoms like skin itching.
Description
Technical field
The present invention relates to Chinese crude drug processing technique field, specifically a kind of compound recipe Caulis Fibraureae washing liquid and preparation method thereof.
Background technology
Caulis Fibraureae (Classification system: Daemonorops margaritae (Hance) Becc.) perennial plant, can medication, and the southeast, Guangdong, Hong Kong, Hainan and Southwestern Kwangsi, China, In Xishuangbanna of Yunnan has cultivation.Seminal propagation.Fruit spherical, more greatly, dark olive drab(O．D), by tool straight thrust, boat shape spathe wrap quilt, tool ornamental value; Rattan quality is better-than-average, can for braiding.
Caulis Fibraureae function is: heat-clearing and toxic substances removing; Dampness removing.Main acute tonsillitis, pharyngolaryngitis, upper respiratory tract infection; Conjunctivitis; Jaundice; Gastroenteritis; Dysentery; Infantile dyspepsia; Food poisoning; Salpingitis; Acute and chronic endometritis; Acute pelvic inflammatory disease; Vaginitis; Furuncle; Burn and scald etc.
Summary of the invention
The object of the invention is the special efficacy for Caulis Fibraureae, a kind of compound recipe Caulis Fibraureae washing liquid and preparation method thereof is provided.
For achieving the above object, the technical solution used in the present invention is: a kind of Caulis Fibraureae washing liquid, is prepared from by following raw materials according: Caulis et Folium hedyotis hedyotideae 20 ~ 30g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 20 ~ 30g, Fructus Gardeniae 5 ~ 15g, Radix Scutellariae 20 ~ 30g, Rhizoma Smilacis Glabrae 10 ~ 20g, Pseudobulbus Bletillae (Rhizoma Bletillae) 5 ~ 10g, Fructus Cnidii 10 ~ 20g, Caulis Fibraureae 45 ~ 55g, Oleum Eucalypti 2 ~ 4ml, Borneolum Syntheticum 0.1 ~ 0.3g, sodium benzoate 1 ~ 3g, ethyl hydroxybenzoate 0.15 ~ 0.35g, tween
~ 802 ~ 4g, chlorhexidine acetate 0.15 ~ 35g, add water and make full dose 1000ml.
Further, be prepared from by the raw material of following parts by weight: Caulis et Folium hedyotis hedyotideae 25g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 25g, Fructus Gardeniae 10g, Radix Scutellariae 25g, Rhizoma Smilacis Glabrae 15g, Pseudobulbus Bletillae (Rhizoma Bletillae) 10g, Fructus Cnidii 15g, Caulis Fibraureae 50g, Oleum Eucalypti 3ml, Borneolum Syntheticum 0.2g, sodium benzoate 2g, ethyl hydroxybenzoate 0.25g, tween
~ 803g, chlorhexidine acetate 0.25g, add water and make full dose 1000ml.
Another object of the present invention is to provide a kind of preparation method of compound recipe Caulis Fibraureae washing liquid, and step comprises:
(1) coarse pulverization is carried out after Caulis Fibraureae pre-treatment, then the sulfuric acid solution dipping adding Caulis Fibraureae 8 times of weight filtered after 3 ~ 6 hours, the pH to 9 that mass concentration is the sodium hydroxide solution adjustment filtrate of 40% is added in filtrate, hold over night, hold over night after sodium chloride is added in supernatant, after precipitate filtration treatment, liquid is incorporated into supernatant, filter after leaving standstill, filtrate reject, solid adds alcohol heat reflux twice, each addition 20ml, 20ml is concentrated into after merge extractive liquid, adding salt acid for adjusting pH is 2, supernatant is abandoned after hold over night, Caulis Fibraureae precipitate is for subsequent use,
(2) Caulis et Folium hedyotis hedyotideae, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi), Rhizoma Smilacis Glabrae, Fructus Gardeniae, Radix Scutellariae, Pseudobulbus Bletillae (Rhizoma Bletillae) and Fructus Cnidii are cleaned, add its 6 ~ 10 times of weight water dippings respectively 1 ~ 2 hour, then 1 ~ 3 hour is decocted, and then its 5 ~ 7 times of weight water that add water decoct 2 ~ 3 hours, after filtering, decoction liquor merges, and it is for subsequent use that the decoction liquor of merging is concentrated into 950ml;
(3) be added in decoction liquor by the Caulis Fibraureae precipitate of gained in step (1), hold over night after natural cooling, abandons sediment after sedimentation and filtration, and filtrate is incorporated into supernatant;
(4) step (3) gained supernatant carries out heated and boiled, adds sodium benzoate simultaneously, ethyl hydroxybenzoate, is dissolved in Oleum Eucalypti and adds, Borneolum Syntheticum and tween
~ 80add after utilizing dissolve with ethanol, finally add chlorhexidine acetate, then moisturizing is to 1000ml, packed products after detection fill.
Further, step (1), the quality simmer down to 1% of described sulfuric acid solution.
Further, step (1), the addition of described sodium chloride makes mass concentration contained by sodium chloride in supernatant be 7%.
Advantageous Effects of the present invention is: the present invention side of one-tenth is simple, it is easy, cheap to prepare, and is widely used in heat-clearing and toxic substances removing, the auxiliary treatment of the symptom such as killing parasites for relieving itching, skin pruritus.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
A kind of compound recipe Caulis Fibraureae washing liquid, is prepared from by following raw materials according: Caulis et Folium hedyotis hedyotideae 20g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 30g, Fructus Gardeniae 5g, Radix Scutellariae 30g, Rhizoma Smilacis Glabrae 10g, Pseudobulbus Bletillae (Rhizoma Bletillae) 10g, Fructus Cnidii 10g, Caulis Fibraureae 55g, Oleum Eucalypti 2ml, Borneolum Syntheticum 0.3g, sodium benzoate 1g, ethyl hydroxybenzoate 0.35g, tween
~ 802g, chlorhexidine acetate 35g, add water and make full dose 1000ml.
Preparation method, step comprises:
(1) coarse pulverization is carried out after Caulis Fibraureae pre-treatment, then the mass concentration adding Caulis Fibraureae 8 times of weight be 1% sulfuric acid solution flood after 3 hours and filter, the pH to 9 that mass concentration is the sodium hydroxide solution adjustment filtrate of 40% is added in filtrate, hold over night, hold over night after sodium chloride is added in supernatant, after precipitate filtration treatment, liquid is incorporated into supernatant, filter after leaving standstill, filtrate reject, solid adds alcohol heat reflux twice, each addition 20ml, 20ml is concentrated into after merge extractive liquid, adding salt acid for adjusting pH is 2, supernatant is abandoned after hold over night, Caulis Fibraureae precipitate is for subsequent use,
(2) Caulis et Folium hedyotis hedyotideae, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi), Rhizoma Smilacis Glabrae, Fructus Gardeniae, Radix Scutellariae, Pseudobulbus Bletillae (Rhizoma Bletillae) and Fructus Cnidii are cleaned, add its 6 times of weight water respectively and flood 2 hours, then decoct 1 hour, and then its 7 times of weight water that add water decoct 2 hours, after filtering, decoction liquor merges, and it is for subsequent use that the decoction liquor of merging is concentrated into 950ml;
(3) be added in decoction liquor by the Caulis Fibraureae precipitate of gained in step (1), hold over night after natural cooling, abandons sediment after sedimentation and filtration, and filtrate is incorporated into supernatant;
(4) step (3) gained supernatant carries out heated and boiled, adds sodium benzoate simultaneously, ethyl hydroxybenzoate, is dissolved in Oleum Eucalypti and adds, Borneolum Syntheticum and tween
~ 80add after utilizing dissolve with ethanol, finally add chlorhexidine acetate, then moisturizing is to 1000ml, packed products after detection fill.
Wherein, the addition of sodium chloride makes mass concentration contained by sodium chloride in supernatant be 7%.
Embodiment 2
A kind of compound recipe Caulis Fibraureae washing liquid, is prepared from by following raw materials according: Caulis et Folium hedyotis hedyotideae 30g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 20g, Fructus Gardeniae 15g, Radix Scutellariae 20g, Rhizoma Smilacis Glabrae 20g, Pseudobulbus Bletillae (Rhizoma Bletillae) 5g, Fructus Cnidii 20g, Caulis Fibraureae 45g, Oleum Eucalypti 4ml, Borneolum Syntheticum 0.1g, sodium benzoate 3g, ethyl hydroxybenzoate 0.15g, tween
~ 804g, chlorhexidine acetate 0.15g, add water and make full dose 1000ml.
Preparation method, step comprises:
(1) coarse pulverization is carried out after Caulis Fibraureae pre-treatment, then the mass concentration adding Caulis Fibraureae 8 times of weight is that 1% sulfuric acid solution floods filtration after 6 hours, the pH to 9 that mass concentration is the sodium hydroxide solution adjustment filtrate of 40% is added in filtrate, hold over night, hold over night after sodium chloride is added in supernatant, after precipitate filtration treatment, liquid is incorporated into supernatant, filter after leaving standstill, filtrate reject, solid adds alcohol heat reflux twice, each addition 20ml, 20ml is concentrated into after merge extractive liquid, adding salt acid for adjusting pH is 2, supernatant is abandoned after hold over night, Caulis Fibraureae precipitate is for subsequent use,
(2) Caulis et Folium hedyotis hedyotideae, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi), Rhizoma Smilacis Glabrae, Fructus Gardeniae, Radix Scutellariae, Pseudobulbus Bletillae (Rhizoma Bletillae) and Fructus Cnidii are cleaned, add its 10 times of weight water respectively and flood 1 hour, then decoct 3 hours, and then its 5 times of weight water that add water decoct 3 hours, after filtering, decoction liquor merges, and it is for subsequent use that the decoction liquor of merging is concentrated into 950ml;
(3) be added in decoction liquor by the Caulis Fibraureae precipitate of gained in step (1), hold over night after natural cooling, abandons sediment after sedimentation and filtration, and filtrate is incorporated into supernatant;
(4) step (3) gained supernatant carries out heated and boiled, adds sodium benzoate simultaneously, ethyl hydroxybenzoate, is dissolved in Oleum Eucalypti and adds, Borneolum Syntheticum and tween
~ 80add after utilizing dissolve with ethanol, finally add chlorhexidine acetate, then moisturizing is to 1000ml, packed products after detection fill.
Wherein, the addition of sodium chloride makes mass concentration contained by sodium chloride in supernatant be 7%.
Embodiment 3
A kind of compound recipe Caulis Fibraureae washing liquid, is prepared from by following raw materials according: Caulis et Folium hedyotis hedyotideae 25g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 25g, Fructus Gardeniae 10g, Radix Scutellariae 25g, Rhizoma Smilacis Glabrae 15g, Pseudobulbus Bletillae (Rhizoma Bletillae) 10g, Fructus Cnidii 15g, Caulis Fibraureae 50g, Oleum Eucalypti 3ml, Borneolum Syntheticum 0.2g, sodium benzoate 2g, ethyl hydroxybenzoate 0.25g, tween
~ 803g, chlorhexidine acetate 0.25g, add water and make full dose 1000ml.
Preparation method, step comprises:
(1) coarse pulverization is carried out after Caulis Fibraureae pre-treatment, then the mass concentration adding Caulis Fibraureae 8 times of weight be 1% sulfuric acid solution flood after 4 hours and filter, the pH to 9 that mass concentration is the sodium hydroxide solution adjustment filtrate of 40% is added in filtrate, hold over night, hold over night after sodium chloride is added in supernatant, after precipitate filtration treatment, liquid is incorporated into supernatant, filter after leaving standstill, filtrate reject, solid adds alcohol heat reflux twice, each addition 20ml, 20ml is concentrated into after merge extractive liquid, adding salt acid for adjusting pH is 2, supernatant is abandoned after hold over night, Caulis Fibraureae precipitate is for subsequent use,
(2) Caulis et Folium hedyotis hedyotideae, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi), Rhizoma Smilacis Glabrae, Fructus Gardeniae, Radix Scutellariae, Pseudobulbus Bletillae (Rhizoma Bletillae) and Fructus Cnidii are cleaned, add its 8 times of weight water respectively and flood 0.5 hour, then decoct 2 hours, and then its 6 times of weight water that add water decoct 1.5 hours, after filtering, decoction liquor merges, and it is for subsequent use that the decoction liquor of merging is concentrated into 950ml;
(3) be added in decoction liquor by the Caulis Fibraureae precipitate of gained in step (1), hold over night after natural cooling, abandons sediment after sedimentation and filtration, and filtrate is incorporated into supernatant;
(4) step (3) gained supernatant carries out heated and boiled, adds sodium benzoate simultaneously, ethyl hydroxybenzoate, is dissolved in Oleum Eucalypti and adds, Borneolum Syntheticum and tween
~ 80add after utilizing dissolve with ethanol, finally add chlorhexidine acetate, then moisturizing is to 1000ml, packed products after detection fill.
Wherein, the addition of sodium chloride makes mass concentration contained by sodium chloride in supernatant be 7%.
Embodiment 4
A kind of compound recipe Caulis Fibraureae washing liquid preparation method (being made into product 12000L to measure, i.e. 6 batches), preparation process comprises:
1, Caulis Fibraureae is extracted: often material takes Caulis Fibraureae coarse powder 600kg
(1) acid dip: take Caulis Fibraureae coarse powder and put in multi-function extractor, adds 1% sulfuric acid solution 4800L and floods 24 hours, filters, obtains filtrate for subsequent use;
(2) alkalize: filtrate mass concentration is 40% sodium hydroxide solution adjust pH to 9, and hold over night, gets supernatant, precipitation filters, and filtrate and supernatant merge, and obtain alkaline medicinal liquid, for subsequent use;
(3) salt adding: get above-mentioned alkaline medicinal liquid, adds sodium chloride and makes content reach 7%, hold over night, leaching precipitate, dries, for subsequent use;
(4) reflux, extract: get above-mentioned dry sediment and add alcohol heating reflux secondary, add ethanol 240L, merge extractive liquid, at every turn, filters, and filtrate recycling ethanol is to about 240L, for subsequent use;
(5) add hydrochloric acid: get above-mentioned concentrated ethanol medicinal liquid and add concentrated hydrochloric acid adjust pH to 2, hold over night, leaching precipitate, collect filtrate ethanol to be recycled, precipitate dries rear censorship, consignment warehouse keeping, for subsequent use;
2, soak by water extracting section weighing: press formula respectively and take each clean medical material (preparation finished product 2000L amount):
Caulis et Folium hedyotis hedyotideae 50kg, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 50kg, Fructus Gardeniae 20kg, Radix Scutellariae 50kg, Rhizoma Smilacis Glabrae 30kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 20kg Fructus Cnidii 30kg;
Extract, concentrate: take seven flavor medicine material by above-mentioned formula ratio, put in multi-function extractor and decoct secondary, first time adds about 2000L water retting 0.5 hour, heating decoction boiling 2 hours, leaching medicinal liquid; Add water about 1500L for the second time, decocts boiling 1.5 hours, leaching medicinal liquid; Merge 2 medicinal liquids, put in dual-effect energy-saving concentration pan and be concentrated into about 1900L, obtain concentrated solution, hold over night, get supernatant, precipitate filters, and filtrate and supernatant merge, and transfer lower operation and treat dosing use, the resting period is no more than 48 hours;
3, dosing: (often criticizing by 2000L amount) water extraction liquid is (1900L); Common fibraurea stem extract (get and often expect 1/6 amount):
Sodium benzoate 4kg, ethyl hydroxybenzoate 0.5kg, Oleum Eucalypti 6L, Borneolum Syntheticum 0.4kg, tween
-806kg, chlorhexidine acetate 0.5kg, ethanol 2L, water adds to 2000L;
(1) get that above-mentioned water extraction is concentrated puts agitator tank herb liquid, add common fibraurea stem extract lysate, stir, hold over night, filter, obtain filtrate for subsequent use;
(2) filtrate heated and boiled is got, first add sodium benzoate, ethyl hydroxybenzoate (add ethanol be about 1000ml make dissolving) while hot, stir evenly, when being down to 60 DEG C-65 DEG C to fluid temperature, get Oleum Eucalypti again, lysate that Borneolum Syntheticum (add ethanol be about 1000ml dissolve) mixes with tween 80 three adds stirring, finally get chlorhexidine acetate hot water to dissolve in right amount, join in above-mentioned solution, add purified water to 2000L total amount, stir evenly, leave standstill, get supernatant to filter, obtain medicinal liquid to be filled please test, airtight being stored between dosing is store in filling, and the resting period is no more than 72 hours;
4, fill: get the above-mentioned medicinal liquid be up to the standards, and when fluid temperature is chilled to room temperature about 25 DEG C, carry out fill, spiral cover, aluminium foil sealing by batch packaging directive and product specification.
5, outer package: carry out outer package by batch packaging directive, packing of product specification, the outer package program of this product specification is: label, mounted box, cartoning, sealing, packing etc.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. compound recipe Caulis Fibraureae washing liquid, it is characterized in that, be prepared from by following raw materials according: Caulis et Folium hedyotis hedyotideae 20 ~ 30g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 20 ~ 30g, Fructus Gardeniae 5 ~ 15g, Radix Scutellariae 20 ~ 30g, Rhizoma Smilacis Glabrae 10 ~ 20g, Pseudobulbus Bletillae (Rhizoma Bletillae) 5 ~ 10g, Fructus Cnidii 10 ~ 20g, Caulis Fibraureae 45 ~ 55g, Oleum Eucalypti 2 ~ 4ml, Borneolum Syntheticum 0.1 ~ 0.3g, sodium benzoate 1 ~ 3g, ethyl hydroxybenzoate 0.15 ~ 0.35g, tween
~ 802 ~ 4g, chlorhexidine acetate 0.15 ~ 35g, add water and make full dose 1000ml.
2. compound recipe Caulis Fibraureae washing liquid according to claim 1, it is characterized in that, be prepared from by the raw material of following parts by weight: Caulis et Folium hedyotis hedyotideae 25g, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi) 25g, Fructus Gardeniae 10g, Radix Scutellariae 25g, Rhizoma Smilacis Glabrae 15g, Pseudobulbus Bletillae (Rhizoma Bletillae) 10g, Fructus Cnidii 15g, Caulis Fibraureae 50g, Oleum Eucalypti 3ml, Borneolum Syntheticum 0.2g, sodium benzoate 2g, ethyl hydroxybenzoate 0.25g, tween
~ 803g, chlorhexidine acetate 0.25g, add water and make full dose 1000ml.
3. the preparation method of compound recipe Caulis Fibraureae washing liquid according to any one of claim 1 ~ 2, it is characterized in that, step comprises:
(1) coarse pulverization is carried out after Caulis Fibraureae pre-treatment, then the dilution heat of sulfuric acid dipping adding Caulis Fibraureae 8 times of weight filtered after 3 ~ 6 hours, the pH to 9 that mass concentration is the sodium hydroxide solution adjustment filtrate of 40% is added in filtrate, hold over night, hold over night after sodium chloride is added in supernatant, after precipitate filtration treatment, liquid is incorporated into supernatant, filter after leaving standstill, filtrate reject, alcohol heat reflux is added twice after solid drying, each addition 20ml, 20ml is concentrated into after merge extractive liquid, adding salt acid for adjusting pH is 2, supernatant is abandoned after hold over night, Caulis Fibraureae precipitate is for subsequent use,
(2) Caulis et Folium hedyotis hedyotideae, Ramulus et folium glochidionis eriocarpi (Folium Glochidii Eriocarpi), Rhizoma Smilacis Glabrae, Fructus Gardeniae, Radix Scutellariae, Pseudobulbus Bletillae (Rhizoma Bletillae) and Fructus Cnidii are cleaned, add its 6 ~ 10 times of weight water dippings respectively 1 ~ 2 hour, then 1 ~ 3 hour is decocted, and then its 5 ~ 7 times of weight water that add water decoct 2 ~ 3 hours, after filtering, decoction liquor merges, and it is for subsequent use that the decoction liquor of merging is concentrated into 950ml;
(3) be added in decoction liquor by the Caulis Fibraureae precipitate of gained in step (1), hold over night after natural cooling, abandons sediment after sedimentation and filtration, and filtrate is incorporated into supernatant;
(4) step (3) gained supernatant carries out heated and boiled, adds sodium benzoate simultaneously, ethyl hydroxybenzoate, is dissolved in Oleum Eucalypti and adds, Borneolum Syntheticum and tween
~ 80add after utilizing dissolve with ethanol, finally add chlorhexidine acetate, then moisturizing is to 1000ml, packed products after detection fill.
4. the preparation method of compound recipe Caulis Fibraureae washing liquid according to claim 3, is characterized in that, step (1), the quality simmer down to 1% of described sulfuric acid solution.
5. the preparation method of compound recipe Caulis Fibraureae washing liquid according to claim 3, it is characterized in that, step (1), the addition of described sodium chloride makes mass concentration contained by sodium chloride in supernatant be 7%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113876902A (en) * | 2021-11-09 | 2022-01-04 | 广西德联制药有限公司 | Compound fibraurea stem washing lotion and extraction and preparation process thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129477A (en) * | 2007-08-10 | 2008-02-27 | 广州市康迪尔医药有限公司 | Traditional Chinese medicine wash liquid used for treating leucorrhea, pruritus vulvae etc. |
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2015
- 2015-05-31 CN CN201510288078.2A patent/CN104906460A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129477A (en) * | 2007-08-10 | 2008-02-27 | 广州市康迪尔医药有限公司 | Traditional Chinese medicine wash liquid used for treating leucorrhea, pruritus vulvae etc. |
Non-Patent Citations (2)
| Title |
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| 李晓莹等: "pH值对黄藤中巴马汀盐析的影响", 《广东药学院学报》 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113876902A (en) * | 2021-11-09 | 2022-01-04 | 广西德联制药有限公司 | Compound fibraurea stem washing lotion and extraction and preparation process thereof |
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